#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/46/2224661.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224661_Fobs loop_ _publ_author_name 'Hashmi, A. Stephen K.' 'Lothsch\"utz, Christian' 'Rominger, Frank' _publ_section_title ; Chlorido[3,3'-dibutyl-5,5'-(pyridine-2,6-diyl)dipyrazol-1-ido]gold(III) ; _journal_coeditor_code HG2593 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m64 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.372 _cell_angle_gamma 90.000 _cell_length_a 9.0003 _cell_length_b 24.2220 _cell_length_c 9.3042 _exptl_crystal_F_000 1072.00 _reflns_d_resolution_high 0.7707 _[local]_cod_data_source_file hg2593Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' clo3 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 417.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4163.64 4379.24 130.60 o 2 0 0 63384.79 60995.82 1951.91 o 3 0 0 29391.17 29596.64 1142.90 o 4 0 0 12499.14 12618.99 313.95 o 5 0 0 37117.39 35360.29 946.70 o 6 0 0 1594.62 1656.62 251.97 o 7 0 0 15058.98 15220.78 789.92 o 8 0 0 9.55 -16.61 356.46 o 9 0 0 4928.01 4037.68 636.91 o 10 0 0 1944.45 1645.00 400.17 o 11 0 0 1102.71 737.42 669.01 o 1 1 0 860.48 794.17 26.22 o 2 1 0 1368.60 1310.81 43.44 o 3 1 0 2179.08 2236.46 61.91 o 4 1 0 179.91 180.65 32.72 o 5 1 0 47.33 32.87 69.02 o 6 1 0 7.85 339.61 133.48 o 7 1 0 14.45 135.24 140.57 o 8 1 0 131.45 -153.20 153.20 o 9 1 0 1.09 42.20 217.13 o 10 1 0 7.02 155.09 243.10 o 11 1 0 24.07 137.32 353.73 o 0 2 0 174183.56 147027.88 4172.32 o 1 2 0 1031.88 1202.28 41.47 o 2 2 0 49521.63 46091.04 686.50 o 3 2 0 23742.04 22263.19 432.16 o 4 2 0 10955.14 10992.91 270.88 o 5 2 0 33144.61 31243.48 736.57 o 6 2 0 1623.37 1820.28 134.05 o 7 2 0 14402.77 14500.92 544.37 o 8 2 0 58.97 279.45 221.41 o 9 2 0 4855.82 3725.11 508.27 o 10 2 0 1136.37 1345.97 285.13 o 11 2 0 1035.66 507.73 296.62 o 1 3 0 6799.28 7636.88 151.67 o 2 3 0 55772.15 56429.31 903.95 o 3 3 0 5660.10 6233.04 163.93 o 4 3 0 4598.05 4661.95 130.51 o 5 3 0 313.93 150.62 66.01 o 6 3 0 628.84 703.24 97.43 o 7 3 0 54.42 311.86 146.75 o 8 3 0 2183.74 1772.08 225.59 o 9 3 0 72.33 289.39 203.62 o 10 3 0 254.23 902.08 263.96 o 11 3 0 160.84 736.90 480.95 o 0 4 0 86380.03 80847.95 1686.43 o 1 4 0 3071.48 3164.93 79.25 o 2 4 0 154219.58 157169.16 2647.21 o 3 4 0 14774.82 15820.58 441.68 o 4 4 0 10047.47 10136.44 269.81 o 5 4 0 19107.98 19751.46 495.97 o 6 4 0 2984.46 2961.07 119.45 o 7 4 0 14101.34 14004.51 534.07 