#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/47/2224784.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224784_Fobs loop_ _publ_author_name 'Foucher, Daniel' 'Wylie, Stephen' 'Acosta, Joshua' 'Lough, Alan J.' _publ_section_title ; 3-Amino-1-methylpyrazin-1-ium chloride ; _journal_coeditor_code TK2586 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o61 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.3164 _cell_length_b 9.5029 _cell_length_c 12.3877 _exptl_crystal_F_000 608.00 _reflns_d_resolution_high 0.7705 _[local]_cod_data_source_file tk2586Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' k08109a in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 135.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 77.77 40.23 2.34 o 4 0 0 18308.09 17702.94 292.68 o 6 0 0 1900.42 1733.68 35.53 o 8 0 0 2080.09 2179.70 53.29 o 10 0 0 2194.50 2265.77 82.92 o 12 0 0 8.26 -1.08 15.78 o 14 0 0 229.29 190.46 32.47 o 2 1 0 790.60 709.44 13.32 o 4 1 0 6104.80 5969.88 85.56 o 6 1 0 1413.83 1353.71 24.57 o 8 1 0 1605.04 1573.89 31.85 o 10 1 0 3884.10 4292.27 86.79 o 12 1 0 450.46 462.50 49.05 o 14 1 0 1331.36 1598.46 80.83 o 0 2 0 252.18 309.41 14.70 o 2 2 0 286.17 297.65 7.13 o 4 2 0 16364.52 16263.10 242.39 o 6 2 0 465.47 421.38 10.51 o 8 2 0 671.08 684.45 16.53 o 10 2 0 492.88 465.69 16.64 o 12 2 0 62.67 35.15 10.94 o 14 2 0 13.17 -4.21 27.69 o 2 3 0 2.88 4.34 1.53 o 4 3 0 318.72 328.62 8.25 o 6 3 0 3027.46 3110.72 50.68 o 8 3 0 155.12 134.10 8.44 o 10 3 0 274.92 295.01 16.91 o 12 3 0 69.17 53.76 12.60 o 14 3 0 316.31 317.15 89.32 o 0 4 0 2283.60 2276.23 77.24 o 2 4 0 396.92 410.44 9.54 o 4 4 0 3.68 11.04 2.40 o 6 4 0 59.06 68.13 5.95 o 8 4 0 219.90 197.73 7.47 o 10 4 0 0.74 -5.38 5.38 o 12 4 0 298.50 308.94 22.93 o 2 5 0 440.83 490.60 12.10 o 4 5 0 9.37 1.15 6.44 o 6 5 0 34.51 28.84 2.68 o 8 5 0 65.14 43.32 4.07 o 10 5 0 8.35 -1.54 5.32 o 12 5 0 387.46 422.99 35.60 o 0 6 0 601.79 618.69 22.06 o 2 6 0 2.67 2.96 1.64 o 4 6 0 30.85 13.79 7.00 o 6 6 0 76.42 61.39 17.91 o 8 6 0 601.40 601.66 14.71 o 10 6 0 195.16 154.84 33.32 o 12 6 0 0.00 -1.38 20.34 o 2 7 0 18.04 12.97 3.20 o 4 7 0 242.62 207.95 14.04 o 6 7 0 354.23 315.53 19.13 o 8 7 0 136.54 103.08 27.28 o 10 7 0 437.62 447.24 36.37 o 12 7 0 103.82 55.27 54.78 o 0 8 0 847.54 862.11 35.06 o 2 8 0 1968.58 2260.39 45.25 o 4 8 0 1365.56 1487.55 49.87 o 6 8 0 862.35 918.53 70.97 o 