#------------------------------------------------------------------------------ #$Date: 2010-01-22 14:33:52 +0200 (Fri, 22 Jan 2010) $ #$Revision: 960 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224519.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224519_Fobs loop_ _publ_author_name 'Huo, Li-Hua' 'Xu, Ying-Ming' 'Gao, Shan' 'Ng, Seik Weng' _publ_section_title ; 4-Hydroxypyridinium hydrogen sulfate ; _journal_coeditor_code XU2677 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3148 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.503 _cell_angle_gamma 90.000 _cell_length_a 10.4541 _cell_length_b 10.7017 _cell_length_c 6.8397 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.7711 _[local]_cod_data_source_file xu2677Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 149.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2290.00 2302.30 56.82 o 3 0 0 7929.56 6955.08 120.22 o 4 0 0 3191.17 3191.48 46.15 o 5 0 0 1261.05 1390.84 23.40 o 6 0 0 211.28 200.56 2.35 o 7 0 0 1893.31 1917.42 30.62 o 8 0 0 362.64 327.01 4.05 o 9 0 0 969.12 921.47 12.59 o 10 0 0 3.75 6.26 0.76 o 11 0 0 15.26 12.18 2.11 o 12 0 0 55.94 58.07 1.59 o 13 0 0 134.43 134.79 4.52 o 2 1 0 5823.68 5348.96 82.03 o 3 1 0 1306.19 1327.74 11.02 o 4 1 0 145.72 161.43 1.35 o 5 1 0 45.27 31.19 0.57 o 6 1 0 2010.27 2234.24 28.33 o 7 1 0 1.90 1.82 0.37 o 8 1 0 16.02 17.74 0.61 o 9 1 0 867.01 848.36 8.21 o 10 1 0 104.32 102.75 1.41 o 11 1 0 23.73 23.13 1.01 o 12 1 0 100.92 108.40 1.55 o 13 1 0 20.90 25.80 1.54 o 0 2 0 3542.26 3473.53 49.39 o 1 2 0 994.01 1046.19 17.30 o 2 2 0 178.34 153.17 1.29 o 3 2 0 1363.01 1426.15 12.17 o 4 2 0 67.38 64.86 0.75 o 5 2 0 64.16 72.26 0.80 o 6 2 0 147.06 138.52 1.55 o 7 2 0 59.76 49.65 0.98 o 8 2 0 34.02 34.42 0.87 o 9 2 0 44.71 37.41 0.92 o 10 2 0 25.81 28.14 0.76 o 11 2 0 0.37 -0.08 0.59 o 12 2 0 0.40 0.30 0.45 o 13 2 0 4.74 3.91 1.02 o 1 3 0 1714.99 1838.97 18.82 o 2 3 0 2070.76 2102.74 19.13 o 3 3 0 9.94 14.27 0.28 o 4 3 0 49.41 46.23 0.61 o 5 3 0 611.68 568.27 4.53 o 6 3 0 2.42 1.28 0.37 o 7 3 0 133.45 118.16 1.25 o 8 3 0 480.56 458.04 4.09 o 9 3 0 29.27 25.25 0.72 o 10 3 0 0.79 0.72 0.45 o 11 3 0 182.27 169.14 2.23 o 12 3 0 28.18 30.24 1.10 o 13 3 0 