o 8 4 0 204.81 464.25 185.54 o 9 4 0 4828.61 4591.93 354.15 o 10 4 0 801.79 217.51 238.10 o 11 4 0 667.87 690.69 305.57 o 1 5 0 26215.85 25712.51 394.03 o 2 5 0 66238.77 65531.14 1390.79 o 3 5 0 18396.19 17430.94 370.20 o 4 5 0 4869.43 5013.31 163.52 o 5 5 0 694.32 712.22 81.34 o 6 5 0 2984.46 2932.72 132.32 o 7 5 0 239.84 179.29 166.55 o 8 5 0 2442.90 2182.06 251.39 o 9 5 0 182.61 345.28 208.26 o 10 5 0 620.40 886.48 267.50 o 11 5 0 333.98 1380.32 417.46 o 0 6 0 16272.15 15309.08 369.11 o 1 6 0 2795.76 2987.48 132.50 o 2 6 0 76070.91 71967.23 1833.69 o 3 6 0 14823.79 15237.68 340.64 o 4 6 0 13127.97 13406.94 348.59 o 5 6 0 13998.50 14921.15 423.64 o 6 6 0 1131.78 1269.48 142.82 o 7 6 0 9899.04 10511.47 535.14 o 8 6 0 217.04 -62.89 163.86 o 9 6 0 3023.32 2837.98 305.59 o 10 6 0 269.99 -5.70 308.95 o 11 6 0 490.05 617.98 325.56 o 1 7 0 26631.71 27293.47 562.81 o 2 7 0 24906.77 26104.01 560.27 o 3 7 0 16642.45 16827.60 405.98 o 4 7 0 11750.45 11801.25 325.74 o 5 7 0 4080.45 4159.23 175.99 o 6 7 0 9418.67 9912.41 301.88 o 7 7 0 35.92 85.12 152.36 o 8 7 0 4488.22 4567.54 324.08 o 9 7 0 512.43 780.36 234.38 o 10 7 0 1657.04 1168.54 335.29 o 11 7 0 504.65 141.51 284.83 o 0 8 0 6774.69 6586.56 193.19 o 1 8 0 2150.27 2195.32 82.30 o 2 8 0 13938.14 14131.83 393.71 o 3 8 0 3139.80 3200.35 136.49 o 4 8 0 32392.38 33473.95 676.94 o 5 8 0 4503.27 4302.52 174.00 o 6 8 0 418.84 325.79 113.04 o 7 8 0 6395.41 5911.39 339.99 o 8 8 0 123.41 193.95 181.07 o 9 8 0 2287.05 2213.69 282.01 o 10 8 0 599.91 50.91 279.45 o 11 8 0 466.69 224.35 297.77 o 1 9 0 32183.85 31413.37 596.16 o 2 9 0 5570.09 5915.82 231.41 o 3 9 0 18227.58 18315.73 412.69 o 4 9 0 29171.61 30042.68 788.64 o 5 9 0 4531.01 4435.04 182.16 o 6 9 0 9882.01 10047.07 299.21 o 7 9 0 1.45 49.34 147.66 o 8 9 0 4569.68 4358.57 328.26 o 9 9 0 1227.28 1018.10 283.10 o 10 9 0 2871.73 2286.35 330.38 o 0 10 0 4266.67 4394.46 145.69 o 1 10 0 704.70 944.43 61.00 o 2 10 0 6097.40 6660.34 237.11 o 3 10 0 1535.38 1692.39 117.32 o 4 10 0 20045.75 19751.27 458.04 o 5 10 0 3043.03 3000.69 177.59 o 6 10 0 12.63 -63.71 86.87 o 7 10 0 2778.13 2458.92 240.73 o 8 10 0 11.61 36.93 261.09 o 9 10 0 713.33 663.54 269.28 o 10 10 0 459.86 -146.02 259.53 o 1 11 0 44754.90 44540.57 829.50 o 2 11 0 681.80 495.44 77.67 o 3 11 0 17498.25 18324.99 427.21 o 4 11 0 24648.49 23726.36 534.82 o 5 11 0 5638.12 5403.25 213.75 o 6 11 0 14886.41 14532.63 397.38 o 7 11 0 233.03 121.43 235.31 o 8 11 0 6302.66 