#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/47/2224765.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224765_Fobs loop_ _publ_author_name 'bin Shawkataly, Omar' 'Khan, Imthyaz Ahmed' 'Yeap, Chin Sing' 'Fun, Hoong-Kun' _publ_section_title ; [\m-Bis(diphenylarsino)methane-1:2\k^2^As:As']nonacarbonyl-1\k^3^C,2\k^3^C,3\k^3^C-[tris(4-methylphenyl)phosphine-3\kP]-triangulo-triruthenium(0) ; _journal_coeditor_code SJ2681 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m36 _journal_page_last m37 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.680 _cell_angle_gamma 90.000 _cell_length_a 16.2585 _cell_length_b 16.9247 _cell_length_c 19.6900 _exptl_crystal_F_000 2632.00 _reflns_d_resolution_high 0.7081 _[local]_cod_data_source_file sj2681Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' iak28_0m in P2(1)/c R.T.' _shelx_refln_list_code 4 _shelx_f_calc_maximum 528.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 49770.39 51469.05 709.63 o 3 0 0 105543.34 110580.22 1472.94 o 4 0 0 39511.04 43489.92 655.65 o 5 0 0 22329.70 23562.97 423.24 o 6 0 0 23781.50 23172.20 333.63 o 7 0 0 61.55 135.30 55.44 o 8 0 0 49975.39 46492.59 598.35 o 9 0 0 11030.50 10603.69 240.76 o 10 0 0 1081.12 1222.13 107.47 o 11 0 0 11894.90 12093.49 313.81 o 12 0 0 48356.02 46603.55 678.23 o 13 0 0 27740.52 26041.98 490.28 o 14 0 0 9911.08 9987.07 307.25 o 15 0 0 4255.01 4907.00 233.88 o 16 0 0 1499.61 1352.59 159.73 o 17 0 0 1121.00 1394.62 432.40 o 18 0 0 872.27 959.99 164.75 o 19 0 0 14.58 156.96 136.28 o 20 0 0 2298.84 2367.30 279.61 o 21 0 0 4525.04 4931.10 297.84 o 22 0 0 212.04 466.61 178.07 o 2 1 0 36637.23 39867.85 313.63 o 3 1 0 62847.88 69500.19 527.20 o 4 1 0 29452.26 31764.21 312.41 o 5 1 0 10481.76 11464.79 148.82 o 6 1 0 1184.23 1150.50 61.20 o 7 1 0 22203.03 23561.77 281.60 o 8 1 0 35.28 28.68 40.74 o 9 1 0 2077.72 2037.45 84.83 o 10 1 0 53.16 54.27 50.85 o 11 1 0 459.57 342.03 64.95 o 12 1 0 196.95 178.68 68.41 o 13 1 0 26.55 42.40 72.93 o 14 1 0 872.94 798.37 97.06 o 15 1 0 647.61 809.34 113.25 o 16 1 0 6047.19 6116.94 304.28 o 17 1 0 1670.60 1869.20 150.01 o 18 1 0 178.10 227.60 119.72 o 19 1 0 466.44 528.89 131.79 o 20 1 0 19.62 14.49 98.65 o 21 1 0 781.02 802.78 131.79 o 22 1 0 143.17 292.42 118.10 o 0 2 0 48278.09 55726.72 1066.77 o 1 2 0 15292.46 17018.79 195.40 o 2 2 0 582.86 529.84 25.36 o 3 2 0 8885.78 9170.69 96.97 o 4 2 0 41000.57 