#------------------------------------------------------------------------------ #$Date: 2010-02-13 12:42:52 +0200 (Sat, 13 Feb 2010) $ #$Revision: 986 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224691.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224691_Fobs loop_ _publ_author_name 'Malassa, Astrid' 'J\"ager, Benjamin' 'G\"orls, Helmar' 'Westerhausen, Matthias' _publ_section_title ; Bis(N-triisopropylsilylquinolin-8-aminato)nickel(II) ; _journal_coeditor_code JH2120 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m6 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 68.956 _cell_angle_beta 72.025 _cell_angle_gamma 85.540 _cell_length_a 12.3062 _cell_length_b 17.7015 _cell_length_c 18.4194 _exptl_crystal_F_000 1416.00 _reflns_d_resolution_high 0.7706 _[local]_cod_data_source_file jh2120Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 208.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 6625.16 6923.15 446.48 o 4 0 0 1043.58 970.60 32.61 o 5 0 0 43.45 61.16 11.62 o 6 0 0 3016.34 3220.89 161.29 o 7 0 0 5485.95 6198.45 170.55 o 8 0 0 2057.35 2119.89 88.45 o 9 0 0 501.53 502.51 28.91 o 10 0 0 76.48 86.92 28.94 o 11 0 0 1537.85 1599.21 62.46 o 12 0 0 1110.69 1114.07 105.04 o 13 0 0 905.28 916.60 43.61 o 14 0 0 28.97 31.87 34.47 o 15 0 0 55.24 100.16 54.63 o -15 1 0 141.15 100.81 53.98 o -14 1 0 63.07 42.27 44.88 o -13 1 0 594.81 487.16 79.35 o -12 1 0 562.34 553.68 34.47 o -11 1 0 1282.45 1322.68 57.24 o -10 1 0 13.79 21.17 41.30 o -9 1 0 186.68 199.93 44.88 o -8 1 0 1243.46 1306.32 48.12 o -7 1 0 55.20 71.00 41.62 o -6 1 0 3237.93 3637.08 100.14 o -5 1 0 5293.53 5734.22 150.49 o -4 1 0 2637.62 3181.70 91.00 o -3 1 0 8670.33 8987.07 492.98 o -2 1 0 3337.42 3943.86 141.78 o 1 1 0 1531.56 1567.40 57.88 o 3 1 0 11.46 -9.43 9.43 o 4 1 0 22981.04 24623.61 1209.04 o 5 1 0 3560.06 3849.58 248.77 o 6 1 0 3890.19 4377.98 117.20 o 7 1 0 3569.90 3724.97 206.49 o 8 1 0 37.43 10.24 15.16 o 9 1 0 50.45 30.00 12.36 o 10 1 0 79.12 73.62 20.49 o 11 1 0 202.99 194.90 15.14 o 12 1 0 1177.26 1191.26 55.93 o 13 1 0 100.77 96.64 41.30 o 14 1 0 155.18 290.07 53.98 o 15 1 0 620.45 725.82 78.04 o -15 2 0 31.05 -7.15 53.33 o -14 2 0 209.19 271.86 53.98 o -13 2 0 52.39 -18.86 40.97 o -12 2 0 4.98 28.54 23.33 o -11 2 0 181.73 226.27 25.24 o -10 2 0 186.76 160.38 23.06 o -9 2 0 2458.76 2540.31 84.80 o -8 2 0 4495.16 5052.95 137.07 o -7 2 0 138.59 147.63 24.39 o -6 2 0 555.58 834.60 31.71 o -5 2 0 2971.74 3369.21 146.98 o -4 2 0 2081.32 2152.38 72.84 o -3 2 0 5247.71 5960.68 155.42 o -2 2 0 235.77 327.39 23.74 o -1 2 0 2754.04 2752.43 227.63 o 0 2 0 4931.11 4756.83 113.16 o 1 2 0 4070.85 4306.77 147.63 o 2 2 0 21858.76 21066.40 1106.61 o 3 2 0 14234.59 14204.20 