#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:26:56 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181168 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/47/2224730.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224730_Fobs loop_ _publ_author_name 'Brewer, Greg' 'Butcher, Ray J.' 'Jasinski, Jerry P.' _publ_section_title ; Tris(ethane-1,2-diamine-\k^2^N,N')nickel(II) diiodide ; _journal_coeditor_code PB2013 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m103 _journal_page_last m104 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.7502 _cell_length_b 13.4881 _cell_length_c 15.9624 _exptl_crystal_F_000 1888.00 _reflns_d_resolution_high 0.6610 _cod_data_source_file pb2013Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I' _shelx_refln_list_code 4 _shelx_f_calc_maximum 935.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 743847.31 753650.69 4974.71 o 12 0 0 7778.36 9698.79 367.44 o 14 0 0 1923.10 2509.05 400.10 o 16 0 0 3410.19 4169.94 502.46 o 18 0 0 30.44 292.22 650.84 o 20 0 0 281.82 694.78 842.94 o 4 1 0 1331.40 1517.11 91.50 o 6 1 0 19495.49 20588.66 281.14 o 8 1 0 2746.76 2917.00 99.16 o 10 1 0 26188.98 28873.08 498.21 o 12 1 0 38151.50 43857.89 640.18 o 14 1 0 5224.41 5529.09 285.14 o 16 1 0 33902.46 39731.03 1037.93 o 18 1 0 699.82 539.92 460.24 o 20 1 0 5729.00 6820.32 600.19 o 4 2 0 10480.07 10470.34 103.05 o 6 2 0 118003.20 126743.55 385.33 o 8 2 0 57170.09 61061.81 381.68 o 10 2 0 17510.99 20757.28 415.82 o 12 2 0 15024.96 15702.46 870.01 o 14 2 0 29.46 325.56 282.36 o 16 2 0 10.94 204.90 361.14 o 18 2 0 12.98 -79.86 347.93 o 20 2 0 816.23 1073.08 594.48 o 2 3 0 5140.30 5360.93 88.54 o 4 3 0 154075.72 155923.17 520.08 o 6 3 0 21668.18 23720.91 179.45 o 8 3 0 123916.96 132104.92 1411.99 o 10 3 0 33589.22 35692.11 506.16 o 12 3 0 24881.19 28432.29 1349.21 o 14 3 0 3980.41 3683.10 290.39 o 16 3 0 3098.42 3648.14 351.18 o 18 3 0 252.36 491.72 465.66 o 20 3 0 2615.11 3078.04 597.47 o 0 4 0 91530.34 97304.06 566.37 o 2 4 0 8637.23 9045.56 101.82 o 4 4 0 40315.95 41355.02 204.04 o 6 4 0 6902.99 7080.30 66.35 o 8 4 0 95652.93 97707.76 519.99 o 10 4 0 16155.07 16119.16 238.88 o 12 4 0 22619.89 23528.51 1067.93 o 14 4 0 22906.32 26261.76 1509.33 o 16 4 0 138.28 301.81 367.65 o 18 4 0 9992.83 11342.41 470.67 o 20 4 0 2251.16 2232.19 603.02 o 2 5 0 401174.13 414172.94 4506.52 o 4 5 0 53726.37 56297.16 