25.19 28.24 1.00 o 0 4 0 1671.64 1739.25 21.92 o 1 4 0 323.70 276.17 2.57 o 2 4 0 2829.82 3096.34 27.72 o 3 4 0 421.14 364.63 2.67 o 4 4 0 374.63 339.78 2.35 o 5 4 0 55.99 61.05 0.74 o 6 4 0 1434.79 1419.23 13.22 o 7 4 0 1246.03 1189.06 11.32 o 8 4 0 14.17 12.30 0.65 o 9 4 0 697.02 646.70 6.17 o 10 4 0 220.16 206.29 2.35 o 11 4 0 35.88 44.14 1.22 o 12 4 0 11.48 7.75 1.11 o 1 5 0 376.15 382.07 4.15 o 2 5 0 291.16 353.19 2.55 o 3 5 0 1035.53 1204.53 19.88 o 4 5 0 764.60 747.86 9.67 o 5 5 0 215.03 184.10 1.69 o 6 5 0 137.58 121.13 1.13 o 7 5 0 130.90 128.38 1.46 o 8 5 0 1039.36 960.99 9.48 o 9 5 0 99.12 97.60 1.33 o 10 5 0 1.03 2.34 0.49 o 11 5 0 39.39 37.00 0.95 o 12 5 0 9.65 6.86 0.92 o 0 6 0 1111.96 1305.57 28.18 o 1 6 0 52.52 50.60 0.66 o 2 6 0 62.23 64.45 0.70 o 3 6 0 31.02 30.43 0.61 o 4 6 0 187.33 199.48 1.71 o 5 6 0 4.43 2.24 0.28 o 6 6 0 437.13 424.02 3.86 o 7 6 0 4.71 6.31 0.56 o 8 6 0 1.55 1.53 0.39 o 9 6 0 12.65 15.09 0.52 o 10 6 0 91.46 85.97 1.46 o 11 6 0 4.02 5.84 0.51 o 12 6 0 0.00 0.46 0.40 o 1 7 0 237.06 233.78 2.12 o 2 7 0 295.74 320.22 2.61 o 3 7 0 201.11 180.94 1.89 o 4 7 0 257.63 241.80 1.96 o 5 7 0 334.50 313.98 2.78 o 6 7 0 532.24 514.95 4.64 o 7 7 0 10.83 11.69 0.55 o 8 7 0 60.37 59.17 1.50 o 9 7 0 70.52 56.49 1.11 o 10 7 0 8.56 6.49 0.69 o 11 7 0 0.13 1.13 0.61 o 0 8 0 846.13 884.63 17.84 o 1 8 0 199.49 199.39 1.58 o 2 8 0 160.54 172.58 1.70 o 3 8 0 631.13 647.90 5.93 o 4 8 0 641.54 609.10 5.88 o 5 8 0 340.50 358.92 2.98 o 6 8 0 99.30 92.64 1.18 o 7 8 0 313.11 279.50 3.59 o 8 8 0 0.02 1.62 0.72 o 9 8 0 118.84 112.04 1.89 o 10 8 0 14.99 12.25 0.76 o 1 9 0 294.36 315.32 2.49 o 2 9 0 217.66 203.54 1.95 o 3 9 0 0.81 2.17 0.51 o 4 9 0 220.26 194.53 2.20 o 5 9 0 150.62 141.61 1.92 o 6 9 0 141.81 122.46 1.53 o 7 9 0 6.37 3.72 0.73 o 8 9 0 138.30 132.01 2.21 o 9 9 0 13.33 11.61 1.00 o 10 9 0 2.11 2.30 0.90 o 0 10 0 243.73 216.46 2.98 o 1 10 0 328.02 304.52 3.33 o 2 10 0 41.16 34.46 0.56 o 3 10 0 65.80 66.40 1.47 o 4 10 0 96.23 88.83 1.54 o 5 10 0 0.01 0.45 0.46 o 6 10 0 0.79 0.59 0.56 o 7 10 0 16.41 20.86 1.19 o 8 10 0 17.99 20.85 0.93 o 9 10 0 35.59 43.91 1.19 o 1 11 0 25.26 26.76 0.83 o 2 11 0 9.56 8.42 0.45 o 3 11 0 30.04 27.33 0.93 o 4 11 0 29.57 28.60 