#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/45/2224590.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224590_Fobs loop_ _publ_author_name 'Jasinski, Jerry P.' 'Hakim Al-arique, Q. N. M.' 'Butcher, Ray J.' 'Yathirajan, H. S.' 'Narayana, B.' _publ_section_title ; 6,11-Dihydrodibenz[b,e]oxepin-11-one ; _journal_coeditor_code CI2982 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o159 _journal_page_last o160 _journal_volume 66 _journal_year 2010 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.654 _cell_angle_gamma 90.000 _cell_length_a 16.5065 _cell_length_b 4.0806 _cell_length_c 15.0392 _exptl_crystal_F_000 440.00 _reflns_d_resolution_high 0.8028 _[local]_cod_data_source_file ci2982Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hsy119 in Cc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 72.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 3155.76 3435.31 27.84 o 6 0 0 1471.98 1676.08 5.60 o 8 0 0 4768.97 5323.58 11.87 o 10 0 0 1055.55 1228.59 6.57 o 12 0 0 220.44 261.30 2.90 o 14 0 0 528.69 519.08 6.07 o 16 0 0 538.30 474.79 5.45 o 18 0 0 70.19 60.73 1.81 o 20 0 0 254.39 302.38 2.56 o 1 1 0 3808.98 3689.48 70.36 o 5 1 0 843.53 899.04 5.91 o 7 1 0 593.62 598.80 8.38 o 9 1 0 305.94 367.27 2.94 o 11 1 0 263.24 319.59 4.43 o 13 1 0 28.10 33.51 1.94 o 15 1 0 51.07 44.50 1.32 o 17 1 0 43.76 44.59 1.84 o 19 1 0 66.90 78.77 1.70 o 0 2 0 21.65 26.43 0.88 o 2 2 0 5294.90 5040.66 124.15 o 4 2 0 668.01 663.96 5.19 o 6 2 0 4191.50 4160.30 13.97 o 8 2 0 23.97 23.56 1.41 o 10 2 0 2.85 3.33 0.83 o 12 2 0 40.42 46.69 6.09 o 14 2 0 101.11 95.57 2.29 o 16 2 0 111.22 110.69 2.35 o 18 2 0 8.41 7.48 0.68 o 1 3 0 153.67 154.06 1.97 o 3 3 0 1115.89 1089.70 5.54 o 5 3 0 1179.25 1055.74 5.46 o 7 3 0 36.78 41.84 1.45 o 9 3 0 43.90 41.67 1.93 o 11 3 0 17.63 14.86 1.30 o 13 3 0 4.84 8.20 1.04 o 15 3 0 141.08 160.52 2.35 o 0 4 0 249.53 232.57 3.74 o 2 4 0 63.41 63.86 1.78 o 4 4 0 310.03 304.05 14.90 o 6 4 0 111.07 117.00 2.77 o 8 4 0 83.85 72.48 2.12 o 10 4 0 2.86 4.11 0.86 o 12 4 0 51.79 54.02 1.33 o -19 1 1 92.09 93.80 1.89 o -17 1 1 117.73 111.66 2.65 o -15 1 1 644.98 595.86 20.21 o -13 1 1 124.59 120.45 2.12 o -11 1 1 506.00 531.23 3.79 o -9 1 1 79.45 94.77 1.45 o -7 1 1 550.53 573.48 5.38 o -5 1 1 2248.84 2098.45 29.60 o -3 1 1 1513.50 1574.30 5.98 