681.89 o 6 5 0 130239.95 130211.84 536.11 o 8 5 0 9615.67 9866.67 104.82 o 10 5 0 5077.99 5294.90 136.44 o 12 5 0 8.41 252.71 127.50 o 14 5 0 784.70 1241.28 290.52 o 16 5 0 283.37 302.92 370.76 o 18 5 0 839.95 1126.82 466.13 o 20 5 0 314.26 385.98 614.39 o 0 6 0 91118.95 96053.17 429.01 o 2 6 0 4877.39 5110.19 62.57 o 4 6 0 47612.81 49588.37 539.97 o 6 6 0 33.86 300.55 52.28 o 8 6 0 1220.68 1166.95 71.45 o 10 6 0 12113.91 13214.99 274.08 o 12 6 0 1019.84 1106.52 190.33 o 14 6 0 18979.63 21783.47 1229.70 o 16 6 0 839.66 790.85 382.31 o 18 6 0 5282.42 5925.37 613.80 o 20 6 0 2163.93 1818.32 626.84 o 2 7 0 5517.13 5289.95 84.23 o 4 7 0 13227.11 12255.76 106.09 o 6 7 0 22399.63 22246.04 133.85 o 8 7 0 199.57 197.37 79.95 o 10 7 0 24551.16 24825.57 530.42 o 12 7 0 5592.74 5531.35 183.12 o 14 7 0 3161.97 3478.86 309.08 o 16 7 0 3726.94 3098.78 417.10 o 18 7 0 553.70 599.85 481.67 o 20 7 0 526.23 469.99 813.63 o 0 8 0 13111.00 13677.26 370.43 o 2 8 0 16455.26 16919.46 290.95 o 4 8 0 373.78 368.37 98.11 o 6 8 0 51392.57 51276.24 773.09 o 8 8 0 1439.90 1547.40 83.65 o 10 8 0 32663.80 33782.16 270.28 o 12 8 0 4798.26 4985.81 433.86 o 14 8 0 6827.14 7597.61 585.28 o 16 8 0 60.14 497.23 379.54 o 18 8 0 3339.86 3987.67 650.33 o 2 9 0 35179.70 38018.57 420.04 o 4 9 0 2183.71 1990.37 92.04 o 6 9 0 58642.06 61985.66 1534.41 o 8 9 0 597.31 832.21 120.83 o 10 9 0 32334.10 33146.77 1337.82 o 12 9 0 11479.99 11774.50 409.61 o 14 9 0 3488.61 3582.58 438.75 o 16 9 0 5906.24 6518.23 412.23 o 18 9 0 502.88 410.43 859.26 o 0 10 0 71457.84 74545.57 463.75 o 2 10 0 226.91 275.30 61.39 o 4 10 0 38797.44 39523.63 273.57 o 6 10 0 3799.68 3701.53 190.55 o 8 10 0 3337.77 3268.06 130.77 o 10 10 0 0.61 190.30 146.15 o 12 10 0 13.45 46.37 194.73 o 14 10 0 897.71 1139.41 369.00 o 16 10 0 116.68 204.05 672.47 o 18 10 0 327.19 466.66 863.56 o 2 11 0 57573.03 66436.27 717.96 o 4 11 0 1565.09 1693.92 104.65 o 6 11 0 9403.40 9725.49 158.17 o 8 11 0 16.56 -87.13 148.08 o 10 11 0 569.61 573.33 216.69 o 12 11 0 3806.61 3820.79 429.73 o 14 11 0 778.32 988.26 397.68 o 16 11 0 2407.68 3042.58 707.00 o 18 11 0 850.71 1157.89 922.96 o 0 12 0 3101.74 3445.55 209.57 o 2 12 0 11.74 73.83 88.86 o 4 12 0 4268.42 4180.68 111.52 o 6 12 0 380.53 65.08 88.06 o 8 12 0 10714.92 11109.33 178.82 o 10 12 0 1217.93 1026.53 229.32 o 12 12 0 2145.04 2291.50 334.70 o 14 12 0 4752.99 4513.36 424.97 o 16 12 0 6.05 