754.43 o 4 2 0 1121.73 1315.15 59.51 o 5 2 0 8.89 64.54 26.34 o 6 2 0 329.51 318.50 14.42 o 7 2 0 50.82 38.13 26.34 o 8 2 0 23.45 21.10 11.16 o 9 2 0 14.56 14.08 15.28 o 10 2 0 700.17 664.01 24.56 o 11 2 0 818.90 803.31 30.61 o 12 2 0 52.26 49.39 17.51 o 13 2 0 70.70 70.24 21.46 o 14 2 0 215.08 209.42 42.92 o 15 2 0 12.73 9.11 49.43 o -15 3 0 155.86 169.10 53.33 o -14 3 0 177.17 267.30 52.03 o -13 3 0 509.19 483.23 35.12 o -12 3 0 66.68 98.39 20.16 o -11 3 0 88.04 93.84 27.03 o -10 3 0 2534.69 2675.07 92.84 o -9 3 0 2140.21 2277.19 73.08 o -8 3 0 881.04 874.00 64.39 o -7 3 0 7.71 6.23 16.26 o -6 3 0 7268.93 8086.27 217.31 o -5 3 0 9.82 28.22 16.91 o -4 3 0 3948.85 4343.91 97.93 o -3 3 0 10988.71 11750.71 561.60 o -2 3 0 115.88 116.22 18.86 o -1 3 0 179.99 243.24 9.76 o 0 3 0 322.54 414.29 13.01 o 1 3 0 2112.17 2417.44 88.45 o 2 3 0 20824.61 20457.97 335.25 o 3 3 0 1210.02 1076.74 24.60 o 4 3 0 7297.92 7727.02 213.65 o 5 3 0 475.69 400.64 15.73 o 6 3 0 1.10 -13.01 13.01 o 7 3 0 7659.51 7846.38 168.77 o 8 3 0 2463.89 2477.10 59.28 o 9 3 0 417.18 408.89 18.20 o 10 3 0 292.68 221.25 16.87 o 11 3 0 167.06 153.53 22.76 o 12 3 0 659.46 620.94 39.02 o 13 3 0 0.04 -41.62 41.62 o 14 3 0 405.33 538.51 62.44 o -14 4 0 0.65 -20.81 46.18 o -13 4 0 0.77 45.53 26.01 o -12 4 0 488.47 499.48 28.84 o -11 4 0 1240.22 1296.77 57.56 o -10 4 0 53.82 55.62 15.92 o -9 4 0 1215.06 1255.17 37.78 o -8 4 0 42.77 37.05 11.79 o -7 4 0 4548.03 5217.01 119.33 o -6 4 0 282.22 318.44 22.11 o -5 4 0 7329.10 8087.83 175.62 o -4 4 0 16225.48 18575.27 369.84 o -3 4 0 6454.40 7136.46 116.19 o -2 4 0 2804.99 3129.07 53.75 o -1 4 0 1201.58 1416.53 31.88 o 0 4 0 14508.14 14284.13 331.69 o 1 4 0 909.81 968.93 31.54 o 2 4 0 191.95 159.47 12.36 o 3 4 0 16611.98 17371.20 293.35 o 4 4 0 9473.69 9450.09 257.22 o 5 4 0 993.76 1438.91 35.83 o 6 4 0 5712.96 5492.12 121.55 o 7 4 0 183.57 212.43 13.33 o 8 4 0 90.84 71.31 10.76 o 9 4 0 227.19 197.77 27.97 o 10 4 0 104.26 102.15 29.59 o 11 4 0 259.32 213.34 18.43 o 12 4 0 359.30 324.40 22.60 o 13 4 0 224.46 183.41 47.48 o 14 4 0 341.74 267.95 57.23 o -14 5 0 236.28 192.51 50.08 o -13 5 0 171.98 200.31 28.62 o -12 5 0 330.55 328.01 23.32 o -11 5 0 17.51 21.79 17.97 o -10 5 0 492.55 516.24 24.90 o -9 5 0 467.38 486.94 22.47 o -8 5 0 3.46 14.12 13.66 o -7 5 0 1827.46 1933.45 51.86 o -6 5 0 124.62 29.64 13.98 o -5 5 0 109.25 75.03 9.37 o -4 5 0 56.83 104.74 8.75 o -3 5 0 9242.92 10368.86 379.49 o -2 5 0 250.27 244.47 8.93 o -1 5 0 1645.44 1662.15 37.82 o 0 5 0 15030.33 14561.84 342.75 o 1 5 0 2048.21 2084.66 58.40 o 2 5 0 1507.83 1529.13 36.72 o 3 5 0 10095.69 10175.09 271.53 o 4 5 0 8627.84 8382.60 154.28 o 5 5 0 744.72 759.94 21.79 o 6 5 0 3215.23 3202.46 100.48 o 7 5 