o 3 1 1 123.30 98.72 1.85 o 5 1 1 3111.13 3205.35 107.24 o 7 1 1 2984.04 3102.78 10.43 o 9 1 1 107.43 121.62 1.54 o 11 1 1 392.53 395.12 8.50 o 13 1 1 25.52 28.27 1.50 o 15 1 1 251.33 213.87 9.55 o 17 1 1 38.57 34.77 1.56 o 19 1 1 5.24 4.67 0.71 o -18 2 1 52.38 58.31 1.29 o -16 2 1 175.59 171.21 2.92 o -14 2 1 20.88 22.34 4.52 o -12 2 1 402.34 400.56 5.04 o -10 2 1 169.06 173.91 8.38 o -8 2 1 150.82 145.66 2.79 o -4 2 1 188.07 178.91 2.74 o -2 2 1 1212.78 1231.08 23.65 o 0 2 1 921.24 935.12 3.40 o 2 2 1 1700.81 1704.37 21.77 o 4 2 1 2390.31 2372.33 10.01 o 6 2 1 113.70 126.18 2.61 o 8 2 1 298.54 299.67 4.12 o 10 2 1 351.61 330.82 4.05 o 12 2 1 184.38 185.19 6.47 o 14 2 1 133.67 116.99 5.04 o 16 2 1 5.62 2.86 0.87 o 18 2 1 27.64 30.21 0.93 o -15 3 1 131.43 168.26 2.35 o -13 3 1 103.86 107.63 2.45 o -11 3 1 17.54 17.82 1.43 o -9 3 1 3.87 3.05 1.13 o -7 3 1 461.77 427.20 5.39 o -5 3 1 983.63 942.30 34.81 o -3 3 1 210.44 233.14 17.95 o -1 3 1 29.60 29.57 1.40 o 1 3 1 213.31 227.33 6.91 o 3 3 1 302.57 297.05 9.52 o 5 3 1 378.53 350.26 5.69 o 7 3 1 149.04 133.86 4.83 o 9 3 1 57.00 55.22 1.49 o 11 3 1 151.20 148.30 3.21 o 13 3 1 7.95 6.86 0.99 o 15 3 1 9.46 11.10 0.84 o -12 4 1 37.43 46.26 1.22 o -10 4 1 176.05 159.20 2.66 o -8 4 1 189.73 185.08 3.26 o -6 4 1 145.34 151.99 3.11 o -4 4 1 22.26 39.41 8.84 o -2 4 1 215.38 228.09 17.27 o 0 4 1 116.69 115.29 8.19 o 2 4 1 213.36 214.83 3.69 o 4 4 1 177.85 164.34 2.21 o 6 4 1 342.12 310.96 9.26 o 8 4 1 77.21 77.47 2.16 o 10 4 1 64.84 70.74 1.85 o 12 4 1 28.16 30.19 1.08 o -20 0 2 165.93 176.71 2.01 o -18 0 2 16.68 19.53 1.18 o -16 0 2 705.41 648.62 6.79 o -14 0 2 1690.68 1503.53 20.21 o -12 0 2 1145.01 1095.80 8.36 o -10 0 2 19.37 24.01 1.04 o -8 0 2 296.12 341.88 2.92 o -6 0 2 328.73 372.50 2.32 o 2 0 2 812.97 755.65 2.39 o 6 0 2 2903.71 3001.69 39.80 o 8 0 2 1717.73 2093.92 13.39 o 10 0 2 564.87 715.70 4.99 o 12 0 2 684.51 698.14 6.34 o 14 0 2 190.95 172.94 3.37 o 16 0 2 160.46 144.81 2.98 o 18 0 2 23.23 20.05 1.14 o 20 0 2 13.71 12.03 0.61 o -19 1 2 54.04 51.00 1.42 o -17 1 2 70.88 59.29 2.06 o -15 1 2 238.97 237.94 4.38 o -13 1 2 547.68 518.56 4.69 o -11 1 2 1037.57 1026.66 4.99 o -9 1 2 72.66 82.58 1.21 o -7 1 2 521.05 560.54 3.14 o -5 1 2 240.78 233.35 2.59 o -3 1 2 804.17 772.55 4.07 o 3 1 2 752.12 751.74 2.60 o 5 1 2 