#------------------------------------------------------------------------------ #$Date: 2010-02-13 12:42:52 +0200 (Sat, 13 Feb 2010) $ #$Revision: 986 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224746.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224746_Fobs loop_ _publ_author_name 'Xia, Guang-Ming' 'Ji, Mu-Wei' 'Lu, Ping' 'Sun, Guo-Xin' 'Xu, Wen-Fang' _publ_section_title ; 5-(Methoxycarbonyl)thiophene-2-carboxylic acid ; _journal_coeditor_code RK2181 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o148 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.081 _cell_angle_gamma 90.000 _cell_length_a 18.2813 _cell_length_b 5.9833 _cell_length_c 7.3446 _exptl_crystal_F_000 384.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file rk2181Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 090930c in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 248.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2333.97 2548.80 28.62 o 3 0 0 56.26 71.87 2.75 o 4 0 0 112.65 134.47 6.52 o 5 0 0 3130.00 3113.84 90.77 o 6 0 0 5193.47 5489.02 81.07 o 7 0 0 2652.74 2650.17 58.84 o 8 0 0 61.90 73.03 4.38 o 9 0 0 159.15 186.32 6.96 o 10 0 0 152.35 160.10 8.18 o 11 0 0 16.31 17.87 3.26 o 12 0 0 0.69 -0.60 2.43 o 13 0 0 160.52 125.26 12.18 o 14 0 0 518.30 498.68 25.14 o 15 0 0 775.90 796.51 34.27 o 16 0 0 402.90 428.66 26.36 o 17 0 0 61.14 55.93 12.18 o 18 0 0 8.90 0.78 7.92 o 19 0 0 0.33 -0.09 5.48 o 20 0 0 72.62 60.02 13.31 o 21 0 0 8.04 12.44 9.83 o 1 1 0 3800.21 3986.18 54.43 o 2 1 0 257.37 230.73 7.43 o 3 1 0 4.19 7.74 1.20 o 4 1 0 235.69 191.84 3.21 o 5 1 0 0.03 -0.14 0.98 o 6 1 0 250.91 242.69 5.68 o 7 1 0 140.29 139.19 4.68 o 8 1 0 3283.66 3652.50 80.62 o 9 1 0 2.08 6.39 2.77 o 10 1 0 136.66 139.05 4.91 o 11 1 0 56.87 45.67 2.83 o 12 1 0 0.67 1.90 2.34 o 13 1 0 229.29 223.61 9.11 o 14 1 0 343.74 371.76 16.74 o 15 1 0 10.13 5.05 4.64 o 16 1 0 47.53 37.96 7.17 o 17 1 0 210.91 199.11 14.35 o 18 1 0 2.37 10.84 5.77 o 19 1 0 159.88 163.80 14.40 o 20 1 0 0.92 3.40 6.11 o 21 1 0 4.68 5.43 5.22 o 0 2 0 1.12 2.02 1.72 o 1 2 0 107.43 116.44 4.92 o 2 2 0 3815.94 3863.45 96.64 o 3 2 0 832.42 838.19 16.55 o 4 2 0 618.24 599.51 10.65 o 5 2 0 1.81 0.85 1.58 o 6 2 0 68.37 63.89 3.47 o 7 2 0 2853.36 3003.05 86.73 o 8 2 0 601.92 647.95 9.06 o 9 2 0 2086.27 2185.75 24.57 o 10 2 0 0.66 2.22 1.93 o 11 2 0 1.08 -0.38 2.70 o 12 2 0 16.04 12.35 3.35 o 13 2 0 734.60 739.32 17.71 o 14 2 