#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/47/2224728.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224728_Fobs loop_ _publ_author_name 'Brito, Iv\'an' 'Vallejos, Javier' 'L\'opez-Rodr\'iguez, Mat\'ias' 'C\'ardenas, Alejandro' _publ_section_title ; Ethane-1,2-diyl bis(pyridine-3-carboxylate) ; _journal_coeditor_code OM2303 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o114 _journal_volume 66 _journal_year 2010 _space_group_IT_number 18 _symmetry_space_group_name_Hall 'P 2 2ab' _symmetry_space_group_name_H-M 'P 21 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.0740 _cell_length_b 21.3404 _cell_length_c 7.3950 _exptl_crystal_F_000 283.95 _reflns_d_resolution_high 0.7681 _[local]_cod_data_source_file om2303Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ELE1 New: P21212' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 89.10 90.13 1.78 o 1 1 0 69.01 77.90 2.23 o 2 1 0 484.69 489.46 5.12 o 3 1 0 9.77 9.55 0.83 o 0 2 0 89.46 -0.17 0.17 o 1 2 0 1855.21 1763.08 15.62 o 2 2 0 1.66 5.09 1.28 o 3 2 0 9.85 9.59 0.82 o 1 3 0 2380.49 2201.51 19.38 o 2 3 0 23.38 24.33 0.69 o 3 3 0 0.46 1.24 0.74 o 4 3 0 11.24 14.22 2.42 o 0 4 0 4946.29 4740.75 70.04 o 1 4 0 1259.73 1205.96 14.02 o 2 4 0 34.06 39.69 1.24 o 3 4 0 0.42 1.21 1.08 o 5 4 0 15.13 3.83 3.34 o 1 5 0 77.17 85.14 1.26 o 2 5 0 6.55 5.52 0.38 o 3 5 0 24.77 24.34 1.30 o 5 5 0 4.31 0.31 3.21 o 1 6 0 165.95 157.16 2.12 o 2 6 0 4.91 5.72 0.41 o 3 6 0 0.82 3.07 1.22 o 1 7 0 498.98 492.95 9.06 o 2 7 0 299.71 311.10 3.67 o 3 7 0 68.69 71.04 2.33 o 4 7 0 2.87 5.39 2.36 o 0 8 0 557.88 552.00 13.18 o 1 8 0 63.15 69.77 1.43 o 2 8 0 64.92 69.80 2.44 o 3 8 0 22.36 23.32 1.41 o 4 8 0 0.09 0.89 2.63 o 1 9 0 894.23 853.13 22.95 o 2 9 0 10.67 9.29 0.76 o 3 9 0 3.78 4.80 1.10 o 4 9 0 0.75 1.57 3.07 o 1 10 0 35.81 60.73 5.26 o 2 10 0 161.82 165.57 3.19 o 3 10 0 11.17 14.00 1.38 o 4 10 0 8.35 13.10 3.77 o 1 11 0 858.57 910.86 14.25 o 2 11 0 72.22 72.15 1.92 o 3 11 0 20.44 23.48 2.53 o 4 11 0 0.28 3.24 3.14 o 0 12 0 188.98 204.97 4.18 o 1 12 0 91.67 87.05 