#------------------------------------------------------------------------------ #$Date: 2010-02-13 12:42:52 +0200 (Sat, 13 Feb 2010) $ #$Revision: 986 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224564.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224564_Fobs loop_ _publ_author_name 'Gowda, B. Thimme' 'Foro, Sabine' 'Nirmala, P. G.' 'Fuess, Hartmut' _publ_section_title ; N-(3,5-Dimethylphenyl)-4-methylbenzenesulfonamide ; _journal_coeditor_code BT5135 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o144 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.860 _cell_angle_beta 97.620 _cell_angle_gamma 108.140 _cell_length_a 8.3110 _cell_length_b 8.5210 _cell_length_c 11.4120 _exptl_crystal_F_000 292.00 _reflns_d_resolution_high 0.8002 _[local]_cod_data_source_file bt5135Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S29 P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 105.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 113.49 119.15 0.60 o 2 0 0 4835.97 4425.54 56.82 o 3 0 0 1141.49 1135.92 4.20 o 4 0 0 3.82 1.76 0.20 o 5 0 0 47.20 44.86 0.80 o 6 0 0 80.77 83.16 1.11 o 7 0 0 127.81 129.48 1.68 o 8 0 0 15.40 16.77 0.86 o 9 0 0 11.09 11.95 1.65 o -9 1 0 1.13 1.14 1.15 o -8 1 0 17.68 15.89 1.29 o -7 1 0 187.05 180.42 1.94 o -6 1 0 0.15 -0.03 0.27 o -5 1 0 0.48 0.11 0.22 o -4 1 0 103.64 123.33 1.93 o -3 1 0 219.72 192.57 1.92 o -2 1 0 131.08 136.82 2.52 o -1 1 0 491.35 513.24 1.52 o 1 1 0 105.14 99.39 0.76 o 2 1 0 30.11 36.63 0.32 o 3 1 0 90.14 82.83 0.69 o 4 1 0 22.67 24.83 0.46 o 5 1 0 133.51 127.66 1.29 o 6 1 0 1.72 2.18 0.54 o 7 1 0 0.13 0.31 0.40 o 8 1 0 90.78 87.46 1.53 o 9 1 0 29.44 29.13 1.65 o -10 2 0 19.62 21.84 1.72 o -9 2 0 1.59 0.56 1.12 o -8 2 0 34.40 31.68 1.58 o -7 2 0 38.69 37.62 1.51 o -6 2 0 0.00 -0.05 0.51 o -5 2 0 14.65 7.87 0.69 o -4 2 0 168.64 169.20 1.50 o -3 2 0 37.71 27.91 0.31 o -2 2 0 2292.02 2324.71 4.90 o -1 2 0 1510.77 1564.10 2.75 o 0 2 0 2.30 1.73 0.11 o 1 2 0 619.24 613.16 2.24 o 2 2 0 669.12 699.74 1.75 o 3 2 0 499.59 516.16 2.33 o 4 2 0 206.29 201.81 1.40 o 5 2 0 347.42 330.82 2.15 o 6 2 0 9.72 8.89 0.50 o 7 2 0 2.06 4.06 0.61 o 8 2 0 37.64 37.30 1.65 