#------------------------------------------------------------------------------ #$Date: 2010-02-13 12:42:52 +0200 (Sat, 13 Feb 2010) $ #$Revision: 986 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224823.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224823_Fobs loop_ _publ_author_name 'Hardy, Aaron M.' 'LaDuca, Robert L.' _publ_section_title ; catena-Poly[[diazidozinc(II)]-\m-di-4-pyridylamine-\k^2^N:N'] ; _journal_coeditor_code ZL2257 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.904 _cell_angle_gamma 90.000 _cell_length_a 6.7988 _cell_length_b 16.0105 _cell_length_c 11.7733 _exptl_crystal_F_000 648.00 _reflns_d_resolution_high 0.8296 _[local]_cod_data_source_file zl2257Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21n in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 235.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2070.62 2095.35 56.50 o 4 0 0 783.57 950.77 14.32 o 6 0 0 1284.58 1250.63 29.63 o 8 0 0 1306.59 1310.40 33.15 o 1 1 0 61.32 57.40 1.33 o 2 1 0 1827.30 1902.36 16.34 o 3 1 0 4025.30 4234.01 38.77 o 4 1 0 5917.25 5807.61 53.07 o 5 1 0 51.41 41.82 1.94 o 6 1 0 151.28 142.65 4.03 o 7 1 0 115.66 113.98 4.06 o 8 1 0 14.48 14.30 2.61 o 0 2 0 5924.94 5939.01 103.70 o 1 2 0 14630.57 14072.11 192.58 o 2 2 0 726.42 673.31 6.66 o 3 2 0 1474.80 1460.31 12.90 o 4 2 0 168.75 178.51 2.82 o 5 2 0 77.41 75.83 2.31 o 6 2 0 49.87 49.26 2.53 o 7 2 0 300.67 274.30 6.18 o 8 2 0 202.72 222.68 9.28 o 1 3 0 14913.39 14962.04 164.90 o 2 3 0 27.10 37.84 0.88 o 3 3 0 5542.49 5488.38 46.30 o 4 3 0 30.55 36.16 1.27 o 5 3 0 2885.18 2848.35 29.28 o 6 3 0 40.76 42.40 2.49 o 7 3 0 58.11 53.17 4.87 o 0 4 0 1992.97 2030.40 26.40 o 1 4 0 2805.81 3006.45 27.96 o 2 4 0 1554.84 1714.39 14.00 o 3 4 0 1275.69 1259.10 12.20 o 4 4 0 145.25 158.17 2.40 o 5 4 0 986.22 996.03 11.42 o 6 4 0 943.84 925.18 11.28 o 7 4 0 278.19 263.18 6.08 o 1 5 0 262.36 285.87 4.78 o 2 5 0 8733.33 9188.39 66.76 o 3 5 0 952.36 876.50 7.14 o 4 5 0 3077.65 3035.57 29.35 o 5 5 0 1136.81 1094.51 12.56 o 6 5 0 110.71 104.03 3.15 o 7 5 0 101.28 96.33 3.59 o 0 6 0 5460.32 5380.90 98.69 o 1 6 0 13.49 19.47 1.00 o 2 6 0 8972.18 9107.52 74.77 o 3 6 0 2106.83 2300.09 17.47 o 4 6 0 100.18 104.45 3.63 o 5 6 0 34.42 34.73 1.79 o 6 6 0 1218.56 1212.91 14.21 o 7 6 0 20.24 15.87 2.49 o 1 7 0 8.63 10.34 0.75 o 2 7 0 2051.71 2060.64 17.59 o 3 7 0 543.13 577.79 5.39 o 4 7 0 3192.09 3111.22 28.94 o 5 7 0 2.82 4.78 1.12 o 6 7 0 738.42 768.64 11.27 o 7 7 