2.62 o 2 12 0 21.02 22.61 1.08 o 3 12 0 16.36 17.75 2.25 o 4 12 0 1.33 3.83 3.18 o 1 13 0 5.74 6.68 1.12 o 2 13 0 18.07 18.39 3.10 o 3 13 0 10.96 11.09 2.13 o 4 13 0 5.35 2.19 3.28 o 1 14 0 140.52 146.29 4.10 o 2 14 0 30.20 31.55 2.79 o 3 14 0 10.33 12.73 2.23 o 1 15 0 67.72 67.85 3.47 o 2 15 0 0.00 1.65 1.15 o 3 15 0 0.65 3.08 1.74 o 4 15 0 12.25 12.02 4.14 o 0 16 0 40.82 45.59 2.76 o 1 16 0 48.99 60.27 3.72 o 2 16 0 68.99 66.74 3.28 o 3 16 0 15.44 12.85 2.99 o 4 16 0 0.00 1.44 3.76 o 1 17 0 60.11 61.18 3.93 o 2 17 0 147.18 149.86 7.06 o 3 17 0 82.77 76.19 6.58 o 4 17 0 0.03 8.11 4.86 o 1 18 0 39.52 37.83 2.24 o 2 18 0 106.05 115.51 5.08 o 3 18 0 3.30 5.92 3.92 o 4 18 0 0.04 7.20 4.46 o 1 19 0 56.45 62.80 3.60 o 2 19 0 0.71 3.09 1.80 o 3 19 0 21.93 15.48 4.69 o 0 20 0 176.72 183.15 12.50 o 1 20 0 2.00 3.90 1.71 o 2 20 0 1.64 3.97 3.67 o 3 20 0 19.46 20.10 5.14 o 1 21 0 36.97 38.88 3.14 o 2 21 0 232.31 219.54 25.29 o 3 21 0 4.39 8.41 5.80 o 0 22 0 3.58 3.35 2.68 o 1 22 0 0.15 4.35 3.26 o 2 22 0 12.04 21.17 4.63 o 3 22 0 0.19 4.09 4.33 o 1 23 0 7.21 6.19 2.21 o 2 23 0 3.62 9.93 4.05 o 0 24 0 6.28 17.82 4.84 o 1 24 0 7.67 8.27 4.46 o 2 24 0 1.77 -1.08 2.32 o 1 25 0 0.11 4.18 2.35 o 2 25 0 8.67 3.92 2.19 o 0 26 0 8.68 25.33 13.42 o 1 26 0 5.72 4.94 2.37 o 1 27 0 14.20 14.99 3.86 o 1 0 1 9746.98 9396.88 154.87 o 2 0 1 134.51 135.88 1.54 o 3 0 1 34.44 36.54 1.25 o 4 0 1 0.24 3.35 1.99 o 0 1 1 1.18 0.81 0.08 o 1 1 1 1459.60 1436.74 12.76 o 2 1 1 54.85 60.88 1.19 o 3 1 1 65.78 65.89 1.10 o 4 1 1 29.63 32.29 3.19 o 0 2 1 288.16 200.50 38.67 o 1 2 1 3927.51 3815.71 22.49 o 2 2 1 632.29 610.74 4.42 o 3 2 1 32.67 34.80 1.19 o 4 2 1 7.56 6.29 2.11 o 0 3 1 2295.02 2020.11 25.17 o 1 3 1 169.06 152.15 1.58 o 2 3 1 230.17 225.68 2.00 o 3 3 1 34.83 35.16 1.58 o 5 3 1 1.86 0.00 0.34 o 0 4 1 51.99 48.36 0.87 o 1 4 1 208.38 215.10 2.35 o 2 4 1 211.45 207.00 2.20 o 3 4 1 78.88 81.56 1.62 o 5 4 1 2.73 0.17 2.45 o 0 5 1 31.70 30.43 1.20 o 1 5 1 269.15 263.53 2.50 o 2 5 1 156.00 157.12 1.33 o 3 5 1 19.27 18.01 0.77 o 5 5 1 8.66 5.50 2.85 