#------------------------------------------------------------------------------ #$Date: 2010-02-13 12:42:52 +0200 (Sat, 13 Feb 2010) $ #$Revision: 986 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224642.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224642_Fobs loop_ _publ_author_name 'Mei, Xiang-Dong' 'Liang, Yan-Hui' 'Wang, Zhong-Yue' _publ_section_title ; (4-Bromo-3,5-dimethyl-1H-pyrazol-1-yl)(2,6-difluorophenyl)methanone ; _journal_coeditor_code HB5260 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o115 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.533 _cell_angle_gamma 90.000 _cell_length_a 7.1162 _cell_length_b 29.3038 _cell_length_c 11.6741 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file hb5260Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SA383 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 483.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 55.07 235.51 20.30 o 2 0 0 234146.38 232005.77 3692.62 o 3 0 0 17.91 67.64 27.19 o 4 0 0 75033.28 75221.16 8139.89 o 5 0 0 393.95 477.48 93.01 o 6 0 0 26466.49 26134.93 1125.78 o 7 0 0 207.30 234.12 48.26 o 8 0 0 4667.50 3814.76 544.95 o 1 1 0 14.18 36.39 7.36 o 2 1 0 355.69 392.13 22.90 o 3 1 0 80.42 88.93 9.12 o 4 1 0 27.57 185.11 38.66 o 5 1 0 7.85 51.36 17.47 o 6 1 0 845.74 805.79 54.09 o 7 1 0 23.83 71.42 39.51 o 8 1 0 0.28 115.67 57.08 o 1 2 0 142.44 132.25 13.59 o 2 2 0 1200.31 1060.29 45.05 o 3 2 0 903.53 836.68 45.00 o 4 2 0 403.40 438.39 34.55 o 5 2 0 4539.37 4581.42 201.34 o 6 2 0 3.12 47.19 41.44 o 7 2 0 494.02 672.55 77.48 o 8 2 0 140.58 189.22 40.05 o 1 3 0 121.91 183.41 8.83 o 2 3 0 1824.50 1811.47 21.86 o 3 3 0 421.68 430.67 32.30 o 4 3 0 3221.00 3011.47 106.63 o 5 3 0 582.97 630.90 49.89 o 6 3 0 1272.57 1341.06 75.13 o 7 3 0 38.77 70.08 35.43 o 8 3 0 382.74 211.26 59.41 o 0 4 0 48067.52 42743.93 462.41 o 1 4 0 3785.73 3755.85 54.21 o 2 4 0 22012.87 21243.06 179.01 o 3 4 0 1933.41 1844.47 59.37 o 4 4 0 9690.49 9312.05 163.78 o 5 4 0 426.92 507.72 46.21 o 6 4 0 3497.21 3515.09 123.96 o 7 4 0 94.49 220.95 50.90 o 8 4 0 970.06 938.51 93.10 o 1 5 0 1497.39 1545.61 38.26 o 2 5 0 76.81 99.94 9.05 o 3 5 0 20.51 42.19 9.42 o 4 5 0 6.52 55.73 16.12 o 5 5 0 64.98 82.85 23.22 o 6 5 0 94.19 105.21 21.94 o 7 5 0 8.51 80.82 29.16 o 8 5 0 48.06 24.20 28.21 o 0 6 0 842.50 976.37 31.19 o 1 6 0 15090.30 14581.91 123.77 o 2 6 0 394.39 376.47 16.38 o 3 6 0 13356.38 12965.96 