0 1.19 1.30 2.04 o 0 8 0 2504.01 2348.46 31.27 o 1 8 0 3641.56 3663.04 33.80 o 2 8 0 3429.17 3440.21 25.84 o 3 8 0 57.41 63.09 2.13 o 4 8 0 57.11 68.70 2.25 o 5 8 0 42.90 41.24 2.72 o 6 8 0 624.21 616.24 9.67 o 7 8 0 489.82 518.72 9.07 o 1 9 0 257.28 243.93 3.68 o 2 9 0 444.96 482.94 4.77 o 3 9 0 5354.05 5306.03 48.31 o 4 9 0 263.94 258.92 4.32 o 5 9 0 535.92 545.94 7.52 o 6 9 0 90.56 98.48 3.64 o 7 9 0 369.90 394.64 8.42 o 0 10 0 2783.31 2912.66 38.77 o 1 10 0 1912.75 1853.87 16.65 o 2 10 0 572.11 573.19 6.03 o 3 10 0 1656.01 1632.79 16.40 o 4 10 0 9.54 10.82 1.31 o 5 10 0 224.45 198.33 4.02 o 6 10 0 13.31 6.94 1.75 o 1 11 0 1024.17 1047.28 10.19 o 2 11 0 988.85 1021.87 12.73 o 3 11 0 271.53 260.42 4.70 o 4 11 0 134.86 135.64 3.13 o 5 11 0 678.98 690.43 9.14 o 6 11 0 518.69 544.18 8.63 o 0 12 0 3072.64 2921.38 48.46 o 1 12 0 179.25 197.76 3.17 o 2 12 0 2873.53 2777.28 24.84 o 3 12 0 291.66 305.34 8.38 o 4 12 0 132.68 125.98 3.69 o 5 12 0 6.21 5.45 1.56 o 6 12 0 257.69 268.17 5.60 o 1 13 0 34.80 35.17 1.77 o 2 13 0 275.16 269.39 4.37 o 3 13 0 33.26 39.86 2.31 o 4 13 0 1985.89 2003.25 29.07 o 5 13 0 9.04 7.87 2.21 o 0 14 0 718.86 702.46 12.03 o 1 14 0 580.77 584.30 7.41 o 2 14 0 3.70 4.74 1.36 o 3 14 0 117.65 123.70 3.76 o 4 14 0 14.23 16.52 1.92 o 5 14 0 16.74 17.79 3.60 o 1 15 0 102.72 101.73 3.11 o 2 15 0 10.79 13.31 1.73 o 3 15 0 377.42 375.46 5.91 o 4 15 0 135.24 146.52 5.00 o 5 15 0 1217.76 1196.43 18.81 o 0 16 0 13.29 17.59 2.55 o 1 16 0 1120.06 1113.17 13.64 o 2 16 0 92.07 93.29 3.06 o 3 16 0 594.37 589.69 8.07 o 4 16 0 71.96 69.72 4.64 o 1 17 0 1.81 3.55 1.83 o 2 17 0 384.42 390.63 6.17 o 3 17 0 472.37 482.99 8.65 o 0 18 0 964.58 992.74 22.10 o 1 18 0 2.72 4.77 1.97 o 2 18 0 385.89 408.92 6.99 o 1 19 0 0.49 1.79 2.22 o -7 0 1 507.27 491.15 14.06 o -5 0 1 3890.76 3866.03 50.91 o -3 0 1 1078.84 1175.66 15.96 o -1 0 1 1363.84 1384.59 24.15 o 1 0 1 21829.73 19821.73 483.68 o 3 0 1 7700.77 7883.41 123.97 o 5 0 1 2619.88 2686.26 44.46 o 7 0 1 1000.34 1007.54 25.62 o -8 1 1 13.15 16.58 2.58 o -7 1 1 516.87 496.98 8.79 o -6 1 1 14.42 13.83 1.82 o -5 1 1 1102.68 1076.99 11.00 o -4 1 1 72.01 56.90 1.47 o -3 1 1 1874.33 1701.37 13.87 o -2 1 1 7.97 11.88 0.92 o -1 1 1 3464.97 3729.11 40.14 o 0 1 1 143.68 168.81 3.20 o 1 1 1 139.67 156.71 3.55 o 2 1 1 689.14 681.07 6.73 o 3 1 1 1252.03 1154.25 11.28 o 4 1 1 1847.75 1902.72 19.94 o 5 1 1 7516.97 7527.15 75.55 o 6 1 1 828.70 801.06 21.79 o 7 1 1 614.92 593.53 12.31 o -8 2 1 583.31 