#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:26:56 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181168 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/47/2224703.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224703_Fobs loop_ _publ_author_name 'Howie, R. Alan' 'de Souza, Marcus V. N.' 'Wardell, Solange M. S. V.' 'Wardell, James L.' 'Tiekink, Edward R. T.' _publ_section_title ; N'-[(E)-2,6-Dichlorobenzylidene]pyrazine-2-carbohydrazide ; _journal_coeditor_code LH2969 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o178 _journal_page_last o179 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.709 _cell_angle_gamma 90.000 _cell_length_a 6.9325 _cell_length_b 24.5997 _cell_length_c 7.6136 _exptl_crystal_F_000 600.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file lh2969Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pptb6 in P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 194.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 3401.31 3586.54 120.75 o 6 0 0 14.51 100.87 20.50 o 1 1 0 10.30 9.66 0.93 o 2 1 0 21492.25 21021.37 398.87 o 3 1 0 26.12 18.46 2.37 o 4 1 0 3276.43 3429.27 84.86 o 5 1 0 115.57 124.39 6.35 o 6 1 0 157.85 136.03 7.09 o 7 1 0 150.10 184.38 19.34 o 1 2 0 2804.82 2751.28 66.11 o 2 2 0 1702.19 1788.86 34.97 o 3 2 0 112.19 110.39 4.26 o 4 2 0 3032.50 3027.15 73.07 o 5 2 0 506.98 517.03 14.23 o 6 2 0 876.65 872.03 31.07 o 7 2 0 7.68 15.62 6.79 o 1 3 0 64.76 65.89 4.21 o 2 3 0 2366.02 2358.79 50.94 o 3 3 0 2168.76 2072.70 42.52 o 4 3 0 196.76 192.10 6.52 o 5 3 0 42.55 78.90 17.34 o 6 3 0 11.61 34.90 6.57 o 7 3 0 90.32 87.19 13.54 o 0 4 0 290.50 315.91 9.66 o 1 4 0 4973.47 4784.05 131.24 o 2 4 0 258.99 284.40 7.20 o 3 4 0 1864.07 1856.32 39.95 o 4 4 0 184.32 207.11 9.80 o 5 4 0 1777.70 1770.48 50.50 o 6 4 0 29.17 31.07 5.03 o 7 4 0 8.15 10.29 5.66 o 1 5 0 88.17 103.02 5.47 o 2 5 0 1150.86 1160.52 31.83 o 3 5 0 268.32 235.32 7.71 o 4 5 0 409.22 393.26 13.25 o 5 5 0 295.75 314.52 12.46 o 6 5 0 285.41 276.44 15.65 o 7 5 0 578.14 538.94 43.02 o 0 6 0 1476.34 1555.01 40.99 o 1 6 0 10637.04 9936.51 243.82 o 2 6 0 169.09 185.78 6.34 o 3 6 0 1929.86 1936.05 45.90 o 4 6 0 136.52 129.58 7.97 o 5 6 0 11.69 9.84 4.10 o 6 6 0 1.12 16.67 9.93 o 7 6 0 63.94 49.43 6.70 o 1 7 0 36.90 37.06 3.41 o 2 7 0 557.14 563.70 18.30 o 