8 8 0 483.11 484.43 36.65 o 10 8 0 16.22 30.45 26.60 o 2 9 0 174.91 177.72 9.05 o 4 9 0 626.82 657.23 34.90 o 6 9 0 70.20 61.94 12.18 o 8 9 0 1152.25 1314.20 86.35 o 10 9 0 318.31 317.71 48.79 o 0 10 0 1229.71 1316.69 68.45 o 2 10 0 1603.26 1670.38 105.23 o 4 10 0 81.42 78.23 21.18 o 6 10 0 375.39 381.72 33.67 o 8 10 0 124.96 113.24 32.01 o 2 11 0 35.49 21.58 9.99 o 4 11 0 27.05 19.82 15.46 o 6 11 0 409.81 415.77 46.26 o 0 12 0 206.55 192.72 40.40 o 2 12 0 695.15 677.63 74.35 o 1 1 1 5.08 15.03 0.73 o 2 1 1 4173.12 3943.76 43.90 o 3 1 1 326.17 322.59 5.05 o 4 1 1 189.00 173.25 3.54 o 5 1 1 371.68 338.75 5.66 o 6 1 1 2413.93 2619.44 28.85 o 7 1 1 5.68 6.95 2.07 o 8 1 1 568.09 565.47 10.48 o 9 1 1 111.94 109.16 7.22 o 10 1 1 0.64 -4.02 4.02 o 11 1 1 225.85 217.56 11.39 o 12 1 1 1.78 -4.15 7.12 o 13 1 1 3.01 12.33 11.25 o 14 1 1 13.74 -0.82 14.96 o 0 2 1 7391.48 7067.45 106.60 o 1 2 1 0.32 -0.35 0.51 o 2 2 1 17235.40 16553.26 208.24 o 3 2 1 688.47 666.43 9.66 o 4 2 1 461.27 451.39 7.56 o 5 2 1 836.88 802.34 10.98 o 6 2 1 939.13 1004.95 14.23 o 7 2 1 213.18 193.71 5.68 o 8 2 1 189.81 186.29 6.18 o 9 2 1 1019.08 1065.03 17.83 o 10 2 1 43.84 39.16 4.77 o 11 2 1 172.40 152.47 8.56 o 12 2 1 346.22 355.83 22.80 o 13 2 1 353.09 338.40 17.95 o 14 2 1 0.01 -7.19 11.37 o 1 3 1 10437.91 10266.61 114.44 o 2 3 1 4452.78 4634.89 68.53 o 3 3 1 678.82 584.15 27.75 o 4 3 1 14.85 23.61 1.94 o 5 3 1 3211.21 3231.15 38.53 o 6 3 1 22.85 6.85 1.96 o 7 3 1 253.16 221.57 6.55 o 8 3 1 50.31 48.48 4.13 o 9 3 1 247.19 230.14 7.36 o 10 3 1 44.97 41.24 4.38 o 11 3 1 126.05 106.55 10.99 o 12 3 1 1276.86 1414.25 40.02 o 13 3 1 48.95 30.96 13.28 o 14 3 1 32.50 31.78 12.28 o 0 4 1 2.39 -0.54 1.61 o 1 4 1 1183.75 1210.60 16.35 o 2 4 1 1170.37 1130.04 18.96 o 3 4 1 6.02 0.11 2.07 o 4 4 1 747.57 784.41 15.32 o 5 4 1 2756.22 2906.26 35.69 o 6 4 1 0.18 -0.29 1.99 o 7 4 1 1018.10 1002.35 16.85 o 8 4 1 115.93 108.62 4.89 o 9 4 1 1644.07 1793.36 27.65 o 10 4 1 1.20 7.11 3.58 o 11 4 1 1019.25 1115.86 27.97 o 12 4 1 197.80 175.47 21.61 o 13 4 1 592.39 738.65 49.42 o 1 5 1 2814.30 2845.77 35.45 o 2 5 1 200.96 211.82 6.02 o 3 5 1 6711.90 7066.44 96.45 o 4 5 1 261.34 267.25 6.99 o 5 5 1 1814.85 1832.11 28.03 o 6 5 1 0.81 1.97 2.61 o 7 5 1 1405.55 1450.10 23.93 o 8 5 1 601.38 612.54 11.54 o 9 5 1 174.33 175.01 7.47 o 10 5 1 102.34 82.22 6.04 o 11 5 1 1.18 10.12 6.67 o 12 5 1 6.48 -11.95 11.95 