637.86 11.31 o -7 2 1 127.12 123.06 4.85 o -6 2 1 2461.61 2371.01 36.76 o -5 2 1 1185.57 1167.96 14.35 o -4 2 1 632.83 634.36 5.84 o -3 2 1 1186.56 1290.35 11.52 o -2 2 1 4355.13 4573.44 36.37 o -1 2 1 293.45 310.80 4.70 o 0 2 1 3475.47 3615.93 44.07 o 1 2 1 3248.12 3520.49 40.93 o 2 2 1 17054.28 16864.52 217.08 o 3 2 1 336.00 283.96 4.90 o 4 2 1 898.03 886.58 9.20 o 5 2 1 63.46 53.07 2.13 o 6 2 1 140.26 138.39 3.91 o 7 2 1 53.75 51.41 3.28 o -8 3 1 164.19 169.94 5.39 o -7 3 1 76.87 77.36 5.92 o -6 3 1 362.31 354.03 6.09 o -5 3 1 22.12 18.62 1.36 o -4 3 1 2256.61 2117.92 18.66 o -3 3 1 164.02 154.90 2.11 o -2 3 1 10452.18 10330.05 96.93 o -1 3 1 147.59 151.60 2.83 o 0 3 1 1245.70 1284.78 32.14 o 1 3 1 198.62 192.11 2.41 o 2 3 1 930.43 988.61 9.82 o 3 3 1 1343.41 1410.88 12.59 o 4 3 1 3576.89 3553.55 33.08 o 5 3 1 274.09 269.73 4.05 o 6 3 1 4296.06 4185.34 47.48 o 7 3 1 17.74 15.69 2.41 o -7 4 1 403.59 370.60 7.44 o -6 4 1 4799.37 4748.47 48.16 o -5 4 1 603.04 598.64 6.82 o -4 4 1 1613.95 1615.05 14.53 o -3 4 1 454.44 516.43 5.21 o -2 4 1 4083.91 4536.23 36.24 o -1 4 1 10407.34 10355.86 82.54 o 0 4 1 7756.74 7463.38 82.10 o 1 4 1 6387.06 6414.75 58.82 o 2 4 1 7840.81 7624.21 77.99 o 3 4 1 661.96 671.65 5.96 o 4 4 1 956.91 906.96 8.67 o 5 4 1 17.18 13.72 1.41 o 6 4 1 440.27 446.78 7.13 o 7 4 1 74.21 78.31 4.25 o -7 5 1 59.44 55.67 3.37 o -6 5 1 168.82 156.87 3.62 o -5 5 1 6.61 6.56 1.27 o -4 5 1 591.08 561.91 6.61 o -3 5 1 6961.82 7154.20 55.84 o -2 5 1 135.55 97.24 1.36 o -1 5 1 5082.97 5111.65 42.54 o 0 5 1 271.33 310.69 3.20 o 1 5 1 4084.85 4396.21 44.84 o 2 5 1 946.33 1114.65 11.22 o 3 5 1 1468.22 1552.39 12.02 o 4 5 1 1200.93 1242.18 11.56 o 5 5 1 2407.77 2339.56 24.51 o 6 5 1 208.37 213.76 4.34 o 7 5 1 784.80 824.76 16.90 o -7 6 1 2519.92 2519.25 31.05 o -6 6 1 2.08 1.46 1.51 o -5 6 1 1352.36 1346.23 13.70 o -4 6 1 6.63 6.76 0.95 o -3 6 1 2143.19 2287.25 18.54 o -2 6 1 585.81 611.47 6.39 o -1 6 1 148.85 117.07 3.86 o 0 6 1 2100.54 2109.39 18.72 o 1 6 1 2012.49 1952.04 18.62 o 2 6 1 8.23 8.27 0.70 o 3 6 1 4321.91 4387.92 34.75 o 4 6 1 5.67 2.86 0.83 o 5 6 1 306.74 300.22 4.72 o 6 6 1 48.40 48.37 2.54 o 7 6 1 70.12 61.53 3.36 o -7 7 1 261.30 266.18 6.16 o -6 7 1 379.39 369.82 6.77 o -5 7 1 1426.76 1348.23 15.30 o -4 7 1 1010.31 1032.14 9.90 o -3 7 1 4125.15 3933.68 31.30 o -2 7 1 675.33 667.16 6.50 o -1 7 1 7167.33 7158.33 64.95 o 0 7 1 6.51 6.94 0.86 o 1 7 1 455.98 425.70 3.91 o 2 7 1 10.55 13.63 0.89 o 3 7 1 3383.32 