#------------------------------------------------------------------------------ #$Date: 2010-02-13 12:42:52 +0200 (Sat, 13 Feb 2010) $ #$Revision: 986 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224717.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224717_Fobs loop_ _publ_author_name 'Wang, Shuping' 'Dong, Huajiang' 'Chen, Hong' 'Zhu, Kunpeng' 'Zhu, Tieliang' _publ_section_title ; Methyl 2-(5-fluoro-1H-indol-3-yl)-2-oxoacetate ; _journal_coeditor_code NG2701 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o155 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.009 _cell_angle_gamma 90.000 _cell_length_a 7.0584 _cell_length_b 20.5860 _cell_length_c 7.3286 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.7600 _[local]_cod_data_source_file ng2701Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' R91012F in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 68.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12.91 12.63 0.42 o 3 0 0 24.93 21.12 0.55 o 4 0 0 1034.71 1109.32 30.97 o 5 0 0 237.37 262.79 8.91 o 6 0 0 44.51 74.37 4.77 o 7 0 0 249.66 269.49 8.48 o 1 1 0 177.25 148.84 1.25 o 3 1 0 307.46 270.51 2.37 o 4 1 0 2091.65 2051.53 23.84 o 5 1 0 171.92 182.20 3.34 o 6 1 0 95.95 96.81 3.54 o 7 1 0 6.23 4.67 1.67 o 1 2 0 234.65 207.47 1.26 o 3 2 0 435.57 432.96 4.00 o 4 2 0 4710.93 4932.90 131.41 o 5 2 0 39.48 47.36 1.95 o 6 2 0 553.06 508.77 54.86 o 7 2 0 17.52 15.89 2.33 o 1 3 0 278.20 252.41 2.30 o 2 3 0 1908.64 1790.92 19.57 o 3 3 0 4.03 3.02 0.27 o 4 3 0 2591.73 2696.37 41.67 o 5 3 0 4.26 3.80 0.77 o 6 3 0 1124.55 1195.07 20.75 o 7 3 0 21.01 21.39 5.10 o 8 3 0 241.58 235.50 12.30 o 0 4 0 143.44 123.91 0.87 o 1 4 0 5.75 6.64 0.15 o 2 4 0 258.27 252.84 1.79 o 3 4 0 137.46 141.00 1.03 o 4 4 0 1125.52 1159.84 19.01 o 5 4 0 347.34 346.95 4.91 o 6 4 0 735.22 767.03 19.09 o 7 4 0 34.70 28.50 1.28 o 1 5 0 264.68 231.71 1.36 o 2 5 0 539.05 506.45 5.87 o 3 5 0 362.24 343.68 2.64 o 4 5 0 94.37 101.36 1.14 o 5 5 0 4.65 5.98 0.66 o 6 5 0 541.33 550.66 15.09 o 7 5 0 63.48 62.43 2.11 o 8 5 0 441.06 404.05 6.98 o 1 6 0 195.24 208.44 1.96 o 2 6 0 268.72 258.50 1.79 o 3 6 0 136.87 134.56 2.47 o 4 6 0 8.19 7.93 0.46 o 5 6 0 34.12 31.35 0.51 o 6 6 0 77.71 85.36 3.11 o 7 6 0 118.07 125.54 3.59 o 8 6 0 