33.06 773.47 o 18 12 0 2311.52 3172.03 943.78 o 2 13 0 601.57 484.70 125.33 o 4 13 0 15436.31 15565.73 350.01 o 6 13 0 1807.94 3029.47 244.23 o 8 13 0 18539.30 18039.31 350.45 o 10 13 0 2182.54 1860.16 216.02 o 12 13 0 6119.83 6168.79 407.63 o 14 13 0 29.05 123.79 413.48 o 0 14 0 5774.69 5868.19 214.01 o 2 14 0 1168.28 1012.66 157.07 o 4 14 0 11328.54 11570.10 327.04 o 6 14 0 1601.50 1525.06 223.23 o 8 14 0 12105.14 12339.42 283.93 o 10 14 0 224.20 83.96 144.94 o 12 14 0 3639.74 3346.32 546.14 o 14 14 0 1118.76 1091.63 647.00 o 2 15 0 6214.55 6122.03 172.55 o 4 15 0 527.33 644.20 221.21 o 6 15 0 128.88 403.08 247.39 o 8 15 0 16.19 57.46 143.17 o 10 15 0 590.58 804.37 319.78 o 12 15 0 1092.35 1204.13 442.17 o 0 16 0 40145.20 47136.38 1115.09 o 2 16 0 429.44 387.36 222.68 o 4 16 0 19518.87 20483.71 337.62 o 6 16 0 229.19 200.45 267.03 o 8 16 0 3381.28 3695.35 301.51 o 10 16 0 231.06 355.64 352.70 o 12 16 0 191.28 479.09 500.02 o 2 17 0 547.73 616.41 250.96 o 4 17 0 103.70 248.60 223.68 o 6 17 0 117.32 -32.34 212.00 o 8 17 0 285.87 270.11 333.09 o 10 17 0 963.54 1106.11 381.74 o 12 17 0 2375.02 2832.28 818.52 o 0 18 0 211.35 -83.84 573.04 o 2 18 0 1222.02 1230.36 392.11 o 4 18 0 2.73 69.11 513.52 o 6 18 0 5665.29 5627.86 331.65 o 8 18 0 1018.41 1237.14 380.79 o 10 18 0 1598.53 1597.79 818.28 o 2 19 0 1541.03 1249.33 458.08 o 4 19 0 2391.80 2210.75 471.23 o 6 19 0 2417.34 2090.38 553.82 o 8 19 0 1873.23 1966.25 635.29 o 3 1 1 10483.05 10639.56 82.96 o 4 1 1 477.98 468.05 104.57 o 5 1 1 1441.38 1456.29 38.66 o 6 1 1 44147.18 44812.42 173.29 o 7 1 1 21019.57 21841.84 227.71 o 8 1 1 80.61 282.00 240.66 o 9 1 1 14814.11 15933.95 205.02 o 10 1 1 17546.30 17643.91 175.37 o 11 1 1 16502.38 18053.11 310.40 o 12 1 1 23.62 95.67 239.37 o 13 1 1 5863.49 6258.72 345.81 o 14 1 1 2506.76 2288.41 206.14 o 15 1 1 6248.98 6577.36 229.46 o 16 1 1 244.91 363.11 254.90 o 17 1 1 2642.05 3114.77 287.14 o 18 1 1 35.40 153.80 328.72 o 19 1 1 1963.02 1914.46 367.25 o 20 1 1 347.93 295.46 420.95 o 21 1 1 562.27 660.88 481.82 o 3 2 1 131751.02 131960.98 411.23 o 4 2 1 26172.43 26894.85 177.73 o 5 2 1 80902.22 84664.29 529.77 o 6 2 1 26453.11 26015.98 196.41 o 7 2 1 60891.32 62362.38 283.50 o 8 2 1 1850.45 1775.60 91.49 o 9 2 1 13843.67 15017.20 178.68 o 10 2 1 13709.74 14324.04 190.74 o 11 2 1 18919.71 19101.69 431.96 o 12 2 1 2038.50 2121.23 185.91 o 13 2 1 237.93 548.36 211.04 