1.04 o 5 11 0 6.28 9.16 0.73 o 6 11 0 44.39 44.11 1.26 o 7 11 0 52.89 59.95 1.62 o 8 11 0 10.77 7.25 0.86 o 0 12 0 143.82 146.63 4.33 o 1 12 0 1.91 3.78 0.51 o 2 12 0 2.77 6.08 0.84 o 3 12 0 63.67 68.46 1.07 o 4 12 0 1.11 0.67 0.43 o 5 12 0 4.98 2.85 1.06 o 6 12 0 54.20 61.05 1.46 o 1 13 0 92.11 92.11 2.93 o 2 13 0 13.01 10.07 0.64 o 3 13 0 32.52 34.49 1.20 o 4 13 0 56.45 64.90 1.42 o -13 1 1 10.35 13.37 0.91 o -12 1 1 94.21 108.68 2.00 o -11 1 1 264.73 257.41 3.05 o -10 1 1 73.90 65.52 1.23 o -9 1 1 34.84 41.12 0.93 o -8 1 1 212.56 216.06 2.21 o -7 1 1 189.41 178.51 1.69 o -6 1 1 11.96 9.69 0.42 o -5 1 1 254.35 227.82 3.91 o -4 1 1 119.42 167.06 1.31 o -3 1 1 173.60 173.58 1.38 o -2 1 1 2416.52 2385.78 22.43 o -1 1 1 1454.47 1580.37 12.98 o 0 1 1 31.29 34.80 0.26 o 1 1 1 274.76 322.93 5.53 o 2 1 1 2044.53 2195.11 19.71 o 3 1 1 866.53 903.97 7.09 o 4 1 1 1360.08 1594.24 13.88 o 5 1 1 303.45 270.44 2.00 o 6 1 1 729.05 749.16 6.18 o 7 1 1 6.71 5.74 1.07 o 8 1 1 21.69 19.80 0.74 o 9 1 1 11.87 11.26 0.56 o 10 1 1 4.28 4.64 0.48 o 11 1 1 38.82 37.07 1.04 o 12 1 1 51.83 57.60 1.13 o 13 1 1 38.59 42.81 1.11 o -13 2 1 25.66 26.16 1.11 o -12 2 1 117.13 114.34 1.83 o -11 2 1 8.04 4.90 0.73 o -10 2 1 49.36 49.74 1.00 o -9 2 1 1476.57 1417.68 13.96 o -8 2 1 154.39 146.08 1.70 o -7 2 1 837.28 811.69 7.54 o -6 2 1 174.78 138.27 1.59 o -5 2 1 760.79 782.90 6.65 o -4 2 1 1.21 5.31 0.30 o -3 2 1 2163.82 2011.94 18.44 o -2 2 1 5267.35 5038.92 56.85 o -1 2 1 56.43 47.73 0.72 o 0 2 1 11136.26 10161.22 122.42 o 1 2 1 4667.66 4616.90 45.01 o 2 2 1 119.76 145.42 1.34 o 3 2 1 261.58 211.38 1.82 o 4 2 1 4178.13 4513.61 50.15 o 5 2 1 86.14 73.67 0.78 o 6 2 1 60.71 51.49 1.12 o 7 2 1 1192.61 1164.59 12.32 o 8 2 1 38.92 33.02 0.82 o 9 2 1 554.67 552.40 4.91 o 10 2 1 142.14 141.72 1.62 o 11 2 1 13.18 16.36 0.83 o 12 2 1 58.15 61.72 1.19 o 13 2 1 104.50 100.56 1.52 o -13 3 1 8.08 8.04 1.77 o -12 3 1 41.96 48.81 1.58 o -11 3 1 59.66 52.72 1.20 o -10 3 1 0.01 0.23 0.41 o -9 3 1 45.69 54.37 1.14 o -8 3 1 788.37 769.32 7.04 o -7 3 1 55.95 49.24 0.83 o -6 3 1 320.45 335.93 2.93 o -5 3 1 1669.41 1748.68 16.28 o -4 3 1 161.85 230.21 1.82 o -3 3 1 1628.09 1872.57 21.99 o -2 3 1 85.87 63.33 0.73 o -1 3 1 