129.63 119.44 6.97 o 1 7 0 1601.69 1555.79 17.33 o 2 7 0 752.56 717.77 4.29 o 3 7 0 399.36 382.82 4.06 o 4 7 0 46.37 50.54 1.12 o 5 7 0 88.82 88.33 1.20 o 6 7 0 43.24 42.80 2.37 o 7 7 0 0.01 0.14 0.56 o 8 7 0 182.69 172.63 9.53 o 0 8 0 2.09 3.20 0.44 o 1 8 0 40.64 36.96 0.48 o 2 8 0 195.62 179.52 1.93 o 3 8 0 19.87 19.11 0.76 o 4 8 0 93.74 88.28 1.20 o 5 8 0 1.92 1.99 0.40 o 6 8 0 5.49 3.85 1.14 o 7 8 0 0.05 0.99 0.64 o 8 8 0 0.00 -0.37 1.09 o 1 9 0 2945.41 2900.30 58.39 o 2 9 0 50.96 65.16 0.65 o 3 9 0 304.42 301.20 4.75 o 4 9 0 228.15 244.28 4.51 o 5 9 0 119.80 125.76 2.44 o 6 9 0 126.62 134.10 3.48 o 7 9 0 22.26 22.56 4.42 o 8 9 0 43.20 44.29 5.55 o 0 10 0 161.20 197.82 2.82 o 1 10 0 340.88 319.34 2.21 o 2 10 0 127.14 162.79 2.97 o 3 10 0 117.51 118.44 2.61 o 4 10 0 53.15 61.63 1.59 o 5 10 0 0.00 0.15 0.33 o 6 10 0 16.92 16.33 1.21 o 7 10 0 100.53 101.04 2.42 o 1 11 0 217.83 239.35 2.15 o 2 11 0 117.12 126.94 1.26 o 3 11 0 775.44 739.92 9.01 o 4 11 0 159.15 147.25 2.35 o 5 11 0 3.52 2.60 0.91 o 6 11 0 100.80 100.10 2.06 o 7 11 0 38.86 41.53 4.87 o 0 12 0 1665.06 1868.66 29.04 o 1 12 0 24.65 23.79 0.59 o 2 12 0 798.28 860.00 7.21 o 3 12 0 213.39 211.81 2.69 o 4 12 0 158.94 166.59 2.90 o 5 12 0 607.73 645.82 9.98 o 6 12 0 38.85 41.86 2.15 o 7 12 0 27.07 28.14 6.12 o 1 13 0 51.36 49.40 0.70 o 2 13 0 186.08 196.86 2.24 o 3 13 0 293.46 269.39 3.12 o 4 13 0 18.25 16.29 1.40 o 5 13 0 2.10 1.43 0.58 o 6 13 0 14.82 15.89 1.68 o 7 13 0 214.49 231.93 8.62 o 0 14 0 107.19 104.62 3.00 o 1 14 0 46.14 43.62 0.76 o 2 14 0 73.55 83.12 1.34 o 3 14 0 6.32 6.53 0.76 o 4 14 0 416.47 442.26 9.25 o 5 14 0 139.09 130.58 3.16 o 6 14 0 162.58 154.92 3.25 o 7 14 0 145.86 148.17 4.81 o 1 15 0 27.29 30.26 0.82 o 2 15 0 510.21 489.43 5.59 o 3 15 0 129.10 116.10 1.67 o 4 15 0 53.61 47.03 2.39 o 5 15 0 480.31 486.47 12.79 o 6 15 0 5.78 4.64 1.08 o 7 15 0 240.40 238.08 7.40 o 0 16 0 1544.31 1540.18 35.45 o 1 16 0 111.21 107.71 1.87 o 2 16 0 314.72 323.82 3.89 o 3 16 0 779.55 753.15 15.82 o 4 16 0 3.08 2.28 0.70 o 5 16 0 475.88 482.52 8.27 o 6 16 0 22.02 22.04 1.22 o 1 17 0 1342.25 1236.67 18.19 o 2 17 0 113.21 114.02 1.43 o 3 17 0 891.44 864.08 11.47 o 4 17 0 1.99 1.46 0.64 o 5 17 0 77.14 66.25 2.62 o 6 17 0 0.86 0.99 0.60 o 0 18 0 319.99 355.18 