0 258.00 240.54 10.39 o 15 2 0 133.95 129.95 15.57 o 16 2 0 8.68 5.55 5.74 o 17 2 0 0.02 -2.03 4.85 o 18 2 0 27.26 35.50 8.30 o 19 2 0 4.54 -0.16 5.50 o 20 2 0 191.20 191.57 14.82 o 1 3 0 608.25 603.55 13.50 o 2 3 0 145.94 164.74 10.58 o 3 3 0 862.75 954.52 17.21 o 4 3 0 19.47 23.18 2.98 o 5 3 0 479.24 476.99 10.58 o 6 3 0 1095.72 1098.99 17.82 o 7 3 0 30.67 30.63 2.91 o 8 3 0 9.33 14.78 2.34 o 9 3 0 5.53 7.08 2.23 o 10 3 0 130.94 117.83 6.43 o 11 3 0 15.40 13.68 4.00 o 12 3 0 540.94 568.01 28.68 o 13 3 0 165.38 152.00 9.15 o 14 3 0 28.25 35.70 4.71 o 15 3 0 57.23 64.34 5.75 o 16 3 0 67.58 79.29 11.87 o 17 3 0 100.30 103.25 11.90 o 18 3 0 10.91 9.57 8.09 o 19 3 0 31.85 40.94 9.63 o 0 4 0 74.18 85.07 10.35 o 1 4 0 4.83 2.61 3.84 o 2 4 0 5.23 6.80 4.09 o 3 4 0 20.57 12.17 3.00 o 4 4 0 658.50 742.45 18.14 o 5 4 0 554.55 549.64 32.29 o 6 4 0 124.01 109.06 6.25 o 7 4 0 0.25 -2.05 2.25 o 8 4 0 1.09 0.37 2.52 o 9 4 0 143.84 125.45 7.61 o 10 4 0 27.15 26.90 4.72 o 11 4 0 1985.18 2011.23 43.04 o 12 4 0 132.22 145.43 8.64 o 13 4 0 49.87 48.76 5.87 o 14 4 0 5.42 1.29 3.77 o 15 4 0 0.11 1.11 4.41 o 16 4 0 200.55 209.91 10.77 o 17 4 0 58.45 63.84 10.48 o 1 5 0 468.26 459.71 18.59 o 2 5 0 42.48 49.64 7.56 o 3 5 0 899.50 907.96 26.96 o 4 5 0 76.42 64.82 8.31 o 5 5 0 20.45 19.63 5.87 o 6 5 0 45.39 45.17 7.15 o 7 5 0 13.72 12.85 3.75 o 8 5 0 178.09 180.69 10.87 o 9 5 0 65.98 65.43 6.09 o 10 5 0 0.06 6.59 4.61 o 11 5 0 1.21 4.26 4.14 o 12 5 0 14.18 26.41 5.77 o 13 5 0 33.50 33.50 5.53 o 14 5 0 111.28 120.07 9.21 o 15 5 0 48.43 48.57 6.61 o 0 6 0 1.88 -2.61 7.57 o 1 6 0 3.06 3.27 6.18 o 2 6 0 196.05 170.41 13.45 o 3 6 0 113.37 84.43 15.57 o 4 6 0 123.12 103.62 11.09 o 5 6 0 6.07 5.99 5.82 o 6 6 0 15.24 13.32 6.35 o 7 6 0 42.49 40.58 7.74 o 8 6 0 2.09 6.49 6.31 o 9 6 0 52.11 47.03 12.18 o 10 6 0 0.24 2.81 7.29 o 11 6 0 25.23 33.69 8.38 o 1 7 0 130.13 132.78 13.38 o 2 7 0 5.20 8.59 7.47 o 3 7 0 47.80 60.04 10.06 o -21 1 1 41.70 36.55 7.58 o -20 1 1 21.39 17.95 6.65 o -19 1 1 35.91 40.71 7.75 o -18 1 1 7.17 12.72 5.26 o -17 1 1 806.03 829.88 25.68 o -16 1 1 0.01 2.55 4.18 o -15 1 1 1482.29 1625.42 34.92 o -14 1 1 31.18 29.39 5.87 o -13 1 1 38.79 39.25 4.28 o -12 1 1 42.60 41.43 3.35 o -11 1 1 116.90 107.23 4.76 o -10 1 1 996.71 945.39 34.17 o -9 1 1 721.69 743.60 14.90 o -8 1 1 3031.53 2894.27 69.71 o -7 1 1 0.01 -0.43 1.32 o -6 1 1 2.69 6.21 1.59 o -5 1 1 88.31 86.04 3.21 o -4 1 1 130.72 134.45 3.77 