43195.70 324.79 o 5 2 0 33116.92 35768.17 358.94 o 6 2 0 126024.23 129391.09 1107.94 o 7 2 0 11413.35 10724.89 180.50 o 8 2 0 36368.06 36134.21 368.14 o 9 2 0 28389.12 28408.18 346.70 o 10 2 0 256.63 284.87 57.22 o 11 2 0 439.91 414.65 65.75 o 12 2 0 4822.48 4765.27 143.66 o 13 2 0 1092.70 1096.49 99.84 o 14 2 0 920.26 966.12 98.62 o 15 2 0 2079.55 2224.30 127.50 o 16 2 0 128.35 -99.41 104.77 o 17 2 0 148.04 189.17 94.06 o 18 2 0 2387.83 2514.34 152.05 o 19 2 0 0.32 -41.77 99.35 o 20 2 0 2036.65 2206.78 158.84 o 21 2 0 1822.21 1929.69 158.13 o 22 2 0 337.04 525.27 150.62 o 1 3 0 16505.45 16956.00 657.14 o 2 3 0 2579.25 2864.92 51.61 o 3 3 0 267.84 312.87 25.92 o 4 3 0 1080.94 1115.58 54.43 o 5 3 0 44416.78 48563.80 413.49 o 6 3 0 1555.32 1758.34 59.39 o 7 3 0 277.48 402.87 48.18 o 8 3 0 19677.29 19016.88 300.48 o 9 3 0 2229.12 2047.11 101.57 o 10 3 0 22656.44 22427.68 305.10 o 11 3 0 2572.98 2637.78 119.18 o 12 3 0 8586.25 8238.84 179.44 o 13 3 0 6147.30 6044.49 167.24 o 14 3 0 934.03 999.86 97.11 o 15 3 0 3341.82 3152.09 141.73 o 16 3 0 747.32 801.85 138.23 o 17 3 0 2504.85 2397.82 237.77 o 18 3 0 257.00 208.06 123.89 o 19 3 0 162.53 350.79 108.64 o 20 3 0 1972.79 1962.21 171.46 o 21 3 0 1319.12 1368.32 172.40 o 22 3 0 505.82 520.91 195.38 o 0 4 0 32309.49 34352.89 511.05 o 1 4 0 2261.84 2166.94 55.90 o 2 4 0 566.15 502.19 43.73 o 3 4 0 71808.13 77210.15 594.31 o 4 4 0 95855.63 100728.48 701.28 o 5 4 0 74902.89 76829.23 558.35 o 6 4 0 2008.66 1888.87 59.78 o 7 4 0 514.99 454.92 44.21 o 8 4 0 33157.07 32279.24 340.30 o 9 4 0 4695.61 4829.40 139.77 o 10 4 0 1304.76 1287.89 83.89 o 11 4 0 3265.15 3313.53 114.32 o 12 4 0 215.85 204.50 66.45 o 13 4 0 8870.02 8389.09 211.88 o 14 4 0 2220.47 2194.63 164.72 o 15 4 0 6282.17 6155.90 232.70 o 16 4 0 11594.93 10834.77 271.28 o 17 4 0 4430.17 4041.27 277.88 o 18 4 0 426.52 486.55 100.54 o 19 4 0 158.44 351.29 110.40 o 20 4 0 10.46 176.21 126.99 o 21 4 0 154.26 180.32 136.09 o 22 4 0 170.56 309.79 142.26 o 1 5 0 7561.39 7880.83 106.22 o 2 5 0 10433.59 11535.80 134.94 o 3 5 0 5595.61 5511.51 105.72 o 4 5 0 7790.87 7930.58 112.16 o 5 5 0 17192.69 17307.39 171.59 o 6 5 0 4735.70 5050.94 90.33 o 7 5 0 2919.17 3000.69 77.23 o 8 5 0 514.65 500.13 48.85 o 9 5 0 3796.74 3733.06 117.29 o 10 5 0 82.78 140.27 58.98 o 11 5 0 2940.32 2731.61 118.68 o 12 5 0 271.03 230.23 68.97 o 13 5 0 353.46 288.22 76.23 o 14 5 0 2173.58 2259.35 