1682.72 1763.23 18.06 o 0 3 1 228.45 241.79 1.53 o 1 3 1 1269.91 1330.17 9.95 o 2 3 1 14.63 9.18 0.47 o 3 3 1 1297.73 1563.14 19.71 o 4 3 1 92.20 111.59 1.27 o 5 3 1 298.72 257.94 2.19 o 6 3 1 472.61 485.94 4.01 o 7 3 1 66.46 67.38 0.97 o 8 3 1 791.37 762.88 6.89 o 9 3 1 20.34 22.52 0.61 o 10 3 1 17.96 17.16 0.74 o 11 3 1 21.01 20.26 1.09 o 12 3 1 27.63 29.21 0.89 o -12 4 1 37.70 40.74 1.25 o -11 4 1 0.03 -0.45 0.58 o -10 4 1 21.90 17.88 0.81 o -9 4 1 7.26 5.08 0.57 o -8 4 1 140.69 121.82 1.63 o -7 4 1 28.57 30.57 0.96 o -6 4 1 11.28 6.97 0.90 o -5 4 1 367.71 401.62 3.40 o -4 4 1 69.60 67.13 0.76 o -3 4 1 200.24 218.42 5.26 o -2 4 1 95.97 103.32 1.04 o -1 4 1 865.18 920.58 13.28 o 0 4 1 2960.14 3412.26 35.42 o 1 4 1 118.96 137.62 1.88 o 2 4 1 260.56 261.47 1.64 o 3 4 1 10.37 13.01 0.46 o 4 4 1 163.25 178.50 1.46 o 5 4 1 1258.42 1420.79 12.92 o 6 4 1 254.98 253.12 3.73 o 7 4 1 84.14 93.12 1.32 o 8 4 1 0.69 1.56 0.39 o 9 4 1 0.07 0.67 0.34 o 10 4 1 104.54 102.83 1.38 o 11 4 1 47.29 50.36 1.14 o 12 4 1 14.16 14.21 2.52 o -12 5 1 7.18 8.06 0.92 o -11 5 1 29.55 24.45 1.21 o -10 5 1 82.75 75.01 1.51 o -9 5 1 297.11 269.93 2.93 o -8 5 1 45.32 45.24 1.00 o -7 5 1 144.67 150.00 1.75 o -6 5 1 404.31 393.21 3.48 o -5 5 1 1.28 0.22 0.19 o -4 5 1 559.77 605.66 9.72 o -3 5 1 14.51 14.54 0.53 o -2 5 1 199.76 207.57 2.04 o -1 5 1 762.52 745.48 12.85 o 0 5 1 3.58 6.05 0.30 o 1 5 1 57.54 72.67 0.70 o 2 5 1 195.57 209.79 1.66 o 3 5 1 357.69 380.49 2.64 o 4 5 1 4.44 1.80 0.28 o 5 5 1 10.11 8.73 0.35 o 6 5 1 577.75 540.66 4.73 o 7 5 1 29.63 30.14 0.55 o 8 5 1 5.28 3.55 0.53 o 9 5 1 183.65 162.19 1.69 o 10 5 1 2.17 0.57 0.33 o 11 5 1 1.62 2.00 0.41 o 12 5 1 39.49 40.22 0.97 o -12 6 1 0.48 1.03 0.51 o -11 6 1 0.88 0.76 0.41 o -10 6 1 40.78 39.70 0.83 o -9 6 1 91.30 81.48 1.29 o -8 6 1 1.47 0.12 0.26 o -7 6 1 562.39 527.99 4.82 o -6 6 1 624.02 598.37 5.29 o -5 6 1 128.04 126.63 1.26 o -4 6 1 57.88 54.17 1.04 o -3 6 1 2036.00 2097.72 28.40 o -2 6 1 1344.04 1561.78 23.19 o -1 6 1 196.59 250.80 2.24 o 0 6 1 3452.49 3869.60 43.06 o 1 6 1 106.44 127.42 1.32 o 2 6 1 0.98 3.61 0.36 o 3 6 1 802.30 839.52 5.68 o 4 6 1 343.13 323.19 2.71 o 5 6 1 90.19 74.77 1.13 o 6 6 1 1210.17 1242.09 11.60 o 7 6 1 700.49 