200.45 o 4 6 0 14.37 35.20 22.08 o 5 6 0 8914.47 8677.83 272.26 o 6 6 0 21.95 65.27 33.28 o 7 6 0 2150.91 2310.93 127.28 o 8 6 0 109.21 95.21 32.40 o 1 7 0 5844.79 5517.19 88.13 o 2 7 0 419.14 421.54 22.04 o 3 7 0 249.34 233.60 25.36 o 4 7 0 1488.77 1440.36 59.44 o 5 7 0 371.94 416.14 44.57 o 6 7 0 46.49 78.19 18.93 o 7 7 0 1.29 6.74 23.85 o 8 7 0 334.62 396.99 62.48 o 0 8 0 147471.05 161298.55 1428.09 o 1 8 0 7522.64 7753.92 69.65 o 2 8 0 4870.12 4609.66 96.49 o 3 8 0 2144.95 1898.34 101.17 o 4 8 0 4293.13 4031.27 149.58 o 5 8 0 2329.12 2296.56 108.17 o 6 8 0 3105.95 3220.86 173.64 o 7 8 0 547.49 540.65 61.10 o 8 8 0 415.71 264.05 97.10 o 1 9 0 6617.61 7083.81 101.50 o 2 9 0 13.94 27.50 11.54 o 3 9 0 912.90 861.38 38.48 o 4 9 0 302.77 334.02 52.97 o 5 9 0 652.38 585.02 52.06 o 6 9 0 559.49 638.39 66.54 o 7 9 0 96.90 184.53 79.16 o 8 9 0 35.12 106.39 58.22 o 0 10 0 4031.88 4070.47 67.80 o 1 10 0 13537.08 14856.27 138.61 o 2 10 0 11971.20 11753.77 192.70 o 3 10 0 3602.94 3705.22 91.04 o 4 10 0 5753.49 5554.23 165.49 o 5 10 0 377.40 376.32 63.91 o 6 10 0 960.57 1152.51 82.93 o 7 10 0 659.71 656.09 138.09 o 8 10 0 247.56 357.48 59.60 o 1 11 0 237.61 268.39 26.83 o 2 11 0 212.05 224.68 21.60 o 3 11 0 108.82 109.60 25.93 o 4 11 0 386.28 373.61 38.11 o 5 11 0 0.15 45.31 16.11 o 6 11 0 0.33 81.31 18.88 o 7 11 0 73.30 69.27 44.31 o 8 11 0 1.05 69.55 23.43 o 0 12 0 35655.47 39062.60 631.20 o 1 12 0 2055.28 2201.94 111.07 o 2 12 0 10388.47 10545.93 188.37 o 3 12 0 459.83 454.10 46.68 o 4 12 0 4356.91 4231.62 147.03 o 5 12 0 36.21 54.57 24.80 o 6 12 0 1969.14 1929.15 114.68 o 7 12 0 0.77 48.12 68.86 o 1 13 0 1148.09 1217.96 69.81 o 2 13 0 9.34 61.17 13.43 o 3 13 0 34.53 66.14 13.78 o 4 13 0 295.10 315.38 60.28 o 5 13 0 341.38 408.30 40.41 o 6 13 0 152.45 145.44 26.65 o 7 13 0 224.99 211.60 41.04 o 0 14 0 14282.52 16401.06 314.85 o 1 14 0 120.92 181.54 20.13 o 2 14 0 4693.57 4991.77 132.06 o 3 14 0 513.21 364.26 39.16 o 4 14 0 2763.21 2811.08 137.64 o 5 14 0 347.46 399.93 61.80 o 6 14 0 756.95 738.46 74.25 o 7 14 0 356.13 358.65 60.13 o 1 15 0 881.73 813.03 51.40 o 2 15 0 285.36 402.70 61.81 o 3 15 0 179.79 185.54 26.00 o 4 15 0 721.08 750.61 62.59 o 5 15 0 372.37 456.96 45.78 o 6 15 0 8.88 88.01 35.39 o 7 15 0 5.54 34.18 27.30 o 0 16 0 176.80 208.72 34.44 o 1 16 0 17393.53 17699.25 502.19 o 2 16 0 1670.69 1615.55 90.07 o 3 16 0 6424.82 5981.47 187.60 o 4 16 0 952.75 846.93 58.17 o 5 