o 0 6 1 30.13 35.64 0.81 o 1 6 1 75.08 81.35 0.88 o 2 6 1 340.41 355.00 2.63 o 3 6 1 3.78 4.81 0.63 o 4 6 1 5.63 5.92 2.36 o 0 7 1 911.32 882.92 14.12 o 1 7 1 158.74 172.36 2.64 o 2 7 1 116.59 119.93 1.60 o 3 7 1 28.81 29.18 1.09 o 4 7 1 1.28 4.78 2.61 o 0 8 1 2.77 1.44 0.56 o 1 8 1 377.48 382.40 3.51 o 2 8 1 89.00 88.96 1.33 o 3 8 1 8.93 9.85 1.24 o 4 8 1 3.24 5.39 2.82 o 0 9 1 1171.67 1111.58 14.42 o 1 9 1 61.19 60.70 0.84 o 2 9 1 8.95 9.09 0.75 o 3 9 1 57.95 58.70 3.52 o 4 9 1 8.29 9.79 2.30 o 0 10 1 577.07 536.20 6.51 o 1 10 1 17.10 23.09 1.28 o 2 10 1 21.62 24.24 1.01 o 3 10 1 18.22 16.70 1.34 o 4 10 1 9.70 10.67 1.77 o 0 11 1 809.79 888.77 10.47 o 1 11 1 22.26 22.82 0.74 o 2 11 1 131.81 140.20 3.02 o 3 11 1 7.44 7.32 2.07 o 4 11 1 13.20 12.47 2.09 o 0 12 1 507.37 554.34 6.81 o 1 12 1 123.30 119.74 2.43 o 2 12 1 70.15 70.95 2.95 o 3 12 1 1.95 3.90 1.28 o 4 12 1 1.68 2.21 1.59 o 0 13 1 19.25 25.75 0.97 o 1 13 1 48.58 52.64 1.41 o 2 13 1 6.77 6.85 0.69 o 3 13 1 0.99 3.58 1.33 o 4 13 1 2.85 2.39 1.61 o 0 14 1 0.67 1.01 0.70 o 1 14 1 79.97 83.52 1.98 o 2 14 1 20.10 21.76 0.85 o 3 14 1 46.75 49.32 2.40 o 4 14 1 5.39 2.05 1.47 o 0 15 1 204.33 190.34 4.24 o 1 15 1 85.58 78.96 3.95 o 2 15 1 63.93 67.06 1.76 o 3 15 1 6.71 4.59 1.99 o 4 15 1 16.91 8.66 3.95 o 0 16 1 354.83 363.71 11.43 o 1 16 1 60.64 63.67 3.82 o 2 16 1 5.15 4.78 1.26 o 3 16 1 12.07 12.95 1.69 o 4 16 1 6.25 7.29 4.37 o 0 17 1 51.10 45.95 2.30 o 1 17 1 57.54 58.20 3.75 o 2 17 1 29.81 33.04 1.61 o 3 17 1 20.63 18.26 2.22 o 4 17 1 9.86 5.13 3.35 o 0 18 1 59.36 76.09 3.24 o 1 18 1 84.80 90.85 2.96 o 2 18 1 43.64 43.19 2.23 o 3 18 1 13.24 10.55 1.62 o 4 18 1 0.25 4.23 3.92 o 0 19 1 112.16 128.05 4.86 o 1 19 1 144.63 140.74 4.83 o 2 19 1 21.61 20.41 1.48 o 3 19 1 23.73 23.82 3.57 o 0 20 1 12.25 15.40 1.92 o 1 20 1 63.96 64.74 2.44 o 2 20 1 10.38 10.94 1.80 o 3 20 1 2.55 4.30 2.95 o 0 21 1 26.14 22.40 2.26 o 1 21 1 99.58 95.75 4.43 o 2 21 1 19.99 21.60 2.71 o 3 21 1 17.84 22.74 4.57 o 0 22 1 0.00 2.49 1.98 o 1 22 1 10.45 12.90 1.61 o 2 22 1 1.05 3.59 2.07 o 3 