651.84 6.28 o 8 6 1 15.64 12.96 0.63 o 9 6 1 249.62 247.14 2.57 o 10 6 1 64.02 68.99 1.21 o 11 6 1 33.81 34.43 0.98 o -11 7 1 31.36 31.32 0.84 o -10 7 1 35.55 27.84 0.70 o -9 7 1 208.79 186.77 4.87 o -8 7 1 295.55 270.39 4.25 o -7 7 1 30.48 31.13 0.53 o -6 7 1 959.16 945.50 8.47 o -5 7 1 103.92 97.07 0.88 o -4 7 1 133.46 136.35 2.06 o -3 7 1 176.32 160.42 1.78 o -2 7 1 133.09 122.43 0.94 o -1 7 1 640.51 637.64 8.26 o 0 7 1 75.91 65.21 0.90 o 1 7 1 657.08 610.45 5.70 o 2 7 1 26.86 23.39 0.60 o 3 7 1 3.57 5.63 0.28 o 4 7 1 120.55 136.78 1.29 o 5 7 1 45.56 47.11 0.64 o 6 7 1 355.66 345.18 3.33 o 7 7 1 18.66 24.92 0.86 o 8 7 1 145.75 158.07 1.70 o 9 7 1 202.08 186.96 2.13 o 10 7 1 2.22 2.12 0.45 o 11 7 1 2.65 2.98 0.60 o -11 8 1 33.88 44.56 1.73 o -10 8 1 28.98 26.44 1.39 o -9 8 1 11.86 16.68 0.94 o -8 8 1 6.00 6.28 0.31 o -7 8 1 3.38 3.24 0.24 o -6 8 1 60.97 64.11 1.45 o -5 8 1 38.89 33.68 1.30 o -4 8 1 8.59 7.05 0.58 o -3 8 1 180.70 177.39 2.07 o -2 8 1 0.03 0.12 0.17 o -1 8 1 326.87 297.27 2.28 o 0 8 1 515.51 516.90 4.21 o 1 8 1 82.81 76.79 1.71 o 2 8 1 0.09 0.63 0.52 o 3 8 1 628.01 635.12 5.12 o 4 8 1 19.25 18.15 0.48 o 5 8 1 114.14 111.33 1.29 o 6 8 1 155.73 154.04 1.50 o 7 8 1 11.15 11.95 0.65 o 8 8 1 2.95 1.93 0.47 o 9 8 1 12.40 14.55 0.67 o 10 8 1 34.72 41.88 1.19 o -10 9 1 17.76 20.02 1.19 o -9 9 1 14.67 18.02 1.07 o -8 9 1 53.19 47.34 1.51 o -7 9 1 11.33 8.48 0.81 o -6 9 1 4.51 5.91 0.83 o -5 9 1 87.35 87.67 1.33 o -4 9 1 5.85 5.61 0.61 o -3 9 1 466.58 470.31 4.00 o -2 9 1 10.86 8.27 0.68 o -1 9 1 39.27 43.89 0.69 o 0 9 1 6.79 11.28 0.44 o 1 9 1 5.01 3.50 0.41 o 2 9 1 36.08 35.29 0.81 o 3 9 1 185.35 183.26 1.73 o 4 9 1 5.16 7.66 0.53 o 5 9 1 29.08 30.56 0.75 o 6 9 1 31.53 29.92 0.69 o 7 9 1 33.24 40.99 0.92 o 8 9 1 71.66 76.33 1.57 o 9 9 1 45.67 50.87 0.98 o -9 10 1 75.94 73.49 2.10 o -8 10 1 26.88 28.74 1.90 o -7 10 1 129.58 133.01 2.05 o -6 10 1 67.85 67.56 1.37 o -5 10 1 17.92 18.64 0.82 o -4 10 1 74.17 72.34 1.30 o -3 10 1 80.10 75.98 1.12 o -2 10 1 18.73 22.72 0.58 o -1 10 1 21.38 19.67 0.50 o 0 10 1 426.91 390.88 3.67 o 1 10 1 4.91 7.81 0.62 o 2 10 1 134.50 131.29 1.78 o 3 10 1 29.94 32.06 0.71 o 4 10 1 187.31 180.07 2.15 o 5 10 1 2.27 4.22 0.69 o 6 10 1 113.65 