o -3 1 1 920.56 894.85 9.42 o -2 1 1 6572.47 6690.73 61.85 o -1 1 1 5726.37 5419.75 220.20 o 0 1 1 886.74 869.02 24.14 o 1 1 1 199.52 178.60 7.75 o 2 1 1 245.95 228.58 8.77 o 3 1 1 0.92 2.25 0.92 o 4 1 1 31.68 33.03 1.38 o 5 1 1 4690.00 4951.95 68.46 o 6 1 1 1416.02 1546.68 53.89 o 7 1 1 1915.91 2135.72 29.65 o 8 1 1 120.47 110.92 3.95 o 9 1 1 26.93 24.89 2.33 o 10 1 1 58.36 61.78 3.36 o 11 1 1 57.65 60.18 3.55 o 12 1 1 3167.19 3296.23 29.22 o 13 1 1 3.76 13.30 3.34 o 14 1 1 1481.26 1478.08 34.10 o 15 1 1 17.61 24.51 6.02 o 16 1 1 75.02 66.75 8.35 o 17 1 1 57.81 49.59 7.12 o 18 1 1 127.16 127.20 14.96 o 19 1 1 197.82 188.11 14.61 o 20 1 1 59.70 59.41 9.06 o -20 2 1 4.18 2.80 5.26 o -19 2 1 14.26 17.68 6.60 o -18 2 1 100.99 90.36 10.37 o -17 2 1 20.54 24.02 6.03 o -16 2 1 24.14 17.84 5.56 o -15 2 1 3.74 1.37 3.49 o -14 2 1 0.17 2.74 2.95 o -13 2 1 17.14 15.65 3.88 o -12 2 1 6.61 4.00 3.13 o -11 2 1 11.04 11.92 2.51 o -10 2 1 94.26 94.69 5.59 o -9 2 1 268.87 296.48 9.29 o -8 2 1 13.05 17.57 2.53 o -7 2 1 1415.64 1660.30 37.31 o -6 2 1 1.11 0.99 1.71 o -5 2 1 116.01 114.44 4.47 o -4 2 1 0.37 2.79 1.94 o -3 2 1 126.73 125.77 5.29 o -2 2 1 1122.20 1112.55 63.98 o -1 2 1 1190.98 1191.57 31.97 o 0 2 1 7.24 5.77 2.06 o 1 2 1 45.12 52.04 4.27 o 2 2 1 260.95 222.27 7.74 o 3 2 1 1.04 0.82 1.30 o 4 2 1 2512.13 2781.39 34.81 o 5 2 1 20.57 26.82 2.05 o 6 2 1 470.04 566.44 14.66 o 7 2 1 172.62 191.14 4.42 o 8 2 1 13.66 16.29 1.83 o 9 2 1 59.23 62.32 3.51 o 10 2 1 9.50 10.31 2.14 o 11 2 1 31.39 32.60 3.74 o 12 2 1 0.00 -0.48 2.80 o 13 2 1 23.16 18.49 3.53 o 14 2 1 48.99 45.17 7.38 o 15 2 1 306.78 268.42 21.40 o 16 2 1 26.98 20.62 6.36 o 17 2 1 12.03 10.53 5.34 o 18 2 1 22.86 18.73 6.04 o 19 2 1 36.77 35.48 8.60 o 20 2 1 32.49 28.14 9.83 o -19 3 1 52.27 48.21 9.21 o -18 3 1 5.60 5.67 6.16 o -17 3 1 5.68 -1.03 5.17 o -16 3 1 3.57 1.03 3.60 o -15 3 1 4.76 1.79 3.68 o -14 3 1 57.71 50.82 6.05 o -13 3 1 396.23 401.71 14.49 o -12 3 1 121.20 122.31 8.14 o -11 3 1 242.10 231.15 8.40 o -10 3 1 359.08 370.11 10.27 o -9 3 1 49.88 56.81 4.86 o -8 3 1 732.60 824.47 15.73 o -7 3 1 46.44 43.89 3.77 o -6 3 1 1352.50 1402.88 21.99 o -5 3 1 140.36 133.00 6.85 o -4 3 1 1250.93 1303.69 44.81 o -3 3 1 35.45 27.79 4.44 o -2 3 1 1.07 1.60 2.92 o -1 3 1 3.33 -0.55 2.24 o 0 3 1 51.81 50.19 4.42 o 1 3 1 1391.04 1477.03 20.94 o 2 3 1 197.86 178.91 7.32 o 3 3 1 1598.89 1747.27 19.79 o 4 3 1 107.51 96.57 5.73 o 5 3 1 1194.17 