3510.62 30.45 o 4 7 1 516.81 539.73 7.64 o 5 7 1 1834.14 1867.89 18.33 o 6 7 1 543.01 511.38 11.38 o 7 7 1 1205.82 1249.07 26.75 o -7 8 1 505.26 506.18 13.05 o -6 8 1 362.18 356.75 5.90 o -5 8 1 16.54 12.54 1.51 o -4 8 1 1549.05 1542.90 15.37 o -3 8 1 39.69 49.37 1.66 o -2 8 1 720.48 740.58 6.70 o -1 8 1 1942.96 1966.80 17.33 o 0 8 1 1248.78 1104.94 10.14 o 1 8 1 2983.54 3063.71 24.30 o 2 8 1 3747.61 3728.13 34.68 o 3 8 1 965.31 974.62 8.70 o 4 8 1 615.26 624.90 7.77 o 5 8 1 0.64 0.37 1.25 o 6 8 1 66.68 73.61 3.25 o 7 8 1 74.07 72.24 4.16 o -7 9 1 22.88 28.73 3.07 o -6 9 1 173.50 168.23 4.02 o -5 9 1 0.41 1.71 1.30 o -4 9 1 1655.40 1673.72 16.62 o -3 9 1 541.00 531.94 6.89 o -2 9 1 6496.99 6421.23 51.72 o -1 9 1 36.51 36.12 1.63 o 0 9 1 1059.12 1033.84 9.69 o 1 9 1 402.87 430.81 6.45 o 2 9 1 95.99 90.81 2.09 o 3 9 1 80.66 81.47 1.48 o 4 9 1 2382.40 2401.03 25.39 o 5 9 1 150.35 133.38 3.17 o 6 9 1 1378.56 1414.08 18.61 o 7 9 1 1.42 -0.37 3.04 o -6 10 1 1487.02 1493.10 17.41 o -5 10 1 70.93 59.69 2.57 o -4 10 1 1265.63 1292.08 13.36 o -3 10 1 186.36 187.09 3.07 o -2 10 1 2358.69 2343.37 24.68 o -1 10 1 479.28 493.17 5.39 o 0 10 1 3073.79 2932.70 25.47 o 1 10 1 104.59 97.29 2.01 o 2 10 1 4480.30 4449.23 41.30 o 3 10 1 818.90 834.96 8.95 o 4 10 1 716.26 689.56 8.70 o 5 10 1 19.47 16.76 1.62 o 6 10 1 46.26 52.26 3.02 o -6 11 1 1.18 0.67 1.81 o -5 11 1 334.65 321.69 5.42 o -4 11 1 685.04 695.94 8.16 o -3 11 1 316.65 316.03 5.05 o -2 11 1 1384.20 1402.69 14.33 o -1 11 1 409.51 380.09 5.09 o 0 11 1 832.63 827.86 8.69 o 1 11 1 106.94 108.21 2.23 o 2 11 1 65.09 70.66 2.07 o 3 11 1 202.81 202.38 3.94 o 4 11 1 8.85 9.24 1.37 o 5 11 1 347.53 343.34 6.25 o 6 11 1 170.29 191.26 5.29 o -6 12 1 60.18 68.91 3.49 o -5 12 1 1073.62 1071.30 15.00 o -4 12 1 321.15 317.15 5.51 o -3 12 1 1115.95 1108.37 11.71 o -2 12 1 1.55 4.32 1.16 o -1 12 1 1657.38 1619.04 16.39 o 0 12 1 45.49 44.63 1.91 o 1 12 1 2213.80 2136.45 19.39 o 2 12 1 73.37 70.07 2.13 o 3 12 1 1281.36 1320.12 14.94 o 4 12 1 24.94 25.58 1.77 o 5 12 1 328.66 335.97 5.57 o 6 12 1 4.04 4.90 2.14 o -6 13 1 41.57 42.53 4.46 o -5 13 1 430.37 427.27 7.96 o -4 13 1 35.56 44.53 2.65 o -3 13 1 3706.46 3623.52 37.49 o -2 13 1 1.24 -0.70 1.17 o -1 13 1 941.52 909.26 10.24 o 0 13 1 66.75 63.69 2.29 o 1 13 1 1211.00 1221.48 12.01 o 2 13 1 51.00 54.12 2.06 o 3 13 1 1417.05 1406.64 14.36 o 4 13 1 736.68 727.20 10.77 o 5 13 1 658.00 623.35 10.83 o -5 14 1 347.53 355.13 8.01 o -4 14 1 59.76 60.36 