6368.58 391.28 o 9 11 0 657.77 341.93 226.67 o 10 11 0 2240.09 2631.24 416.73 o 0 12 0 48.13 165.88 45.81 o 1 12 0 535.95 466.43 63.25 o 2 12 0 1894.96 1980.93 126.35 o 3 12 0 1408.04 1281.88 117.88 o 4 12 0 1920.38 1936.33 136.15 o 5 12 0 537.73 420.82 102.89 o 6 12 0 318.70 576.15 137.45 o 7 12 0 96.75 161.91 173.13 o 8 12 0 173.30 301.66 198.88 o 9 12 0 250.86 408.41 287.25 o 10 12 0 153.80 369.00 293.98 o 1 13 0 25841.08 25791.30 456.42 o 2 13 0 495.75 485.77 88.80 o 3 13 0 15529.24 15927.95 415.16 o 4 13 0 13261.03 14311.02 414.26 o 5 13 0 5429.23 5677.89 229.88 o 6 13 0 19065.75 19895.93 551.55 o 7 13 0 12.51 -172.05 172.05 o 8 13 0 7634.42 7574.79 432.84 o 9 13 0 827.26 641.75 404.05 o 10 13 0 2066.51 4153.13 571.02 o 0 14 0 157.09 88.93 153.24 o 1 14 0 54.22 164.27 54.04 o 2 14 0 293.49 426.24 82.16 o 3 14 0 144.75 137.42 86.56 o 4 14 0 148.22 115.49 100.83 o 5 14 0 37.02 -94.68 94.68 o 6 14 0 1904.54 1726.90 162.73 o 7 14 0 179.02 207.79 186.38 o 8 14 0 398.24 567.55 229.51 o 9 14 0 2.88 -139.75 402.10 o 10 14 0 6.61 576.92 304.20 o 1 15 0 27752.30 27159.23 476.59 o 2 15 0 1755.74 1551.14 117.64 o 3 15 0 14118.22 13876.11 601.87 o 4 15 0 10329.72 10272.55 321.80 o 5 15 0 3758.10 3855.57 201.05 o 6 15 0 15499.79 14937.80 433.98 o 7 15 0 4.80 52.04 187.83 o 8 15 0 5506.90 6068.53 408.29 o 9 15 0 574.30 640.58 281.35 o 10 15 0 1467.72 899.62 336.68 o 0 16 0 56.58 56.33 184.64 o 1 16 0 85.57 54.85 51.75 o 2 16 0 1468.31 1275.99 128.80 o 3 16 0 157.76 88.78 97.48 o 4 16 0 2497.20 2901.97 185.11 o 5 16 0 312.30 126.46 124.36 o 6 16 0 17.00 -34.74 126.52 o 7 16 0 768.83 776.78 250.54 o 8 16 0 42.82 108.27 331.73 o 9 16 0 535.36 547.18 337.24 o 1 17 0 22478.07 22218.21 689.90 o 2 17 0 2871.83 2602.82 145.45 o 3 17 0 9196.39 8919.25 290.44 o 4 17 0 6872.18 6820.51 263.44 o 5 17 0 787.40 1209.61 155.62 o 6 17 0 11220.52 11092.47 378.19 o 7 17 0 8.90 72.29 197.11 o 8 17 0 5841.76 5933.89 418.17 o 9 17 0 420.98 791.46 303.30 o 0 18 0 186.25 -157.25 204.96 o 1 18 0 13.79 301.18 155.98 o 2 18 0 3314.93 3247.72 249.69 o 3 18 0 208.92 376.68 155.40 o 4 18 0 1541.75 1430.37 148.46 o 5 18 0 2156.14 2492.56 192.13 o 6 18 0 653.51 466.05 187.04 o 7 18 0 1552.63 913.97 474.72 o 8 18 0 185.15 112.58 337.91 o 9 18 0 711.88 624.06 441.25 o 1 19 0 10037.58 9969.25 444.13 o 2 19 0 3308.97 3111.13 256.34 o 3 19 0 7740.43 7980.40 437.21 o 4 19 0 3589.12 3913.31 282.67 o 5 19 0 463.95 270.34 287.11 o 6 19 0 5229.63 5180.94 