#------------------------------------------------------------------------------ #$Date: 2010-02-13 12:42:52 +0200 (Sat, 13 Feb 2010) $ #$Revision: 986 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224594.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224594_Fobs loop_ _publ_author_name 'Sadeghi, Omid' 'Amini, Mostafa M.' 'Ng, Seik Weng' _publ_section_title ; Diaquahexa-\m~2~-dichloroacetato-\m~3~-oxido-tetrahydrofurandiiron(III)manganese(II) ; _journal_coeditor_code CI2991 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m101 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.131 _cell_angle_beta 100.067 _cell_angle_gamma 97.677 _cell_length_a 9.3800 _cell_length_b 13.3160 _cell_length_c 15.4320 _exptl_crystal_F_000 1046.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file ci2991Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 243.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 20301.30 21040.43 228.42 o 2 0 0 591.63 534.31 11.53 o 3 0 0 731.75 1124.83 20.84 o 4 0 0 4708.48 4040.62 55.20 o 5 0 0 1648.08 1122.38 28.90 o 6 0 0 1950.12 2249.50 41.88 o 7 0 0 980.20 899.54 28.42 o 8 0 0 439.70 450.08 22.88 o 9 0 0 239.40 233.24 45.76 o 10 0 0 714.93 835.79 44.19 o 11 0 0 1.99 -17.48 18.80 o -11 1 0 2.57 6.95 37.20 o -10 1 0 91.20 103.29 26.02 o -9 1 0 69.54 72.98 14.60 o -8 1 0 95.90 130.86 15.31 o -7 1 0 1278.00 1099.91 30.83 o -6 1 0 2059.40 1827.85 37.23 o -5 1 0 2522.14 2309.62 39.96 o -4 1 0 7747.43 8489.32 102.39 o -3 1 0 1305.82 1119.20 25.69 o -2 1 0 2858.77 4218.06 62.40 o -1 1 0 23064.64 22496.57 721.34 o 1 1 0 17.63 20.23 2.39 o 2 1 0 4430.87 5371.96 63.12 o 3 1 0 2314.99 3097.33 47.75 o 4 1 0 1184.40 1031.58 22.06 o 5 1 0 1505.58 1893.30 34.34 o 6 1 0 45.33 23.04 22.03 o 7 1 0 1174.93 1303.71 35.10 o 8 1 0 4104.20 4199.28 69.82 o 9 1 0 482.25 527.58 34.73 o 10 1 0 33.33 38.64 20.51 o 11 1 0 13.59 -9.16 20.19 o -11 2 0 119.43 116.10 45.43 o -10 2 0 262.28 271.15 29.91 o -9 2 0 132.96 87.99 15.24 o -8 2 0 287.54 261.87 25.78 o -7 2 0 118.87 153.62 16.49 o -6 2 0 125.51 135.68 12.85 o -5 2 0 1444.86 1683.30 33.32 o -4 2 0 7166.98 5069.55 81.78 o -2 2 0 1777.92 1430.65 51.62 o -1 2 0 4771.03 4045.74 210.07 o 0 2 0 5175.54 5092.25 101.98 o 1 2 0 1478.66 1170.23 17.51 o 2 2 0 1305.55 1640.50 24.27 o 3 2 0 29133.09 28522.72 307.04 o 4 2 