5.38 o 1 18 0 58.83 55.37 2.47 o 2 18 0 345.17 357.58 6.24 o 3 18 0 29.07 19.94 3.51 o 4 18 0 171.96 172.54 2.96 o 5 18 0 5.97 5.48 1.32 o 6 18 0 30.61 28.06 1.61 o 1 19 0 1347.03 1271.28 12.81 o 2 19 0 161.72 167.76 2.29 o 3 19 0 164.84 158.25 3.33 o 4 19 0 140.26 148.53 2.92 o 5 19 0 0.77 0.62 0.42 o 6 19 0 45.43 44.72 2.36 o 0 20 0 276.89 283.16 5.11 o 1 20 0 129.80 137.60 3.20 o 2 20 0 5.94 6.34 0.91 o 3 20 0 346.74 356.97 5.56 o 4 20 0 108.33 104.66 2.47 o 5 20 0 80.65 78.86 2.51 o 1 21 0 29.98 20.74 0.90 o 2 21 0 248.01 246.25 4.13 o 3 21 0 138.15 127.05 2.59 o 4 21 0 7.41 4.23 1.10 o 5 21 0 161.61 155.37 4.07 o 0 22 0 166.10 151.99 3.89 o 1 22 0 7.40 5.64 0.96 o 2 22 0 5.19 6.04 1.36 o 3 22 0 49.12 45.05 1.96 o 4 22 0 107.94 112.17 3.19 o 5 22 0 85.76 84.80 3.21 o 1 23 0 0.35 0.66 0.44 o 2 23 0 66.45 76.21 1.82 o 3 23 0 21.53 18.48 1.44 o 4 23 0 16.97 9.82 2.57 o 0 24 0 24.13 33.31 1.66 o 1 24 0 4.04 4.22 0.99 o 2 24 0 6.86 3.84 0.92 o 3 24 0 12.64 10.30 2.86 o 1 25 0 26.81 28.00 1.28 o 2 25 0 18.50 19.58 1.26 o 3 25 0 7.43 5.40 1.69 o 0 26 0 43.49 45.01 2.08 o 1 26 0 0.10 0.11 0.32 o 2 26 0 35.24 31.79 1.82 o -8 1 1 23.61 20.81 1.42 o -7 1 1 30.68 32.78 1.49 o -6 1 1 20.17 24.89 1.53 o -5 1 1 140.68 164.72 2.86 o -4 1 1 103.05 136.86 1.51 o -3 1 1 1055.95 1104.28 6.12 o -2 1 1 1221.08 1177.58 10.46 o 0 1 1 970.85 909.21 13.91 o 1 1 1 135.30 111.30 1.48 o 2 1 1 29.72 32.43 0.37 o 3 1 1 1252.53 1227.27 10.17 o 4 1 1 0.31 0.14 0.22 o 5 1 1 147.37 168.70 2.86 o 6 1 1 1.17 0.92 0.33 o 7 1 1 5.95 5.88 1.84 o -8 2 1 1.98 1.04 1.10 o -7 2 1 20.73 18.80 0.85 o -6 2 1 9.42 8.11 1.58 o -5 2 1 1.40 3.19 0.52 o -4 2 1 297.39 288.55 2.32 o -3 2 1 0.72 0.34 0.10 o -2 2 1 306.84 299.65 1.66 o 0 2 1 33.19 31.43 0.39 o 2 2 1 1.56 3.79 0.28 o 3 2 1 301.16 341.34 3.14 o 4 2 1 0.12 -0.21 0.34 o 5 2 1 176.15 182.75 5.55 o 6 2 1 0.31 0.35 0.31 o 7 2 1 12.85 10.91 3.12 o -8 3 1 43.82 35.11 5.29 o -7 3 1 1.22 0.40 0.57 o -6 3 1 371.15 399.34 8.87 o -5 3 1 31.79 32.04 0.81 o -4 3 1 977.39 988.37 7.71 o -3 3 1 102.62 102.37 0.84 o -2 3 1 812.65 752.85 7.62 o 0 3 1 706.37 628.26 4.99 o 2 3 1 197.92 207.35 1.78 o 4 3 1 27.60 33.42 0.85 o 5 3 1 93.38 106.38 3.66 o 6 3 1 5.12 5.56 1.39 o 7 3 1 71.71 69.43 3.65 o -8 4 1 212.10 203.60 13.65 o -7 4 1 12.35 12.65 1.47 o -6 4 1 316.81 338.13 7.31 o -5 4 1 19.75 17.92 0.57 o -4 4 1 54.45 54.56 0.62 o -3 4 1 331.03 345.03 2.27 o -2 4 1 352.36 340.80 1.90 o -1 4 1 312.17 261.98 1.47 o 0 4 1 1329.96 1269.74 19.42 o 1 4 1 1660.67 1536.21 15.25 o 2 4 1 355.25 364.55 3.21 o 3 4 1 372.76 380.46 4.25 o 4 4 1 95.67 104.82 1.79 o 5 4 1 920.93 954.26 14.23 o 6 4 1 82.43 87.38 3.48 o 7 4 1 142.09 124.59 3.82 o -8 5 1 37.79 37.63 3.80 o -7 5 1 26.83 27.82 1.76 o -6 5 1 9.05 9.47 0.81 o -5 5 1 73.99 78.37 1.06 o -4 5 1 185.46 171.93 1.60 o -3 5 1 92.65 86.20 0.73 o -2 5 1 741.21 666.32 3.65 o -1 5 1 261.22 268.19 1.34 o 0 5 1 29.84 26.47 0.28 o 1 5 1 135.46 110.76 1.24 o 2 5 1 303.02 285.57 3.84 o 3 5 1 327.49 289.69 4.58 o 4 5 1 0.15 0.55 0.31 o 5 5 1 8.11 8.70 0.94 o 6 5 1 0.98 2.02 0.91 o 7 5 1 20.87 16.41 3.92 o 8 5 1 0.80 0.73 0.52 o -8 6 1 128.38 125.83 5.44 o -7 6 1 47.59 49.05 1.97 o -6 6 1 14.40 16.84 1.03 o -5 6 1 77.50 78.90 1.40 o -4 6 1 80.42 83.72 0.83 o -3 6 1 114.82 120.44 0.89 o -2 6 1 216.35 178.85 2.26 o -1 6 1 139.22 140.03 1.08 o 0 6 1 906.99 802.55 3.76 o 1 6 1 6.88 7.16 0.19 o 2 6 1 486.37 495.02 6.23 o 3 6 1 33.26 46.60 0.60 o 4 6 1 508.23 539.85 13.48 o 5 6 1 96.72 107.46 3.43 o 6 6 1 89.81 86.42 5.49 o 7 6 1 200.98 188.91 5.24 o -8 7 1 19.30 15.57 1.89 o -7 7 1 1.48 1.10 0.40 o -6 7 1 378.17 410.05 5.71 o -5 7 1 105.65 109.10 1.43 o -4 7 1 152.20 174.02 2.16 o -3 7 1 243.95 238.71 2.46 o -2 7 1 70.77 73.62 0.85 o -1 7 1 5.44 7.64 0.17 o 0 7 1 1760.92 1612.86 12.38 o 1 7 1 468.63 454.50 3.30 o 2 7 1 2197.37 2049.70 22.05 o 3 7 1 593.88 640.51 8.55 o 4 7 1 27.64 23.44 1.37 o 5 7 1 154.20 150.73 4.72 o 6 7 1 0.01 1.02 0.75 o 7 7 1 8.36 9.15 2.57 o -8 8 1 5.68 4.65 2.98 o -7 8 1 1.43 0.98 0.39 o -6 8 1 24.85 24.29 1.36 o -5 8 1 4.77 6.12 0.27 o -4 8 1 674.17 687.31 7.14 o -3 8 1 161.50 166.84 2.39 o -2 8 1 20.10 15.72 0.24 o -1 8 1 811.33 784.96 3.65 o 0 8 1 1792.54 1807.46 11.89 o 1 8 1 1294.62 1274.92 9.73 o 2 8 1 15.90 10.77 0.64 o 3 8 1 179.65 186.33 3.13 o 4 8 1 34.82 31.34 1.53 o 5 8 1 32.17 32.52 2.25 o 6 8 1 3.79 2.69 1.01 o 7 8 1 39.70 37.78 2.54 o -8 9 1 13.73 9.72 2.87 o -7 9 1 0.18 0.11 0.48 o -6 9 1 3.95 5.77 0.98 o -5 9 1 0.02 0.42 0.20 o -4 9 1 425.71 414.49 5.84 o -3 9 1 0.19 0.38 0.17 