341.41 o 7 19 0 54.09 523.72 522.03 o 8 19 0 3846.34 4848.83 910.59 o 9 19 0 248.76 -287.03 379.11 o 0 20 0 5260.12 5154.66 444.88 o 1 20 0 687.10 1214.14 253.35 o 2 20 0 5788.67 4918.57 324.15 o 3 20 0 2493.99 2220.61 233.87 o 4 20 0 2451.37 2620.98 251.11 o 5 20 0 2896.58 3106.35 276.63 o 6 20 0 1038.91 1293.39 431.81 o 7 20 0 2092.46 2933.97 493.85 o 8 20 0 445.41 1096.43 620.01 o 1 21 0 8967.43 8611.34 481.84 o 2 21 0 3802.77 3690.35 349.38 o 3 21 0 2318.43 2163.95 259.45 o 4 21 0 3115.10 3435.97 326.35 o 5 21 0 155.69 534.97 253.63 o 6 21 0 2754.60 2953.74 300.89 o 7 21 0 69.52 -179.04 518.65 o 8 21 0 1807.59 3548.88 705.33 o 0 22 0 8305.69 9180.36 837.95 o 1 22 0 197.64 840.97 205.67 o 2 22 0 4159.01 4529.42 320.97 o 3 22 0 3093.90 3012.06 281.27 o 4 22 0 3433.62 3500.99 308.88 o 5 22 0 3628.11 3732.82 319.39 o 6 22 0 552.75 497.12 312.85 o 7 22 0 2214.31 2382.33 582.00 o 8 22 0 94.50 -406.98 1006.04 o 1 23 0 2623.01 2410.00 265.88 o 2 23 0 959.69 975.56 352.11 o 3 23 0 446.44 306.97 205.87 o 4 23 0 1807.19 1475.01 251.61 o 5 23 0 45.92 430.58 238.12 o 6 23 0 775.28 736.78 261.85 o 7 23 0 112.76 -143.60 648.73 o 0 24 0 12057.48 11657.38 1011.11 o 1 24 0 261.25 144.67 201.80 o 2 24 0 4538.28 4677.67 347.73 o 3 24 0 3587.61 3240.58 409.42 o 4 24 0 2580.90 2843.32 312.62 o 5 24 0 3674.77 3254.07 396.26 o 6 24 0 241.52 44.12 297.53 o 7 24 0 2047.27 2021.46 702.79 o 1 25 0 335.25 99.71 203.23 o 2 25 0 271.87 305.57 207.81 o 3 25 0 133.41 -0.58 297.59 o 4 25 0 895.44 1431.96 309.80 o 5 25 0 37.52 343.81 435.03 o 6 25 0 135.79 -386.16 386.16 o 0 26 0 8405.03 7847.43 637.49 o 1 26 0 807.46 720.45 237.40 o 2 26 0 5665.02 6111.60 409.35 o 3 26 0 3345.15 3491.03 401.61 o 4 26 0 1666.69 2009.72 355.63 o 5 26 0 3463.94 4279.65 511.59 o 6 26 0 169.92 -456.30 456.30 o 1 27 0 15.31 155.77 259.69 o 2 27 0 1.23 560.11 300.05 o 3 27 0 14.19 30.79 245.79 o 4 27 0 148.38 333.05 309.75 o 5 27 0 61.01 -52.81 345.04 o 0 28 0 4962.15 5274.62 842.17 o 1 28 0 650.31 521.12 296.52 o 2 28 0 4941.28 4340.23 541.67 o 3 28 0 1262.84 1301.91 301.68 o 4 28 0 796.54 470.81 396.98 o 5 28 0 2020.34 1539.17 356.73 o 1 29 0 584.95 1204.32 336.59 o 2 29 0 6.32 596.09 278.09 o 3 29 0 212.01 -229.90 267.70 o 4 29 0 26.89 -314.44 314.44 o 0 30 0 2830.26 3506.05 542.49 o 1 30 0 236.55 355.98 290.75 o 2 30 0 3230.57 3678.86 396.56 o 3 30 0 1176.38 1300.57 340.57 o 1 31 0 972.74 1425.43 586.93 o -11 1 1 1727.31 1862.93 332.29 o -10 1 1 7.89 -256.89 