o 13 5 1 14.36 15.83 13.70 o 0 6 1 369.59 359.39 10.09 o 1 6 1 243.82 221.73 6.64 o 2 6 1 344.94 329.69 10.36 o 3 6 1 150.53 155.43 7.10 o 4 6 1 385.28 385.70 8.40 o 5 6 1 950.39 966.48 23.77 o 6 6 1 446.39 456.66 11.08 o 7 6 1 716.64 740.19 14.29 o 8 6 1 1.39 4.44 4.91 o 9 6 1 1094.99 1226.84 24.45 o 10 6 1 75.03 54.97 6.96 o 11 6 1 459.69 512.89 26.77 o 12 6 1 2.07 -1.18 13.77 o 1 7 1 2317.38 2457.94 31.90 o 2 7 1 100.16 106.90 5.26 o 3 7 1 301.66 276.58 10.91 o 4 7 1 29.11 21.24 5.10 o 5 7 1 719.93 733.01 18.55 o 6 7 1 383.26 379.19 12.85 o 7 7 1 113.34 100.78 13.19 o 8 7 1 6.45 -8.04 9.55 o 9 7 1 147.12 124.17 22.32 o 10 7 1 179.03 149.07 24.59 o 11 7 1 15.89 13.73 14.59 o 12 7 1 45.07 52.27 24.25 o 0 8 1 363.32 385.46 14.59 o 1 8 1 36.62 26.14 2.79 o 2 8 1 15.57 9.92 2.46 o 3 8 1 77.68 76.27 6.08 o 4 8 1 310.44 293.03 11.46 o 5 8 1 209.99 183.22 10.37 o 6 8 1 178.60 175.48 15.37 o 7 8 1 121.34 104.50 11.87 o 8 8 1 25.76 12.44 10.06 o 9 8 1 323.91 337.24 22.17 o 10 8 1 124.32 105.70 19.89 o 11 8 1 104.46 89.68 18.95 o 1 9 1 61.02 40.99 3.63 o 2 9 1 179.54 187.40 8.45 o 3 9 1 503.74 526.97 17.35 o 4 9 1 44.40 19.25 6.04 o 5 9 1 68.77 63.08 9.35 o 6 9 1 0.06 -7.24 7.24 o 7 9 1 146.86 168.04 20.90 o 8 9 1 12.79 40.64 21.79 o 9 9 1 11.47 -9.80 13.22 o 10 9 1 85.70 28.17 26.51 o 0 10 1 49.60 38.82 7.79 o 1 10 1 46.76 34.46 6.41 o 2 10 1 91.11 83.31 9.18 o 3 10 1 59.85 66.91 16.53 o 4 10 1 95.20 67.85 15.93 o 5 10 1 37.91 40.34 10.70 o 6 10 1 7.71 -13.28 13.28 o 7 10 1 0.06 25.74 21.27 o 8 10 1 13.23 11.47 18.62 o 1 11 1 7.31 4.49 12.10 o 2 11 1 116.26 98.91 11.52 o 3 11 1 72.84 85.61 9.79 o 4 11 1 5.65 2.38 11.69 o 5 11 1 11.93 -10.24 15.09 o 6 11 1 119.99 87.04 16.47 o 0 12 1 151.69 88.82 24.87 o 1 12 1 3.65 11.03 12.86 o 2 12 1 68.21 59.08 14.16 o 3 12 1 45.01 36.36 26.76 o 0 0 2 4796.51 4366.85 109.54 o 1 0 2 1382.70 1416.80 28.19 o 2 0 2 8120.20 8236.56 141.89 o 3 0 2 1677.75 1732.25 31.16 o 4 0 2 4784.68 4784.44 78.83 o 5 0 2 337.49 415.70 12.43 o 6 0 2 2421.69 2417.19 40.19 o 7 0 2 3684.28 3709.02 58.26 o 8 0 2 71.35 49.52 4.88 o 9 0 2 227.20 226.01 11.98 o 10 0 2 319.43 314.74 12.35 o 11 0 2 1806.86 1916.17 51.35 o 12 0 2 117.22 104.66 28.27 o 13 0 2 153.12 93.49 20.71 o 14 0 2 8.46 18.41 18.08 o 1 1 2 744.18 814.83 11.13 o 2 1 2 226.78 245.24 4.54 o 3 1 2 5727.80 5723.11 65.90 o 4 1 2 153.29 137.79 3.38 o 5 1 2 0.84 2.80 1.38 o 6 1 2 