#------------------------------------------------------------------------------ #$Date: 2010-02-13 12:42:52 +0200 (Sat, 13 Feb 2010) $ #$Revision: 986 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224804.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224804_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Mason, Jennifer M.' 'Gulab, Shivali A.' _publ_section_title ; 7-Benzyloxymethyl-9-bromo-6-chloro-9-deazapurine ; _journal_coeditor_code WN2368 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o138 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 86.111 _cell_angle_beta 84.564 _cell_angle_gamma 89.037 _cell_length_a 7.8999 _cell_length_b 11.5023 _cell_length_c 15.5571 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.6706 _[local]_cod_data_source_file wn2368Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sgta in P-1 relabelled/cell 4aug09' _shelx_refln_list_code 4 _shelx_f_calc_maximum 307.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 99.03 163.78 10.69 o 3 0 0 460.58 462.88 16.77 o 4 0 0 4361.83 4244.34 75.84 o 5 0 0 554.07 520.54 26.77 o 6 0 0 2799.39 2804.89 63.31 o 7 0 0 283.49 271.80 28.96 o 8 0 0 312.12 330.88 45.54 o 9 0 0 195.76 156.30 55.38 o 10 0 0 57.90 88.14 59.17 o 11 0 0 27.23 53.52 62.54 o -11 1 0 510.46 549.62 91.04 o -10 1 0 249.46 241.47 65.96 o -9 1 0 152.12 89.12 58.45 o -8 1 0 872.29 854.40 103.21 o -7 1 0 1656.62 1494.02 45.96 o -6 1 0 35.53 39.30 9.08 o -5 1 0 6660.67 6578.00 85.27 o -4 1 0 4030.42 4075.50 54.35 o -3 1 0 637.56 654.79 13.52 o -2 1 0 6221.78 6575.33 61.16 o -1 1 0 2840.94 2810.74 71.91 o 1 1 0 422.43 455.71 9.78 o 2 1 0 3522.19 3760.50 51.08 o 3 1 0 22.32 18.59 9.60 o 4 1 0 1148.33 1107.49 30.56 o 5 1 0 57.33 90.74 15.92 o 6 1 0 268.52 221.19 22.48 o 7 1 0 143.16 140.44 23.04 o 8 1 0 4017.64 3937.12 105.47 o 9 1 0 1.88 -3.88 55.28 o 10 1 0 237.78 347.53 104.26 o -11 2 0 683.74 800.07 124.80 o -10 2 0 0.41 18.03 55.72 o -9 2 0 825.28 834.62 147.96 o -8 2 0 365.09 371.77 25.06 o -7 2 0 1835.17 1799.88 48.27 o -6 2 0 3027.47 3081.85 59.36 o -5 2 0 3277.61 3296.55 56.52 o -4 2 0 34.30 61.72 8.85 o -3 2 0 5791.50 5975.49 84.14 o -2 2 0 15825.75 16598.74 196.68 o -1 2 0 7326.44 7228.02 92.26 o 0 2 0 346.26 357.71 12.87 o 1 2 0 243.66 265.03 6.71 o 2 2 0 4019.96 4284.74 43.58 o 3 2 0 11233.94 11627.73 147.06 o 4 2 0 2460.78 2486.38 41.74 o 5 2 0 1844.52 1833.61 45.34 o 6 2 0 260.43 277.40 23.24 o 7 2 0 2875.10 2706.03 66.22 o 8 2 0 63.51 82.66 30.21 o 9 2 0 48.35 56.69 48.69 o 10 2 0 719.89 881.47 120.06 o -11 3 0 71.79 -21.19 64.77 o -10 3 0 9.63 18.59 21.54 o -9 3 0 