3 7 0 308.30 268.30 8.60 o 4 7 0 651.33 618.47 18.19 o 5 7 0 31.86 51.01 12.01 o 6 7 0 601.62 615.87 29.25 o 7 7 0 208.56 222.42 20.57 o 0 8 0 10589.68 11859.94 315.22 o 1 8 0 3860.18 3735.93 92.16 o 2 8 0 97.53 93.58 4.87 o 3 8 0 2517.27 2500.86 73.31 o 4 8 0 391.63 416.76 19.75 o 5 8 0 1179.63 1208.14 39.35 o 6 8 0 75.89 76.47 6.32 o 7 8 0 372.54 316.51 25.17 o 1 9 0 535.76 552.66 15.35 o 2 9 0 5913.46 5859.44 171.15 o 3 9 0 754.66 746.44 23.21 o 4 9 0 464.02 473.64 15.66 o 5 9 0 682.06 715.92 39.06 o 6 9 0 21.39 31.50 8.04 o 7 9 0 211.18 232.99 20.10 o 0 10 0 3649.20 4201.65 113.93 o 1 10 0 3994.58 4150.76 99.62 o 2 10 0 131.43 149.15 7.59 o 3 10 0 1367.29 1391.17 39.31 o 4 10 0 1581.39 1589.27 47.81 o 5 10 0 711.90 671.61 24.37 o 6 10 0 437.59 443.58 25.50 o 7 10 0 9.49 16.70 5.61 o 1 11 0 3.55 9.38 2.62 o 2 11 0 3036.94 3141.72 96.08 o 3 11 0 722.51 633.44 24.07 o 4 11 0 443.70 375.99 25.18 o 5 11 0 1.09 29.51 7.30 o 6 11 0 52.66 44.83 7.37 o 7 11 0 119.76 159.37 21.87 o 0 12 0 4368.97 4725.05 219.30 o 1 12 0 335.70 346.10 12.29 o 2 12 0 942.02 972.69 36.25 o 3 12 0 398.65 400.60 22.99 o 4 12 0 112.75 105.85 6.86 o 5 12 0 798.53 820.74 33.56 o 6 12 0 204.16 185.54 27.42 o 1 13 0 13.17 10.93 3.05 o 2 13 0 0.13 1.67 6.67 o 3 13 0 69.75 73.07 10.13 o 4 13 0 3.44 -0.70 3.84 o 5 13 0 429.40 426.95 22.90 o 6 13 0 217.65 241.84 40.90 o 0 14 0 4486.26 4941.44 233.41 o 1 14 0 891.11 844.48 26.87 o 2 14 0 1344.84 1283.40 114.31 o 3 14 0 3.67 13.31 5.20 o 4 14 0 605.76 631.86 24.20 o 5 14 0 402.15 371.91 22.95 o 6 14 0 99.90 125.66 13.93 o 1 15 0 165.84 171.27 8.95 o 2 15 0 213.30 250.25 14.22 o 3 15 0 688.46 733.63 31.58 o 4 15 0 51.85 54.85 6.38 o 5 15 0 8.60 5.07 3.72 o 6 15 0 1.92 14.25 11.35 o 0 16 0 423.85 404.32 33.81 o 1 16 0 10.37 23.94 4.80 o 2 16 0 302.06 284.96 16.96 o 3 16 0 249.51 217.37 13.90 o 4 16 0 541.00 473.30 31.34 o 5 16 0 243.33 266.39 13.72 o 6 16 0 206.03 207.66 37.15 o 1 17 0 91.99 79.25 5.82 o 2 17 0 2218.93 1999.00 83.63 o 3 17 0 54.09 76.54 20.17 o 4 17 0 559.80 617.64 24.37 o 5 17 0 9.01 52.93 12.24 o 6 17 0 66.24 76.36 12.35 o 0 18 0 1381.86 1393.69 78.25 o 1 18 0 301.12 272.71 14.02 o 2 18 0 0.15 -3.80 6.95 o 3 18 0 64.95 85.01 12.11 o 4 18 0 412.07 410.57 18.55 o 5 18 0 50.21 52.91 9.10 o 6 18 0 157.72 117.74 19.13 o 1 19 0 49.13 32.72 6.70 o 2 19 0 