16 0 4826.96 4541.61 139.97 o 6 16 0 104.13 141.41 33.78 o 7 16 0 764.93 764.44 66.38 o 1 17 0 5466.25 5770.36 292.77 o 2 17 0 10.94 55.34 25.87 o 3 17 0 110.95 144.95 27.46 o 4 17 0 39.61 105.90 43.59 o 5 17 0 124.61 166.07 32.65 o 6 17 0 4.34 26.67 40.93 o 7 17 0 0.06 27.82 47.80 o 0 18 0 43.11 94.23 63.37 o 1 18 0 5105.46 5093.61 167.56 o 2 18 0 692.42 736.67 115.80 o 3 18 0 1845.59 1763.82 107.77 o 4 18 0 767.78 696.69 65.60 o 5 18 0 883.63 915.23 80.05 o 6 18 0 140.66 210.42 49.00 o 7 18 0 580.82 601.89 78.22 o 1 19 0 26.60 76.64 25.36 o 2 19 0 299.64 304.55 37.76 o 3 19 0 409.26 343.42 42.42 o 4 19 0 48.71 92.83 55.22 o 5 19 0 117.71 146.24 30.77 o 6 19 0 125.33 144.40 40.81 o 7 19 0 119.20 78.78 62.03 o 0 20 0 1839.49 2861.02 622.91 o 1 20 0 1461.27 1503.39 81.43 o 2 20 0 3.79 36.99 25.17 o 3 20 0 2734.23 2599.70 101.88 o 4 20 0 102.27 106.18 34.90 o 5 20 0 1097.85 1120.34 92.97 o 6 20 0 16.63 83.56 48.00 o 1 21 0 26.92 43.31 19.70 o 2 21 0 14.76 53.80 32.50 o 3 21 0 3.85 52.74 19.60 o 4 21 0 1.52 106.54 44.44 o 5 21 0 317.25 300.21 59.41 o 6 21 0 62.92 133.14 46.25 o 0 22 0 6321.68 6228.95 311.42 o 1 22 0 332.16 346.75 41.52 o 2 22 0 4838.26 5058.68 165.35 o 3 22 0 66.07 82.10 18.98 o 4 22 0 1621.04 1465.16 85.01 o 5 22 0 31.95 42.37 25.83 o 6 22 0 586.56 741.13 100.91 o 1 23 0 4.28 50.03 35.16 o 2 23 0 236.15 124.72 70.29 o 3 23 0 22.86 64.01 27.53 o 4 23 0 17.44 42.09 24.70 o 5 23 0 51.69 131.98 49.93 o 6 23 0 49.22 113.34 41.69 o 0 24 0 499.17 528.64 68.40 o 1 24 0 4404.81 4510.74 204.50 o 2 24 0 1234.63 1455.60 106.40 o 3 24 0 2009.41 1724.23 142.89 o 4 24 0 117.94 78.45 23.07 o 5 24 0 1577.85 1860.32 221.49 o 6 24 0 33.61 48.39 37.92 o 1 25 0 1528.49 1604.41 87.76 o 2 25 0 12.53 75.50 21.22 o 3 25 0 95.13 79.00 31.06 o 4 25 0 310.80 395.82 50.05 o 5 25 0 9.64 104.11 36.83 o 0 26 0 906.59 795.82 74.33 o 1 26 0 2861.73 3023.34 127.68 o 2 26 0 774.80 844.80 56.23 o 3 26 0 1488.50 1444.93 84.63 o 4 26 0 207.49 168.44 38.32 o 5 26 0 570.32 593.82 84.21 o 1 27 0 2.37 94.42 25.82 o 2 27 0 35.43 109.48 30.68 o 3 27 0 58.51 118.08 47.35 o 4 27 0 6.20 86.09 24.37 o 5 27 0 25.27 69.30 42.46 o 0 28 0 241.38 214.55 50.90 o 1 28 0 3241.70 3439.78 177.12 o 2 28 0 326.48 443.42 53.21 o 3 28 0 3047.72 2942.92 148.99 o 4 28 0 188.34 202.60 83.69 o 5 28 0 1103.75 1160.00 167.45 o 1 29 0 38.71 108.96 33.79 o 2 29 0 13.72 99.62 62.36 o 3 29 0 1.90 47.07 23.17 o 4 29 0 10.43 122.23 