77.32 77.90 21.25 o -8 3 0 302.21 308.90 26.57 o -7 3 0 5406.16 5323.55 107.56 o -6 3 0 7.03 31.64 13.23 o -5 3 0 138.95 153.28 14.20 o -4 3 0 57.10 49.39 8.70 o -3 3 0 141.34 143.49 14.99 o -2 3 0 21.64 19.30 7.41 o -1 3 0 15985.65 15986.97 215.24 o 0 3 0 642.84 657.76 16.56 o 1 3 0 3318.39 3405.30 38.21 o 2 3 0 2836.24 2952.24 35.74 o 3 3 0 2506.60 2482.56 34.14 o 4 3 0 295.10 354.69 12.39 o 5 3 0 3364.57 3417.22 53.43 o 6 3 0 3676.95 3571.13 62.59 o 7 3 0 1289.98 1152.61 63.84 o 8 3 0 978.25 1008.72 51.34 o 9 3 0 852.21 854.37 70.31 o 10 3 0 46.21 142.53 58.32 o 11 3 0 238.45 335.95 109.53 o -11 4 0 342.97 344.55 39.71 o -10 4 0 111.05 65.13 33.49 o -9 4 0 32.17 47.95 38.31 o -8 4 0 92.63 71.22 31.16 o -7 4 0 14.16 -5.30 22.66 o -6 4 0 34.95 30.46 14.49 o -5 4 0 5947.98 6069.89 118.29 o -4 4 0 474.49 546.25 18.93 o -3 4 0 742.15 790.37 22.94 o -2 4 0 243.17 285.47 13.40 o -1 4 0 6826.86 6696.34 95.12 o 0 4 0 522.71 571.49 16.24 o 1 4 0 22244.66 22461.37 295.58 o 2 4 0 1386.85 1404.01 23.23 o 3 4 0 222.31 241.72 10.56 o 4 4 0 6.85 17.87 9.01 o 5 4 0 2731.86 2771.44 46.72 o 6 4 0 141.19 148.39 12.76 o 7 4 0 2245.24 2216.85 41.15 o 8 4 0 28.38 -9.27 26.86 o 9 4 0 667.83 663.36 56.56 o 10 4 0 2.11 -62.87 52.46 o 11 4 0 75.90 -68.45 81.09 o -11 5 0 4.32 11.13 22.46 o -10 5 0 1008.57 1078.34 52.91 o -9 5 0 571.29 642.51 42.08 o -8 5 0 163.33 131.79 27.61 o -7 5 0 338.31 352.87 40.74 o -6 5 0 3092.95 3126.06 84.71 o -5 5 0 504.11 548.58 21.05 o -4 5 0 3141.08 3120.32 57.87 o -3 5 0 2606.29 2694.41 52.99 o -2 5 0 2714.37 2892.66 68.93 o -1 5 0 1240.38 1216.56 30.30 o 0 5 0 2831.64 2855.99 54.09 o 1 5 0 79.15 55.95 9.64 o 2 5 0 1046.84 1159.92 20.30 o 3 5 0 4346.44 4523.30 63.54 o 4 5 0 340.44 411.68 14.81 o 5 5 0 1139.77 1131.83 27.88 o 6 5 0 311.33 337.18 16.71 o 7 5 0 4598.58 4372.12 84.07 o 8 5 0 10.70 12.14 15.06 o 9 5 0 894.66 914.57 82.02 o 10 5 0 0.23 25.11 55.32 o 11 5 0 5.01 3.16 86.36 o -10 6 0 440.89 475.25 41.70 o -9 6 0 3.84 -7.63 27.81 o -8 6 0 448.10 526.43 39.64 o -7 6 0 91.49 71.27 26.06 o -6 6 0 90.38 74.46 25.39 o -5 6 0 84.05 72.33 17.29 o -4 6 0 3366.18 3395.06 63.33 o -3 6 0 109.01 107.11 15.83 o -2 6 0 3754.46 3801.48 75.20 o -1 6 0 6664.47 6393.81 134.39 o 0 6 0 245.02 194.16 19.07 o 1 6 0 3365.79 3432.75 72.15 o 2 6 0 6653.77 6696.37 85.63 o 3 6 0 2.23 1.45 8.96 o 4 6 0 2283.52 2276.48 38.84 o 5 6 0 343.48 351.75 19.50 o 6 6 0 421.33 408.49 23.86 o 7 6 0 1063.91 1109.65 37.20 o 8 6 0 557.20 557.21 28.49 o 9 6 0 13.18 4.60 17.61 o 10 6 0 193.51 131.99 109.53 o 11 6 0 205.97 222.21 102.15 o -10 7 0 18.43 32.10 31.05 o -9 7 0 