256.89 o -9 1 1 6424.06 6669.21 407.99 o -8 1 1 2270.97 2315.37 244.60 o -7 1 1 12706.48 12841.62 585.09 o -6 1 1 19649.69 19438.70 575.96 o -5 1 1 9294.46 9410.94 265.54 o -4 1 1 61137.36 58889.86 1360.95 o -3 1 1 1070.65 1133.90 89.03 o -2 1 1 61327.02 57535.66 997.49 o -1 1 1 10618.65 10917.63 176.96 o 0 1 1 110353.73 104201.50 1482.45 o 1 1 1 42204.73 43116.31 780.50 o 2 1 1 346.21 332.82 31.79 o 3 1 1 33177.49 33259.19 721.70 o 4 1 1 41.73 -51.78 92.90 o 5 1 1 18443.70 18706.01 662.72 o 6 1 1 1928.48 1631.30 179.66 o 7 1 1 9747.77 9358.44 508.47 o 8 1 1 3137.78 3104.61 274.08 o 9 1 1 1472.28 1899.53 270.62 o 10 1 1 3764.49 4280.20 386.81 o 11 1 1 3.75 836.24 332.85 o -11 2 1 77.47 42.02 283.97 o -10 2 1 43.57 95.24 273.68 o -9 2 1 24.29 462.10 254.97 o -8 2 1 1533.24 1375.99 213.18 o -7 2 1 372.70 404.92 253.11 o -6 2 1 204.67 188.37 70.92 o -5 2 1 2270.63 2662.30 119.38 o -4 2 1 91.69 155.49 64.68 o -3 2 1 6251.49 6953.49 236.02 o -2 2 1 4637.64 5108.93 138.79 o -1 2 1 7112.54 7357.18 129.09 o 0 2 1 66.28 134.78 25.75 o 1 2 1 371.10 526.07 36.88 o 2 2 1 16308.34 17043.33 286.79 o 3 2 1 3.10 -12.57 39.90 o 4 2 1 554.16 613.99 77.69 o 5 2 1 14.18 144.90 110.73 o 6 2 1 291.91 84.39 126.04 o 7 2 1 7.39 -56.75 202.15 o 8 2 1 650.77 970.38 211.68 o 9 2 1 241.55 75.32 204.81 o 10 2 1 91.68 275.97 256.92 o 11 2 1 150.21 805.86 321.67 o -11 3 1 1971.88 2469.41 356.75 o -10 3 1 23.61 -65.23 266.28 o -9 3 1 6006.18 5900.29 389.42 o -8 3 1 1920.49 1932.74 264.05 o -7 3 1 9530.58 9249.11 414.60 o -6 3 1 17884.78 17672.20 476.09 o -5 3 1 7319.14 6861.30 205.11 o -4 3 1 41344.87 42352.77 1341.32 o -3 3 1 1112.27 1254.85 80.73 o -2 3 1 61159.25 60302.12 1164.73 o -1 3 1 17089.57 18965.30 419.92 o 0 3 1 43169.61 42131.04 666.97 o 1 3 1 26077.85 24772.11 420.37 o 2 3 1 24110.05 25120.04 404.53 o 3 3 1 23267.26 22187.99 366.56 o 4 3 1 449.69 421.56 68.42 o 5 3 1 17575.79 17503.33 379.43 o 6 3 1 1405.05 1403.55 175.83 o 7 3 1 7479.83 7080.48 375.14 o 8 3 1 3859.88 3707.12 294.89 o 9 3 1 1429.90 1947.87 267.02 o 10 3 1 3121.03 3317.91 352.53 o 11 3 1 1.26 85.50 297.93 o -11 4 1 39.73 -3.52 344.10 o -10 4 1 373.22 409.40 236.53 o -9 4 1 5.99 350.37 199.03 o -8 4 1 3186.03 2997.58 267.86 o -7 4 1 1231.84 1340.99 189.32 o -6 4 1 2255.46 2433.05 180.19 o -5 4 1 9623.38 9532.48 309.58 o -4 4 1 355.76 490.53 71.44 o -3 4 1 13375.00 12911.78 291.23 o -2 4 1 754.25 661.62 73.36 o -1 4 1 6443.71 6758.85 151.93 o 0 4 1 15423.76 