0 797.53 604.49 16.57 o 5 2 0 509.35 471.75 16.88 o 6 2 0 1487.45 1553.72 33.68 o 7 2 0 2754.22 2460.34 46.62 o 8 2 0 1842.36 1925.33 57.39 o 9 2 0 11.97 -8.84 15.84 o 10 2 0 83.55 70.38 22.33 o 11 2 0 28.36 45.49 23.65 o -11 3 0 39.05 60.10 22.79 o -10 3 0 62.41 68.03 16.41 o -9 3 0 121.32 157.11 17.96 o -8 3 0 10.95 25.84 12.10 o -7 3 0 1503.89 1382.32 35.42 o -6 3 0 3177.21 3190.44 56.39 o -5 3 0 669.50 680.38 26.00 o -4 3 0 89.09 54.95 15.88 o -3 3 0 196.83 269.39 21.82 o -2 3 0 435.53 640.06 19.25 o -1 3 0 8156.49 6427.54 133.39 o 0 3 0 169.52 39.98 4.85 o 2 3 0 13991.86 14837.20 223.65 o 3 3 0 2235.19 2428.27 35.70 o 4 3 0 2393.73 2120.65 34.63 o 5 3 0 6531.45 5568.69 74.68 o 6 3 0 2078.37 2574.92 58.32 o 7 3 0 885.88 794.75 36.15 o 8 3 0 3.76 -5.36 20.16 o 9 3 0 9.89 -4.34 16.71 o 10 3 0 44.87 41.15 20.95 o 11 3 0 25.20 25.19 32.56 o -11 4 0 124.80 212.11 23.33 o -10 4 0 101.37 97.88 19.40 o -9 4 0 71.50 88.59 16.32 o -8 4 0 101.61 93.85 15.10 o -7 4 0 311.09 399.97 21.24 o -6 4 0 893.57 772.72 30.84 o -5 4 0 78.27 31.35 11.06 o -4 4 0 1725.10 1482.16 75.26 o -3 4 0 2026.32 3046.00 55.93 o -2 4 0 5180.99 4853.17 76.00 o -1 4 0 13977.08 13552.26 183.16 o 0 4 0 6174.19 6340.29 75.54 o 1 4 0 16.70 -0.54 4.54 o 2 4 0 9990.32 9762.12 112.45 o 3 4 0 886.15 945.43 21.94 o 4 4 0 1615.77 1721.24 30.81 o 5 4 0 269.18 347.49 15.95 o 6 4 0 279.41 330.76 32.20 o 7 4 0 206.31 163.74 21.38 o 8 4 0 370.95 313.33 28.27 o 9 4 0 29.97 50.36 20.43 o 10 4 0 16.45 14.14 19.78 o 11 4 0 53.33 29.89 23.65 o -11 5 0 27.66 6.50 16.58 o -10 5 0 11.08 2.67 18.94 o -9 5 0 660.99 618.89 29.66 o -8 5 0 1223.32 1199.85 36.19 o -7 5 0 19.28 24.57 18.38 o -6 5 0 650.45 570.92 27.97 o -5 5 0 6590.50 6718.35 112.35 o -4 5 0 604.69 680.25 36.51 o -3 5 0 7764.96 7747.22 136.09 o -2 5 0 19054.70 18509.35 366.02 o -1 5 0 3009.83 4186.94 55.53 o 0 5 0 3755.82 3029.35 42.74 o 2 5 0 5802.32 4795.68 62.44 o 3 5 0 357.25 292.26 13.00 o 4 5 0 0.01 -0.36 5.82 o 5 5 0 2811.82 3026.13 48.21 o 6 5 0 150.20 107.07 19.13 o 7 5 0 10.67 -8.16 13.34 o 8 5 0 61.11 -12.46 16.64 o 9 5 0 29.55 20.56 21.02 o 10 5 0 167.53 196.22 28.92 o -11 6 0 62.75 87.74 20.06 o -10 6 0 10.49 31.42 16.20 o -9 6 0 9.30 12.82 14.47 o -8 6 0 504.03 615.15 27.98 o -7 6 0 816.16 844.47 77.84 o -6 6 0 649.25 666.38 30.72 o -5 6 0 3292.33 3195.18 