o 14 2 1 15639.93 17143.55 257.20 o 15 2 1 4065.43 3781.49 226.03 o 16 2 1 59.63 214.07 257.18 o 17 2 1 293.74 227.43 292.55 o 18 2 1 5529.55 6037.26 319.91 o 19 2 1 457.16 572.05 372.88 o 20 2 1 3.27 3.13 372.20 o 21 2 1 454.07 355.81 648.79 o 1 3 1 80219.52 80664.26 900.12 o 2 3 1 4970.02 5209.57 36.53 o 3 3 1 48395.48 49356.89 321.89 o 4 3 1 4643.12 4487.87 76.14 o 5 3 1 31083.66 32184.34 400.96 o 6 3 1 328.71 312.04 34.16 o 7 3 1 2869.67 2720.22 84.11 o 8 3 1 14543.19 14987.22 158.81 o 9 3 1 27410.86 28513.65 311.18 o 10 3 1 2001.88 2187.78 142.93 o 11 3 1 114.89 185.49 137.72 o 12 3 1 10077.91 10925.12 246.27 o 13 3 1 4094.97 3842.06 202.81 o 14 3 1 1194.24 936.55 207.56 o 15 3 1 532.91 541.35 230.44 o 16 3 1 5634.10 5845.09 257.48 o 17 3 1 723.41 621.02 294.73 o 18 3 1 38.31 98.35 105.66 o 19 3 1 540.29 447.17 372.88 o 20 3 1 2271.03 2564.51 421.17 o 21 3 1 139.72 440.30 641.23 o 0 4 1 70933.06 75122.19 1048.49 o 1 4 1 55176.98 54743.52 975.69 o 2 4 1 1161.85 1232.97 24.74 o 3 4 1 16311.49 17458.50 117.04 o 4 4 1 39763.43 40866.96 173.64 o 5 4 1 12772.18 12382.80 171.07 o 6 4 1 3682.81 3237.23 64.27 o 7 4 1 82.42 154.99 41.85 o 8 4 1 13127.67 13674.96 184.63 o 9 4 1 9765.45 10013.47 200.53 o 10 4 1 5168.76 5202.08 72.93 o 11 4 1 1250.22 1597.23 89.22 o 12 4 1 1540.92 1463.93 106.82 o 13 4 1 7281.09 7083.18 135.11 o 14 4 1 1355.69 1387.22 130.92 o 15 4 1 1072.15 1259.89 228.33 o 16 4 1 48.09 39.13 242.48 o 17 4 1 1769.85 1423.08 293.42 o 18 4 1 130.55 250.21 326.95 o 19 4 1 455.35 457.83 370.80 o 20 4 1 58.14 363.60 511.18 o 21 4 1 174.19 6.46 386.00 o 1 5 1 177.89 160.78 25.60 o 2 5 1 23671.52 22951.09 224.65 o 3 5 1 4448.87 4682.49 32.64 o 4 5 1 396.13 436.60 27.92 o 5 5 1 187.44 224.22 31.06 o 6 5 1 19840.00 19364.16 243.52 o 7 5 1 825.41 809.43 48.38 o 8 5 1 529.27 564.72 50.03 o 9 5 1 2025.15 1941.62 61.41 o 10 5 1 6191.13 6144.95 81.92 o 11 5 1 1524.08 1397.64 78.08 o 12 5 1 1400.17 1270.88 90.83 o 13 5 1 2206.85 2077.07 108.41 o 14 5 1 428.43 440.90 149.25 o 15 5 1 1899.09 1666.28 231.92 o 16 5 1 679.00 728.66 260.36 o 17 5 1 1972.97 1992.85 294.41 o 18 5 1 78.71 -47.44 277.03 o 19 5 1 1132.21 954.31 379.95 o 20 5 1 215.24 216.68 428.52 o 21 5 1 125.58 -15.17 341.26 o 0 6 1 82021.20 80755.41 496.50 o 1 6 1 1851.32 1742.86 26.66 o 2 6 1 2373.04 2538.92 34.41 o 3 6 1 29000.84 29543.84 274.93 o 4 6 1 93574.66 96036.78 612.65 o 5 6 1 