87.28 o 0 30 0 303.67 420.88 90.29 o 1 30 0 49.94 159.95 31.13 o 2 30 0 664.84 674.60 61.68 o 3 30 0 5.25 69.15 29.96 o 4 30 0 139.55 187.18 43.58 o 1 31 0 0.57 125.12 23.46 o 2 31 0 24.56 69.71 32.58 o 3 31 0 92.99 120.51 31.08 o 0 32 0 193.86 132.92 38.72 o 1 32 0 133.18 126.47 26.71 o 2 32 0 699.85 638.48 82.45 o 3 32 0 146.63 207.40 42.71 o 1 33 0 120.02 119.63 44.65 o 2 33 0 15.52 97.35 37.95 o 0 34 0 855.72 882.12 287.76 o 1 34 0 423.01 416.96 71.30 o -8 1 1 1481.20 1584.17 184.56 o -7 1 1 48.49 71.49 20.80 o -6 1 1 4124.09 4282.69 143.91 o -5 1 1 445.24 387.98 41.01 o -4 1 1 17682.15 17231.37 376.44 o -3 1 1 132.45 115.10 15.69 o -2 1 1 79149.05 76761.81 830.55 o -1 1 1 2210.20 2033.40 43.96 o 1 1 1 2736.71 2484.22 43.13 o 2 1 1 59539.86 58288.08 537.97 o 3 1 1 490.16 511.51 29.09 o 4 1 1 12536.48 12330.45 486.70 o 5 1 1 15.60 43.49 19.77 o 6 1 1 1457.67 1336.82 74.70 o 7 1 1 166.15 145.33 31.85 o 8 1 1 550.78 594.89 54.89 o -8 2 1 296.44 233.74 106.81 o -7 2 1 104.22 84.66 39.77 o -6 2 1 3.02 73.66 22.83 o -5 2 1 145.87 204.46 26.81 o -4 2 1 1089.89 1069.52 60.94 o -3 2 1 6891.62 7423.30 132.12 o -2 2 1 995.26 881.91 21.60 o -1 2 1 1954.72 1871.52 23.48 o 1 2 1 1822.52 1845.91 26.64 o 2 2 1 914.61 825.49 27.38 o 3 2 1 2252.07 2310.29 69.87 o 4 2 1 822.23 913.36 83.65 o 5 2 1 211.95 234.07 44.82 o 6 2 1 11.90 137.47 32.04 o 7 2 1 131.97 177.57 33.83 o 8 2 1 154.93 137.60 39.68 o -8 3 1 1251.03 1090.14 187.75 o -7 3 1 894.01 882.98 54.61 o -6 3 1 3147.59 3062.81 99.17 o -5 3 1 108.49 229.61 28.45 o -4 3 1 11419.78 10585.92 164.67 o -3 3 1 4746.14 4498.73 79.16 o -2 3 1 40028.98 37900.95 355.00 o -1 3 1 22372.00 21203.95 323.43 o 1 3 1 12353.06 12888.32 116.96 o 2 3 1 22192.04 22687.67 383.76 o 3 3 1 6164.16 5592.17 142.53 o 4 3 1 6414.35 6017.93 154.69 o 5 3 1 835.57 760.40 65.41 o 6 3 1 4711.30 4745.78 176.13 o 7 3 1 212.01 210.90 47.66 o 8 3 1 294.63 225.11 52.78 o -8 4 1 41.93 164.02 81.35 o -7 4 1 401.06 404.28 51.67 o -6 4 1 1161.38 1043.90 55.39 o -5 4 1 34.15 53.47 15.73 o -4 4 1 4642.88 4601.95 79.54 o -3 4 1 36.83 51.11 14.40 o -2 4 1 4936.64 4781.87 168.33 o -1 4 1 709.10 550.53 32.04 o 0 4 1 48953.25 53342.18 286.98 o 1 4 1 157.86 145.93 8.98 o 2 4 1 10776.86 10274.63 81.76 o 3 4 1 0.09 86.09 13.79 o 4 4 1 7126.10 7003.20 299.48 o 5 4 1 88.94 77.56 15.96 o 6 4 1 7724.08 8682.42 231.20 o 7 4 1 24.97 68.31 28.17 o 8 4 1 595.82 578.95 76.73 o -8 5 1 14.78 