0 222.11 181.58 11.91 o 8 5 0 83.12 89.66 11.21 o 9 5 0 205.04 213.79 14.42 o 10 5 0 1078.47 925.01 32.20 o 11 5 0 242.20 210.34 26.67 o 12 5 0 341.42 369.56 44.23 o 13 5 0 174.12 59.18 34.47 o 14 5 0 191.16 107.31 52.03 o -14 6 0 45.89 42.27 42.27 o -13 6 0 1734.02 1828.20 81.95 o -12 6 0 1273.02 1349.33 49.30 o -11 6 0 204.14 214.40 30.24 o -10 6 0 69.31 46.40 30.57 o -9 6 0 6.15 -4.53 33.17 o -8 6 0 2844.08 2999.55 78.07 o -7 6 0 44.38 58.59 15.28 o -6 6 0 4424.40 4458.61 108.40 o -5 6 0 299.99 328.69 19.84 o -4 6 0 4574.48 4844.38 84.07 o -3 6 0 3453.38 3717.52 66.29 o -2 6 0 830.63 670.43 22.11 o -1 6 0 6.44 -19.84 19.84 o 0 6 0 4413.49 4691.79 122.27 o 1 6 0 1710.31 1691.41 47.80 o 2 6 0 2906.12 2783.53 126.82 o 3 6 0 3139.79 3515.38 78.18 o 4 6 0 117.49 81.01 10.71 o 5 6 0 6579.29 6282.55 115.65 o 6 6 0 1796.11 1670.38 41.50 o 7 6 0 456.88 433.97 17.13 o 8 6 0 810.64 872.80 26.39 o 9 6 0 229.51 212.31 19.51 o 10 6 0 2.83 -6.48 13.05 o 11 6 0 176.86 122.34 17.03 o 12 6 0 19.45 26.19 25.36 o 13 6 0 230.49 211.37 48.78 o 14 6 0 125.28 85.85 39.02 o -14 7 0 507.63 597.04 65.04 o -13 7 0 7.31 -33.82 33.82 o -12 7 0 24.24 43.40 34.14 o -11 7 0 21.49 26.20 21.46 o -10 7 0 247.81 240.77 18.29 o -9 7 0 149.63 180.29 41.30 o -8 7 0 1253.55 1255.93 95.28 o -7 7 0 480.35 479.45 15.18 o -6 7 0 300.38 260.03 14.63 o -5 7 0 63.00 36.19 7.58 o -4 7 0 10956.65 11564.62 186.90 o -3 7 0 2521.74 2542.26 52.86 o -2 7 0 3840.15 3848.58 65.03 o -1 7 0 433.55 444.85 14.14 o 0 7 0 10478.52 10270.03 251.04 o 1 7 0 225.86 244.57 32.52 o 2 7 0 4604.78 4583.28 101.40 o 3 7 0 3506.92 2944.10 66.89 o 4 7 0 2318.46 2252.64 55.38 o 5 7 0 1526.61 1335.70 35.13 o 6 7 0 161.86 128.94 14.96 o 7 7 0 5643.10 5370.04 139.18 o 8 7 0 645.48 589.43 31.22 o 9 7 0 2552.99 2280.08 58.38 o 10 7 0 2791.59 2656.26 71.87 o 11 7 0 12.67 55.84 28.29 o 12 7 0 181.23 144.38 42.92 o 13 7 0 206.33 145.03 48.78 o 14 7 0 220.27 132.03 40.97 o -13 8 0 196.72 238.56 27.97 o -12 8 0 14.88 36.28 30.24 o -11 8 0 698.02 701.44 67.64 o -10 8 0 3193.72 3224.12 139.18 o -9 8 0 972.93 1058.32 68.29 o -8 8 0 12.02 0.94 11.47 o -7 8 0 95.07 87.68 28.62 o -6 8 0 52.20 64.39 8.89 o -5 8 0 973.44 863.67 21.41 o -4 8 0 730.81 684.10 25.04 o -3 8 0 374.34 262.64 21.46 o -2 8 0 1221.63 1190.68 27.84 o -1 8 0 779.74 810.79 21.75 o 0 8 0 796.32 843.05 59.51 o 1 8 0 4608.26 4944.63 113.49 o 2 8 0 3108.69 2936.18 69.01 o 3 8 0 207.95 175.37 36.10 o 4 8 0 493.29 446.97 17.69 o 5 8 0 23.21 8.58 19.51 o 6 8 0 511.73 466.32 22.11 o 7 8 0 208.68 180.73 18.44 o 8 8 0 3557.18 3614.69 101.02 o 9 8 0 8.03 -14.87 26.01 o 10 8 0 276.63 241.13 40.65 o 11 8 0 194.77 228.20 27.65 o 12 8 0 247.99 230.88 49.43 o 13 8 0 0.46 -0.65 46.18 o -13 9 0 