359.57 340.85 16.97 o 3 19 0 743.40 717.13 43.94 o 4 19 0 5.77 34.82 8.31 o 5 19 0 61.62 87.86 10.09 o 0 20 0 598.89 679.57 57.59 o 1 20 0 1439.60 1489.17 59.27 o 2 20 0 36.82 38.24 5.62 o 3 20 0 102.25 83.58 9.96 o 4 20 0 264.27 244.93 13.65 o 5 20 0 355.23 305.00 27.03 o 1 21 0 32.40 41.80 9.58 o 2 21 0 161.75 163.47 15.84 o 3 21 0 274.17 264.63 16.02 o 4 21 0 106.13 116.96 11.61 o 5 21 0 70.16 67.75 8.23 o 0 22 0 74.05 81.32 16.96 o 1 22 0 181.71 116.78 33.94 o 2 22 0 211.80 159.60 10.30 o 3 22 0 48.73 87.73 17.06 o 4 22 0 26.70 23.17 8.03 o 5 22 0 304.23 307.18 21.55 o 1 23 0 186.67 141.52 16.66 o 2 23 0 75.55 61.59 13.44 o 3 23 0 651.42 589.42 36.25 o 4 23 0 495.69 477.31 30.71 o 0 24 0 698.26 761.24 63.90 o 1 24 0 308.06 316.85 29.05 o 2 24 0 1145.96 1082.73 49.83 o 3 24 0 0.59 -2.90 16.52 o 4 24 0 177.22 138.86 13.89 o 1 25 0 57.27 58.33 12.47 o 2 25 0 70.44 81.94 12.47 o 3 25 0 36.00 39.32 8.92 o 0 26 0 1129.73 1043.40 91.36 o 1 26 0 198.87 223.39 20.12 o 2 26 0 233.38 243.19 30.72 o 3 26 0 1.92 4.07 11.91 o 1 27 0 31.85 23.47 12.21 o 2 27 0 142.78 156.29 18.17 o 0 28 0 513.24 588.06 49.70 o 1 28 0 91.81 88.31 11.12 o 2 28 0 130.41 140.37 14.26 o 1 29 0 19.31 12.08 16.78 o -7 0 1 15.61 43.52 16.98 o -5 0 1 1034.58 1043.71 46.59 o -3 0 1 626.66 581.15 16.36 o -1 0 1 70.05 65.15 2.41 o 1 0 1 1327.36 1362.70 51.78 o 3 0 1 2531.59 2473.82 76.60 o 5 0 1 31.61 58.64 14.54 o 7 0 1 33.46 62.86 23.01 o -7 1 1 24.86 26.14 10.34 o -6 1 1 651.71 663.89 20.56 o -5 1 1 14.30 10.79 2.68 o -4 1 1 1985.42 2034.05 43.45 o -3 1 1 237.70 253.85 5.90 o -2 1 1 280.03 268.95 6.54 o -1 1 1 124.77 136.43 2.67 o 0 1 1 120.66 134.46 5.37 o 1 1 1 232.57 280.49 7.05 o 2 1 1 305.37 258.10 8.15 o 3 1 1 838.40 727.34 15.98 o 4 1 1 153.91 136.50 6.33 o 5 1 1 237.65 239.47 11.91 o 6 1 1 71.58 79.98 6.54 o 7 1 1 61.75 63.73 8.28 o -7 2 1 924.84 926.36 37.68 o -6 2 1 823.19 793.70 27.67 o -5 2 1 1069.76 1092.28 26.84 o -4 2 1 9039.34 9429.19 201.55 o -3 2 1 2713.13 2785.75 51.65 o -2 2 1 37639.50 37891.40 1217.73 o -1 2 1 1199.44 1124.35 21.34 o 0 2 1 8347.31 8275.42 380.98 o 1 2 1 4.06 -0.79 1.66 o 2 2 1 158.95 199.45 5.38 o 3 2 1 19.62 19.60 2.15 o 4 2 1 9.82 14.93 2.66 o 5 2 1 855.38 873.32 26.95 o 6 2 1 15.30 26.59 6.04 o 7 2 1 177.15 242.23 18.48 o -7 3 1 5.78 2.10 3.99 o -6 3 1 2159.40 2136.43 63.34 