101.07 22.62 o -7 5 1 1583.28 1773.35 117.77 o -6 5 1 132.99 163.97 27.89 o -5 5 1 3522.27 3251.61 181.73 o -4 5 1 1238.76 1243.00 45.27 o -3 5 1 17409.38 17580.34 213.18 o -2 5 1 115.19 102.98 8.86 o -1 5 1 29599.62 31213.99 377.54 o 0 5 1 7478.95 7504.31 111.91 o 1 5 1 44420.41 44081.47 259.60 o 2 5 1 631.59 642.46 23.31 o 3 5 1 14529.90 14339.62 358.71 o 4 5 1 9.30 44.65 19.47 o 5 5 1 2824.84 2764.29 129.59 o 6 5 1 308.28 291.08 37.71 o 7 5 1 1047.52 1187.48 93.49 o 8 5 1 1.78 240.31 57.45 o -8 6 1 40.80 100.20 33.08 o -7 6 1 50.06 31.25 31.12 o -6 6 1 248.93 272.51 34.96 o -5 6 1 135.52 152.97 29.43 o -4 6 1 1364.95 1213.42 67.26 o -3 6 1 198.08 240.44 32.75 o -2 6 1 2278.64 2114.02 31.71 o -1 6 1 75.84 72.08 9.15 o 0 6 1 1166.32 1213.49 28.42 o 1 6 1 20.24 53.30 9.73 o 2 6 1 2753.30 2496.52 40.41 o 3 6 1 222.81 272.49 23.76 o 4 6 1 275.62 261.97 41.84 o 5 6 1 554.47 632.61 57.51 o 6 6 1 1124.51 1081.05 54.33 o 7 6 1 5.24 65.90 23.81 o 8 6 1 99.80 178.36 43.86 o -8 7 1 167.30 197.91 51.73 o -7 7 1 169.85 219.67 47.80 o -6 7 1 361.87 430.88 35.09 o -5 7 1 1738.57 1629.92 90.26 o -4 7 1 3697.48 3534.75 79.20 o -3 7 1 2033.04 1644.60 69.99 o -2 7 1 5083.48 4968.64 126.79 o -1 7 1 8051.35 8134.61 74.74 o 0 7 1 377.32 447.91 22.71 o 1 7 1 6402.45 6573.95 69.63 o 2 7 1 7068.20 7197.14 122.37 o 3 7 1 324.10 260.13 45.85 o 4 7 1 205.09 244.76 29.28 o 5 7 1 169.84 147.27 25.29 o 6 7 1 15.13 62.27 18.70 o 7 7 1 0.87 46.83 27.07 o 8 7 1 38.13 142.95 42.74 o -8 8 1 24.70 110.31 43.35 o -7 8 1 2.58 68.81 43.59 o -6 8 1 252.33 303.51 45.64 o -5 8 1 283.62 328.27 46.99 o -4 8 1 699.58 677.62 41.03 o -3 8 1 3241.73 3256.47 198.87 o -2 8 1 3106.64 2841.96 79.31 o -1 8 1 3514.75 4610.53 255.87 o 0 8 1 4224.76 4437.49 64.07 o 1 8 1 15944.22 15016.10 128.37 o 2 8 1 4074.35 3784.48 90.79 o 3 8 1 2029.18 1949.66 87.52 o 4 8 1 3096.93 3149.49 109.03 o 5 8 1 989.54 1028.33 62.73 o 6 8 1 3020.74 3139.62 166.20 o 7 8 1 528.74 588.47 76.28 o 8 8 1 351.05 456.37 61.42 o -8 9 1 44.79 85.21 43.13 o -7 9 1 514.24 504.93 73.35 o -6 9 1 4.71 67.82 34.83 o -5 9 1 1566.34 1462.43 111.20 o -4 9 1 70.76 76.71 13.23 o -3 9 1 7198.56 6656.21 131.44 o -2 9 1 2816.99 2557.03 112.92 o -1 9 1 9947.70 9796.94 131.31 o 0 9 1 21856.74 24773.47 198.83 o 1 9 1 4784.71 5577.15 71.07 o 2 9 1 1470.26 1433.58 79.89 o 3 9 1 2734.92 2709.98 178.98 o 4 9 1 1880.35 1739.45 87.03 o 5 9 1 1195.60 1250.42 97.05 o 6 9 1 166.60 