7.93 102.76 41.62 o -12 9 0 673.09 771.02 29.64 o -11 9 0 6.35 4.41 13.56 o -10 9 0 244.52 250.96 17.59 o -9 9 0 271.84 235.93 14.94 o -8 9 0 646.04 598.46 20.69 o -7 9 0 463.72 367.10 15.74 o -6 9 0 280.60 221.52 10.62 o -5 9 0 115.82 100.91 8.45 o -4 9 0 138.32 96.62 9.51 o -3 9 0 45.55 20.10 6.24 o -2 9 0 359.63 341.98 13.38 o -1 9 0 1988.57 1795.10 40.65 o 0 9 0 4428.43 4275.96 180.48 o 1 9 0 2564.52 2577.64 59.17 o 2 9 0 262.64 209.53 14.63 o 3 9 0 303.72 251.39 17.56 o 4 9 0 508.78 485.50 26.34 o 5 9 0 1490.73 1444.99 38.26 o 6 9 0 943.14 910.21 32.52 o 7 9 0 18.69 15.77 13.66 o 8 9 0 315.69 246.47 21.67 o 9 9 0 219.49 208.23 23.58 o 10 9 0 583.15 475.62 41.95 o 11 9 0 2.64 -14.96 37.07 o 12 9 0 128.69 152.19 44.23 o -13 10 0 596.22 738.08 126.82 o -12 10 0 37.90 51.46 26.01 o -11 10 0 34.32 56.08 42.60 o -10 10 0 166.88 131.12 16.32 o -9 10 0 386.31 339.95 20.93 o -8 10 0 140.21 134.34 16.91 o -7 10 0 1400.93 1395.24 37.46 o -6 10 0 452.42 392.01 16.50 o -5 10 0 1276.99 1141.57 29.22 o -4 10 0 134.12 130.23 26.34 o -3 10 0 1434.50 1413.20 39.67 o -2 10 0 847.58 805.13 46.50 o -1 10 0 1027.21 940.81 39.02 o 0 10 0 4610.26 4044.52 85.79 o 1 10 0 810.94 853.40 21.57 o 2 10 0 243.35 189.40 38.70 o 3 10 0 5060.69 5037.79 112.25 o 4 10 0 3020.23 2952.94 99.51 o 5 10 0 430.04 383.56 16.58 o 6 10 0 356.44 340.16 36.75 o 7 10 0 9.14 9.78 13.84 o 8 10 0 27.05 5.65 17.40 o 9 10 0 70.14 52.12 20.56 o 10 10 0 184.24 188.53 32.84 o 11 10 0 127.56 89.10 39.02 o 12 10 0 102.14 152.84 44.23 o 13 10 0 14.21 115.77 37.07 o -13 11 0 86.08 102.34 30.27 o -12 11 0 429.38 426.50 24.82 o -11 11 0 70.14 74.27 18.54 o -10 11 0 86.72 56.19 31.22 o -9 11 0 1004.01 1010.03 44.23 o -8 11 0 3550.42 3613.94 119.02 o -7 11 0 819.84 791.30 69.26 o -6 11 0 1683.66 1615.33 60.48 o -5 11 0 500.90 506.92 32.52 o -4 11 0 1408.50 1286.14 84.87 o -3 11 0 136.39 136.86 6.90 o -2 11 0 5308.83 5723.19 129.10 o -1 11 0 2438.73 2319.52 76.09 o 0 11 0 1521.99 1385.35 34.95 o 1 11 0 8.78 4.57 12.03 o 2 11 0 5148.46 5046.33 92.79 o 3 11 0 448.02 486.95 18.73 o 4 11 0 1129.16 1148.44 34.20 o 5 11 0 5513.83 5742.75 123.92 o 6 11 0 1270.99 1147.59 35.63 o 7 11 0 50.99 39.76 32.19 o 8 11 0 3.73 31.53 13.71 o 9 11 0 624.46 563.42 42.60 o 10 11 0 1540.16 1536.43 64.38 o 11 11 0 562.46 530.70 59.83 o 12 11 0 596.35 472.17 55.28 o -12 12 0 99.25 120.95 28.57 o -11 12 0 245.41 233.33 19.63 o -10 12 0 107.79 83.02 18.52 o -9 12 0 591.91 533.06 26.68 o -8 12 0 876.18 764.19 39.67 o -7 12 0 122.68 113.82 13.01 o -6 12 0 65.05 37.35 9.43 o -5 12 0 812.64 787.05 23.67 o -4 12 0 2272.33 2141.54 217.55 o -3 12 0 18.06 8.14 24.06 o -2 12 0 2.75 -1.30 6.50 o -1 12 0 2.10 6.35 10.41 o 0 12 0 2.62 -1.30 7.80 o 1 12 0 732.15 