120.31 o 15 5 0 460.70 423.10 89.05 o 16 5 0 490.11 456.20 94.75 o 17 5 0 957.42 1277.61 133.46 o 18 5 0 379.83 330.48 129.53 o 19 5 0 1003.76 1263.54 164.62 o 20 5 0 150.20 293.72 135.79 o 21 5 0 167.04 302.29 141.77 o 22 5 0 193.61 188.44 244.25 o 0 6 0 163985.33 174933.06 2746.79 o 1 6 0 8262.55 9558.06 156.37 o 2 6 0 93721.13 98945.72 1121.86 o 3 6 0 27.06 -29.01 29.01 o 4 6 0 104424.17 103371.84 823.37 o 5 6 0 36781.46 36650.16 302.65 o 6 6 0 1561.93 1604.37 54.35 o 7 6 0 528.74 514.04 42.49 o 8 6 0 32962.65 32848.19 306.53 o 9 6 0 886.57 963.08 72.39 o 10 6 0 33950.33 33310.47 374.77 o 11 6 0 11388.05 10847.59 204.03 o 12 6 0 6275.26 6438.50 157.27 o 13 6 0 6895.15 6578.73 167.04 o 14 6 0 684.38 809.22 91.19 o 15 6 0 317.96 154.36 83.18 o 16 6 0 6717.64 6078.49 232.19 o 17 6 0 5173.89 5407.51 236.55 o 18 6 0 182.35 175.29 114.83 o 19 6 0 903.59 1177.39 162.78 o 20 6 0 4.15 34.50 117.50 o 21 6 0 20.94 -91.88 223.59 o 1 7 0 869.79 982.34 61.48 o 2 7 0 10024.21 10744.76 211.26 o 3 7 0 12983.24 14011.82 155.92 o 4 7 0 680.50 747.04 43.06 o 5 7 0 415.62 376.30 39.09 o 6 7 0 1333.87 1350.06 51.40 o 7 7 0 357.71 385.18 38.89 o 8 7 0 654.42 702.93 52.09 o 9 7 0 90.26 86.27 47.00 o 10 7 0 1566.34 1647.13 92.12 o 11 7 0 609.37 711.73 82.03 o 12 7 0 1042.16 1279.36 90.04 o 13 7 0 2315.57 2483.05 113.66 o 14 7 0 301.60 197.09 96.57 o 15 7 0 23.75 -65.47 92.60 o 16 7 0 259.24 134.12 107.00 o 17 7 0 134.18 -43.78 110.93 o 18 7 0 141.35 185.67 121.18 o 19 7 0 17.07 201.20 124.58 o 20 7 0 92.56 117.98 116.65 o 21 7 0 131.85 70.31 131.44 o 0 8 0 3435.87 3480.30 149.58 o 1 8 0 6357.84 6492.26 142.78 o 2 8 0 97127.32 98187.71 1311.79 o 3 8 0 21404.70 22325.94 279.32 o 4 8 0 31162.83 31422.50 332.43 o 5 8 0 1656.50 1624.92 76.13 o 6 8 0 8711.51 8914.42 120.51 o 7 8 0 14.55 5.56 30.25 o 8 8 0 15.77 -41.32 41.32 o 9 8 0 7119.09 7264.91 130.46 o 10 8 0 57498.43 57279.48 550.95 o 11 8 0 13957.88 13597.53 262.31 o 12 8 0 6.41 -78.47 91.38 o 13 8 0 549.47 523.68 99.74 o 14 8 0 2222.68 2161.81 145.04 o 15 8 0 306.23 406.82 124.37 o 16 8 0 1234.60 1022.02 140.52 o 17 8 0 1256.61 1089.89 150.92 o 18 8 0 1741.95 1721.51 170.31 o 19 8 0 1729.43 1729.13 177.93 o 20 8 0 445.42 675.32 150.37 o 21 8 0 1500.50 1164.54 230.55 o 1 9 0 4692.67 5023.09 134.09 o 2 9 0 52.88 94.72 49.35 o 3 9 0 119.36 67.66 32.45 o 4 9 0 9786.18 9378.46 203.56 o 5 9 0 6444.60 6308.08 131.26 o 6 9 0 1891.69 