1280.98 27.04 o 6 3 1 33.39 33.08 3.32 o 7 3 1 531.55 534.93 13.73 o 8 3 1 447.13 445.64 17.82 o 9 3 1 224.80 197.27 9.21 o 10 3 1 800.11 724.99 18.19 o 11 3 1 122.71 121.36 8.04 o 12 3 1 12.38 7.18 4.05 o 13 3 1 3.79 0.92 4.03 o 14 3 1 2.24 5.91 3.81 o 15 3 1 7.78 9.42 6.22 o 16 3 1 114.87 127.45 12.39 o 17 3 1 8.18 7.48 6.98 o 18 3 1 28.59 34.94 8.27 o -17 4 1 0.07 2.97 4.08 o -16 4 1 114.35 117.53 9.66 o -15 4 1 0.11 6.78 5.42 o -14 4 1 128.16 135.19 10.97 o -13 4 1 1.01 4.51 4.36 o -12 4 1 1.79 3.18 5.95 o -11 4 1 25.04 24.50 5.24 o -10 4 1 10.11 9.03 3.52 o -9 4 1 92.65 83.14 6.35 o -8 4 1 76.13 72.44 7.82 o -7 4 1 30.71 28.38 3.77 o -6 4 1 2.49 1.71 3.55 o -5 4 1 170.37 153.74 11.87 o -4 4 1 230.36 209.87 9.55 o -3 4 1 611.30 595.29 15.99 o -2 4 1 351.00 367.64 12.32 o -1 4 1 373.31 403.66 13.07 o 0 4 1 615.47 630.48 16.48 o 1 4 1 236.14 233.68 10.01 o 2 4 1 200.20 160.30 8.16 o 3 4 1 1.08 -4.03 3.18 o 4 4 1 86.66 88.42 7.68 o 5 4 1 102.21 107.57 6.87 o 6 4 1 155.30 145.80 6.83 o 7 4 1 27.95 25.85 3.74 o 8 4 1 16.58 20.08 4.79 o 9 4 1 2.87 6.28 3.72 o 10 4 1 4.45 13.90 4.86 o 11 4 1 230.49 244.68 12.04 o 12 4 1 0.97 1.25 3.76 o 13 4 1 209.22 220.86 12.10 o 14 4 1 0.06 1.07 4.93 o 15 4 1 108.22 124.50 12.70 o 16 4 1 0.02 2.65 7.27 o 17 4 1 43.57 48.52 9.71 o -15 5 1 1.37 3.15 5.19 o -14 5 1 0.03 0.43 4.93 o -13 5 1 53.08 54.01 6.41 o -12 5 1 70.26 75.09 7.57 o -11 5 1 36.55 33.64 5.78 o -10 5 1 0.07 1.95 4.29 o -9 5 1 12.29 10.88 3.55 o -8 5 1 35.79 28.66 4.39 o -7 5 1 1.07 3.51 4.20 o -6 5 1 642.03 693.63 26.22 o -5 5 1 70.99 72.10 8.41 o -4 5 1 873.15 909.82 22.89 o -3 5 1 95.06 93.87 7.99 o -2 5 1 29.67 28.60 4.85 o -1 5 1 36.95 34.65 5.28 o 0 5 1 105.46 94.02 9.40 o 1 5 1 1036.60 1004.42 91.16 o 2 5 1 99.74 109.01 10.18 o 3 5 1 812.94 791.27 24.12 o 4 5 1 2.00 1.09 4.78 o 5 5 1 50.57 35.09 6.53 o 6 5 1 11.28 7.97 4.85 o 7 5 1 0.27 4.51 5.19 o 8 5 1 65.65 60.36 6.84 o 9 5 1 143.34 147.96 13.49 o 10 5 1 73.81 81.66 8.14 o 11 5 1 0.00 2.26 4.76 o 12 5 1 3.08 1.01 4.73 o 13 5 1 0.05 -0.96 5.11 o 14 5 1 9.62 10.19 4.74 o -11 6 1 95.17 110.03 10.91 o -10 6 1 20.03 14.73 6.06 o -9 6 1 131.45 143.16 11.35 o -8 6 1 12.62 11.53 5.32 o -7 6 1 99.48 98.48 9.00 o -6 6 1 10.56 8.60 5.50 o -5 6 1 34.61 36.27 6.51 o -4 6 1 14.29 15.02 5.78 o -3 6 1 4.63 8.50 7.83 o -2 6 1 21.23 20.09 6.24 o -1 6 1 21.35 18.31 6.61 o 0 6 1 7.04 12.46 6.16 o 1 6 1 22.46 20.50 8.52 o 2 6 1 36.74 38.29 