123.10 1.53 o 7 10 1 246.51 259.73 3.32 o 8 10 1 3.01 3.13 0.49 o 9 10 1 95.85 111.54 2.22 o -8 11 1 98.76 99.04 2.16 o -7 11 1 5.11 6.91 0.83 o -6 11 1 0.12 1.26 0.62 o -5 11 1 25.83 23.11 0.97 o -4 11 1 38.55 41.15 0.87 o -3 11 1 4.87 3.14 0.52 o -2 11 1 278.18 249.11 3.72 o -1 11 1 55.82 54.67 0.94 o 0 11 1 61.23 50.30 1.09 o 1 11 1 99.32 106.63 1.28 o 2 11 1 185.64 186.08 1.82 o 3 11 1 16.79 15.26 0.64 o 4 11 1 59.09 68.65 1.28 o 5 11 1 167.54 173.04 2.26 o 6 11 1 4.75 2.59 0.65 o 7 11 1 21.45 24.87 1.03 o -6 12 1 86.57 97.74 1.52 o -5 12 1 2.91 1.90 0.52 o -4 12 1 1.35 1.13 0.51 o -3 12 1 3.89 2.88 0.54 o -2 12 1 25.38 23.14 0.78 o -1 12 1 0.42 0.35 0.55 o 0 12 1 137.52 113.72 1.42 o 1 12 1 13.00 11.84 0.68 o 2 12 1 40.09 37.19 0.90 o 3 12 1 39.03 38.93 1.23 o 4 12 1 0.78 0.66 0.49 o 5 12 1 13.25 15.36 1.04 o 6 12 1 15.56 14.62 2.84 o -4 13 1 54.46 58.15 1.31 o -3 13 1 7.98 8.61 0.74 o -2 13 1 10.22 11.47 2.11 o -1 13 1 6.74 7.25 1.27 o 0 13 1 1.03 0.79 0.69 o 1 13 1 44.86 43.82 1.04 o 2 13 1 9.88 11.43 0.62 o 3 13 1 0.00 0.20 0.49 o 4 13 1 13.63 12.71 0.77 o -13 0 2 34.03 37.86 1.67 o -12 0 2 20.92 24.34 2.22 o -11 0 2 6.84 6.41 0.95 o -10 0 2 34.34 35.60 2.60 o -9 0 2 109.24 109.91 4.50 o -8 0 2 1205.26 1187.14 15.84 o -7 0 2 351.63 340.98 4.24 o -6 0 2 4.16 2.54 0.49 o -5 0 2 134.73 114.50 1.50 o -4 0 2 319.83 322.09 6.22 o -3 0 2 457.87 385.11 3.99 o -2 0 2 387.39 330.75 2.76 o -1 0 2 6380.57 6492.38 77.60 o 0 0 2 22465.47 19933.98 327.45 o 1 0 2 4659.63 5064.38 64.42 o 2 0 2 81.80 72.18 0.62 o 3 0 2 806.90 809.70 11.67 o 4 0 2 2376.64 2652.56 37.36 o 5 0 2 2410.05 2657.18 36.97 o 6 0 2 26.97 25.72 0.56 o 7 0 2 830.58 830.33 26.79 o 8 0 2 191.61 191.85 2.36 o 9 0 2 674.07 697.31 9.27 o 10 0 2 0.14 0.18 0.63 o 11 0 2 8.89 11.36 0.93 o 12 0 2 33.28 38.32 1.75 o -13 1 2 2.79 2.62 0.69 o -12 1 2 37.68 46.23 1.86 o -11 1 2 74.94 76.49 1.38 o -10 1 2 532.44 536.42 5.61 o -9 1 2 581.58 579.27 5.47 o -8 1 2 325.67 317.40 3.16 o -7 1 2 15.03 18.39 0.83 o -6 1 2 722.13 728.82 6.41 o -5 1 2 120.63 122.46 1.19 o -4 1 2 93.54 78.01 0.96 o -3 1 2 271.54 243.90 1.94 o -2 1 2 2911.82 3147.11 25.76 o -1 1 2 2711.66 2939.09 20.38 o 0 1 2 5639.52 5910.88 51.92 o 1 1 2 154.74 170.03 