o -5 3 1 60.69 61.00 5.35 o -4 3 1 6523.57 6777.81 159.99 o -3 3 1 239.93 239.34 5.90 o -2 3 1 75.96 90.33 2.83 o -1 3 1 1622.62 1566.68 30.18 o 0 3 1 3836.12 4056.08 165.98 o 1 3 1 20.02 15.52 3.24 o 2 3 1 5.67 13.31 2.11 o 3 3 1 18.53 20.41 2.36 o 4 3 1 8.70 5.46 4.59 o 5 3 1 1.57 29.62 9.53 o 6 3 1 94.11 88.74 12.44 o 7 3 1 6.72 13.75 11.39 o -7 4 1 27.89 18.97 6.36 o -6 4 1 2713.30 2600.88 85.37 o -5 4 1 10.73 15.81 3.21 o -4 4 1 650.83 657.91 18.03 o -3 4 1 53.19 56.15 3.16 o -2 4 1 2048.59 2023.63 43.69 o -1 4 1 732.07 686.12 13.91 o 0 4 1 594.93 601.18 23.37 o 1 4 1 1048.73 1064.69 28.32 o 2 4 1 0.86 -3.79 2.52 o 3 4 1 113.69 112.77 4.74 o 4 4 1 217.49 241.01 18.81 o 5 4 1 8.83 16.83 5.71 o 6 4 1 386.27 403.47 17.93 o 7 4 1 40.87 36.11 7.97 o -7 5 1 68.38 52.62 6.29 o -6 5 1 51.66 66.86 5.21 o -5 5 1 1.47 7.48 2.28 o -4 5 1 2388.22 2405.92 63.65 o -3 5 1 1179.66 1134.43 31.67 o -2 5 1 8.58 11.74 1.87 o -1 5 1 3821.22 3491.27 75.25 o 0 5 1 870.21 881.47 26.22 o 1 5 1 4022.87 3714.15 133.95 o 2 5 1 542.55 497.89 13.35 o 3 5 1 170.78 150.28 7.90 o 4 5 1 96.52 81.36 5.25 o 5 5 1 1.26 0.65 4.40 o 6 5 1 0.80 -2.44 3.28 o 7 5 1 29.22 30.72 6.19 o -7 6 1 4.09 -1.43 4.20 o -6 6 1 96.20 86.36 6.36 o -5 6 1 308.40 318.26 11.39 o -4 6 1 288.28 275.50 9.35 o -3 6 1 531.56 487.59 12.98 o -2 6 1 3265.13 3098.13 67.07 o -1 6 1 754.58 727.13 16.31 o 0 6 1 532.20 488.70 14.64 o 1 6 1 16.01 22.10 3.73 o 2 6 1 664.85 580.79 15.78 o 3 6 1 129.35 111.01 5.01 o 4 6 1 56.11 69.94 7.28 o 5 6 1 301.27 319.69 17.76 o 6 6 1 45.43 61.14 5.96 o 7 6 1 57.88 67.92 9.07 o -7 7 1 27.48 20.47 11.20 o -6 7 1 27.62 24.80 4.79 o -5 7 1 72.30 77.45 5.11 o -4 7 1 850.30 857.40 25.90 o -3 7 1 17.12 31.69 2.92 o -2 7 1 92.38 104.51 4.19 o -1 7 1 321.45 291.52 7.49 o 0 7 1 14.84 3.68 2.93 o 1 7 1 0.23 7.95 3.38 o 2 7 1 554.99 520.23 17.24 o 3 7 1 1516.20 1557.29 41.51 o 4 7 1 246.01 234.11 10.73 o 5 7 1 471.52 468.77 17.69 o 6 7 1 0.55 5.96 3.91 o 7 7 1 17.49 6.48 11.62 o -7 8 1 0.27 2.71 13.73 o -6 8 1 351.96 390.68 19.50 o -5 8 1 617.63 606.04 21.56 o -4 8 1 86.10 101.55 5.77 o -3 8 1 362.76 265.80 10.44 o -2 8 1 49.32 46.11 3.77 o -1 8 1 9.73 29.29 3.24 o 0 8 1 39.04 50.80 3.53 o 1 8 1 2015.24 1881.45 58.44 o 2 8 1 44.44 51.27 4.42 o 3 8 1 2801.17 2753.15 75.72 o 4 8 1 280.08 303.50 13.18 o 5 8 1 0.05 50.14 