2.65 o -3 14 1 10.34 9.06 1.96 o -2 14 1 282.43 288.40 4.72 o -1 14 1 466.77 468.91 6.45 o 0 14 1 1159.27 1114.42 12.22 o 1 14 1 523.33 525.99 6.30 o 2 14 1 6.45 5.66 1.42 o 3 14 1 5.86 7.26 1.60 o 4 14 1 151.07 137.66 5.73 o 5 14 1 89.44 91.31 4.07 o -5 15 1 65.75 72.22 3.57 o -4 15 1 1179.31 1159.57 18.12 o -3 15 1 227.75 243.00 4.70 o -2 15 1 779.89 811.92 9.63 o -1 15 1 258.02 254.09 4.97 o 0 15 1 618.98 613.36 7.88 o 1 15 1 0.97 0.12 1.23 o 2 15 1 904.81 918.84 10.67 o 3 15 1 112.77 109.93 3.27 o 4 15 1 547.97 565.23 8.55 o -4 16 1 357.65 337.10 7.95 o -3 16 1 15.56 14.64 1.97 o -2 16 1 33.63 35.19 2.29 o -1 16 1 47.69 44.47 2.64 o 0 16 1 759.20 757.04 10.14 o 1 16 1 30.20 31.98 2.06 o 2 16 1 2017.41 2063.95 20.93 o 3 16 1 95.50 94.43 3.22 o 4 16 1 52.30 52.78 3.59 o -3 17 1 45.24 49.78 3.27 o -2 17 1 687.19 693.69 10.00 o -1 17 1 339.85 340.89 6.18 o 0 17 1 55.13 58.93 3.04 o 1 17 1 461.06 452.31 7.24 o 2 17 1 32.51 32.61 2.25 o 3 17 1 76.10 77.11 3.41 o -2 18 1 8.54 10.46 2.49 o -1 18 1 42.43 47.73 2.97 o 0 18 1 140.36 144.19 5.03 o 1 18 1 1232.80 1232.23 16.94 o 2 18 1 147.61 159.23 4.35 o -1 19 1 510.06 516.28 9.17 o 0 19 1 42.40 44.38 3.40 o 1 19 1 33.55 33.88 3.41 o -8 0 2 91.73 103.94 5.50 o -6 0 2 1004.19 981.83 17.58 o -4 0 2 5326.48 5355.58 69.50 o -2 0 2 2512.67 2809.74 28.25 o 2 0 2 4253.32 3890.54 61.83 o 4 0 2 6619.72 6826.83 108.09 o 6 0 2 3.44 3.16 2.41 o -8 1 2 600.55 594.66 13.14 o -7 1 2 37.25 37.26 2.63 o -6 1 2 25.49 24.02 1.92 o -5 1 2 247.99 257.39 3.97 o -4 1 2 1431.78 1451.22 12.99 o -3 1 2 277.62 275.66 2.87 o -2 1 2 200.32 180.43 1.69 o -1 1 2 490.70 533.60 5.42 o 0 1 2 18765.19 17338.99 263.06 o 1 1 2 7934.84 8245.20 92.11 o 2 1 2 982.71 959.93 10.25 o 3 1 2 198.64 211.75 3.90 o 4 1 2 570.19 539.31 6.62 o 5 1 2 199.81 195.92 4.13 o 6 1 2 44.07 50.40 3.17 o 7 1 2 446.88 476.33 10.47 o -8 2 2 19.66 13.97 2.61 o -7 2 2 198.73 185.79 5.02 o -6 2 2 1316.42 1258.45 17.77 o -5 2 2 1367.38 1285.96 13.91 o -4 2 2 2513.95 2513.33 20.47 o -3 2 2 3519.15 3672.39 29.21 o -2 2 2 340.74 339.03 3.20 o -1 2 2 1409.58 1443.46 13.61 o 0 2 2 2.60 5.28 0.59 o 1 2 2 682.85 719.28 7.92 o 2 2 2 325.46 257.64 2.70 o 3 2 2 6450.88 6353.58 67.83 o 4 2 2 667.22 638.12 7.61 o 5 2 2 422.16 407.64 5.74 o 6 2 2 76.36 77.77 3.01 o 7 2 2 4.37 5.32 3.01 o -8 3 2 14.90 16.11 2.70 o -7 3 2 698.13 691.24 11.50 o -6 3 2 101.94 107.72 3.33 o -5 3 2 2.15 6.68 1.39 o -4 3 2 120.82 136.98 1.92 o -3 3 2 4578.10 4644.32 33.00 o -2 3 