462.26 461.62 2.42 o 7 1 2 1635.26 1845.11 7.90 o 9 1 2 772.10 870.54 12.44 o 11 1 2 140.92 166.82 1.70 o 13 1 2 10.06 8.96 1.47 o 15 1 2 158.37 137.33 7.57 o 17 1 2 2.37 2.23 0.85 o 19 1 2 79.12 83.55 1.65 o -18 2 2 85.51 95.23 1.60 o -16 2 2 177.62 167.71 2.88 o -14 2 2 107.28 128.71 8.76 o -12 2 2 278.83 300.85 8.58 o -10 2 2 167.37 174.92 5.47 o -8 2 2 332.16 290.99 3.85 o -6 2 2 961.22 917.00 6.38 o -4 2 2 1158.91 1203.30 28.45 o -2 2 2 117.77 116.08 1.03 o 0 2 2 284.14 308.07 2.17 o 2 2 2 2207.92 2232.37 5.68 o 4 2 2 2002.65 2014.19 10.75 o 6 2 2 334.75 343.92 4.29 o 8 2 2 206.34 196.91 3.53 o 10 2 2 218.12 237.41 3.62 o 12 2 2 72.62 72.56 2.16 o 14 2 2 16.87 21.30 0.96 o 16 2 2 23.27 24.30 1.17 o 18 2 2 47.11 44.87 1.02 o -15 3 2 9.89 21.54 1.01 o -13 3 2 62.34 73.80 2.11 o -11 3 2 469.28 456.88 5.38 o -9 3 2 386.41 364.22 5.02 o -7 3 2 216.52 226.02 3.96 o -5 3 2 349.29 312.33 12.65 o -3 3 2 313.42 295.10 2.87 o -1 3 2 167.94 148.81 2.81 o 1 3 2 499.44 565.68 7.12 o 3 3 2 546.09 541.60 8.12 o 5 3 2 774.01 715.58 20.39 o 7 3 2 63.74 53.35 1.57 o 9 3 2 73.16 70.53 4.94 o 11 3 2 200.74 191.00 3.53 o 13 3 2 34.56 30.33 1.50 o 15 3 2 28.89 40.25 1.27 o -12 4 2 22.83 25.95 0.98 o -10 4 2 59.35 69.51 1.82 o -8 4 2 233.10 219.46 3.49 o -6 4 2 238.90 239.79 3.79 o -4 4 2 7.72 9.57 1.16 o -2 4 2 26.54 28.34 1.09 o 0 4 2 56.53 53.81 2.00 o 2 4 2 141.66 141.31 3.11 o 4 4 2 219.21 195.20 2.39 o 6 4 2 160.73 148.61 2.05 o 8 4 2 54.65 55.31 1.22 o 10 4 2 121.89 130.31 2.40 o 12 4 2 6.70 6.18 0.72 o -19 1 3 77.60 76.86 1.69 o -17 1 3 86.14 79.77 2.33 o -15 1 3 157.28 151.09 5.41 o -13 1 3 718.91 669.47 7.18 o -11 1 3 170.82 177.62 9.43 o -9 1 3 730.80 728.91 9.85 o -7 1 3 1062.60 1061.47 6.61 o -5 1 3 239.08 273.96 36.16 o -3 1 3 1021.53 999.20 7.36 o -1 1 3 1396.99 1354.76 3.41 o 1 1 3 784.54 754.21 7.51 o 3 1 3 647.33 610.08 3.90 o 5 1 3 15.70 9.14 0.50 o 7 1 3 625.66 677.56 11.22 o 9 1 3 493.45 572.17 6.12 o 11 1 3 34.80 37.59 7.85 o 13 1 3 121.57 145.17 3.83 o 15 1 3 40.93 40.25 1.76 o 17 1 3 30.68 30.37 1.41 o 19 1 3 23.12 26.74 0.97 o -18 2 3 89.72 99.22 1.59 o -16 2 3 223.71 219.00 3.28 o -14 2 3 113.02 126.64 10.71 o -12 2 3 764.44 753.96 13.47 o -10 2 3 630.20 608.38 5.73 o -8 2 3 78.83 79.49 2.16 o -6 2 3 478.80 495.79 4.27 o -4 2 3 1253.65 1266.26 5.17 o -2 2 3 