22 1 2.31 3.61 2.99 o 0 23 1 18.55 17.79 2.75 o 1 23 1 13.02 9.00 1.66 o 2 23 1 3.35 3.94 1.87 o 0 24 1 0.41 0.43 2.25 o 1 24 1 5.57 6.85 1.96 o 2 24 1 5.01 1.76 1.72 o 0 25 1 0.20 6.91 3.08 o 1 25 1 6.37 6.55 1.66 o 2 25 1 1.76 1.47 1.72 o 0 26 1 2.03 5.19 3.39 o 1 26 1 16.48 16.60 2.37 o 0 27 1 23.50 27.71 9.22 o 1 27 1 2.35 3.08 2.40 o 0 0 2 23.44 24.63 0.52 o 1 0 2 434.59 457.62 4.16 o 2 0 2 331.12 321.38 4.93 o 3 0 2 22.36 25.46 1.82 o 0 1 2 2292.73 2267.35 40.46 o 1 1 2 52.06 55.52 0.50 o 2 1 2 109.58 122.68 3.41 o 3 1 2 162.54 162.07 2.64 o 0 2 2 0.03 2.31 0.44 o 1 2 2 26.27 26.50 0.50 o 2 2 2 1194.00 1211.09 7.57 o 3 2 2 140.72 138.77 2.32 o 0 3 2 125.12 113.95 1.24 o 1 3 2 301.66 283.15 2.14 o 2 3 2 486.36 490.23 3.48 o 3 3 2 58.73 57.79 1.52 o 5 3 2 2.89 0.63 4.57 o 0 4 2 840.52 786.89 13.27 o 1 4 2 168.81 167.74 1.67 o 2 4 2 96.71 93.73 1.23 o 3 4 2 78.06 76.93 2.38 o 5 4 2 1.50 1.18 1.86 o 0 5 2 152.17 148.38 1.96 o 1 5 2 48.35 49.07 0.97 o 2 5 2 78.71 76.10 0.96 o 3 5 2 28.06 27.03 0.93 o 5 5 2 6.80 0.31 3.63 o 0 6 2 52.37 65.66 1.33 o 1 6 2 569.67 574.09 6.48 o 2 6 2 18.46 22.55 0.47 o 3 6 2 54.00 51.19 2.33 o 4 6 2 12.85 11.54 3.06 o 5 6 2 4.41 5.80 3.83 o 0 7 2 61.68 78.08 1.12 o 1 7 2 381.12 379.32 3.51 o 2 7 2 31.16 32.98 0.74 o 3 7 2 40.89 45.99 1.28 o 4 7 2 16.94 20.63 3.66 o 0 8 2 237.07 251.36 2.93 o 1 8 2 49.12 54.89 0.87 o 2 8 2 67.71 66.33 1.52 o 3 8 2 41.35 45.57 6.51 o 4 8 2 9.90 5.19 1.70 o 0 9 2 232.51 242.29 2.88 o 1 9 2 14.45 14.53 0.65 o 2 9 2 23.71 27.33 0.72 o 3 9 2 16.83 19.53 1.64 o 4 9 2 23.66 26.73 3.17 o 0 10 2 55.86 61.47 1.13 o 1 10 2 450.91 441.57 5.18 o 2 10 2 20.57 21.69 0.84 o 3 10 2 33.57 32.66 1.46 o 4 10 2 26.33 24.35 3.05 o 0 11 2 4.87 3.89 0.86 o 1 11 2 184.36 201.86 2.73 o 2 11 2 34.92 34.63 1.03 o 3 11 2 57.12 61.01 2.48 o 4 11 2 12.11 7.77 2.44 o 0 12 2 0.43 0.78 0.89 o 1 12 2 43.92 54.78 1.41 o 2 12 2 104.79 97.66 3.50 o 3 12 2 13.70 12.66 1.28 o 4 12 2 8.54 7.79 3.06 o 0 13 2 120.26 119.44 4.54 o 1 13 2 2.69 3.31 0.81 o 2 13 2 25.46 25.62 1.44 o 3 13 2 59.57 64.47 