1988.50 59.62 o 7 9 0 3960.99 3822.61 89.53 o 8 9 0 825.11 829.58 65.59 o 9 9 0 266.98 83.52 63.99 o 10 9 0 909.63 840.54 110.35 o 11 9 0 207.71 200.57 90.82 o 12 9 0 4447.19 4565.24 195.06 o 13 9 0 2098.13 2087.19 143.03 o 14 9 0 2186.79 2205.90 144.90 o 15 9 0 286.68 162.80 98.44 o 16 9 0 1392.10 1355.01 139.15 o 17 9 0 1180.46 964.77 149.70 o 18 9 0 1283.25 1684.73 373.45 o 19 9 0 3448.76 3435.42 301.62 o 20 9 0 135.82 560.36 196.22 o 21 9 0 673.97 1009.67 684.82 o 0 10 0 46034.08 47000.78 833.73 o 1 10 0 30804.83 30780.91 399.90 o 2 10 0 134.40 104.16 57.53 o 3 10 0 755.33 911.26 85.78 o 4 10 0 148.23 188.81 45.27 o 5 10 0 41.65 56.61 44.62 o 6 10 0 499.11 579.44 61.66 o 7 10 0 205.66 228.61 47.49 o 8 10 0 1562.65 1514.19 105.41 o 9 10 0 3531.68 3891.62 164.22 o 10 10 0 5665.14 5675.60 198.26 o 11 10 0 3983.25 4209.88 203.45 o 12 10 0 12799.94 12639.98 305.40 o 13 10 0 1651.41 1779.42 134.24 o 14 10 0 281.94 351.93 98.09 o 15 10 0 4335.92 4665.96 368.23 o 16 10 0 598.31 709.49 163.36 o 17 10 0 479.44 604.38 239.03 o 18 10 0 576.70 580.84 181.12 o 19 10 0 152.01 293.11 176.42 o 20 10 0 562.96 651.02 199.73 o 1 11 0 14096.28 14020.00 310.25 o 2 11 0 2931.21 2812.43 124.88 o 3 11 0 128.44 99.00 77.15 o 4 11 0 525.33 605.25 61.86 o 5 11 0 87.44 94.91 50.14 o 6 11 0 251.15 189.44 64.45 o 7 11 0 54.30 -40.10 58.45 o 8 11 0 99.66 137.34 73.39 o 9 11 0 81.28 55.65 82.67 o 10 11 0 6035.43 6152.16 287.80 o 11 11 0 4413.06 4526.33 274.43 o 12 11 0 1742.00 1954.77 266.58 o 13 11 0 5142.61 5580.07 252.57 o 14 11 0 176.34 292.31 135.63 o 15 11 0 1936.27 1962.62 188.53 o 16 11 0 41.85 169.61 142.68 o 17 11 0 9.23 196.66 195.80 o 18 11 0 840.14 674.63 194.91 o 19 11 0 755.51 839.56 207.99 o 20 11 0 71.98 619.16 356.66 o 0 12 0 9269.84 8593.30 500.75 o 1 12 0 493.93 586.67 87.64 o 2 12 0 19238.36 18325.49 386.49 o 3 12 0 1060.18 1229.64 139.35 o 4 12 0 8924.59 8699.82 224.96 o 5 12 0 13881.34 12494.33 542.48 o 6 12 0 52220.65 49966.98 953.51 o 7 12 0 18115.59 16857.87 509.11 o 8 12 0 5795.51 5391.25 316.98 o 9 12 0 11619.64 10972.81 439.18 o 10 12 0 1971.73 1897.16 236.33 o 11 12 0 2579.89 2497.58 225.74 o 12 12 0 1707.40 1924.52 172.68 o 13 12 0 55.26 83.96 127.88 o 14 12 0 2751.89 2775.99 214.11 o 15 12 0 4416.72 4212.93 251.93 o 16 12 0 314.90 149.20 148.44 o 17 12 0 170.99 325.94 164.72 o 18 12 0 2579.83 3153.87 287.99 o 19 12 0 509.36 93.26 543.47 o 1 13 0 113.73 -45.86 86.36 o 2 13 0 3610.59 3468.67 188.08 o 3 13 0 41.78 -11.21 89.62 o 4 13 0 3295.49 3166.61 195.93 o 5 13 0 6834.63 6415.91 258.86 o 6 13 0 5.42 113.63 158.41 o 7 13 0 14226.96 13488.89 463.80 o 8 13 0 3455.11 3687.39 275.35 o 9 13 0 124.20 113.82 157.52 o 10 13 0 1161.12 1069.03 215.99 o 11 13 0 727.23 722.64 351.85 o 12 13 0 256.20 458.81 147.63 o 13 13 0 88.91 130.10 142.09 o 14 13 0 755.26 972.56 191.23 o 15 13 0 6.31 220.40 162.73 o 16 13 0 177.24 86.77 162.74 o 17 13 0 31.80 272.78 224.14 o 18 13 0 66.35 203.16 262.39 o 19 13 0 356.35 772.40 307.73 o 0 14 0 36433.23 34693.26 1158.17 o 1 14 0 771.63 580.07 132.30 o 2 14 0 14344.68 13776.12 355.74 o 3 14 0 18875.93 17589.00 414.20 o 4 14 0 188.21 117.94 104.01 o 5 14 0 1127.77 1270.46 157.37 o 6 14 0 17818.94 17681.34 512.32 o 7 14 0 3339.03 3539.21 274.12 o 8 14 0 1063.33 1160.94 354.39 o 9 14 0 1377.33 894.94 259.06 o 10 14 0 4303.13 4847.21 343.19 o 11 14 0 123.32 -1.24 174.80 o 12 14 0 2122.37 2326.93 296.04 o 13 14 0 38.87 215.78 156.46 o 14 14 0 7801.62 8292.12 362.36 o 15 14 0 6082.87 5820.17 331.92 o 16 14 0 168.86 778.51 255.93 o 17 14 0 190.01 195.93 236.07 o 18 14 0 544.07 155.73 222.47 o 1 15 0 4890.29 4608.88 320.70 o 2 15 0 4981.46 4675.88 314.06 o 3 15 0 0.63 -88.97 88.97 o 4 15 0 443.07 302.49 118.13 o 5 15 0 505.14 301.56 121.13 o 6 15 0 981.15 985.49 172.90 o 7 15 0 58.75 -44.77 212.94 o 8 15 0 136.74 209.02 165.88 o 9 15 0 887.77 804.74 397.71 o 10 15 0 54.69 -97.56 299.96 o 11 15 0 43.74 101.58 206.63 o 12 15 0 48.14 3.30 136.46 o 13 15 0 562.40 603.79 179.45 o 14 15 0 2117.28 2463.35 388.11 o 15 15 0 976.74 1126.85 213.14 o 16 15 0 708.04 733.52 206.22 o 17 15 0 945.51 655.84 208.43 o 0 16 0 271.82 35.37 199.17 o 1 16 0 639.51 615.45 180.60 o 2 16 0 2184.81 2359.30 260.04 o 3 16 0 2905.90 2796.66 277.21 o 4 16 0 561.69 793.20 193.03 o 5 16 0 1154.40 1234.28 304.92 o 6 16 0 1165.09 1278.38 169.08 o 7 16 0 71.53 48.96 119.86 o 8 16 0 2639.31 2907.48 233.44 o 9 16 0 862.36 671.88 284.67 o 10 16 0 2803.42 3032.96 318.16 o 11 16 0 1035.73 1314.64 255.47 o 12 16 0 232.02 643.43 246.21 o 13 16 0 82.06 401.82 427.37 o 14 16 0 235.45 541.18 179.74 o 15 16 0 322.09 508.25 221.45 o 16 16 0 1.30 259.75 200.68 o 1 17 0 832.77 899.12 325.08 o 2 17 0 1461.67 1610.33 335.00 o 3 17 0 1766.92 1780.01 254.49 o 4 17 0 322.35 478.73 187.03 o 5 17 0 106.82 -44.75 393.52 o 6 17 0 64.70 10.55 