100.60 116.07 1.46 o 0 2 3 326.63 361.67 4.26 o 2 2 3 24.80 25.50 0.93 o 4 2 3 386.88 369.17 3.48 o 6 2 3 468.48 455.03 5.08 o 8 2 3 2.60 1.48 0.96 o 10 2 3 228.34 227.50 8.18 o 12 2 3 0.49 0.56 0.64 o 14 2 3 200.43 183.72 7.31 o 16 2 3 73.80 76.83 1.80 o -15 3 3 34.61 36.42 1.07 o -13 3 3 19.02 19.37 1.21 o -11 3 3 71.10 71.46 2.25 o -9 3 3 24.90 25.26 1.62 o -7 3 3 224.89 206.44 3.71 o -5 3 3 51.22 43.75 1.34 o -3 3 3 6.89 7.35 1.39 o -1 3 3 15.21 16.15 2.92 o 1 3 3 15.17 16.91 0.85 o 3 3 3 468.41 453.54 6.41 o 5 3 3 159.47 151.86 6.38 o 7 3 3 68.04 58.64 1.65 o 9 3 3 203.80 190.63 9.23 o 11 3 3 230.12 210.77 8.02 o 13 3 3 123.58 129.61 2.74 o -12 4 3 46.01 42.59 1.12 o -10 4 3 208.96 211.51 2.93 o -8 4 3 3.03 3.37 0.93 o -6 4 3 208.86 195.61 3.35 o -4 4 3 75.71 75.81 2.25 o -2 4 3 25.98 17.17 1.38 o 0 4 3 40.29 37.09 1.72 o 2 4 3 46.89 47.59 1.97 o 4 4 3 37.05 33.10 1.64 o 6 4 3 79.41 71.36 1.49 o 8 4 3 19.75 20.18 1.99 o 10 4 3 34.86 36.97 0.88 o 12 4 3 147.30 177.69 2.14 o -20 0 4 20.25 17.61 0.67 o -18 0 4 309.95 294.30 3.81 o -16 0 4 72.93 68.30 2.83 o -14 0 4 325.83 289.35 4.77 o -12 0 4 482.19 455.65 5.64 o -10 0 4 36.94 77.41 29.72 o -8 0 4 1286.40 1493.60 8.42 o -6 0 4 2202.39 2428.61 7.80 o 0 0 4 2175.44 2306.83 23.26 o 2 0 4 451.12 436.42 1.31 o 4 0 4 342.70 327.28 2.60 o 6 0 4 206.23 180.73 1.80 o 8 0 4 1216.06 1478.35 55.57 o 10 0 4 15.41 12.99 1.24 o 12 0 4 357.21 323.91 4.29 o 14 0 4 440.30 392.04 4.89 o 16 0 4 30.42 27.38 1.40 o 18 0 4 46.77 39.94 1.33 o -19 1 4 17.67 17.35 0.96 o -17 1 4 67.91 71.63 2.31 o -15 1 4 527.07 498.44 15.49 o -13 1 4 393.96 370.74 8.47 o -11 1 4 178.19 168.26 2.40 o -9 1 4 427.30 434.36 11.23 o -7 1 4 729.19 793.78 18.98 o -5 1 4 646.87 718.36 10.07 o -3 1 4 277.35 288.87 1.89 o -1 1 4 812.09 844.64 2.11 o 1 1 4 1190.50 1136.54 7.35 o 3 1 4 26.47 27.90 0.59 o 5 1 4 1067.60 1066.69 4.92 o 7 1 4 34.65 37.75 5.48 o 9 1 4 96.00 90.85 1.59 o 11 1 4 273.21 291.94 2.74 o 13 1 4 214.11 233.79 2.49 o 15 1 4 387.41 352.46 10.60 o 17 1 4 77.92 76.36 1.95 o 19 1 4 17.70 27.20 0.90 o -18 2 4 34.93 41.64 1.04 o -16 2 4 43.79 41.61 1.53 o -14 2 4 10.87 11.18 1.61 o -12 2 4 525.64 551.83 5.54 o -10 2 4 933.35 928.46 7.04 o -8 2 4 145.91 141.20 2.04 o -6 2 4 0.27 0.38 0.51 o -4 2 4 72.30 72.29 1.88 o -2 2 4 530.46 515.32 6.56 o 0 2 4 