2.42 o 4 13 2 6.02 8.94 2.36 o 0 14 2 3.71 2.73 0.74 o 1 14 2 315.11 303.36 6.29 o 2 14 2 48.74 54.63 5.57 o 3 14 2 8.68 9.69 1.59 o 4 14 2 8.80 6.42 2.53 o 0 15 2 160.43 147.58 5.36 o 1 15 2 184.11 176.62 4.83 o 2 15 2 36.79 31.55 1.66 o 3 15 2 12.55 14.18 2.32 o 4 15 2 5.10 1.89 1.65 o 0 16 2 50.52 48.22 2.32 o 1 16 2 110.02 110.85 5.79 o 2 16 2 10.02 7.37 1.62 o 3 16 2 7.71 6.98 1.96 o 4 16 2 2.45 2.72 2.00 o 0 17 2 43.71 58.18 2.68 o 1 17 2 83.27 83.24 3.35 o 2 17 2 32.66 35.21 2.88 o 3 17 2 7.46 9.05 2.34 o 4 17 2 3.12 4.04 4.00 o 0 18 2 340.23 354.39 11.44 o 1 18 2 20.68 21.25 1.40 o 2 18 2 10.80 12.17 1.68 o 3 18 2 20.96 21.63 2.61 o 0 19 2 409.33 410.69 18.59 o 1 19 2 24.18 23.13 2.24 o 2 19 2 0.09 1.91 1.53 o 3 19 2 1.21 1.43 1.83 o 0 20 2 4.90 9.67 1.84 o 1 20 2 36.18 35.86 2.09 o 2 20 2 8.14 9.83 1.78 o 3 20 2 3.03 1.94 1.83 o 0 21 2 0.07 2.16 1.79 o 1 21 2 22.96 21.12 1.89 o 2 21 2 1.96 0.86 1.76 o 3 21 2 0.64 -0.14 2.66 o 0 22 2 14.00 14.62 3.46 o 1 22 2 1.66 3.23 1.39 o 2 22 2 7.65 9.57 2.26 o 3 22 2 2.41 0.51 2.61 o 0 23 2 37.59 35.72 4.79 o 1 23 2 2.68 3.86 1.46 o 2 23 2 7.77 8.37 2.27 o 0 24 2 16.41 23.94 4.43 o 1 24 2 3.76 3.76 1.46 o 2 24 2 1.69 2.29 1.56 o 0 25 2 9.91 6.48 2.81 o 1 25 2 3.47 3.46 1.71 o 2 25 2 3.09 0.94 2.05 o 0 26 2 5.84 7.90 3.11 o 1 26 2 7.34 6.27 2.14 o 0 27 2 2.69 2.66 3.15 o 1 0 3 333.46 344.75 3.69 o 2 0 3 198.84 214.08 2.96 o 3 0 3 149.98 145.57 3.57 o 0 1 3 17.12 16.98 0.86 o 1 1 3 306.71 315.38 2.07 o 2 1 3 266.19 276.13 2.64 o 3 1 3 19.86 20.35 1.20 o 5 1 3 0.85 -0.38 1.92 o 0 2 3 112.71 108.52 1.71 o 1 2 3 70.43 80.14 1.05 o 2 2 3 8.19 10.12 0.40 o 3 2 3 74.05 70.96 1.67 o 5 2 3 0.25 -2.02 2.02 o 0 3 3 33.22 37.42 0.89 o 1 3 3 690.03 704.66 4.90 o 2 3 3 43.33 45.87 0.86 o 3 3 3 22.61 26.35 1.80 o 4 3 3 27.72 28.30 4.35 o 5 3 3 4.32 1.13 2.68 o 0 4 3 498.35 550.77 5.24 o 1 4 3 751.17 804.54 6.45 o 2 4 3 6.38 6.26 0.35 o 3 4 3 42.69 40.99 1.74 o 4 4 3 54.68 52.38 6.94 o 0 5 3 32.35 29.10 0.47 o 1 5 3 148.65 160.57 1.62 o 2 5 3 91.90 85.53 1.09 o 3 5 3 52.35 49.36 1.85 