5409.17 5313.90 43.11 o 6 6 1 9.41 27.75 20.15 o 7 6 1 17285.79 17287.68 106.30 o 8 6 1 28247.58 29195.02 284.59 o 9 6 1 9608.21 9949.56 96.18 o 10 6 1 43.78 62.93 63.64 o 11 6 1 9612.55 9583.36 172.23 o 12 6 1 7755.67 7636.23 196.56 o 13 6 1 3659.02 3869.78 173.74 o 14 6 1 708.56 599.04 210.14 o 15 6 1 3940.49 3948.87 269.35 o 16 6 1 307.02 329.58 263.92 o 17 6 1 1838.98 2070.25 297.82 o 18 6 1 415.40 306.48 331.05 o 19 6 1 892.62 1196.24 387.81 o 20 6 1 0.00 134.29 432.13 o 21 6 1 945.70 836.79 658.54 o 1 7 1 47173.63 46823.43 688.20 o 2 7 1 1160.74 1049.63 36.59 o 3 7 1 42611.34 42868.38 478.13 o 4 7 1 6349.55 6173.91 58.82 o 5 7 1 20649.64 20811.45 177.14 o 6 7 1 10.97 84.20 42.29 o 7 7 1 19399.79 19378.35 137.68 o 8 7 1 21031.75 21333.09 236.28 o 9 7 1 13811.75 13747.33 241.35 o 10 7 1 256.32 367.46 82.72 o 11 7 1 5037.90 4871.98 112.18 o 12 7 1 17414.31 18070.90 321.26 o 13 7 1 3908.50 3604.91 202.78 o 14 7 1 53.34 106.78 210.48 o 15 7 1 0.86 156.62 247.66 o 16 7 1 7489.99 8044.29 267.49 o 17 7 1 873.23 570.49 301.84 o 18 7 1 4.26 -43.40 352.63 o 19 7 1 477.45 464.09 441.46 o 20 7 1 2075.69 2340.35 572.31 o 0 8 1 4424.37 4391.91 105.82 o 1 8 1 584.08 495.09 33.38 o 2 8 1 856.48 738.62 45.90 o 3 8 1 7525.53 7778.14 95.48 o 4 8 1 3236.07 2859.54 113.02 o 5 8 1 439.07 429.86 51.49 o 6 8 1 643.11 697.03 55.17 o 7 8 1 1612.02 1561.48 60.58 o 8 8 1 1933.53 1782.63 64.22 o 9 8 1 1140.09 916.95 79.89 o 10 8 1 754.13 806.90 100.07 o 11 8 1 71.44 99.13 115.08 o 12 8 1 101.46 200.35 135.59 o 13 8 1 635.63 604.68 200.97 o 14 8 1 248.71 384.27 219.00 o 15 8 1 43.81 18.88 165.14 o 16 8 1 120.36 6.04 63.98 o 17 8 1 272.98 279.36 311.30 o 18 8 1 265.82 135.07 381.27 o 19 8 1 67.33 -3.33 316.85 o 1 9 1 22108.13 23785.18 218.30 o 2 9 1 10321.85 10520.12 140.35 o 3 9 1 12786.86 12845.87 210.80 o 4 9 1 7241.81 7213.33 85.29 o 5 9 1 10967.24 11181.89 403.45 o 6 9 1 4470.95 4433.99 61.51 o 7 9 1 8815.08 8965.33 127.01 o 8 9 1 6750.43 6678.50 105.77 o 9 9 1 1220.17 1259.62 88.16 o 10 9 1 1415.53 1356.26 102.79 o 11 9 1 1497.91 1329.31 119.09 o 12 9 1 4183.54 4207.29 162.03 o 13 9 1 69.88 174.34 219.07 o 14 9 1 93.97 92.15 134.70 o 15 9 1 525.83 425.42 259.45 o 16 9 1 2041.53 2255.57 283.90 o 17 9 1 32.00 1.16 119.38 o 18 9 1 88.37 174.52 595.20 o 19 9 1 95.44 32.82 360.81 o 0 10 1 36310.04 39036.96 372.06 o 1 10 1 75.94 124.78 38.92 o 2 10 1 1133.50 997.20 51.12 