1.71 o 2 1 2 576.80 643.21 11.28 o 3 1 2 240.42 242.15 4.24 o 4 1 2 206.18 227.48 1.63 o 5 1 2 0.10 1.01 0.24 o 6 1 2 611.86 644.91 5.21 o 7 1 2 82.62 81.49 1.09 o 8 1 2 238.26 223.14 2.12 o 9 1 2 95.94 100.50 1.22 o 10 1 2 5.92 5.70 0.54 o 11 1 2 0.03 0.05 0.29 o 12 1 2 46.02 51.41 0.98 o -13 2 2 8.59 9.79 0.94 o -12 2 2 4.01 3.49 0.75 o -11 2 2 6.54 8.49 0.74 o -10 2 2 0.08 0.52 0.58 o -9 2 2 455.91 440.32 4.25 o -8 2 2 3.21 4.12 0.52 o -7 2 2 97.90 102.69 1.23 o -6 2 2 5.96 5.80 0.45 o -5 2 2 17.65 23.22 0.60 o -4 2 2 303.66 297.02 2.39 o -3 2 2 2766.96 3123.47 42.95 o -2 2 2 372.04 407.41 3.15 o -1 2 2 906.82 1045.10 6.21 o 0 2 2 2460.61 2732.69 23.40 o 1 2 2 337.28 372.93 9.25 o 2 2 2 1277.41 1356.11 16.53 o 3 2 2 67.78 68.28 0.76 o 4 2 2 128.52 146.24 1.25 o 5 2 2 97.40 98.83 1.08 o 6 2 2 161.65 170.96 2.43 o 7 2 2 57.46 60.77 0.74 o 8 2 2 0.00 0.40 0.25 o 9 2 2 99.58 97.51 1.13 o 10 2 2 10.14 9.66 0.64 o 11 2 2 14.34 16.04 0.67 o 12 2 2 1.33 1.61 0.46 o -13 3 2 14.43 17.38 1.19 o -12 3 2 18.53 24.70 1.12 o -11 3 2 267.86 266.34 3.16 o -10 3 2 45.70 46.11 1.15 o -9 3 2 0.49 0.39 0.48 o -8 3 2 220.86 212.10 2.22 o -7 3 2 182.40 181.83 1.96 o -6 3 2 495.49 504.44 4.43 o -5 3 2 214.97 253.46 3.82 o -4 3 2 22.55 29.75 0.66 o -3 3 2 1404.60 1502.33 21.28 o -2 3 2 0.06 3.63 0.37 o -1 3 2 252.65 289.54 3.53 o 0 3 2 237.69 241.28 1.53 o 1 3 2 287.83 277.58 1.97 o 2 3 2 51.59 62.99 0.43 o 3 3 2 19.91 19.07 0.33 o 4 3 2 0.11 0.44 0.18 o 5 3 2 540.58 521.56 3.74 o 6 3 2 165.08 153.35 1.16 o 7 3 2 15.95 16.15 0.47 o 8 3 2 319.74 316.38 2.77 o 9 3 2 34.53 27.33 0.68 o 10 3 2 21.07 19.42 0.60 o 11 3 2 28.72 30.95 0.80 o 12 3 2 23.41 27.66 0.98 o -12 4 2 110.34 118.57 2.05 o -11 4 2 2.42 0.77 0.68 o -10 4 2 59.57 72.34 1.58 o -9 4 2 780.46 773.98 8.13 o -8 4 2 13.27 15.11 0.85 o -7 4 2 263.33 263.28 2.65 o -6 4 2 532.69 529.70 4.59 o -5 4 2 468.13 474.25 4.23 o -4 4 2 67.82 74.95 0.91 o -3 4 2 242.36 196.04 2.27 o -2 4 2 1890.37 2015.83 19.03 o -1 4 2 2.89 8.77 0.19 o 0 4 2 88.86 66.92 0.63 o 1 4 2 43.59 29.55 0.39 o 2 4 2 353.53 364.40 2.59 o 3 4 2 10.47 15.02 0.70 o 4 4 2 336.00 318.74 2.58 o 5 4 2 35.13 37.78 0.56 o 6 4 2 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