25.50 o 6 8 1 315.99 323.07 12.97 o -6 9 1 6.18 11.56 10.70 o -5 9 1 0.88 -0.99 2.76 o -4 9 1 151.45 130.25 6.51 o -3 9 1 1762.99 1664.87 47.28 o -2 9 1 697.97 683.64 19.60 o -1 9 1 2637.40 2424.01 53.24 o 0 9 1 2374.15 2537.76 64.76 o 1 9 1 3000.56 2780.85 76.13 o 2 9 1 1988.36 1924.95 59.69 o 3 9 1 231.94 253.58 10.83 o 4 9 1 228.30 227.46 11.20 o 5 9 1 429.30 414.95 22.93 o 6 9 1 86.06 93.24 16.15 o -7 10 1 535.91 577.02 34.42 o -6 10 1 62.70 54.54 8.49 o -5 10 1 302.80 291.08 14.01 o -4 10 1 1.26 4.12 2.88 o -3 10 1 715.42 775.54 23.09 o -2 10 1 245.87 202.79 11.87 o -1 10 1 1181.15 1134.10 30.98 o 0 10 1 458.29 540.04 13.38 o 1 10 1 1445.55 1268.35 53.78 o 2 10 1 21.50 13.92 5.84 o 3 10 1 774.27 739.75 25.90 o 4 10 1 208.66 227.67 12.97 o 5 10 1 90.02 87.54 9.75 o 6 10 1 263.10 221.61 21.61 o -7 11 1 1.62 16.07 15.64 o -6 11 1 111.92 116.58 9.52 o -5 11 1 3.38 31.54 6.14 o -4 11 1 144.28 129.95 7.92 o -3 11 1 267.44 281.11 9.30 o -2 11 1 2642.39 2602.43 75.50 o -1 11 1 1026.82 1091.92 27.38 o 0 11 1 4692.17 5041.29 128.09 o 1 11 1 1707.80 1804.77 68.54 o 2 11 1 78.32 34.89 15.01 o 3 11 1 80.12 70.67 7.87 o 4 11 1 1.48 3.24 3.09 o 5 11 1 0.83 3.32 4.70 o 6 11 1 85.66 55.79 10.42 o -7 12 1 142.13 36.61 11.99 o -6 12 1 2.87 15.99 9.76 o -5 12 1 596.79 566.47 21.45 o -4 12 1 826.67 821.70 28.88 o -3 12 1 1484.22 1624.88 71.75 o -2 12 1 3780.40 3735.87 114.12 o -1 12 1 1226.86 1305.41 34.79 o 0 12 1 209.88 261.81 10.68 o 1 12 1 16.06 37.56 10.52 o 2 12 1 313.60 257.57 17.54 o 3 12 1 449.70 444.64 20.20 o 4 12 1 38.37 24.61 4.30 o 5 12 1 566.15 615.70 60.25 o 6 12 1 8.67 22.32 25.14 o -7 13 1 48.20 37.54 10.92 o -6 13 1 445.04 460.02 28.65 o -5 13 1 176.44 117.83 13.44 o -4 13 1 1810.86 1743.64 55.76 o -3 13 1 875.52 934.53 40.74 o -2 13 1 62.14 88.39 7.11 o -1 13 1 640.08 670.74 18.97 o 0 13 1 1181.84 1449.35 45.40 o 1 13 1 230.52 193.24 17.07 o 2 13 1 48.79 27.34 4.88 o 3 13 1 39.69 59.79 8.28 o 4 13 1 52.26 47.26 6.16 o 5 13 1 0.13 6.36 7.82 o 6 13 1 3.75 20.68 6.23 o -7 14 1 3.75 11.52 15.30 o -6 14 1 24.04 35.72 10.20 o -5 14 1 144.09 114.98 8.27 o -4 14 1 847.43 893.09 33.13 o -3 14 1 31.51 27.54 10.26 o -2 14 1 3078.31 3148.59 113.67 o -1 14 1 70.93 91.96 7.18 o 0 14 1 107.74 70.25 8.86 o 1 14 1 519.16 545.78 30.96 o 2 14 1 1112.96 1122.86 45.91 o 3 14 1 368.66 376.69 17.00 