o -10 3 0 2.15 2.68 1.17 o -9 3 0 14.76 16.69 1.58 o -8 3 0 43.78 42.02 1.78 o -7 3 0 26.87 24.02 1.36 o -6 3 0 33.03 34.76 1.02 o -5 3 0 0.25 0.24 0.26 o -4 3 0 175.76 167.08 1.78 o -3 3 0 145.43 150.12 3.35 o -2 3 0 209.67 192.25 4.80 o -1 3 0 0.19 0.42 0.10 o 0 3 0 184.61 183.23 2.61 o 1 3 0 3.73 13.36 0.96 o 2 3 0 276.26 269.08 4.03 o 3 3 0 9.12 6.43 0.30 o 4 3 0 112.40 101.67 1.19 o 5 3 0 1.79 2.53 0.48 o 6 3 0 41.63 43.82 1.77 o 7 3 0 18.75 20.98 0.85 o 8 3 0 8.84 7.85 1.24 o -10 4 0 0.43 0.68 1.13 o -9 4 0 5.21 5.29 1.17 o -8 4 0 5.59 3.97 1.06 o -7 4 0 45.58 42.43 1.60 o -6 4 0 3.82 3.67 0.77 o -5 4 0 87.09 71.45 0.65 o -4 4 0 123.98 106.73 0.82 o -3 4 0 224.37 239.92 1.40 o -2 4 0 389.49 456.74 2.06 o -1 4 0 138.93 142.60 1.19 o 0 4 0 961.93 1048.54 3.59 o 1 4 0 237.21 237.10 3.32 o 2 4 0 18.21 18.97 0.53 o 3 4 0 46.43 41.29 0.67 o 4 4 0 74.20 72.10 1.11 o 5 4 0 21.45 19.72 0.76 o 6 4 0 8.88 8.75 0.82 o 7 4 0 29.95 33.97 3.13 o -10 5 0 0.29 -0.54 1.47 o -9 5 0 16.15 15.22 1.42 o -8 5 0 4.94 4.11 1.11 o -7 5 0 27.42 25.21 1.37 o -6 5 0 220.29 219.48 8.32 o -5 5 0 75.75 70.73 0.71 o -4 5 0 487.62 516.76 3.73 o -3 5 0 325.40 354.11 2.42 o -2 5 0 23.41 35.04 0.57 o -1 5 0 2.28 3.09 0.63 o 0 5 0 111.98 118.42 2.01 o 1 5 0 34.68 37.12 1.31 o 2 5 0 2.01 2.75 0.39 o 3 5 0 18.91 17.74 0.57 o 4 5 0 25.08 23.84 0.83 o 5 5 0 124.29 120.35 2.15 o 6 5 0 25.58 33.07 1.63 o -9 6 0 5.16 3.00 1.44 o -8 6 0 1.48 2.07 1.06 o -7 6 0 3.65 1.04 0.63 o -6 6 0 78.79 75.78 3.81 o -5 6 0 0.81 0.83 0.33 o -4 6 0 97.62 90.48 1.33 o -3 6 0 129.75 121.34 1.40 o -2 6 0 4.46 3.01 0.53 o -1 6 0 43.12 40.84 1.44 o 0 6 0 13.22 14.52 1.88 o 1 6 0 35.97 33.87 1.34 o 2 6 0 55.22 58.81 1.03 o 3 6 0 3.07 1.47 0.94 o 4 6 0 42.28 37.67 1.59 o 5 6 0 99.71 106.84 2.51 o -9 7 0 5.59 6.21 1.35 o -8 7 0 30.87 31.80 1.67 o -7 7 0 0.00 -0.45 0.67 o -6 7 0 42.36 39.83 1.04 o -5 7 0 132.57 138.11 6.35 o -4 7 0 18.26 20.70 0.82 o -3 7 0 45.45 45.78 1.05 o -2 7 0 126.32 122.49 2.48 o -1 7 0 16.33 18.47 1.28 o 0 7 0 13.68 13.06 1.17 o 1 7 0 1.24 0.47 0.87 o 2 7 0 69.14 66.97 2.49 o 3 7 0 2.02 2.58 0.93 o 4 7 0 1.16 0.22 1.06 o -8 8 0 13.06 16.50 1.32 o -7 8 0 17.84 