o 4 5 3 0.03 1.44 2.83 o 0 6 3 1145.88 1167.94 9.96 o 1 6 3 4.15 2.73 0.30 o 2 6 3 13.84 14.01 0.44 o 3 6 3 11.28 11.57 1.52 o 4 6 3 3.18 5.65 1.74 o 0 7 3 255.38 282.41 8.91 o 1 7 3 16.56 18.18 0.39 o 2 7 3 34.85 34.17 0.74 o 3 7 3 40.93 42.52 1.31 o 4 7 3 25.97 21.94 2.80 o 0 8 3 19.98 26.70 0.60 o 1 8 3 25.92 30.91 0.70 o 2 8 3 55.44 55.60 1.21 o 3 8 3 1.25 1.09 0.73 o 4 8 3 49.14 48.58 6.13 o 0 9 3 166.44 182.37 3.31 o 1 9 3 10.74 11.16 0.53 o 2 9 3 22.75 26.32 1.67 o 3 9 3 27.70 29.48 2.60 o 4 9 3 4.67 8.24 1.90 o 0 10 3 307.49 328.16 6.24 o 1 10 3 9.18 9.34 0.61 o 2 10 3 67.30 64.70 1.47 o 3 10 3 97.50 97.38 3.38 o 4 10 3 20.16 22.11 3.37 o 0 11 3 0.51 0.47 0.42 o 1 11 3 63.97 66.09 1.27 o 2 11 3 199.70 200.93 4.72 o 3 11 3 80.13 92.94 3.13 o 4 11 3 1.59 3.45 1.88 o 0 12 3 77.26 75.38 1.51 o 1 12 3 7.37 6.92 0.68 o 2 12 3 57.15 53.99 1.74 o 3 12 3 50.61 54.44 3.10 o 4 12 3 2.45 4.81 3.00 o 0 13 3 8.96 10.59 0.67 o 1 13 3 68.97 65.23 1.68 o 2 13 3 193.10 186.20 5.24 o 3 13 3 20.17 17.95 2.67 o 4 13 3 0.97 0.17 2.28 o 0 14 3 1.99 4.53 0.90 o 1 14 3 4.09 4.32 0.82 o 2 14 3 205.32 206.20 5.75 o 3 14 3 15.99 16.69 2.16 o 4 14 3 7.09 6.50 2.05 o 0 15 3 64.87 68.23 3.33 o 1 15 3 39.82 35.84 2.61 o 2 15 3 109.76 114.90 4.67 o 3 15 3 19.60 16.05 2.12 o 4 15 3 7.13 6.56 2.18 o 0 16 3 33.58 34.33 1.29 o 1 16 3 67.00 66.83 3.80 o 2 16 3 31.58 38.21 2.09 o 3 16 3 12.83 11.80 2.57 o 4 16 3 1.17 4.58 4.91 o 0 17 3 90.45 86.44 2.75 o 1 17 3 118.49 117.58 3.97 o 2 17 3 56.80 53.81 3.21 o 3 17 3 13.90 11.90 2.42 o 0 18 3 27.28 28.45 6.04 o 1 18 3 70.99 68.23 4.52 o 2 18 3 17.42 13.47 1.79 o 3 18 3 4.63 5.65 3.02 o 0 19 3 31.03 36.87 2.46 o 1 19 3 22.59 22.50 2.39 o 2 19 3 5.34 5.46 1.65 o 3 19 3 8.50 10.23 3.57 o 0 20 3 1.02 3.87 2.41 o 1 20 3 28.98 34.21 2.45 o 2 20 3 16.88 19.92 2.43 o 3 20 3 0.28 -0.32 1.97 o 0 21 3 1.92 2.73 1.83 o 1 21 3 31.96 28.37 2.60 o 2 21 3 2.27 3.44 1.89 o 3 21 3 5.93 2.67 1.87 o 0 22 3 6.52 6.57 2.12 o 1 22 3 1.64 2.64 1.43 o 2 22 3 1.64 2.97 1.82 o 0 23 3 0.88 4.43 2.27 o 1 23 3 0.99 2.55 1.45 o 