o 3 10 1 295.46 286.16 61.42 o 4 10 1 34961.14 36984.97 498.06 o 5 10 1 549.76 377.75 87.27 o 6 10 1 315.13 286.04 99.01 o 7 10 1 3503.72 3145.39 87.23 o 8 10 1 14171.45 14137.94 227.53 o 9 10 1 1996.18 1663.49 100.18 o 10 10 1 2.86 30.58 59.64 o 11 10 1 7579.35 7928.94 157.04 o 12 10 1 5744.66 5811.14 173.84 o 13 10 1 1711.90 1460.19 226.34 o 14 10 1 289.01 119.61 303.06 o 15 10 1 2826.96 2755.91 433.99 o 16 10 1 134.37 74.02 610.10 o 17 10 1 1579.70 1626.56 554.98 o 18 10 1 151.46 -67.06 449.63 o 1 11 1 6198.30 6751.55 105.74 o 2 11 1 13852.20 14752.53 125.10 o 3 11 1 168.81 185.71 66.02 o 4 11 1 1349.20 1217.01 78.76 o 5 11 1 8922.47 8942.83 136.17 o 6 11 1 6275.22 5903.91 126.50 o 7 11 1 774.52 687.53 106.04 o 8 11 1 1227.06 1017.90 116.27 o 9 11 1 4193.12 3861.36 121.98 o 10 11 1 767.90 722.54 142.65 o 11 11 1 935.61 1065.66 188.61 o 12 11 1 560.14 410.74 233.85 o 13 11 1 1284.86 1174.99 256.59 o 14 11 1 27.38 70.28 327.23 o 15 11 1 622.37 795.68 454.89 o 16 11 1 379.44 309.09 500.71 o 17 11 1 1165.91 1304.60 565.03 o 18 11 1 39.06 -15.89 155.97 o 0 12 1 9775.06 10284.73 127.20 o 1 12 1 10307.72 10683.34 107.11 o 2 12 1 194.27 300.85 76.46 o 3 12 1 6360.76 6145.52 70.76 o 4 12 1 5840.16 5918.43 82.78 o 5 12 1 11804.78 11569.00 158.01 o 6 12 1 1231.04 1044.28 99.70 o 7 12 1 2618.15 2313.50 107.91 o 8 12 1 416.77 383.91 123.12 o 9 12 1 4581.93 4515.31 136.75 o 10 12 1 5328.75 5059.22 143.37 o 11 12 1 1870.18 1602.16 181.24 o 12 12 1 58.63 132.40 215.57 o 13 12 1 625.90 586.37 241.00 o 14 12 1 3272.91 3414.38 297.60 o 15 12 1 252.51 -25.62 121.65 o 16 12 1 70.77 13.08 155.52 o 17 12 1 97.63 -98.24 340.89 o 18 12 1 1320.79 1390.43 674.86 o 1 13 1 342.37 586.76 84.79 o 2 13 1 4045.55 3836.78 92.61 o 3 13 1 1417.96 1428.38 98.45 o 4 13 1 3.34 125.96 119.88 o 5 13 1 55.22 181.31 125.10 o 6 13 1 752.88 456.85 130.18 o 7 13 1 2772.02 2653.16 138.85 o 8 13 1 94.52 205.93 136.51 o 9 13 1 651.35 849.09 145.93 o 10 13 1 6.32 24.61 166.67 o 11 13 1 277.32 50.76 62.11 o 12 13 1 742.64 795.23 240.47 o 13 13 1 159.90 29.87 90.31 o 14 13 1 17.03 160.50 469.96 o 15 13 1 0.46 -175.62 513.98 o 0 14 1 1559.70 1820.29 152.21 o 1 14 1 5549.57 5724.34 99.61 o 2 14 1 525.60 478.62 103.38 o 3 14 1 5238.79 5552.65 107.28 o 4 14 1 662.81 687.38 129.14 o 5 14 1 2236.29 2064.04 138.98 o 6 14 1 3695.84 3677.27 141.93 o 7 14 1 2036.76 2056.80 153.25 o 8 14 1 54.25 28.43 