20.82 1.30 o -6 8 0 8.77 7.05 0.74 o -5 8 0 131.97 130.57 3.10 o -4 8 0 0.18 0.07 0.64 o -3 8 0 79.95 74.67 2.21 o -2 8 0 28.85 24.80 1.58 o -1 8 0 15.42 12.56 1.40 o 0 8 0 34.75 32.64 1.70 o 1 8 0 0.46 0.06 1.12 o 2 8 0 7.47 6.29 0.74 o 3 8 0 19.94 21.76 1.45 o -7 9 0 11.48 12.96 1.12 o -6 9 0 3.60 2.27 0.71 o -5 9 0 3.18 3.10 0.65 o -4 9 0 7.29 6.69 1.19 o -3 9 0 9.77 10.13 1.34 o -2 9 0 46.98 53.01 2.17 o -1 9 0 5.50 5.56 1.21 o 0 9 0 60.78 66.78 2.39 o 1 9 0 2.45 2.18 1.27 o -6 10 0 2.08 2.26 0.73 o -5 10 0 1.10 -0.69 0.73 o -4 10 0 4.93 3.95 1.35 o -3 10 0 6.26 6.15 1.37 o -2 10 0 24.75 26.40 1.90 o -1 10 0 8.85 10.77 1.54 o 1 -10 1 12.14 11.75 1.72 o 2 -10 1 26.47 27.03 1.81 o 3 -10 1 36.18 37.56 1.97 o 4 -10 1 2.95 2.70 1.29 o 5 -10 1 2.56 2.26 0.92 o 6 -10 1 1.63 2.34 0.74 o -2 -9 1 9.95 9.40 0.97 o -1 -9 1 17.95 18.32 1.48 o 0 -9 1 8.08 6.55 1.32 o 1 -9 1 17.17 17.14 1.55 o 2 -9 1 67.63 63.67 2.29 o 3 -9 1 9.73 9.27 1.38 o 4 -9 1 54.80 51.87 1.28 o 5 -9 1 4.00 2.10 0.62 o 6 -9 1 8.30 9.36 0.79 o 7 -9 1 11.96 11.92 1.09 o -3 -8 1 19.55 18.81 1.44 o -2 -8 1 0.96 0.61 0.97 o -1 -8 1 46.11 46.27 1.84 o 0 -8 1 11.26 12.06 1.29 o 1 -8 1 139.52 130.13 2.77 o 2 -8 1 77.31 77.86 2.22 o 3 -8 1 25.35 20.77 0.95 o 4 -8 1 83.28 87.29 1.47 o 5 -8 1 74.63 73.35 1.26 o 6 -8 1 14.31 15.05 0.88 o 7 -8 1 37.10 40.14 1.59 o 8 -8 1 0.27 0.46 0.99 o -5 -7 1 22.81 23.34 1.62 o -4 -7 1 7.84 6.60 1.20 o -3 -7 1 6.89 5.67 0.98 o -2 -7 1 88.88 89.65 1.37 o -1 -7 1 0.04 0.04 0.46 o 0 -7 1 15.92 18.68 0.73 o 1 -7 1 1.34 0.39 0.95 o 2 -7 1 84.15 82.92 1.36 o 3 -7 1 24.20 23.82 0.84 o 4 -7 1 0.83 0.76 0.57 o 5 -7 1 198.46 183.88 1.84 o 6 -7 1 17.18 16.31 1.10 o 7 -7 1 41.12 44.54 1.16 o 8 -7 1 4.37 4.76 1.17 o 9 -7 1 14.70 17.98 1.71 o -6 -6 1 29.15 27.35 1.50 o -5 -6 1 27.43 26.11 1.48 o -4 -6 1 5.48 4.42 0.88 o -3 -6 1 27.21 28.62 0.83 o -2 -6 1 18.50 16.23 1.86 o -1 -6 1 0.60 1.48 0.43 o 0 -6 1 22.12 20.88 1.12 o 1 -6 1 11.19 11.10 0.97 o 2 -6 1 111.50 119.30 4.22 o 3 -6 1 303.08 304.30 2.74 o 4 -6 1 8.28 8.30 0.76 o 5 -6 1 72.55 71.08 0.87 o 6 -6 1 58.71 56.74 2.60 o 7 -6 1 1.50 0.80 0.58 o 8 -6 1 1.84 2.48 0.99 o 9 -6 1 0.00 0.39 1.16 o -7 -5 