68.18 o -4 6 0 0.73 -2.14 11.66 o -3 6 0 112.71 51.28 23.16 o -1 6 0 8507.53 8579.65 103.72 o 0 6 0 3469.83 3541.32 50.32 o 1 6 0 18.31 56.34 7.10 o 2 6 0 1028.49 1082.85 23.03 o 3 6 0 2029.57 1886.37 33.51 o 4 6 0 2902.22 3124.50 51.42 o 5 6 0 825.75 832.68 34.54 o 6 6 0 158.70 191.13 22.29 o 7 6 0 0.29 -22.61 25.04 o 8 6 0 54.20 79.53 21.42 o 9 6 0 692.04 821.31 70.83 o 10 6 0 278.28 297.04 49.06 o -11 7 0 18.00 28.44 21.66 o -10 7 0 567.61 615.02 33.12 o -9 7 0 258.49 246.44 22.66 o -8 7 0 246.05 197.70 24.20 o -7 7 0 1791.75 1637.89 52.91 o -6 7 0 39.60 32.01 14.49 o -5 7 0 706.42 654.00 30.89 o -4 7 0 1109.57 1080.05 49.42 o -3 7 0 256.64 246.44 31.43 o -2 7 0 59.21 89.76 24.23 o -1 7 0 557.39 719.66 20.29 o 0 7 0 387.92 579.29 18.08 o 1 7 0 770.23 721.90 20.10 o 2 7 0 793.56 455.68 19.00 o 3 7 0 5376.96 6025.59 80.37 o 4 7 0 46.53 14.94 28.99 o 5 7 0 194.42 170.36 20.68 o 6 7 0 48.73 84.48 18.75 o 7 7 0 1018.68 1147.88 46.04 o 8 7 0 432.21 388.54 33.37 o 9 7 0 212.11 232.99 43.77 o 10 7 0 0.12 0.89 28.31 o -11 8 0 499.58 497.77 51.62 o -10 8 0 285.18 296.80 32.47 o -9 8 0 14.44 9.10 18.28 o -8 8 0 60.80 51.84 19.06 o -7 8 0 549.08 571.02 34.12 o -6 8 0 180.11 220.62 23.24 o -5 8 0 518.27 659.30 32.22 o -4 8 0 183.15 198.68 26.05 o -3 8 0 450.57 437.32 36.93 o -2 8 0 5381.78 4819.95 115.43 o -1 8 0 0.18 7.26 7.39 o 0 8 0 7637.51 7694.57 98.68 o 1 8 0 2045.89 2096.32 38.54 o 2 8 0 4393.11 5039.48 84.78 o 3 8 0 226.25 233.05 16.04 o 4 8 0 808.38 980.86 42.34 o 5 8 0 21.39 45.54 16.38 o 6 8 0 1.54 1.10 16.31 o 7 8 0 502.88 462.17 74.04 o 8 8 0 0.93 25.33 26.88 o 9 8 0 5.71 17.54 28.43 o -11 9 0 292.03 245.54 57.77 o -10 9 0 2.20 13.11 21.22 o -9 9 0 19.42 12.77 20.30 o -8 9 0 131.17 103.33 23.13 o -7 9 0 2.68 -8.01 14.74 o -6 9 0 5.98 -18.03 12.02 o -5 9 0 403.58 404.58 28.93 o -4 9 0 33.61 17.36 16.47 o -3 9 0 754.55 728.51 39.01 o -2 9 0 117.54 124.34 16.05 o -1 9 0 381.17 385.88 18.74 o 0 9 0 569.38 505.72 25.19 o 1 9 0 2045.35 2087.63 40.63 o 2 9 0 622.30 388.33 22.30 o 3 9 0 2.33 6.21 12.21 o 4 9 0 22.13 28.50 15.71 o 5 9 0 81.41 106.33 19.83 o 6 9 0 1.32 -13.02 16.28 o 7 9 0 30.53 1.07 23.25 o 8 9 0 101.25 98.78 34.43 o 9 9 0 140.62 108.71 35.92 o -10 10 0 12.31 10.23 21.42 o -9 10 0 102.75 98.41 33.81 o -8 10 0 195.81 217.74 28.10 o -7 10 0 216.17 184.39 24.60 o -6 10 0 25.88 -2.04 13.83 o -5 10 0 225.79 225.05 23.14 o -3 10 0 3895.40 3876.50 248.72 o -2 10 0 154.35 227.70 29.41 o -1 10 0 568.36 575.41 27.00 o 0 10 0 0.75 -3.10 8.92 o 1 10 0 8.92 43.03 10.38 o 2 10 0 764.01 583.34 23.08 o 3 10 0 1516.02 1863.53 73.80 o 4 10 0 4.14 -12.11 14.06 o 5 10 0 128.83 142.98 23.59 o 6 10 0 51.03 39.25 26.28 o 7 10 0 10.60 34.85 26.76 o 8 10 0 147.03 130.35 37.52 o -10 11 0 162.30 151.43 31.01 o -9 11 0 104.25 65.02 23.69 o -8 11 0 216.50 212.48 28.77 o -7 11 0 9.57 16.45 18.23 o -6 11 0 609.59 673.99 37.82 o -5 11 0 2189.67 2037.61 59.94 o -4 11 0 1373.93 1281.46 59.88 o -3 11 0 13.94 -12.76 8.50 o -2 11 0 405.52 340.16 24.13 o -1 11 0 22.33 19.67 11.05 o 0 11 0 2054.39 2258.85 57.41 o 1 11 0 1700.86 1720.84 39.72 o 2 11 0 225.99 313.02 25.40 o 3 11 0 1378.23 1257.08 63.87 o 4 11 0 1134.62 1048.60 44.19 o 5 11 0 1493.10 1448.80 76.95 o 6 11 0 44.07 105.26 33.06 o 7 11 0 324.05 248.28 44.42 o 8 11 0 8.60 17.78 30.98 o -9 12 0 77.68 52.14 24.65 o -8 12 0 154.82 142.23 33.66 o -7 12 0 204.64 192.40 30.66 o -6 12 0 808.12 850.46 43.18 o -5 12 0 470.95 522.18 49.30 o -4 12 0 151.05 107.52 26.88 o -3 12 0 142.48 238.23 31.46 o -2 12 0 116.67 91.27 36.01 o -1 12 0 0.61 6.07 10.81 o 0 12 0 65.99 84.10 17.15 o 1 12 0 227.21 302.19 19.96 o 2 12 0 968.53 906.92 40.03 o 3 12 0 1860.68 2031.69 60.56 o 4 12 0 376.56 387.01 44.96 o 5 12 0 5.81 22.36 25.51 o 6 12 0 569.24 618.64 57.03 o 7 12 0 11.82 58.87 32.29 o -9 13 0 39.30 30.27 23.36 o -8 13 0 36.62 45.05 22.89 o -7 13 0 25.14 26.67 20.24 o -6 13 0 157.84 174.52 25.85 o -5 13 0 30.42 54.79 20.96 o -4 13 0 2.79 -2.84 15.70 o -3 13 0 42.86 -8.98 22.54 o -2 13 0 12.44 17.15 17.09 o -1 13 0 34.68 51.22 14.17 o 0 13 0 608.43 687.25 41.66 o 1 13 0 72.63 122.52 21.15 o 2 13 0 1381.57 1430.93 51.17 o 3 13 0 3.34 -12.79 21.59 o 4 13 0 0.83 2.14 14.39 o 5 13 0 80.76 31.34 28.66 o 6 13 0 30.22 38.83 30.39 o -8 14 0 44.42 52.00 23.20 o -7 14 0 27.66 30.91 21.22 o -6 14 0 0.32 -2.10 12.48 o -5 14 0 8.74 -2.44 24.86 o -4 14 0 55.27 55.17 30.09 o -3 14 0 32.26 16.65 23.55 o -2 14 0 317.61 376.19 40.50 o -1 14 0 156.46 128.22 19.15 o 0 14 0 243.21 232.09 21.15 o 1 14 0 1442.95 1392.55 73.32 o 2 14 0 250.00 288.60 41.81 o 3 14 0 21.71 44.01 27.71 o 4 14 0 131.76 105.73 32.29 o 5 14 0 1.01 6.72 28.54 o -7 15 0 0.40 -12.66 19.19 o -6 15 0 39.61 60.31 22.19 o -5 15 0 36.23 39.21 20.09 o -4 15 0 7.39 5.03 17.25 o -3 15 0 600.46 581.39 36.34 o -2 15 0 267.97 335.93 40.44 o 0 15 0 245.08 346.16 44.54 o 1 15 0 20.47 47.51 28.19 o 2 15 0 13.98 22.30 25.04 o 3 15 0 23.34 32.17 28.66 o 4 15 0 1.31 6.36 28.48 o -6 16 0 0.02 -21.72 18.16 o -5 16 0 68.69 94.60 24.41 o -4 16 0 276.99 258.06 29.45 o -3 16 0 288.45 307.57 29.45 o -2 16 0 66.85 46.09 25.42 o 0 16 0 111.67 57.39 29.97 o 1 16 0 420.01 517.25 54.17 o 2 16 0 116.14 95.09 35.50 o 3 16 0 18.39 59.53 33.72 o -3 17 0 0.85 -4.74 21.50 o 0 -17 1 259.73 231.86 43.89 o 3 -17 1 27.24 6.54 24.50 o -3 -16 1 0.90 -10.59 27.36 o -2 -16 1 4.02 -3.21 27.00 o -1 -16 1 36.48 1.31 27.41 o 0 -16 1 6.15 -22.06 24.26 o 3 -16 1 6.00 -37.11 24.74 o 4 -16 1 92.49 130.48 32.26 o 5 -16 1 64.32 76.25 47.78 o -4 -15 1 23.67 19.68 17.72 o -3 -15 1 4.54 34.37 29.79 o -2 -15 1 39.08 36.51 29.08 o -1 -15 1 1.51 17.13 26.58 o 0 -15 1 10.58 31.58 27.53 o 1 -15 1 77.93 32.83 28.43 o 2 -15 1 161.28 132.40 23.82 o 3 -15 1 314.01 358.65 41.09 o 4 -15 1 472.03 412.17 45.85 o 5 -15 1 1.85 -8.86 16.98 o 6 -15 1 136.23 172.11 27.77 o 7 -15 1 92.82 61.73 22.81 o -5 -14 1 53.30 20.10 30.03 o -4 -14 1 0.94 -1.25 25.57 o -3 -14 1 238.99 219.79 38.42 o -2 -14 1 433.02 545.79 50.96 o -1 -14 1 121.81 99.31 31.99 o 0 -14 1 1.02 -8.73 12.63 o 1 -14 1 0.15 17.82 17.64 o 2 -14 1 550.32 494.86 33.93 o 3 -14 1 713.31 765.86 39.13 o 4 -14 1 402.46 432.03 44.48 o 5 -14 1 64.07 98.76 24.08 o 6 -14 1 21.35 12.98 19.07 o 7 -14 1 11.01 5.60 18.81 o 8 -14 1 16.95 -2.00 19.95 o -6 -13 1 24.63 40.97 32.17 o -5 -13 1 72.76 106.86 35.98 o -4 -13 1 974.29 1010.41 66.72 o -2 -13 1 21.77 12.67 22.18 o -1 -13 1 256.53 279.95 20.77 o 0 -13 1 14.07 4.71 12.39 o 1 -13 1 1202.27 1309.40 39.78 o 2 -13 1 3288.61 3676.95 81.76 o 3 -13 1 563.70 532.30 33.52 o 4 -13 1 70.94 44.66 26.28 o 5 -13 1 375.18 297.10 38.53 o 6 -13 1 276.41 313.10 45.37 o 7 -13 1 29.28 14.93 21.50 o 8 -13 1 9.37 27.72 33.51 o -7 -12 1 8.58 -9.10 25.10 o -6 -12 1 126.89 128.03 35.50 o -5 -12 1 814.63 766.12 60.06 o -4 -12 1 422.71 536.22 50.37 o -3 -12 1 18.22 21.82 20.34 o -2 -12 1 612.53 628.91 34.49 o -1 -12 1 114.47 147.30 18.11 o 0 -12 1 14.74 25.73 22.18 o 1 -12 1 275.45 325.04 20.41 o 2 -12 1 5.86 7.98 12.98 o 3 -12 1 225.42 147.66 26.70 