690.00 18.51 o 2 12 0 1748.48 1607.71 76.42 o 3 12 0 440.47 461.08 20.16 o 4 12 0 580.51 505.67 19.35 o 5 12 0 1294.44 1302.28 37.97 o 6 12 0 8.56 -20.49 20.49 o 7 12 0 1179.77 1146.65 98.53 o 8 12 0 50.15 54.37 15.64 o 9 12 0 25.18 3.71 34.79 o 10 12 0 365.60 414.55 109.59 o 11 12 0 30.89 74.79 42.92 o 12 12 0 8.78 -13.01 42.92 o -12 13 0 306.20 373.79 36.10 o -11 13 0 744.09 741.90 43.57 o -10 13 0 960.83 1010.72 123.57 o -9 13 0 601.99 546.69 38.05 o -8 13 0 273.10 276.11 27.32 o -7 13 0 142.07 144.94 15.71 o -6 13 0 2079.18 2129.18 110.56 o -5 13 0 6.63 -8.08 8.08 o -4 13 0 1005.10 886.47 84.22 o -3 13 0 1.68 -1.16 7.15 o -2 13 0 77.88 50.73 7.15 o -1 13 0 44.31 44.23 7.15 o 0 13 0 306.23 208.61 8.89 o 1 13 0 3425.05 3354.61 67.31 o 2 13 0 211.54 170.12 10.23 o 3 13 0 20.64 -4.21 10.41 o 4 13 0 116.65 97.11 13.24 o 5 13 0 1006.01 961.99 32.84 o 6 13 0 984.28 915.45 30.60 o 7 13 0 1518.38 1583.14 76.42 o 8 13 0 987.84 856.46 58.21 o 9 13 0 27.94 16.46 39.67 o 10 13 0 104.71 172.35 40.97 o 11 13 0 25.27 -26.67 41.62 o -11 14 0 82.37 76.89 22.84 o -10 14 0 602.74 604.58 40.09 o -9 14 0 17.33 12.81 18.54 o -8 14 0 129.86 102.03 15.61 o -7 14 0 376.37 322.58 18.21 o -6 14 0 88.31 61.14 9.76 o -5 14 0 152.28 117.54 33.82 o -4 14 0 384.63 331.11 34.47 o -3 14 0 584.48 508.59 14.31 o -2 14 0 457.78 516.40 27.97 o -1 14 0 382.87 324.54 14.31 o 0 14 0 529.91 468.27 17.56 o 1 14 0 64.13 54.34 7.19 o 2 14 0 1231.21 1182.76 27.87 o 3 14 0 606.48 614.12 19.48 o 4 14 0 1291.34 1284.90 49.50 o 5 14 0 45.43 17.72 12.75 o 6 14 0 542.31 561.56 23.46 o 7 14 0 52.29 40.88 15.75 o 8 14 0 265.16 235.55 29.92 o 9 14 0 878.13 788.86 49.75 o 10 14 0 286.31 398.03 48.13 o 11 14 0 3.13 3.90 41.62 o -11 15 0 10.89 21.46 41.62 o -10 15 0 15.93 1.68 20.91 o -9 15 0 1.83 -6.28 28.62 o -8 15 0 479.49 382.61 62.76 o -7 15 0 589.82 559.44 37.72 o -6 15 0 1116.05 1088.30 46.83 o -5 15 0 5.28 -15.61 15.61 o -4 15 0 10.21 -2.58 26.34 o -3 15 0 1139.65 1203.84 49.43 o -2 15 0 2278.98 2251.59 82.60 o -1 15 0 65.23 41.62 25.36 o 0 15 0 1107.77 1013.93 42.27 o 1 15 0 100.99 124.40 7.96 o 2 15 0 302.16 277.91 12.96 o 3 15 0 9.76 16.00 9.11 o 4 15 0 2105.36 2230.71 53.08 o 5 15 0 1434.07 1427.17 50.82 o 6 15 0 17.46 23.63 14.66 o 7 15 0 415.90 395.46 22.60 o 8 15 0 127.70 146.72 36.42 o 9 15 0 15.52 -0.98 17.91 o 10 15 0 185.10 273.16 48.13 o -10 16 0 150.95 122.27 45.53 o -9 16 0 262.57 236.74 46.83 o -8 16 0 193.65 227.50 47.15 o -7 16 0 163.94 125.37 19.19 o -6 16 0 80.11 70.89 9.76 o -5 16 0 252.16 217.02 10.05 o -4 16 0 42.53 23.41 28.62 o -3 16 0 260.73 212.67 24.06 o -2 16 0 1019.03 959.30 44.23 o -1 16 0 186.96 198.36 19.51 o 0 16 0 20.33 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