1 1.90 4.10 1.31 o -6 -5 1 21.01 27.17 1.02 o -5 -5 1 15.66 16.14 0.82 o -4 -5 1 28.16 24.10 0.78 o -3 -5 1 65.55 64.04 1.67 o -2 -5 1 13.98 10.15 0.55 o -1 -5 1 11.28 11.21 1.31 o 0 -5 1 343.02 348.69 3.21 o 1 -5 1 4.69 3.74 0.41 o 2 -5 1 87.46 73.76 1.05 o 3 -5 1 928.21 875.89 5.53 o 4 -5 1 31.04 36.11 0.84 o 5 -5 1 70.53 66.98 0.71 o 6 -5 1 243.68 242.93 1.57 o 7 -5 1 2.91 2.47 0.98 o 8 -5 1 6.77 6.88 1.15 o 9 -5 1 9.79 7.48 1.35 o 10 -5 1 4.20 3.88 1.31 o -7 -4 1 50.49 58.86 1.48 o -6 -4 1 1.69 2.33 0.58 o -5 -4 1 27.22 29.40 0.84 o -4 -4 1 0.92 0.90 0.44 o -3 -4 1 31.52 25.74 0.64 o -2 -4 1 94.91 109.38 5.78 o -1 -4 1 25.60 24.61 0.51 o 0 -4 1 142.40 153.67 1.06 o 1 -4 1 80.72 130.37 1.16 o 2 -4 1 58.44 58.17 0.58 o 3 -4 1 1.05 0.30 0.21 o 4 -4 1 179.22 169.84 2.48 o 5 -4 1 0.09 0.83 0.32 o 6 -4 1 7.04 7.71 0.49 o 7 -4 1 61.00 55.59 1.82 o 8 -4 1 2.60 2.61 1.12 o 9 -4 1 12.00 13.02 1.45 o 10 -4 1 0.08 -0.19 1.17 o -8 -3 1 9.11 13.82 1.38 o -7 -3 1 60.81 58.39 1.83 o -6 -3 1 5.67 4.98 0.72 o -5 -3 1 43.97 44.05 0.91 o -4 -3 1 58.97 53.84 0.89 o -3 -3 1 14.19 12.53 0.32 o -2 -3 1 1475.89 1465.00 2.89 o -1 -3 1 9.83 5.29 0.29 o 0 -3 1 240.64 246.77 1.08 o 1 -3 1 952.42 980.28 4.94 o 2 -3 1 70.31 93.09 0.88 o 3 -3 1 28.58 25.56 0.33 o 4 -3 1 355.24 358.81 1.66 o 5 -3 1 23.23 24.02 0.58 o 6 -3 1 15.07 13.58 0.54 o 7 -3 1 126.67 123.84 2.53 o 8 -3 1 3.00 1.28 1.22 o 9 -3 1 64.39 59.38 2.22 o 10 -3 1 7.84 11.40 1.38 o -8 -2 1 1.19 0.28 1.03 o -7 -2 1 72.43 69.69 1.86 o -6 -2 1 20.16 18.17 0.56 o -5 -2 1 6.82 4.86 0.63 o -4 -2 1 98.74 96.90 1.05 o -3 -2 1 61.45 71.68 0.85 o -2 -2 1 1986.34 1931.83 5.24 o -1 -2 1 1415.73 1303.10 18.47 o 0 -2 1 42.30 43.74 0.76 o 1 -2 1 370.06 361.45 1.29 o 2 -2 1 227.65 228.06 2.17 o 3 -2 1 33.59 38.48 0.38 o 4 -2 1 12.85 14.87 0.29 o 5 -2 1 15.73 16.22 0.65 o 6 -2 1 32.32 32.99 0.73 o 7 -2 1 22.38 22.41 1.52 o 8 -2 1 22.71 19.30 1.50 o 9 -2 1 7.80 9.00 1.43 o 10 -2 1 3.53 4.14 1.39 o -9 -1 1 26.67 26.62 1.63 o -8 -1 1 4.20 4.77 0.71 o -7 -1 1 13.96 13.18 0.72 o -6 -1 1 71.14 65.42 1.02 o -5 -1 1 4.41 5.48 0.40 o -4 -1 1 402.76 377.26 3.52 o -3 -1 1 10.10 10.72 0.26 o -2 -1 1 2277.69 2109.83 