o 4 14 1 522.77 532.78 25.71 o 5 14 1 110.14 113.98 13.52 o 6 14 1 53.82 46.53 9.24 o -6 15 1 70.51 39.91 14.10 o -5 15 1 306.76 299.95 16.43 o -4 15 1 81.40 106.93 8.99 o -3 15 1 88.13 85.43 11.28 o -2 15 1 1283.27 1116.85 41.37 o -1 15 1 353.37 324.12 16.91 o 0 15 1 3672.12 3798.80 116.29 o 1 15 1 107.06 124.70 7.52 o 2 15 1 674.43 616.40 30.62 o 3 15 1 1079.83 1051.99 76.94 o 4 15 1 13.56 19.21 5.27 o 5 15 1 111.85 166.44 17.09 o 6 15 1 12.53 6.34 8.74 o -6 16 1 291.14 357.26 21.55 o -5 16 1 20.74 45.99 8.95 o -4 16 1 22.53 33.22 5.13 o -3 16 1 215.22 255.09 19.57 o -2 16 1 36.12 23.96 3.55 o -1 16 1 149.18 101.64 10.11 o 0 16 1 8.53 44.24 10.67 o 1 16 1 49.74 34.58 8.13 o 2 16 1 27.10 41.38 16.35 o 3 16 1 55.68 44.77 7.62 o 4 16 1 155.04 136.73 10.84 o 5 16 1 824.77 992.46 47.47 o 6 16 1 463.56 451.11 28.67 o -6 17 1 10.87 -3.92 13.41 o -5 17 1 186.25 199.61 14.13 o -4 17 1 58.76 53.19 5.80 o -3 17 1 554.92 571.99 23.36 o -2 17 1 140.20 166.10 17.80 o -1 17 1 2258.81 2233.24 72.54 o 0 17 1 222.13 259.29 11.78 o 1 17 1 2309.92 2104.55 81.25 o 2 17 1 25.89 44.95 8.24 o 3 17 1 68.66 78.40 14.33 o 4 17 1 112.94 112.49 15.37 o 5 17 1 291.07 302.80 17.40 o -6 18 1 59.61 64.63 18.01 o -5 18 1 63.37 92.06 11.15 o -4 18 1 68.55 71.75 12.26 o -3 18 1 264.61 250.26 14.64 o -2 18 1 16.42 5.41 5.99 o -1 18 1 1.46 -1.82 4.27 o 0 18 1 1.56 9.38 3.48 o 1 18 1 1146.79 1024.39 38.57 o 2 18 1 358.99 386.64 22.38 o 3 18 1 1301.00 1315.96 57.67 o 4 18 1 246.87 294.98 18.55 o 5 18 1 11.88 24.51 11.34 o -6 19 1 26.08 34.54 8.65 o -5 19 1 391.32 482.40 27.87 o -4 19 1 47.17 38.84 6.42 o -3 19 1 136.68 129.42 8.41 o -2 19 1 1313.97 1415.87 80.73 o -1 19 1 11.78 46.92 17.62 o 0 19 1 1422.39 1538.14 56.61 o 1 19 1 64.93 69.52 6.79 o 2 19 1 89.10 60.71 6.88 o 3 19 1 891.53 936.82 61.07 o 4 19 1 49.71 38.85 9.14 o 5 19 1 596.65 616.76 36.84 o -5 20 1 10.73 40.98 8.36 o -4 20 1 41.73 38.95 7.00 o -3 20 1 162.70 160.10 11.43 o -2 20 1 51.19 109.28 10.90 o -1 20 1 9.46 19.38 8.05 o 0 20 1 1535.79 1542.85 56.10 o 1 20 1 233.41 282.98 18.16 o 2 20 1 1153.72 1126.67 46.33 o 3 20 1 267.04 265.09 19.08 o 4 20 1 329.91 358.33 21.82 o 5 20 1 51.25 40.68 10.47 o -5 21 1 0.35 1.79 5.09 o -4 21 1 164.88 166.40 18.36 o -3 21 1 9.76 -2.95 5.20 o -2 21 1 0.00 36.78 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