2273.77 2264.70 25.19 o 7 1 2 1381.21 1355.36 17.23 o 8 1 2 1538.38 1541.52 21.03 o 9 1 2 54.60 52.29 4.41 o 10 1 2 218.78 213.96 9.24 o 11 1 2 72.52 64.15 10.23 o 12 1 2 1207.17 1316.22 39.65 o 13 1 2 47.80 23.27 13.88 o 14 1 2 145.67 138.42 17.85 o 0 2 2 12374.08 11971.15 165.37 o 1 2 2 10601.41 10221.00 100.66 o 2 2 2 11093.05 10922.09 106.84 o 3 2 2 4551.06 4706.42 53.41 o 4 2 2 444.28 362.98 6.76 o 5 2 2 67.32 48.78 2.89 o 6 2 2 216.14 169.88 4.85 o 7 2 2 1757.55 1842.68 23.16 o 8 2 2 1567.41 1588.35 21.94 o 9 2 2 672.90 675.68 13.99 o 10 2 2 252.95 240.42 8.20 o 11 2 2 518.57 528.24 15.96 o 12 2 2 1.39 -8.08 8.54 o 13 2 2 31.61 33.26 11.98 o 14 2 2 79.33 56.79 14.31 o 1 3 2 6456.83 6377.88 68.00 o 2 3 2 2085.03 2143.59 24.46 o 3 3 2 608.51 594.70 8.29 o 4 3 2 593.05 615.17 9.75 o 5 3 2 2049.33 2185.45 27.91 o 6 3 2 112.87 78.63 4.03 o 7 3 2 225.24 219.03 6.17 o 8 3 2 413.55 422.80 10.39 o 9 3 2 452.05 428.72 10.62 o 10 3 2 1018.96 1086.07 22.08 o 11 3 2 16.15 9.07 7.88 o 12 3 2 332.49 350.03 16.32 o 13 3 2 0.40 -7.49 8.59 o 14 3 2 117.24 83.00 15.76 o 0 4 2 3044.66 2979.47 49.28 o 1 4 2 3.15 2.80 1.52 o 2 4 2 167.57 189.53 4.43 o 3 4 2 1740.88 1782.98 26.35 o 4 4 2 1746.54 1809.02 73.93 o 5 4 2 204.62 224.93 6.33 o 6 4 2 606.76 633.80 11.06 o 7 4 2 157.37 149.81 5.44 o 8 4 2 0.02 -0.50 2.94 o 9 4 2 14.84 2.88 3.86 o 10 4 2 11.91 15.76 5.66 o 11 4 2 283.55 275.15 13.91 o 12 4 2 21.47 12.11 7.58 o 13 4 2 80.45 60.58 13.21 o 1 5 2 111.73 124.84 5.69 o 2 5 2 558.99 611.50 10.42 o 3 5 2 76.89 69.86 3.40 o 4 5 2 33.83 26.54 3.74 o 5 5 2 0.00 -0.13 2.35 o 6 5 2 29.92 29.16 4.24 o 7 5 2 34.58 26.98 4.14 o 8 5 2 28.14 21.30 3.21 o 9 5 2 42.35 31.58 3.59 o 10 5 2 19.64 12.91 3.76 o 11 5 2 5.97 -2.31 7.37 o 12 5 2 227.99 220.40 18.56 o 13 5 2 25.94 -12.13 15.20 o 0 6 2 55.80 54.82 4.81 o 1 6 2 634.68 676.77 11.20 o 2 6 2 1647.69 1773.98 24.92 o 3 6 2 323.90 321.94 8.03 o 4 6 2 32.15 18.75 2.56 o 5 6 2 1.71 4.26 2.17 o 6 6 2 321.02 322.11 9.16 o 7 6 2 28.39 18.25 3.94 o 8 6 2 291.06 276.30 11.11 o 9 6 2 29.10 31.21 7.33 o 10 6 2 22.70 15.02 7.59 o 11 6 2 59.16 35.82 13.45 o 12 6 2 0.93 -1.70 13.42 o 1 7 2 370.86 374.34 9.40 o 2 7 2 105.14 101.03 4.56 o 3 7 2 198.62 201.65 6.86 o 4 7 2 49.65 37.02 3.47 o 5 7 2 133.55 123.01 10.17 o 6 7 2 178.45 192.31 6.84 o 7 7 2 39.73 30.50 5.82 o 8 7 2 303.29 303.55 21.63 o 9 7 2 69.43 60.08 14.16 o 10 7 2 69.17 52.16 