2 23 3 0.02 0.76 1.34 o 0 24 3 13.63 8.94 2.76 o 1 24 3 9.47 4.54 2.15 o 2 24 3 3.92 0.93 2.02 o 0 25 3 2.23 3.20 4.73 o 1 25 3 7.34 2.33 1.70 o 0 26 3 10.36 7.58 4.06 o 0 0 4 83.02 88.25 2.31 o 1 0 4 132.65 135.60 1.68 o 2 0 4 0.00 1.40 0.73 o 3 0 4 132.28 138.82 16.55 o 0 1 4 495.26 510.21 5.23 o 1 1 4 38.29 46.18 0.54 o 2 1 4 24.12 22.92 0.69 o 3 1 4 7.93 10.49 0.83 o 4 1 4 3.74 4.21 3.05 o 0 2 4 442.30 458.63 6.09 o 1 2 4 35.61 31.28 0.91 o 2 2 4 114.39 114.81 1.43 o 3 2 4 28.61 30.64 2.04 o 4 2 4 11.93 14.89 4.06 o 0 3 4 17.00 19.89 0.84 o 1 3 4 56.59 55.61 0.93 o 2 3 4 43.13 50.42 1.34 o 3 3 4 47.41 44.11 1.82 o 4 3 4 19.53 19.63 4.23 o 0 4 4 89.62 110.39 2.06 o 1 4 4 152.68 157.86 1.72 o 2 4 4 275.03 268.27 2.86 o 3 4 4 33.51 32.54 2.21 o 4 4 4 1.04 4.91 2.50 o 0 5 4 306.44 317.59 6.36 o 1 5 4 253.53 258.85 2.70 o 2 5 4 37.48 38.38 0.78 o 3 5 4 20.85 22.13 2.30 o 4 5 4 3.22 2.85 1.78 o 0 6 4 182.50 193.92 3.83 o 1 6 4 97.23 100.69 1.13 o 2 6 4 6.48 6.50 0.46 o 3 6 4 64.30 67.96 2.26 o 4 6 4 3.28 5.43 1.80 o 0 7 4 15.12 15.02 0.59 o 1 7 4 14.12 13.41 0.36 o 2 7 4 15.77 17.91 1.04 o 3 7 4 26.05 27.98 1.42 o 4 7 4 11.62 9.33 2.16 o 0 8 4 1.61 3.55 0.46 o 1 8 4 198.69 194.05 2.51 o 2 8 4 1.65 2.30 0.70 o 3 8 4 66.46 67.75 5.69 o 4 8 4 11.25 10.33 2.27 o 0 9 4 11.61 13.00 0.61 o 1 9 4 57.08 54.98 0.97 o 2 9 4 73.96 74.08 2.03 o 3 9 4 31.51 31.89 1.68 o 4 9 4 12.56 11.22 2.14 o 0 10 4 11.02 12.01 0.56 o 1 10 4 3.74 4.38 0.54 o 2 10 4 24.95 24.57 0.93 o 3 10 4 37.01 41.03 2.22 o 4 10 4 3.27 2.30 3.42 o 0 11 4 0.04 0.70 0.51 o 1 11 4 100.63 93.40 3.16 o 2 11 4 125.82 126.08 4.02 o 3 11 4 5.21 9.48 1.70 o 4 11 4 13.04 9.17 2.73 o 0 12 4 0.82 1.46 0.56 o 1 12 4 99.41 97.93 2.09 o 2 12 4 11.89 14.41 2.15 o 3 12 4 47.05 46.71 3.62 o 4 12 4 19.46 15.34 2.73 o 0 13 4 68.15 71.86 2.00 o 1 13 4 340.53 307.99 9.28 o 2 13 4 26.61 25.44 2.12 o 3 13 4 11.52 11.55 1.96 o 4 13 4 2.35 2.75 1.96 o 0 14 4 49.12 46.38 2.47 o 1 14 4 27.58 29.77 1.12 o 2 14 4 2.18 2.69 1.28 o 3 14 4 22.99 23.43 2.99 o 4 14 4 10.47 3.49 2.05 o 0 15 4 1.48 