2 0.52 4.72 0.52 o -1 3 2 55354.21 46337.62 906.33 o 0 3 2 470.25 524.21 5.81 o 1 3 2 8176.04 8283.72 101.10 o 2 3 2 1514.57 1690.81 16.24 o 3 3 2 1479.94 1710.28 14.93 o 4 3 2 754.77 780.71 8.40 o 5 3 2 1442.85 1446.48 15.95 o 6 3 2 70.39 68.79 2.92 o 7 3 2 1991.46 2032.01 27.67 o -8 4 2 143.83 168.76 9.04 o -7 4 2 413.04 395.05 7.92 o -6 4 2 162.12 146.57 3.59 o -5 4 2 3601.77 3561.03 33.13 o -4 4 2 511.41 519.15 5.51 o -3 4 2 3143.71 3181.01 29.19 o -2 4 2 1121.52 1195.84 11.46 o -1 4 2 13233.58 12935.41 168.65 o 0 4 2 219.08 260.62 2.56 o 1 4 2 498.70 481.02 9.42 o 2 4 2 5960.77 6418.80 59.08 o 3 4 2 4012.64 3665.37 28.93 o 4 4 2 3.46 7.42 2.55 o 5 4 2 950.26 961.56 11.21 o 6 4 2 59.63 65.67 2.92 o 7 4 2 156.10 141.97 4.05 o -7 5 2 274.67 256.01 7.46 o -6 5 2 1.87 0.03 1.56 o -5 5 2 166.78 167.14 3.36 o -4 5 2 147.88 154.76 2.53 o -3 5 2 2093.37 2118.23 18.32 o -2 5 2 6820.52 6744.52 60.42 o -1 5 2 10455.38 10116.91 91.75 o 0 5 2 3294.75 3215.85 25.47 o 1 5 2 105.39 139.28 2.30 o 2 5 2 1315.29 1375.82 13.59 o 3 5 2 4.98 4.67 0.82 o 4 5 2 1.92 3.89 0.77 o 5 5 2 1494.48 1507.81 16.57 o 6 5 2 1786.28 1749.38 19.38 o 7 5 2 180.57 211.80 7.83 o -7 6 2 18.01 16.68 2.53 o -6 6 2 1006.20 1032.51 14.17 o -5 6 2 23.68 21.92 1.49 o -4 6 2 5042.80 5042.26 42.25 o -3 6 2 103.79 112.20 1.99 o -2 6 2 2634.06 2750.59 23.71 o -1 6 2 602.75 674.10 7.69 o 0 6 2 3306.56 3307.06 26.29 o 1 6 2 16.39 12.70 0.87 o 2 6 2 2971.23 2911.49 25.24 o 3 6 2 183.92 186.19 3.15 o 4 6 2 2476.83 2455.96 23.55 o 5 6 2 5.53 2.97 1.27 o 6 6 2 186.51 178.17 3.95 o 7 6 2 47.28 41.08 2.97 o -7 7 2 43.92 46.78 3.19 o -6 7 2 629.70 601.81 8.25 o -5 7 2 404.34 408.00 5.98 o -4 7 2 1137.80 1106.43 11.47 o -3 7 2 318.56 331.08 4.53 o -2 7 2 2276.76 2204.20 20.87 o -1 7 2 1499.05 1564.83 17.59 o 0 7 2 2662.07 2618.75 22.52 o 1 7 2 1729.02 1804.91 17.49 o 2 7 2 1441.75 1427.80 13.07 o 3 7 2 399.52 462.70 5.27 o 4 7 2 294.72 301.82 5.63 o 5 7 2 7.91 6.86 1.34 o 6 7 2 776.32 789.76 10.21 o 7 7 2 199.47 181.87 6.01 o -7 8 2 89.30 91.57 3.90 o -6 8 2 784.61 781.50 10.14 o -5 8 2 304.13 306.05 5.27 o -4 8 2 13.85 12.63 1.26 o -3 8 2 1121.56 1113.14 11.31 o -2 8 2 1084.74 1110.05 9.65 o -1 8 2 115.85 108.67 1.69 o 0 8 2 5307.48 5470.30 46.14 o 1 8 2 2408.58 2497.19 22.02 o 2 8 2 2561.85 2561.21 23.06 o 3 8 2 2234.09 2242.45 20.17 o 4 8 2 835.60 815.50 9.60 o 5 8 2 1211.75 1236.78 21.32 o 6 8 2 29.64 25.40 2.32 o 7 8 2 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