14.06 o 11 7 2 1.06 -10.65 12.19 o 0 8 2 563.39 579.72 16.91 o 1 8 2 3.52 -1.24 2.82 o 2 8 2 577.16 598.82 13.58 o 3 8 2 91.50 87.02 5.01 o 4 8 2 280.13 273.36 10.62 o 5 8 2 454.76 485.76 15.77 o 6 8 2 43.61 38.03 6.75 o 7 8 2 83.93 65.83 11.46 o 8 8 2 28.02 19.59 11.09 o 9 8 2 337.25 365.64 28.13 o 10 8 2 22.94 4.04 13.41 o 11 8 2 10.29 6.92 16.14 o 1 9 2 144.33 134.30 5.81 o 2 9 2 0.81 -2.18 4.11 o 3 9 2 356.71 359.33 10.55 o 4 9 2 156.24 144.07 15.88 o 5 9 2 131.77 117.45 11.84 o 6 9 2 438.28 420.08 18.82 o 7 9 2 55.39 46.51 11.98 o 8 9 2 203.71 197.61 19.11 o 9 9 2 5.37 16.26 14.47 o 0 10 2 962.40 1042.48 39.03 o 1 10 2 291.55 298.59 14.34 o 2 10 2 124.29 138.14 12.75 o 3 10 2 33.94 31.84 8.48 o 4 10 2 1036.92 1145.27 35.75 o 5 10 2 149.93 133.36 14.63 o 6 10 2 364.46 376.36 23.69 o 7 10 2 97.30 75.72 25.75 o 8 10 2 10.01 3.21 16.03 o 1 11 2 657.93 715.98 35.48 o 2 11 2 57.35 24.11 17.11 o 3 11 2 106.33 102.69 15.13 o 4 11 2 149.13 151.57 15.76 o 5 11 2 455.74 494.93 26.92 o 6 11 2 96.19 89.32 16.53 o 0 12 2 1111.37 1098.04 61.01 o 1 12 2 62.31 39.72 13.98 o 2 12 2 152.53 133.21 19.23 o 1 1 3 4019.62 3828.55 51.15 o 2 1 3 754.15 724.18 12.13 o 3 1 3 2788.92 2858.78 34.92 o 4 1 3 1347.26 1403.50 18.67 o 5 1 3 37.25 44.46 2.84 o 6 1 3 159.58 182.97 4.74 o 7 1 3 783.11 840.50 12.71 o 8 1 3 104.35 88.87 4.30 o 9 1 3 25.93 18.44 3.83 o 10 1 3 1137.11 1188.82 21.44 o 11 1 3 527.42 474.10 15.59 o 12 1 3 0.09 -4.91 7.38 o 13 1 3 0.03 3.47 9.34 o 14 1 3 87.25 47.95 16.61 o 0 2 3 7357.65 7529.48 108.77 o 1 2 3 113.94 117.74 2.97 o 2 2 3 790.21 762.95 10.85 o 3 2 3 0.93 -1.16 1.24 o 4 2 3 269.66 143.12 23.25 o 5 2 3 101.52 90.59 4.36 o 6 2 3 705.33 714.59 11.98 o 7 2 3 1490.53 1476.24 20.80 o 8 2 3 114.56 92.20 4.88 o 9 2 3 1.75 -1.04 3.74 o 10 2 3 182.05 179.37 7.53 o 11 2 3 431.28 462.95 21.93 o 12 2 3 54.34 25.95 15.75 o 13 2 3 116.31 95.46 16.40 o 14 2 3 41.43 18.00 19.25 o 1 3 3 19.05 19.32 1.63 o 2 3 3 0.05 0.43 1.11 o 3 3 3 4841.20 4973.45 61.61 o 4 3 3 169.58 144.64 4.68 o 5 3 3 147.54 117.06 6.23 o 6 3 3 1362.95 1388.26 21.88 o 7 3 3 1112.00 1172.72 17.50 o 8 3 3 1095.13 1151.97 18.16 o 9 3 3 53.52 43.13 4.23 o 10 3 3 742.15 750.76 20.76 o 11 3 3 37.75 24.10 6.02 o 12 3 3 157.00 156.47 12.73 o 13 3 3 9.41 5.05 9.70 o 0 4 3 6103.73 6376.25 100.23 o 1 4 3 84.42 75.07 3.23 o 2 4 3 1567.19 1463.46 18.68 o 3 4 3 1430.22 1452.21 19.95 o 4 4 3 4664.61 