145.04 o 7 17 0 1.66 -77.11 118.00 o 8 17 0 2943.51 3111.95 246.84 o 9 17 0 1923.25 2445.39 232.53 o 10 17 0 232.83 694.81 486.59 o 11 17 0 996.28 1092.57 253.51 o 12 17 0 22.56 -211.84 211.84 o 13 17 0 87.41 5.51 443.00 o 14 17 0 203.35 521.46 286.53 o 15 17 0 1338.03 822.19 310.54 o 0 18 0 451.31 -91.14 204.42 o 1 18 0 4877.59 4659.34 357.60 o 2 18 0 9051.76 8921.31 559.29 o 3 18 0 148.89 -61.26 156.34 o 4 18 0 3106.73 3658.84 336.96 o 5 18 0 445.24 399.95 200.58 o 6 18 0 4080.28 4728.46 498.44 o 7 18 0 2063.07 2111.39 297.66 o 8 18 0 774.02 638.79 232.52 o 9 18 0 176.51 180.06 469.70 o 10 18 0 4745.01 4658.63 462.00 o 11 18 0 4641.66 4969.28 745.79 o 12 18 0 257.76 744.26 472.61 o 13 18 0 82.89 321.90 424.11 o 14 18 0 642.03 1293.73 465.24 o 1 19 0 21.82 423.63 184.95 o 2 19 0 656.08 1316.85 248.19 o 3 19 0 2449.48 2359.83 640.22 o 4 19 0 232.98 -147.30 248.81 o 5 19 0 834.77 1142.08 258.10 o 6 19 0 358.13 164.28 201.39 o 7 19 0 20.25 317.03 205.90 o 8 19 0 245.66 398.81 219.78 o 9 19 0 1278.12 1751.37 545.36 o 10 19 0 353.38 375.28 400.39 o 11 19 0 100.30 -198.41 198.41 o 12 19 0 159.33 -85.08 214.62 o 13 19 0 13.25 301.17 252.98 o 0 20 0 680.61 -54.89 245.74 o 1 20 0 348.48 16.23 189.74 o 2 20 0 4090.18 3851.23 374.13 o 3 20 0 39.98 175.20 197.76 o 4 20 0 3441.49 3074.16 345.95 o 5 20 0 2406.85 2713.09 459.44 o 6 20 0 531.77 554.58 239.77 o 7 20 0 9.44 -190.96 190.96 o 8 20 0 1780.38 2197.71 335.82 o 9 20 0 2.99 516.94 962.93 o 10 20 0 1763.51 1082.88 302.73 o 11 20 0 671.05 897.62 287.53 o 12 20 0 113.67 -58.11 220.97 o 1 21 0 199.83 164.39 232.82 o 2 21 0 169.36 505.37 269.20 o 3 21 0 1462.75 2364.37 325.93 o 4 21 0 190.03 224.11 205.86 o 5 21 0 488.95 1093.64 273.47 o 6 21 0 274.31 662.01 248.27 o 7 21 0 172.39 -84.07 198.66 o 8 21 0 47.09 496.19 439.09 o 9 21 0 180.93 230.29 294.01 o 10 21 0 938.72 696.79 273.00 o 0 22 0 38.99 192.64 287.49 o 1 22 0 174.62 434.57 393.79 o 2 22 0 2.37 -158.11 163.10 o 3 22 0 199.32 295.73 338.72 o 4 22 0 1447.95 1427.63 464.04 o 5 22 0 1093.63 632.75 482.60 o 6 22 0 1502.63 1557.41 306.93 o 7 22 0 1419.68 2067.60 346.06 o 8 22 0 58.23 274.03 823.31 o 1 23 0 20.01 280.79 216.94 o 2 23 0 7.68 512.29 609.07 o 3 23 0 2.51 -218.96 218.96 o 4 23 0 571.01 528.30 647.86 o 5 23 0 459.19 719.90 258.63 o 6 23 0 321.58 211.20 227.69 o -22 1 1 466.92 434.00 127.81 o -21 1 1 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