8.02 o 3 6 1 13.21 11.87 5.06 o 4 6 1 108.45 110.96 11.24 o 5 6 1 14.85 13.94 6.08 o 6 6 1 168.01 167.79 19.92 o 7 6 1 27.52 27.80 6.73 o 8 6 1 148.80 154.93 13.62 o 9 6 1 167.92 138.31 13.45 o 10 6 1 47.03 58.60 9.78 o -3 7 1 8.04 15.58 7.81 o -2 7 1 3.02 4.94 7.28 o -1 7 1 3.72 12.53 7.53 o 0 7 1 7.46 12.72 7.72 o 1 7 1 1.33 4.92 7.04 o 2 7 1 0.30 -2.35 5.79 o -21 0 2 0.02 -5.13 5.83 o -20 0 2 26.50 36.97 10.35 o -19 0 2 177.26 168.84 17.83 o -18 0 2 321.67 331.23 23.05 o -17 0 2 244.38 249.64 20.53 o -16 0 2 34.02 30.62 8.87 o -15 0 2 6.97 8.71 3.81 o -14 0 2 0.40 0.22 2.80 o -13 0 2 24.70 20.07 4.01 o -12 0 2 7.80 3.68 3.26 o -11 0 2 3.60 -0.62 2.84 o -10 0 2 781.04 785.95 17.26 o -9 0 2 1351.60 1401.18 22.42 o -8 0 2 1198.15 1183.06 19.73 o -7 0 2 30.79 36.12 3.56 o -6 0 2 159.67 150.44 6.25 o -5 0 2 1177.33 1183.85 16.12 o -4 0 2 316.77 358.17 31.75 o -3 0 2 61856.38 48748.89 180.38 o -2 0 2 161.35 157.72 5.97 o -1 0 2 2185.42 2214.14 116.04 o 0 0 2 1.20 1.51 1.54 o 1 0 2 57.22 75.66 3.42 o 2 0 2 2036.63 2180.16 19.94 o 3 0 2 4955.37 5296.82 103.56 o 4 0 2 4165.26 4294.44 27.59 o 5 0 2 21.97 35.08 3.94 o 6 0 2 374.26 452.67 8.26 o 7 0 2 275.10 331.64 7.13 o 8 0 2 112.39 147.15 11.48 o 9 0 2 30.45 34.60 3.18 o 10 0 2 540.23 539.21 23.40 o 11 0 2 518.75 475.63 23.57 o 12 0 2 927.39 967.52 35.92 o 13 0 2 459.95 529.12 28.10 o 14 0 2 75.80 58.37 11.74 o 15 0 2 82.22 86.90 13.66 o 16 0 2 0.68 0.70 7.31 o 17 0 2 93.13 96.22 12.05 o 18 0 2 13.27 10.00 7.05 o 19 0 2 531.24 545.39 34.10 o 20 0 2 84.89 111.25 17.22 o -21 1 2 0.17 -2.81 5.07 o -20 1 2 40.06 29.63 6.87 o -19 1 2 11.89 10.60 5.39 o -18 1 2 0.18 3.02 4.41 o -17 1 2 47.87 53.68 7.35 o -16 1 2 50.98 45.22 5.00 o -15 1 2 17.01 17.91 3.72 o -14 1 2 10.01 8.09 2.70 o -13 1 2 62.53 51.15 4.21 o -12 1 2 2.90 2.26 2.38 o -11 1 2 974.37 994.20 16.53 o -10 1 2 139.77 133.96 5.42 o -9 1 2 0.01 -2.49 1.81 o -8 1 2 37.88 32.42 2.67 o -7 1 2 0.36 0.43 1.63 o -6 1 2 4.80 4.81 1.57 o -5 1 2 43.76 38.88 2.04 o -4 1 2 557.58 565.70 11.13 o -3 1 2 49.51 53.41 3.14 o -2 1 2 3881.84 3862.63 84.69 o -1 1 2 116.58 93.73 3.42 o 0 1 2 1.24 7.68 1.80 o 1 1 2 358.00 309.61 4.99 o 2 1 2 58.02 64.94 3.12 o 3 1 2 491.04 482.84 11.52 o 4 1 2 21.00 18.67 1.65 o 5 1 2 3421.71 3764.72 58.80 o 6 1 2 1.33 1.52 1.15 o 7 1 2 266.18 314.74 7.49 o 8 1 2 63.99 61.51 3.72 o 9 1 2 7.28 7.63 2.13 o 10 1 2 380.43 396.93 20.79 o 11 1 2 760.88 802.76 29.63 o 12 1 2 