166.20 168.30 4.20 o 2 2 4 217.79 209.80 7.72 o 4 2 4 393.88 375.46 3.70 o 8 2 4 294.79 292.00 8.97 o 10 2 4 220.83 222.10 3.60 o 12 2 4 130.05 123.12 3.12 o 14 2 4 128.14 127.35 14.20 o 16 2 4 131.72 157.21 2.35 o -15 3 4 22.31 29.22 0.93 o -13 3 4 106.76 114.93 2.40 o -11 3 4 411.24 429.48 5.04 o -9 3 4 397.08 380.13 4.98 o -7 3 4 448.17 417.43 5.19 o -5 3 4 343.20 311.19 14.45 o -3 3 4 140.88 126.82 5.38 o -1 3 4 58.65 69.71 5.14 o 1 3 4 229.67 246.57 3.82 o 3 3 4 224.22 218.92 2.97 o 5 3 4 78.46 74.36 4.44 o 7 3 4 193.75 173.38 5.94 o 9 3 4 24.39 22.61 1.54 o 11 3 4 140.36 151.64 2.19 o 13 3 4 15.25 20.42 1.36 o -12 4 4 27.87 28.61 0.85 o -10 4 4 169.73 172.93 2.56 o -8 4 4 191.04 192.96 3.03 o -6 4 4 195.62 195.47 3.28 o -4 4 4 91.03 88.24 1.65 o -2 4 4 40.40 38.33 1.18 o 0 4 4 43.40 42.50 1.93 o 2 4 4 59.89 54.60 2.12 o 4 4 4 71.84 69.00 2.27 o 6 4 4 15.05 16.21 0.88 o 8 4 4 17.88 15.89 0.81 o 10 4 4 2.93 2.23 0.47 o -19 1 5 6.03 11.00 0.80 o -17 1 5 52.31 61.20 2.14 o -15 1 5 126.24 123.84 2.09 o -13 1 5 316.98 297.02 3.53 o -11 1 5 610.04 588.41 4.49 o -9 1 5 181.18 193.37 5.35 o -7 1 5 142.87 148.75 1.69 o -5 1 5 650.50 702.41 13.90 o -3 1 5 1365.65 1342.03 6.20 o -1 1 5 71.24 70.59 1.01 o 1 1 5 664.49 674.78 8.66 o 3 1 5 563.58 571.93 2.50 o 5 1 5 1128.35 1131.67 3.83 o 7 1 5 260.10 279.63 2.65 o 9 1 5 171.82 180.93 5.29 o 11 1 5 576.35 524.27 2.89 o 13 1 5 800.50 728.53 9.28 o 15 1 5 64.07 67.30 4.04 o 17 1 5 63.24 58.95 1.69 o 19 1 5 67.86 76.08 1.23 o -18 2 5 29.40 22.85 0.80 o -16 2 5 73.51 68.71 1.89 o -14 2 5 12.54 13.40 1.32 o -12 2 5 164.51 186.43 3.22 o -10 2 5 93.56 94.41 2.40 o -8 2 5 3.02 4.18 0.96 o -6 2 5 32.77 41.27 1.06 o -4 2 5 683.97 745.49 4.46 o -2 2 5 131.82 133.31 1.60 o 0 2 5 1616.94 1569.95 14.25 o 2 2 5 327.67 331.59 3.27 o 4 2 5 1.74 0.85 0.51 o 6 2 5 71.19 68.21 1.85 o 8 2 5 161.00 132.26 4.22 o 10 2 5 232.82 211.61 2.66 o 12 2 5 45.24 44.11 1.02 o 14 2 5 178.99 186.25 14.02 o 16 2 5 13.72 11.16 0.77 o -15 3 5 55.59 57.82 1.09 o -13 3 5 12.00 11.22 0.94 o -11 3 5 100.42 111.22 2.62 o -9 3 5 586.18 535.99 5.77 o -7 3 5 363.97 336.33 4.65 o -5 3 5 1.38 1.29 0.66 o -3 3 5 264.58 243.99 14.27 o -1 3 5 472.27 537.67 22.66 o 1 3 5 15.74 18.70 1.31 o 3 3 5 163.84 172.56 6.32 o 5 3 5 29.48 24.06 1.80 o 7 3 5 399.45 379.35 3.75 o 9 3 5 53.52 