o -2 9 1 3835.51 3737.80 75.63 o -1 9 1 165.02 176.00 1.47 o 0 9 1 869.70 918.29 4.53 o 1 9 1 144.83 159.93 1.26 o 2 9 1 2.35 4.96 0.95 o 3 9 1 58.26 59.04 3.09 o 4 9 1 68.94 73.98 1.77 o 5 9 1 96.46 96.31 5.17 o 6 9 1 5.03 4.61 1.24 o 7 9 1 16.59 11.52 3.15 o -8 10 1 34.84 34.50 2.14 o -7 10 1 0.01 0.85 0.40 o -6 10 1 6.92 5.20 0.96 o -5 10 1 7.46 7.11 0.56 o -4 10 1 209.38 207.19 2.77 o -3 10 1 331.68 333.36 2.98 o -2 10 1 16.74 22.84 0.42 o -1 10 1 1483.41 1500.53 8.48 o 0 10 1 813.10 798.24 4.92 o 1 10 1 1090.33 1136.15 9.62 o 2 10 1 103.73 101.43 1.66 o 3 10 1 375.31 388.59 6.63 o 4 10 1 54.63 53.27 1.24 o 5 10 1 29.25 32.70 2.38 o 6 10 1 55.22 58.40 2.13 o 7 10 1 1.89 1.21 0.88 o -8 11 1 88.89 79.70 3.36 o -7 11 1 1.11 0.08 0.61 o -6 11 1 101.44 100.80 2.42 o -5 11 1 56.14 59.47 1.96 o -4 11 1 38.32 45.07 1.06 o -3 11 1 270.60 292.83 3.10 o -2 11 1 16.94 29.91 0.37 o -1 11 1 192.94 225.83 2.03 o 0 11 1 74.13 101.42 1.18 o 1 11 1 20.01 20.05 0.48 o 2 11 1 55.46 60.76 1.14 o 3 11 1 129.24 126.14 2.22 o 4 11 1 0.61 0.86 0.38 o 5 11 1 51.27 48.91 1.94 o 6 11 1 2.85 1.93 1.41 o 7 11 1 4.93 3.65 2.67 o -8 12 1 57.00 58.73 2.40 o -7 12 1 2.92 1.53 1.10 o -6 12 1 24.84 25.12 1.94 o -5 12 1 26.94 27.22 1.37 o -4 12 1 45.41 49.67 0.79 o -3 12 1 39.57 44.77 0.72 o -2 12 1 5.32 4.19 0.42 o -1 12 1 18.36 24.47 0.47 o 0 12 1 107.23 123.45 1.46 o 1 12 1 70.13 86.71 1.00 o 2 12 1 45.86 53.26 0.88 o 3 12 1 13.72 13.63 0.80 o 4 12 1 15.43 15.89 1.51 o 5 12 1 49.46 44.51 1.51 o 6 12 1 2.30 2.73 1.12 o 7 12 1 2.19 0.78 0.90 o -7 13 1 31.61 28.99 1.81 o -6 13 1 617.83 654.11 9.75 o -5 13 1 55.06 56.76 2.37 o -4 13 1 320.91 322.19 3.65 o -3 13 1 39.22 38.39 0.83 o -2 13 1 27.50 26.88 0.53 o -1 13 1 0.13 0.26 0.45 o 0 13 1 62.42 74.83 1.33 o 1 13 1 47.93 50.02 0.75 o 2 13 1 238.94 254.46 3.02 o 3 13 1 39.11 41.42 0.83 o 4 13 1 99.82 102.46 2.14 o 5 13 1 18.89 19.42 0.90 o 6 13 1 169.71 177.08 3.84 o 7 13 1 53.43 48.47 2.46 o -7 14 1 0.08 0.52 0.63 o -6 14 1 38.88 34.85 2.40 o -5 14 1 0.39 0.75 0.50 o -4 14 1 720.38 707.01 14.61 o -3 14 1 13.97 11.07 0.65 o -2 14 1 81.48 72.70 1.88 o -1 14 1 18.75 16.81 0.53 o 0 14 1 267.47 265.63 5.69 o 1 14 1 0.83 0.20 0.30 o 2 14 1 13.23 11.50 0.48 o 3 14 1 24.29 22.59 1.09 o 4 14 1 32.49 31.39 1.32 