14143.07 329.09 o 1 4 1 3613.83 4072.63 112.42 o 2 4 1 23383.36 24328.01 475.79 o 3 4 1 14.31 14.23 86.43 o 4 4 1 909.31 822.96 89.90 o 5 4 1 42.57 103.60 153.62 o 6 4 1 1544.49 1438.64 180.18 o 7 4 1 358.78 217.19 160.05 o 8 4 1 1336.57 1213.39 210.20 o 9 4 1 969.87 1313.83 461.39 o 10 4 1 213.89 -293.60 503.40 o 11 4 1 415.07 -228.60 290.87 o -11 5 1 1553.37 1616.18 341.93 o -10 5 1 156.44 214.65 242.17 o -9 5 1 3608.20 3047.78 306.49 o -8 5 1 1703.05 1501.70 218.05 o -7 5 1 5783.25 5684.06 325.53 o -6 5 1 10498.14 10643.19 326.78 o -5 5 1 2517.68 2589.67 127.56 o -4 5 1 21271.18 20337.91 436.77 o -3 5 1 274.30 456.61 65.59 o -2 5 1 74242.76 77811.26 1350.62 o -1 5 1 7086.57 7338.55 177.42 o 0 5 1 13645.82 13482.11 246.17 o 1 5 1 15963.48 16093.95 303.84 o 2 5 1 20287.60 21796.57 407.78 o 3 5 1 28912.13 27913.27 595.50 o 4 5 1 260.38 354.71 102.72 o 5 5 1 19397.35 19290.97 375.83 o 6 5 1 1248.54 1014.82 180.30 o 7 5 1 5284.65 5239.03 324.13 o 8 5 1 3861.54 3946.60 312.09 o 9 5 1 747.28 832.27 285.85 o 10 5 1 1992.97 2175.53 321.70 o 11 5 1 0.13 468.12 326.98 o -11 6 1 3.26 -256.93 277.87 o -10 6 1 1518.76 1339.40 280.82 o -9 6 1 19.55 -12.83 206.08 o -8 6 1 3520.24 3246.65 280.49 o -7 6 1 2070.06 2047.69 256.04 o -6 6 1 5979.01 6078.58 252.64 o -5 6 1 15364.91 15803.75 390.86 o -4 6 1 233.48 228.85 67.71 o -3 6 1 35747.28 34444.09 662.36 o -2 6 1 984.73 1033.46 79.01 o -1 6 1 18799.27 18735.67 348.81 o 0 6 1 28991.45 29155.56 630.00 o 1 6 1 7191.07 7916.77 201.10 o 2 6 1 25019.00 23828.79 479.38 o 3 6 1 23.09 169.13 76.86 o 4 6 1 13755.60 14297.91 340.16 o 5 6 1 38.29 88.54 66.54 o 6 6 1 6604.44 6722.98 257.93 o 7 6 1 1055.84 1046.39 184.41 o 8 6 1 2122.76 1380.84 267.63 o 9 6 1 1745.32 1994.99 375.28 o 10 6 1 404.32 19.17 448.19 o 11 6 1 921.60 853.49 328.28 o -11 7 1 1736.75 2546.52 355.65 o -10 7 1 34.28 455.64 390.88 o -9 7 1 1795.07 2260.92 295.05 o -8 7 1 1469.16 2273.63 448.54 o -7 7 1 3793.99 3871.19 219.81 o -6 7 1 4392.17 4546.11 201.15 o -5 7 1 4342.87 4074.58 181.81 o -4 7 1 16446.90 17642.98 460.37 o -3 7 1 513.90 447.46 70.23 o -2 7 1 33606.35 34558.32 847.80 o -1 7 1 709.79 686.90 55.83 o 0 7 1 16758.86 17406.16 364.23 o 1 7 1 6694.23 7218.55 209.76 o 2 7 1 19910.46 19288.81 472.58 o 3 7 1 15645.46 15110.25 604.79 o 4 7 1 2998.34 2949.25 134.01 o 5 7 1 12891.89 12796.53 327.50 o 6 7 1 3951.77 4048.27 244.02 o 7 7 1 3207.43 2954.71 253.63 o 8 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