6.94 68.71 31.33 o -8 7 0 955.74 962.23 51.88 o -7 7 0 142.77 138.50 30.80 o -6 7 0 2281.64 2417.31 77.21 o -5 7 0 1231.31 1165.72 51.78 o -4 7 0 4.72 4.96 16.11 o -3 7 0 671.77 728.09 45.45 o -2 7 0 2560.02 2327.15 59.37 o -1 7 0 495.67 566.43 29.72 o 0 7 0 175.47 134.00 14.40 o 1 7 0 94.90 132.09 11.97 o 2 7 0 221.98 233.65 12.85 o 3 7 0 185.75 169.38 12.23 o 4 7 0 2597.55 2599.42 42.00 o 5 7 0 1153.66 1162.26 39.40 o 6 7 0 1018.52 1036.58 35.92 o 7 7 0 611.70 605.31 41.13 o 8 7 0 12.09 1.94 18.52 o 9 7 0 26.31 18.26 21.46 o 10 7 0 1012.86 1206.43 108.47 o -10 8 0 252.55 296.51 43.32 o -9 8 0 322.56 345.11 41.95 o -8 8 0 10.99 -26.18 28.58 o -7 8 0 209.66 211.70 39.52 o -6 8 0 599.53 615.61 45.91 o -5 8 0 126.01 107.49 28.17 o -4 8 0 3043.58 3077.07 81.63 o -3 8 0 196.84 197.19 25.54 o -2 8 0 2062.85 2082.93 62.62 o -1 8 0 755.65 724.65 35.79 o 0 8 0 6351.73 6174.11 103.68 o 1 8 0 265.36 246.41 15.45 o 2 8 0 5150.83 4948.16 75.57 o 3 8 0 2284.57 2275.19 43.11 o 4 8 0 36.16 48.63 16.41 o 5 8 0 678.85 688.83 29.24 o 6 8 0 1325.36 1254.99 40.88 o 7 8 0 287.39 283.91 26.99 o 8 8 0 1452.87 1516.97 48.06 o 9 8 0 0.56 -32.55 21.87 o 10 8 0 120.86 103.59 23.67 o -9 9 0 370.66 461.65 46.55 o -8 9 0 198.47 160.53 38.63 o -7 9 0 233.26 247.53 38.66 o -6 9 0 394.52 376.16 56.09 o -5 9 0 1566.21 1497.10 95.61 o -4 9 0 342.14 364.90 40.34 o -3 9 0 560.33 605.87 36.76 o -2 9 0 366.93 333.59 31.57 o -1 9 0 173.54 136.99 26.19 o 0 9 0 170.31 200.49 23.61 o 1 9 0 1294.94 1286.78 43.02 o 2 9 0 655.06 645.32 21.96 o 3 9 0 102.85 111.23 14.72 o 4 9 0 823.31 784.08 29.89 o 5 9 0 313.37 331.45 41.84 o 6 9 0 619.47 578.67 42.54 o 7 9 0 101.06 121.53 23.56 o 8 9 0 454.17 447.23 43.33 o 9 9 0 1.38 -18.22 23.11 o 10 9 0 291.88 247.79 31.82 o -9 10 0 527.20 471.39 50.07 o -8 10 0 12.59 43.80 41.04 o -7 10 0 149.07 141.13 38.43 o -6 10 0 15.28 10.31 41.80 o -5 10 0 221.87 162.50 34.86 o -4 10 0 4.02 12.94 43.70 o -3 10 0 4242.54 4010.25 103.96 o -2 10 0 0.56 27.15 26.14 o -1 10 0 587.60 663.32 39.71 o 0 10 0 853.61 847.63 33.29 o 1 10 0 1053.03 1068.17 32.50 o 2 10 0 567.72 590.28 24.58 o 3 10 0 4132.98 4150.07 83.99 o 4 10 0 438.87 403.70 24.16 o 5 10 0 213.15 216.61 22.73 o 6 10 0 281.74 273.24 25.55 o 7 10 0 271.89 273.30 27.47 o 8 10 0 148.26 125.55 28.16 o 9 10 0 318.44 278.42 34.94 o -8 11 0 102.77 69.99 38.23 o -7 11 0 606.47 570.45 77.22 o -6 11 0 37.41 5.71 37.55 o -5 11 0 880.64 900.78 56.76 o -4 11 0 193.91 175.48 48.77 o -3 11 0 161.54 121.95 28.94 o -2 11 0 347.87 361.01 35.60 o -1 11 0 1090.84 1087.31 51.27 o 0 11 0 0.11 25.67 25.06 o 1 11 0 1913.99 1900.02 