o 5 14 1 21.92 21.12 1.57 o 6 14 1 48.12 50.41 3.94 o -7 15 1 16.08 10.91 2.81 o -6 15 1 10.62 7.04 1.76 o -5 15 1 11.32 10.86 0.83 o -4 15 1 526.06 506.92 10.54 o -3 15 1 5.13 4.52 0.49 o -2 15 1 2135.98 2082.74 20.02 o -1 15 1 45.86 48.01 1.22 o 0 15 1 494.13 466.09 6.97 o 1 15 1 140.67 157.02 1.72 o 2 15 1 79.92 73.87 0.95 o 3 15 1 78.77 79.86 1.94 o 4 15 1 221.85 229.53 5.03 o 5 15 1 4.93 3.26 0.86 o 6 15 1 36.36 34.70 1.81 o -7 16 1 7.23 6.06 1.66 o -6 16 1 45.96 47.44 1.61 o -5 16 1 16.74 17.35 0.96 o -4 16 1 43.94 46.05 2.12 o -3 16 1 29.56 31.67 0.94 o -2 16 1 288.76 280.61 5.19 o -1 16 1 144.54 162.95 2.19 o 0 16 1 694.87 699.77 12.70 o 1 16 1 81.97 89.48 1.40 o 2 16 1 3.40 5.38 0.70 o 3 16 1 77.49 74.57 1.20 o 4 16 1 2.37 1.06 0.42 o 5 16 1 183.33 188.74 3.83 o 6 16 1 28.51 27.92 1.89 o -7 17 1 20.61 16.98 4.59 o -6 17 1 0.55 2.02 0.66 o -5 17 1 13.05 10.66 2.12 o -4 17 1 40.15 39.43 1.04 o -3 17 1 21.65 23.46 0.75 o -2 17 1 2.63 1.90 0.37 o -1 17 1 43.98 45.12 1.33 o 0 17 1 719.84 697.68 8.51 o 1 17 1 195.18 191.16 2.60 o 2 17 1 702.68 684.40 12.58 o 3 17 1 390.32 404.73 8.52 o 4 17 1 37.20 31.94 1.58 o 5 17 1 7.74 6.68 1.66 o 6 17 1 0.18 1.33 0.67 o -6 18 1 3.47 3.06 0.97 o -5 18 1 1.86 0.94 0.48 o -4 18 1 50.53 51.60 2.41 o -3 18 1 4.15 6.75 0.98 o -2 18 1 272.21 283.22 4.86 o -1 18 1 159.79 150.18 2.94 o 0 18 1 61.61 55.52 2.39 o 1 18 1 639.96 610.71 10.24 o 2 18 1 125.08 140.00 2.24 o 3 18 1 13.37 13.89 0.92 o 4 18 1 200.13 218.36 3.93 o 5 18 1 29.42 28.57 1.93 o 6 18 1 19.96 19.84 1.60 o -6 19 1 46.51 45.69 2.07 o -5 19 1 0.43 0.09 0.53 o -4 19 1 89.69 87.71 1.93 o -3 19 1 40.06 35.13 1.44 o -2 19 1 6.14 3.38 0.49 o -1 19 1 446.20 441.28 5.60 o 0 19 1 13.93 23.41 0.97 o 1 19 1 8.36 8.43 0.79 o 2 19 1 2.38 3.51 0.68 o 3 19 1 127.25 123.42 2.88 o 4 19 1 32.40 28.61 1.22 o 5 19 1 0.14 0.66 0.41 o -6 20 1 15.37 11.13 3.08 o -5 20 1 15.69 13.24 3.11 o -4 20 1 3.90 2.95 0.72 o -3 20 1 350.87 360.53 5.42 o -2 20 1 3.83 2.21 0.49 o -1 20 1 158.01 153.93 3.05 o 0 20 1 5.69 3.67 0.61 o 1 20 1 9.78 7.61 0.79 o 2 20 1 0.61 1.00 0.35 o 3 20 1 29.03 30.69 1.41 o 4 20 1 0.82 0.95 0.49 o 5 20 1 75.16 75.98 2.26 o -5 21 1 256.67 271.32 4.72 o -4 21 1 67.41 69.64 1.70 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