5.23 o -1 -1 1 6135.83 5785.63 308.96 o 0 -1 1 3070.73 2676.25 74.40 o 1 -1 1 6310.16 6026.30 160.82 o 2 -1 1 1138.89 1145.84 3.03 o 3 -1 1 14.77 18.36 0.48 o 4 -1 1 46.82 52.67 0.60 o 5 -1 1 0.38 0.41 0.34 o 6 -1 1 2.70 2.15 0.84 o 7 -1 1 182.41 177.77 1.75 o 8 -1 1 5.50 4.97 1.07 o 9 -1 1 5.49 5.83 1.30 o -9 0 1 15.19 17.58 1.48 o -8 0 1 1.83 1.63 0.60 o -7 0 1 111.84 110.09 3.82 o -6 0 1 324.60 298.95 2.21 o -5 0 1 0.62 0.53 0.27 o -4 0 1 1495.95 1454.12 2.55 o -3 0 1 11.76 12.95 0.56 o -2 0 1 8788.74 9376.87 66.50 o -1 0 1 818.78 862.75 6.57 o 1 0 1 1988.57 1963.70 10.77 o 2 0 1 149.18 146.73 2.46 o 3 0 1 3.09 2.74 0.22 o 4 0 1 2.31 1.52 0.19 o 5 0 1 12.95 14.24 0.61 o 6 0 1 8.34 6.13 0.47 o 7 0 1 81.08 86.16 1.08 o 8 0 1 42.26 44.33 1.27 o 9 0 1 0.44 -0.17 0.95 o -10 1 1 2.04 -0.71 1.39 o -9 1 1 13.54 15.49 1.31 o -8 1 1 0.08 0.48 0.59 o -7 1 1 37.25 36.44 1.01 o -6 1 1 0.86 0.49 0.44 o -5 1 1 0.10 1.80 0.21 o -4 1 1 150.80 150.74 1.92 o -3 1 1 258.83 269.75 2.72 o -2 1 1 594.67 584.18 2.64 o -1 1 1 86.80 98.71 1.28 o 0 1 1 307.76 316.52 1.35 o 1 1 1 332.99 348.46 2.72 o 2 1 1 740.45 707.03 2.82 o 3 1 1 128.24 111.09 1.41 o 4 1 1 255.55 246.82 1.56 o 5 1 1 379.31 346.67 5.27 o 6 1 1 365.73 359.83 1.97 o 7 1 1 18.58 17.09 0.60 o 8 1 1 18.44 18.31 0.90 o 9 1 1 0.07 -1.12 1.12 o -9 2 1 0.51 -1.04 1.04 o -8 2 1 128.87 134.65 2.73 o -7 2 1 1.57 2.08 0.86 o -6 2 1 74.78 72.25 1.68 o -5 2 1 158.26 142.26 4.54 o -4 2 1 321.70 316.12 1.36 o -3 2 1 18.68 22.18 0.26 o -2 2 1 8445.20 9118.46 38.36 o -1 2 1 583.95 628.97 24.03 o 0 2 1 336.42 314.75 1.09 o 1 2 1 477.86 493.91 2.06 o 2 2 1 6.98 6.34 0.31 o 3 2 1 238.18 226.53 1.56 o 4 2 1 59.92 57.58 2.11 o 5 2 1 232.09 226.92 1.49 o 6 2 1 0.12 0.23 0.39 o 7 2 1 0.99 0.83 0.56 o 8 2 1 13.69 14.20 1.23 o -10 3 1 4.49 2.84 1.19 o -9 3 1 16.21 12.27 1.37 o -8 3 1 27.07 30.02 1.64 o -7 3 1 0.01 -0.92 0.92 o -6 3 1 62.30 59.99 1.59 o -5 3 1 64.03 62.87 0.97 o -4 3 1 185.15 220.07 0.87 o -3 3 1 187.03 213.83 1.19 o -2 3 1 497.68 499.67 2.86 o -1 3 1 538.35 578.96 3.10 o 0 3 1 24.33 27.25 0.66 o 1 3 1 53.30 64.75 1.35 o 2 3 1 41.75 50.65 0.58 o 3 3 1 235.00 230.36 1.51 o 4 3 1 0.06 0.14 