192.28 32.32 o 7 9 1 36.99 106.51 27.91 o 8 9 1 27.58 100.00 31.41 o -8 10 1 124.61 165.99 40.06 o -7 10 1 185.29 138.79 37.18 o -6 10 1 163.84 199.08 49.75 o -5 10 1 1022.46 916.57 58.78 o -4 10 1 1173.38 1087.60 53.52 o -3 10 1 2257.80 1850.45 69.72 o -2 10 1 1271.32 1248.55 48.25 o -1 10 1 19550.20 23015.24 285.10 o 0 10 1 632.12 736.71 31.90 o 1 10 1 34726.02 35497.36 330.09 o 2 10 1 0.67 28.62 21.66 o 3 10 1 5564.62 4909.79 170.77 o 4 10 1 204.19 193.58 45.96 o 5 10 1 1623.16 1416.41 102.15 o 6 10 1 424.84 462.99 49.58 o 7 10 1 1040.57 1104.21 103.04 o 8 10 1 0.08 63.21 30.34 o -8 11 1 1145.94 1289.44 124.46 o -7 11 1 77.18 194.81 178.92 o -6 11 1 3052.57 3211.66 221.42 o -5 11 1 343.34 417.36 43.17 o -4 11 1 12461.40 11495.12 308.38 o -3 11 1 88.40 117.30 15.24 o -2 11 1 20265.35 20594.04 458.92 o -1 11 1 5075.64 4815.65 142.27 o 0 11 1 10241.45 10602.04 123.12 o 1 11 1 53.69 574.06 71.95 o 2 11 1 23530.03 23767.39 435.74 o 3 11 1 82.12 93.00 18.97 o 4 11 1 6987.28 6667.41 195.14 o 5 11 1 22.21 84.07 18.20 o 6 11 1 3587.39 3406.54 272.01 o 7 11 1 22.30 77.55 45.52 o -7 12 1 226.59 265.05 51.64 o -6 12 1 322.91 357.37 57.06 o -5 12 1 416.78 514.90 62.97 o -4 12 1 1385.68 1275.54 99.82 o -3 12 1 852.73 808.88 86.07 o -2 12 1 242.61 278.53 33.49 o -1 12 1 2586.61 2852.82 82.31 o 0 12 1 2022.23 2297.91 61.50 o 1 12 1 6073.64 6015.08 160.47 o 2 12 1 58.06 84.67 30.78 o 3 12 1 2768.59 2719.43 115.60 o 4 12 1 10.98 63.45 21.45 o 5 12 1 1347.92 1335.44 75.55 o 6 12 1 680.46 677.57 49.60 o 7 12 1 202.82 319.84 56.57 o -7 13 1 329.37 228.85 47.90 o -6 13 1 10.83 92.53 23.69 o -5 13 1 1911.22 1751.18 124.04 o -4 13 1 554.38 611.69 46.16 o -3 13 1 5567.44 5114.25 97.08 o -2 13 1 127.45 140.31 14.32 o -1 13 1 2789.05 3645.54 104.10 o 0 13 1 167.86 207.01 25.09 o 1 13 1 7730.45 7309.27 139.85 o 2 13 1 5.46 45.99 19.40 o 3 13 1 441.66 463.93 48.19 o 4 13 1 219.49 225.10 28.52 o 5 13 1 22.33 45.69 15.59 o 6 13 1 84.54 98.51 21.74 o 7 13 1 246.99 216.09 54.16 o -7 14 1 1.66 98.05 26.64 o -6 14 1 108.68 160.64 41.23 o -5 14 1 51.41 85.15 17.47 o -4 14 1 1005.04 937.98 63.42 o -3 14 1 151.54 126.81 18.55 o -2 14 1 1550.34 1596.40 72.05 o -1 14 1 469.56 364.93 34.13 o 0 14 1 2741.87 2670.92 101.99 o 1 14 1 22.54 44.86 14.62 o 2 14 1 3171.24 3033.92 130.66 o 3 14 1 683.32 711.71 61.89 o 4 14 1 1503.76 1521.15 63.03 o 5 14 1 165.17 264.22 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