57.11 o 2 11 0 7.76 10.25 20.17 o 3 11 0 50.10 5.58 21.30 o 4 11 0 1.44 8.92 17.49 o 5 11 0 1268.35 1313.81 43.08 o 6 11 0 246.69 282.10 27.01 o 7 11 0 368.49 403.35 30.97 o 8 11 0 166.12 180.29 30.83 o 9 11 0 45.62 28.04 74.87 o -8 12 0 193.66 190.62 108.47 o -7 12 0 0.38 -27.18 36.21 o -6 12 0 288.41 282.54 47.06 o -5 12 0 346.02 272.48 50.77 o -4 12 0 26.39 66.51 46.15 o -3 12 0 1572.69 1494.24 93.08 o -2 12 0 7.26 -8.41 27.66 o -1 12 0 67.24 76.78 29.30 o 0 12 0 1057.11 1161.88 54.73 o 1 12 0 1345.05 1437.85 45.72 o 2 12 0 389.81 370.96 34.04 o 3 12 0 461.06 541.80 78.27 o 4 12 0 419.49 404.14 49.55 o 5 12 0 22.97 39.20 29.76 o 6 12 0 2.01 13.49 29.99 o 7 12 0 402.46 491.24 43.91 o 8 12 0 5.18 -2.87 29.70 o -7 13 0 150.53 232.60 46.60 o -6 13 0 234.44 301.41 48.07 o -5 13 0 6.60 -0.42 37.53 o -4 13 0 1608.23 1615.96 103.86 o -3 13 0 127.97 97.44 51.24 o -2 13 0 8.21 -24.58 27.97 o -1 13 0 8.02 -9.27 27.80 o 0 13 0 215.66 265.56 36.04 o 1 13 0 9.07 -25.71 24.34 o 2 13 0 661.02 682.60 42.19 o 3 13 0 223.35 242.55 33.34 o 4 13 0 423.26 410.51 38.81 o 5 13 0 446.67 378.85 40.40 o 6 13 0 46.67 35.33 31.95 o 7 13 0 16.98 -16.33 29.81 o -6 14 0 73.67 65.79 43.37 o -5 14 0 39.76 4.95 54.11 o -4 14 0 42.99 107.27 56.22 o -3 14 0 46.52 25.25 55.82 o -2 14 0 547.96 648.51 71.86 o -1 14 0 9.31 21.20 30.35 o 0 14 0 176.24 123.48 51.32 o 1 14 0 405.46 392.88 63.28 o 2 14 0 159.20 187.19 90.04 o 3 14 0 0.24 27.44 63.71 o 4 14 0 1009.67 1061.27 86.64 o 5 14 0 4.27 33.99 49.48 o 6 14 0 15.62 -18.68 46.32 o -5 15 0 2.12 21.15 45.36 o -4 15 0 172.06 171.91 110.05 o -3 15 0 284.50 278.36 119.00 o -2 15 0 23.76 4.71 81.09 o -1 15 0 107.22 68.49 48.25 o 0 15 0 714.29 632.57 75.86 o 1 15 0 1.07 -63.71 49.15 o 2 15 0 357.48 357.69 127.95 o 3 15 0 0.85 -30.80 50.97 o 4 15 0 4.07 27.61 75.83 o 5 15 0 4.84 -34.64 48.39 o -4 16 0 61.86 149.02 57.34 o -3 16 0 3.67 59.61 52.31 o 0 16 0 72.69 144.01 76.35 o 1 16 0 309.18 207.17 72.67 o 2 16 0 608.49 568.49 97.41 o 3 16 0 4.70 -3.16 51.38 o 1 17 0 106.23 -1.01 50.23 o -3 -16 1 0.22 -107.42 71.61 o -2 -16 1 207.90 265.96 69.51 o -1 -16 1 80.32 107.93 57.62 o 0 -16 1 22.53 -58.52 53.71 o 3 -16 1 22.62 132.24 53.80 o -4 -15 1 73.45 81.52 80.04 o -3 -15 1 52.22 0.11 72.14 o -2 -15 1 259.01 213.65 69.51 o -1 -15 1 74.02 64.44 52.31 o 0 -15 1 498.56 503.19 135.85 o 1 -15 1 1.82 -52.41 47.39 o 2 -15 1 0.68 -36.54 76.35 o 3 -15 1 90.69 57.17 51.73 o 4 -15 1 84.73 152.93 57.28 o 5 -15 1 24.11 67.80 51.48 o -6 -14 1 225.47 254.47 57.11 o -5 -14 1 6.76 -17.97 47.92 o -4 -14 1 750.98 882.66 82.26 o -3 -14 1 231.11 240.72 93.20 o -2 -14 1 7.53 20.18 50.23 o -1 -14 1 70.91 65.26 50.81 o 0 -14 1 222.19 288.18 58.70 o 1 -14 1 3.19 -37.11 28.57 o 2 -14 1 1381.73 1481.75 99.31 o 3 -14 1 61.31 17.00 50.02 o 4 -14 1 64.62 24.55 64.24 o 5 -14 1 92.12 49.44 41.13 o 6 -14 1 384.16 301.96 50.48 o -7 -13 1 8.13 -42.73 34.35 o -6 -13 1 69.17 48.12 37.84 o -5 -13 1 856.52 962.75 57.91 o -4 -13 1 39.73 91.98 30.32 o -3 -13 1 449.57 439.66 60.19 o -2 -13 1 612.26 553.81 97.94 o -1 -13 1 60.50 126.18 48.43 o 0 -13 1 26.88 48.92 29.61 o 1 -13 1 324.02 343.13 39.19 o 2 -13 1 109.41 102.44 31.17 o 3 -13 1 127.06 163.00 53.60 o 4 -13 1 476.69 708.70 76.69 o 5 -13 1 33.26 28.15 41.02 o 6 -13 1 57.47 14.16 39.73 o 7 -13 1 46.72 30.88 39.50 o -8 -12 1 28.97 9.24 31.40 o -7 -12 1 244.26 192.00 35.39 o -6 -12 1 1.21 -14.93 28.14 o -5 -12 1 551.07 558.67 61.56 o -4 -12 1 450.28 529.44 38.82 o -3 -12 1 467.30 521.56 37.02 o -2 -12 1 235.99 240.00 30.05 o -1 -12 1 516.74 486.57 29.01 o 0 -12 1 1293.32 1304.92 58.03 o 1 -12 1 87.32 76.38 29.69 o 2 -12 1 202.24 193.22 32.53 o 3 -12 1 918.11 983.57 77.82 o 4 -12 1 88.14 148.33 50.49 o 5 -12 1 388.63 428.16 50.47 o 6 -12 1 192.67 170.82 44.15 o 7 -12 1 152.70 151.40 43.30 o 8 -12 1 109.66 120.06 97.94 o -8 -11 1 63.44 38.87 26.06 o -7 -11 1 399.06 428.69 31.71 o -6 -11 1 160.36 134.64 23.43 o -5 -11 1 1187.56 1205.34 42.70 o -4 -11 1 54.71 49.83 18.33 o -3 -11 1 105.46 87.76 17.57 o -2 -11 1 2153.86 2221.19 55.63 o -1 -11 1 1860.98 1877.52 50.07 o 0 -11 1 0.05 13.19 24.33 o 1 -11 1 1868.24 1936.95 67.76 o 2 -11 1 46.67 26.54 25.28 o 3 -11 1 7.82 -34.42 22.95 o 4 -11 1 0.75 41.02 43.17 o 5 -11 1 779.42 769.93 53.13 o 6 -11 1 4.94 -22.63 33.20 o 7 -11 1 563.26 438.28 50.02 o 8 -11 1 186.22 169.82 41.88 o -9 -10 1 222.64 177.08 29.61 o -8 -10 1 170.41 161.38 27.98 o -7 -10 1 136.14 177.02 25.45 o -6 -10 1 102.91 84.34 22.37 o -5 -10 1 16.69 13.95 18.49 o -4 -10 1 0.88 -11.44 15.70 o -3 -10 1 1600.84 1596.61 47.13 o -2 -10 1 45.50 49.99 12.98 o -1 -10 1 371.68 391.97 17.99 o 0 -10 1 162.78 160.13 15.00 o 1 -10 1 3161.44 3185.77 88.05 o 2 -10 1 71.75 86.70 25.02 o 3 -10 1 3772.50 3687.99 98.46 o 4 -10 1 322.86 311.58 50.23 o 5 -10 1 15.94 2.46 29.73 o 6 -10 1 159.95 125.60 35.38 o 7 -10 1 968.68 982.35 59.94 o 8 -10 1 2.40 20.93 35.79 o 9 -10 1 423.56 513.88 63.37 o -9 -9 1 73.94 45.75 25.76 o -8 -9 1 367.19 360.70 30.11 o -7 -9 1 114.20 125.50 23.08 o -6 -9 1 303.26 282.89 28.10 o -5 -9 1 187.53 135.46 25.10 o -4 -9 1 6455.65 6254.76 110.69 o -3 -9 1 38.98 19.85 12.97 o -2 -9 1 1491.13 1493.22 34.03 o -1 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