o 4 -12 1 554.61 451.95 31.06 o 5 -12 1 951.91 876.07 55.66 o 6 -12 1 181.57 184.68 24.80 o 7 -12 1 109.92 93.43 36.30 o 8 -12 1 26.84 5.24 17.96 o 9 -12 1 191.20 189.55 30.16 o -8 -11 1 11.58 -21.59 25.39 o -7 -11 1 46.98 67.97 32.53 o -6 -11 1 198.53 171.80 37.64 o -5 -11 1 66.73 105.85 30.03 o -4 -11 1 65.04 108.41 30.27 o -3 -11 1 1082.75 978.64 40.68 o -2 -11 1 352.61 282.62 18.62 o -1 -11 1 28.73 28.98 11.77 o 0 -11 1 326.02 340.93 19.80 o 1 -11 1 175.92 173.97 15.79 o 2 -11 1 4.72 15.81 12.83 o 3 -11 1 735.12 696.33 32.76 o 4 -11 1 307.72 341.06 26.50 o 5 -11 1 21.04 12.84 12.96 o 6 -11 1 6.20 12.65 15.83 o 7 -11 1 72.24 76.43 21.57 o 8 -11 1 86.40 106.45 24.26 o 9 -11 1 108.46 95.03 25.58 o 10 -11 1 82.70 64.58 26.85 o -8 -10 1 19.40 36.28 28.78 o -7 -10 1 272.63 240.19 42.94 o -6 -10 1 163.81 171.39 36.10 o -5 -10 1 594.24 671.63 53.34 o -4 -10 1 669.05 500.96 31.49 o -3 -10 1 594.99 678.08 33.10 o -2 -10 1 2.22 6.88 6.46 o -1 -10 1 36.51 20.49 9.60 o 0 -10 1 3.98 -9.06 8.54 o 1 -10 1 2569.42 2708.77 60.04 o 2 -10 1 424.83 435.79 26.69 o 3 -10 1 3124.93 3058.57 68.48 o 4 -10 1 233.64 231.81 22.41 o 5 -10 1 309.19 272.06 32.11 o 6 -10 1 54.35 68.52 18.30 o 7 -10 1 518.80 650.62 38.36 o 8 -10 1 256.85 269.85 30.25 o 9 -10 1 1.03 11.73 24.02 o 10 -10 1 4.51 8.83 21.61 o -9 -9 1 39.45 15.82 28.25 o -8 -9 1 19.16 13.38 27.77 o -7 -9 1 20.99 -2.91 24.08 o -6 -9 1 24.55 11.60 22.78 o -5 -9 1 48.78 40.84 16.52 o -4 -9 1 1059.16 1244.47 43.26 o -3 -9 1 768.52 633.10 23.54 o -2 -9 1 3930.47 4201.62 76.03 o -1 -9 1 4518.29 4611.37 97.17 o 0 -9 1 2599.12 2682.38 47.32 o 1 -9 1 3494.12 3360.16 55.42 o 2 -9 1 1128.44 1037.88 46.68 o 3 -9 1 2617.59 2508.41 58.91 o 4 -9 1 2658.76 2618.77 94.32 o 5 -9 1 21.07 11.36 19.56 o 6 -9 1 188.84 148.86 21.01 o 7 -9 1 76.37 37.08 16.68 o 8 -9 1 44.93 38.49 19.11 o 9 -9 1 4.08 -6.25 18.17 o 10 -9 1 25.31 3.57 15.72 o -9 -8 1 65.80 24.02 29.38 o -8 -8 1 497.64 382.85 49.18 o -7 -8 1 116.80 176.62 35.86 o -6 -8 1 35.15 30.89 17.27 o -5 -8 1 252.35 289.62 24.64 o -4 -8 1 1512.77 1332.11 42.46 o -3 -8 1 9839.91 10291.17 127.68 o -2 -8 1 6837.75 6369.71 113.35 o -1 -8 1 265.58 196.88 12.57 o 0 -8 1 83.77 89.34 10.65 o 1 -8 1 891.18 911.39 25.12 o 2 -8 1 1018.76 952.27 83.37 o 3 -8 1 5422.83 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