57.80 1.54 o 11 3 5 213.17 216.38 6.40 o 13 3 5 21.18 23.22 1.20 o -10 4 5 109.95 116.80 2.01 o -8 4 5 14.63 17.34 1.11 o -6 4 5 181.96 181.44 3.07 o -4 4 5 346.44 318.87 4.54 o -2 4 5 150.94 138.51 2.01 o 0 4 5 75.88 70.52 2.39 o 2 4 5 114.60 112.43 2.90 o 4 4 5 319.78 317.74 4.64 o 6 4 5 143.49 165.97 2.94 o 8 4 5 15.20 16.66 0.80 o 10 4 5 112.52 123.26 1.86 o -18 0 6 41.05 39.90 1.55 o -16 0 6 192.16 192.04 2.66 o -14 0 6 2263.58 1887.76 12.03 o -12 0 6 1025.56 915.73 8.41 o -10 0 6 926.86 1078.06 6.98 o -8 0 6 103.87 120.61 2.18 o -6 0 6 1420.64 1961.08 7.71 o -4 0 6 1800.99 2063.84 7.70 o -2 0 6 824.32 908.50 4.61 o 0 0 6 235.51 229.72 2.25 o 4 0 6 1806.75 1897.84 59.23 o 6 0 6 2045.44 2093.97 8.26 o 8 0 6 9.33 14.68 1.23 o 10 0 6 1367.89 1139.44 7.55 o 12 0 6 2545.63 2193.61 11.20 o 14 0 6 844.27 764.81 6.63 o 16 0 6 372.38 359.85 4.15 o 18 0 6 73.04 70.34 1.45 o -19 1 6 81.77 79.78 1.54 o -17 1 6 65.20 57.62 2.06 o -15 1 6 88.93 84.35 2.83 o -13 1 6 165.25 141.39 2.40 o -11 1 6 427.61 411.18 3.89 o -9 1 6 106.60 133.68 2.73 o -7 1 6 57.64 56.77 1.15 o -5 1 6 1393.64 1467.69 7.44 o -3 1 6 122.48 149.65 10.24 o -1 1 6 1025.31 1041.85 9.77 o 1 1 6 87.17 92.40 3.27 o 3 1 6 397.42 452.22 2.75 o 5 1 6 748.13 751.91 7.54 o 7 1 6 99.17 85.30 1.14 o 9 1 6 362.43 352.11 14.18 o 11 1 6 483.29 459.33 6.99 o 13 1 6 172.06 159.39 7.19 o 15 1 6 91.15 102.25 1.59 o 17 1 6 39.32 37.37 1.30 o -16 2 6 418.51 437.95 4.43 o -14 2 6 26.73 24.01 1.60 o -12 2 6 228.91 266.67 3.74 o -10 2 6 550.56 547.56 5.55 o -8 2 6 1275.98 1430.17 9.16 o -6 2 6 45.52 57.79 3.93 o -4 2 6 320.57 363.07 6.45 o -2 2 6 349.09 354.68 10.56 o 0 2 6 610.54 594.48 17.67 o 2 2 6 47.09 46.15 1.43 o 4 2 6 179.25 187.24 2.27 o 6 2 6 384.48 374.41 5.01 o 8 2 6 1691.60 1522.71 34.43 o 10 2 6 373.45 359.27 3.67 o 12 2 6 190.67 179.09 2.34 o 14 2 6 63.57 65.40 1.74 o 16 2 6 236.15 255.12 2.53 o -13 3 6 5.63 5.25 0.77 o -11 3 6 237.23 243.17 3.61 o -9 3 6 23.97 23.92 1.49 o -7 3 6 33.07 33.69 1.68 o -5 3 6 62.15 57.57 1.43 o -3 3 6 142.98 121.88 7.65 o -1 3 6 7.82 10.03 1.18 o 1 3 6 82.59 92.30 1.76 o 3 3 6 2.77 3.10 0.70 o 5 3 6 389.53 387.10 3.68 o 7 3 6 21.08 23.64 1.20 o 9 3 6 63.42 60.32 3.24 o 11 3 6 47.86 47.99 1.24 o 13 3 6 68.75 88.64 1.59 o -10 4 6 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