0.59 o 5 3 1 0.36 0.30 0.63 o 6 3 1 91.57 84.52 2.60 o 7 3 1 2.56 2.98 0.66 o 8 3 1 19.67 20.77 1.38 o -10 4 1 8.60 8.84 1.57 o -9 4 1 0.03 0.17 1.40 o -8 4 1 38.74 37.01 1.73 o -7 4 1 15.40 13.37 1.16 o -6 4 1 0.95 1.55 0.76 o -5 4 1 550.54 541.59 9.29 o -4 4 1 978.70 979.12 2.13 o -3 4 1 181.39 226.01 1.19 o -2 4 1 286.59 296.48 2.90 o -1 4 1 161.57 151.98 1.69 o 0 4 1 26.02 22.44 0.48 o 1 4 1 295.27 300.48 3.91 o 2 4 1 6.81 8.18 0.37 o 3 4 1 352.51 317.08 2.06 o 4 4 1 56.21 54.84 1.01 o 5 4 1 21.56 26.15 1.48 o 6 4 1 57.00 56.43 1.74 o 7 4 1 51.71 60.30 1.88 o -10 5 1 7.86 7.05 1.53 o -9 5 1 1.82 0.46 1.29 o -8 5 1 36.23 30.47 1.59 o -7 5 1 0.41 0.70 0.87 o -6 5 1 2.06 0.41 0.49 o -5 5 1 124.04 124.88 1.37 o -4 5 1 71.06 80.16 0.71 o -3 5 1 0.54 0.26 0.24 o -2 5 1 22.54 24.80 0.57 o -1 5 1 0.62 0.90 0.61 o 0 5 1 130.93 122.07 4.15 o 1 5 1 39.50 38.00 0.70 o 2 5 1 46.86 40.50 1.51 o 3 5 1 92.72 86.28 1.96 o 4 5 1 263.77 271.03 3.35 o 5 5 1 17.11 23.37 1.45 o 6 5 1 57.92 64.43 2.04 o -9 6 1 14.35 17.17 1.75 o -8 6 1 0.02 -0.14 1.11 o -7 6 1 47.70 44.89 1.13 o -6 6 1 22.56 22.02 0.89 o -5 6 1 30.73 29.90 0.66 o -4 6 1 97.78 83.99 1.10 o -3 6 1 0.73 0.07 0.67 o -2 6 1 0.01 -0.35 0.71 o -1 6 1 42.69 39.47 1.44 o 0 6 1 116.13 119.79 2.29 o 1 6 1 22.67 20.03 1.19 o 2 6 1 6.06 4.94 0.84 o 3 6 1 52.58 53.57 1.74 o 4 6 1 32.15 36.67 1.59 o 5 6 1 11.35 12.30 1.28 o -9 7 1 6.18 8.15 1.53 o -8 7 1 29.28 31.54 1.67 o -7 7 1 22.91 21.04 1.13 o -6 7 1 77.70 81.31 2.19 o -5 7 1 17.18 16.80 1.80 o -4 7 1 115.62 113.49 2.78 o -3 7 1 32.04 32.19 1.48 o -2 7 1 3.79 1.84 1.00 o -1 7 1 102.93 99.47 2.35 o 0 7 1 2.91 3.07 1.06 o 1 7 1 2.54 1.88 0.93 o 2 7 1 21.69 23.73 0.98 o 3 7 1 3.53 2.57 0.90 o 4 7 1 3.12 2.48 0.95 o -8 8 1 9.88 12.70 1.27 o -7 8 1 3.95 3.73 0.89 o -6 8 1 14.76 14.78 0.82 o -5 8 1 0.14 -0.43 0.63 o -4 8 1 10.13 8.25 1.18 o -3 8 1 14.41 14.53 1.42 o -2 8 1 15.09 12.62 1.43 o -1 8 1 44.99 47.00 1.97 o 0 8 1 16.32 17.13 1.41 o 1 8 1 14.28 15.84 0.95 o 2 8 1 8.41 8.12 0.83 o 3 8 1 11.91 8.07 1.16 o -7 9 1 18.11 20.83 1.40 o -6 9 1 7.87 8.21 0.80 o -5 9 1 3.99 3.97 0.78 o -4 9 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