4860.25 56.04 o 5 4 3 20.47 29.64 2.74 o 6 4 3 1810.72 1815.40 25.49 o 7 4 3 547.90 578.31 12.17 o 8 4 3 0.22 -2.26 2.73 o 9 4 3 139.79 126.19 6.40 o 10 4 3 316.03 282.97 11.20 o 11 4 3 250.04 266.96 14.13 o 12 4 3 11.52 18.96 8.77 o 13 4 3 129.49 142.27 20.53 o 1 5 3 2913.39 3069.45 37.22 o 2 5 3 26.67 26.80 2.09 o 3 5 3 1.24 -0.66 0.66 o 4 5 3 2866.67 2951.89 42.70 o 5 5 3 19.18 14.93 3.29 o 6 5 3 386.07 376.89 10.75 o 7 5 3 7.66 3.14 2.18 o 8 5 3 1002.90 1066.00 24.48 o 9 5 3 233.56 218.27 8.17 o 10 5 3 778.49 858.18 23.21 o 11 5 3 17.71 11.25 8.18 o 12 5 3 443.39 459.48 33.09 o 13 5 3 142.40 143.97 18.10 o 0 6 3 951.92 821.51 18.75 o 1 6 3 1.88 -1.19 1.72 o 2 6 3 3907.62 4066.64 52.14 o 3 6 3 194.67 175.97 7.13 o 4 6 3 344.74 304.56 8.85 o 5 6 3 226.23 214.05 7.08 o 6 6 3 1025.06 1091.65 22.33 o 7 6 3 383.30 369.81 13.95 o 8 6 3 198.40 197.57 12.58 o 9 6 3 290.82 282.70 14.18 o 10 6 3 81.17 84.64 10.13 o 11 6 3 340.10 336.60 24.76 o 12 6 3 2.28 4.01 12.72 o 1 7 3 211.19 191.12 6.21 o 2 7 3 561.95 584.77 11.06 o 3 7 3 1467.15 1611.52 28.71 o 4 7 3 7.44 4.58 3.55 o 5 7 3 1610.15 1681.79 32.09 o 6 7 3 562.19 606.55 19.77 o 7 7 3 283.83 262.81 12.21 o 8 7 3 511.09 545.34 17.93 o 9 7 3 10.37 -1.19 10.12 o 10 7 3 239.38 231.94 20.93 o 11 7 3 4.32 12.33 13.47 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870.78 834.96 26.27 o 1 0 4 61.99 53.12 3.97 o 2 0 4 3859.37 4100.07 76.58 o 3 0 4 653.16 587.64 21.60 o 4 0 4 1372.16 1702.68 31.79 o 5 0 4 2501.82 2430.52 44.16 o 6 0 4 290.25 280.90 10.35 o 7 0 4 2574.29 2698.20 53.31 o 8 0 4 21.75 23.62 4.78 o 9 0 4 4047.24 4490.97 81.37 o 10 0 4 94.99 85.55 10.48 o 11 0 4 1244.92 1317.15 41.38 o 12 0 4 154.62 145.45 18.28 o 13 0 4 450.43 516.92 64.84 o 14 0 4 1.25 0.26 18.07 o 1 1 4 14469.00 14226.95 165.31 o 2 1 4 137.22 121.68 3.95 o 3 1 4 3367.09 3176.67 41.75 o 4 1 4 169.02 165.67 7.05 o 5 1 4 6001.07 6408.81 80.08 o 6 1 4 21.83 13.76 2.86 o 7 1 4 576.07 522.90 9.90 o 8 1 4 28.74 34.13 3.57 o 9 1 4 910.85 946.43 16.02 o 10 1 4 311.68 301.09 13.90 o 11 1 4 22.70 23.27 5.81 o 12 1 4 9.88 5.44 7.61 o 13 1 4 16.48 17.54 12.77 o 14 1 4 30.15 12.64 13.79 o 0 2 4 893.04 955.89 19.62 o 1 2 4 26.19 26.79 2.09 o 2 2 4 196.35 194.46 4.41 o 3 2 4 2125.95 2102.51 26.01 o 4 2 4 119.59 120.84 3.80 o 5 2 4 1343.71 1350.81 19.66 o 6 2 4 1490.20 1524.53 22.33 o 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