29.82 24.63 4.24 o 13 1 2 93.31 82.60 6.67 o 14 1 2 437.79 384.28 33.71 o 15 1 2 8.04 9.37 4.66 o 16 1 2 284.31 258.01 27.36 o 17 1 2 2.96 10.06 6.19 o 18 1 2 23.96 10.67 5.62 o 19 1 2 0.01 -3.30 4.58 o -20 2 2 0.09 -0.12 5.00 o -19 2 2 3.06 4.01 6.32 o -18 2 2 31.23 32.73 7.76 o -17 2 2 70.58 64.54 6.84 o -16 2 2 274.98 270.65 12.09 o -15 2 2 11.99 10.61 4.10 o -14 2 2 4.50 3.42 3.28 o -13 2 2 0.00 -0.39 2.15 o -12 2 2 716.96 704.22 15.20 o -11 2 2 213.23 234.66 7.87 o -10 2 2 1472.26 1521.95 26.24 o -9 2 2 62.05 58.68 4.09 o -8 2 2 3.35 3.20 1.91 o -7 2 2 209.35 197.02 6.49 o -6 2 2 318.05 300.44 6.40 o -5 2 2 2241.06 2238.51 27.31 o -4 2 2 96.77 91.31 3.61 o -3 2 2 8.61 7.54 2.52 o -2 2 2 35.51 26.53 3.28 o -1 2 2 1846.98 1766.24 115.69 o 0 2 2 636.43 656.23 14.98 o 1 2 2 744.25 804.75 32.44 o 2 2 2 48.60 42.42 2.96 o 3 2 2 73.81 63.45 3.04 o 4 2 2 2166.29 2309.84 17.54 o 5 2 2 675.82 711.39 9.63 o 6 2 2 2696.43 2704.48 23.79 o 7 2 2 7.51 9.61 1.73 o 8 2 2 0.49 1.21 1.89 o 9 2 2 6.08 2.46 2.24 o 10 2 2 869.87 890.34 25.05 o 11 2 2 409.91 405.70 10.65 o 12 2 2 289.99 270.87 14.96 o 13 2 2 25.97 31.97 5.81 o 14 2 2 0.01 -0.14 4.79 o 15 2 2 15.26 14.40 5.83 o 16 2 2 4.63 3.50 6.18 o 17 2 2 445.13 470.80 22.60 o 18 2 2 14.16 14.50 7.31 o 19 2 2 73.33 65.56 9.68 o -19 3 2 31.57 36.83 11.13 o -18 3 2 35.27 41.24 8.76 o -17 3 2 10.49 11.00 5.12 o -16 3 2 54.70 51.75 6.48 o -15 3 2 155.24 159.13 9.76 o -14 3 2 4.03 5.01 3.74 o -13 3 2 148.41 155.20 9.20 o -12 3 2 3.26 3.32 3.29 o -11 3 2 0.08 -0.17 2.63 o -10 3 2 3.79 3.17 2.43 o -9 3 2 332.33 341.34 10.71 o -8 3 2 180.48 176.69 7.16 o -7 3 2 1.26 1.48 2.05 o -6 3 2 174.95 172.52 14.71 o -5 3 2 56.69 53.88 3.89 o -4 3 2 237.62 211.90 22.88 o -3 3 2 2.37 2.25 3.38 o -2 3 2 415.81 396.70 13.84 o -1 3 2 73.33 84.74 8.65 o 0 3 2 662.78 730.13 18.41 o 1 3 2 40.64 40.67 4.76 o 2 3 2 359.21 333.70 12.24 o 3 3 2 1302.46 1265.64 33.02 o 4 3 2 85.42 76.99 3.83 o 5 3 2 12.53 16.38 2.28 o 6 3 2 7.33 6.54 2.37 o 7 3 2 22.01 16.93 2.94 o 8 3 2 41.31 43.56 4.17 o 9 3 2 1022.78 1121.51 29.47 o 10 3 2 278.03 273.80 11.54 o 11 3 2 53.22 54.80 7.30 o 12 3 2 34.71 49.21 5.68 o 13 3 2 59.80 61.94 8.13 o 14 3 2 174.21 186.63 13.68 o 15 3 2 21.57 18.43 7.18 o 16 3 2 70.83 71.60 10.01 o 17 3 2 3.59 2.26 7.18 o 18 3 2 82.31 97.25 12.75 o -17 4 2 0.54 7.76 5.73 o -16 4 2 25.76 33.67 6.75 o -15 4 2 55.06 53.16 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