112.26 o 9 14 1 353.34 154.20 173.01 o 10 14 1 1641.12 1465.31 204.32 o 11 14 1 243.45 151.40 114.54 o 12 14 1 39.95 57.92 83.84 o 13 14 1 185.33 268.17 313.61 o 14 14 1 575.47 628.61 393.04 o 1 15 1 605.10 713.08 121.78 o 2 15 1 8927.87 9228.07 157.73 o 3 15 1 750.79 766.90 149.23 o 4 15 1 418.04 270.04 124.35 o 5 15 1 185.87 178.60 150.04 o 6 15 1 9084.93 9263.91 194.88 o 7 15 1 572.63 429.03 184.27 o 8 15 1 469.57 437.48 195.70 o 9 15 1 1799.40 1703.95 211.15 o 10 15 1 4874.33 4800.06 227.27 o 11 15 1 1437.67 1255.92 242.88 o 12 15 1 6.96 -45.91 55.06 o 13 15 1 1396.21 1353.27 399.40 o 0 16 1 1979.21 2230.28 188.64 o 1 16 1 644.71 716.35 146.41 o 2 16 1 498.31 535.86 161.65 o 3 16 1 1194.05 1255.99 172.74 o 4 16 1 130.91 179.10 173.66 o 5 16 1 2.50 68.92 156.81 o 6 16 1 1002.49 1002.89 192.44 o 7 16 1 566.13 435.01 203.03 o 8 16 1 130.81 113.58 196.80 o 9 16 1 279.61 275.17 233.41 o 10 16 1 588.45 489.28 251.98 o 11 16 1 171.26 219.44 322.47 o 12 16 1 164.51 32.21 297.18 o 13 16 1 14.81 235.86 823.19 o 1 17 1 117.28 160.39 159.18 o 2 17 1 2541.40 2828.03 183.61 o 3 17 1 1822.18 1755.23 183.81 o 4 17 1 3.29 18.26 89.28 o 5 17 1 146.92 218.92 200.83 o 6 17 1 348.03 412.62 213.05 o 7 17 1 2450.63 2457.48 226.63 o 8 17 1 27.90 66.65 136.52 o 9 17 1 49.92 -1.63 170.92 o 10 17 1 2.89 120.17 372.95 o 11 17 1 748.04 650.56 301.92 o 12 17 1 501.76 34.07 412.04 o 0 18 1 2297.43 1796.66 387.95 o 1 18 1 1121.02 1314.79 274.97 o 2 18 1 48.11 347.33 276.87 o 3 18 1 628.94 842.51 235.71 o 4 18 1 610.27 488.34 287.52 o 5 18 1 2037.11 1952.62 220.33 o 6 18 1 0.57 343.28 233.62 o 7 18 1 527.99 845.36 252.85 o 8 18 1 5.51 -19.32 123.87 o 9 18 1 1392.93 1590.02 307.98 o 10 18 1 269.57 367.45 817.31 o 1 19 1 1554.18 1407.94 306.67 o 2 19 1 724.16 694.01 322.79 o 3 19 1 456.23 340.24 326.83 o 4 19 1 724.30 849.97 332.95 o 5 19 1 1121.63 1118.35 421.96 o 6 19 1 79.51 300.14 523.48 o 7 19 1 0.47 -129.84 277.75 o 8 19 1 667.36 589.39 614.31 o 4 0 2 2012.07 2114.11 131.30 o 5 0 2 59978.70 63001.86 445.80 o 6 0 2 2658.67 2723.65 42.98 o 7 0 2 57439.58 54285.65 1636.97 o 8 0 2 676.28 682.00 56.34 o 9 0 2 81032.81 78332.41 2769.47 o 10 0 2 80.96 229.82 87.85 o 11 0 2 17063.46 17763.05 677.29 o 12 0 2 2.26 103.75 127.33 o 13 0 2 19084.75 21825.85 536.03 o 14 0 2 645.33 938.80 448.16 o 15 0 2 5149.26 6801.69 343.28 o 16 0 2 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