2.44 0.80 o 1 15 4 196.51 179.89 5.24 o 2 15 4 27.52 30.44 2.17 o 3 15 4 22.49 20.42 2.54 o 0 16 4 31.38 33.47 1.51 o 1 16 4 29.49 28.10 2.68 o 2 16 4 54.53 52.96 3.92 o 3 16 4 18.53 16.73 2.88 o 0 17 4 165.82 158.93 5.34 o 1 17 4 7.99 7.14 1.18 o 2 17 4 26.89 21.39 2.20 o 3 17 4 13.77 12.97 4.27 o 0 18 4 0.04 -0.92 1.53 o 1 18 4 18.82 21.68 1.86 o 2 18 4 2.61 1.90 1.33 o 3 18 4 1.73 2.62 2.56 o 0 19 4 14.32 16.56 2.27 o 1 19 4 46.08 46.77 3.05 o 2 19 4 16.50 17.24 2.22 o 3 19 4 1.83 2.53 2.18 o 0 20 4 12.68 14.67 4.23 o 1 20 4 2.51 2.11 1.31 o 2 20 4 5.25 4.55 1.54 o 0 21 4 10.22 12.74 2.85 o 1 21 4 6.34 5.51 1.45 o 2 21 4 16.78 12.04 3.40 o 0 22 4 0.00 0.97 2.11 o 1 22 4 2.52 3.82 1.56 o 2 22 4 2.50 2.21 1.64 o 0 23 4 5.56 5.99 2.26 o 1 23 4 1.88 3.19 2.08 o 2 23 4 1.20 1.33 3.76 o 0 24 4 3.50 8.02 4.07 o 1 24 4 9.73 4.88 2.16 o 0 25 4 10.01 2.15 2.62 o 0 0 5 7.99 6.83 0.89 o 1 0 5 30.53 34.14 0.84 o 2 0 5 36.27 36.64 1.12 o 3 0 5 2.42 2.32 1.59 o 4 0 5 27.09 23.66 5.23 o 0 1 5 54.83 54.45 1.37 o 1 1 5 16.10 15.09 0.75 o 2 1 5 16.11 14.89 0.67 o 3 1 5 3.30 5.13 1.27 o 4 1 5 1.89 3.99 1.78 o 0 2 5 3.54 4.14 0.38 o 1 2 5 340.33 335.13 3.50 o 2 2 5 31.60 28.03 0.67 o 3 2 5 6.77 5.59 1.08 o 4 2 5 4.12 6.05 2.02 o 0 3 5 67.93 63.07 3.76 o 1 3 5 134.79 126.58 1.48 o 2 3 5 26.78 23.22 0.62 o 3 3 5 50.01 52.48 3.71 o 4 3 5 2.02 2.80 3.89 o 0 4 5 0.61 1.33 0.55 o 1 4 5 78.54 80.52 0.97 o 2 4 5 131.58 129.05 2.10 o 3 4 5 7.29 9.09 1.23 o 4 4 5 2.44 3.98 1.70 o 0 5 5 80.81 84.26 2.21 o 1 5 5 3.88 5.64 0.49 o 2 5 5 153.20 146.63 2.90 o 3 5 5 1.16 4.00 2.49 o 4 5 5 8.65 8.69 3.06 o 0 6 5 0.92 2.66 0.73 o 1 6 5 194.70 191.86 2.81 o 2 6 5 120.90 114.20 2.05 o 3 6 5 15.01 14.35 1.28 o 4 6 5 0.48 0.98 1.67 o 0 7 5 99.97 102.08 5.91 o 1 7 5 16.42 16.78 0.58 o 2 7 5 60.36 62.98 1.44 o 3 7 5 3.58 5.26 1.18 o 4 7 5 1.13 1.85 1.63 o 0 8 5 7.40 8.52 1.16 o 1 8 5 0.47 1.94 0.35 o 2 8 5 131.34 129.20 4.70 o 3 8 5 17.61 16.45 1.57 o 4 8 5 0.58 4.72 2.05 o 0 9 5 20.29 25.28 2.00 o 1 9 5 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