#------------------------------------------------------------------------------ #$Date: 2010-03-05 20:15:21 +0200 (Fri, 05 Mar 2010) $ #$Revision: 1024 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224862.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224862_Fobs loop_ _publ_author_name 'Najafi, Ezzatollah' 'Amini, Mostafa M.' 'Ng, Seik Weng' _publ_section_title ; (2-Methylquinolin-8-olato-\k^2^N,O)diphenyl(thiocyanato-\kN)tin(IV) ; _journal_coeditor_code BT5150 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m164 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.717 _cell_angle_beta 85.412 _cell_angle_gamma 78.244 _cell_length_a 9.0093 _cell_length_b 11.5809 _cell_length_c 20.5129 _exptl_crystal_F_000 976.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file bt5150Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 409.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 19898.44 17316.81 399.18 o 3 0 0 13425.97 13074.81 210.22 o 4 0 0 4610.22 4671.83 82.68 o 5 0 0 276.19 247.46 13.39 o 6 0 0 112.06 128.74 23.45 o 7 0 0 1.33 4.34 6.46 o 8 0 0 586.63 608.19 21.63 o 9 0 0 106.65 113.44 12.65 o 10 0 0 362.31 375.20 20.22 o 11 0 0 655.02 663.01 33.35 o -11 1 0 56.34 47.90 22.39 o -10 1 0 965.25 973.98 33.89 o -9 1 0 648.60 641.17 23.61 o -8 1 0 68.84 86.99 15.29 o -7 1 0 0.12 -3.92 6.17 o -6 1 0 60.63 92.60 9.01 o -5 1 0 2693.74 2895.33 58.63 o -4 1 0 669.82 663.14 16.16 o -3 1 0 1349.39 1150.38 21.09 o -2 1 0 64266.66 59010.43 2038.65 o -1 1 0 19467.75 20618.95 408.95 o 0 1 0 1154.49 1507.79 22.27 o 1 1 0 29935.06 27099.43 803.10 o 2 1 0 31174.75 31433.24 766.65 o 3 1 0 33.56 40.18 3.37 o 4 1 0 1474.94 1566.58 31.03 o 5 1 0 730.05 773.94 18.31 o 6 1 0 108.19 113.49 8.60 o 7 1 0 132.91 127.55 16.85 o 8 1 0 557.95 552.55 27.23 o 9 1 0 1080.82 1033.56 34.54 o 10 1 0 915.61 911.75 37.49 o 11 1 0 21.71 18.33 13.13 o -11 2 0 309.29 382.39 28.06 o -10 2 0 99.58 99.09 17.02 o -9 2 0 40.91 57.70 10.93 o -8 2 0 247.34 298.46 16.42 o -7 2 0 4.26 2.86 6.32 o -6 2 0 232.45 225.13 22.49 o -5 2 0 144.80 160.01 10.20 o -4 2 0 11828.23 12383.69 165.76 o -3 2 0 9290.51 10461.83 139.35 o -2 2 0 3772.27 3590.62 50.90 o -1 2 0 57696.29 51467.91 1572.62 o 0 2 0 18950.92 20060.13 401.47 o 1 2 0 12839.50 14696.39 190.79 o 2 2 0 1206.65 1377.74 21.38 o 3 2 0 7721.78 8112.42 108.20 o 4 2 0 1339.56 1412.29 24.95 o 5 2 0 20.77 15.94 4.84 o 6 2 0 33.40 24.99 6.37 o 7 2 0 402.26 398.85 22.77 o 8 2 0 942.38 864.34 38.74 o 9 2 0 28.65 24.26 12.52 o 10 2 0 304.58 279.15 39.64 o 11 2 0 1013.60 974.93 40.74 o -10 3 0 423.18 411.99 27.66 o -9 3 0 101.96 139.02 18.10 o -8 3 0 114.53 138.11 48.70 o -7 3 0 11.91 0.37 6.75 o -6 3 0 251.15 317.13 17.40 o -5 3 0 1727.52 1879.77 82.35 o -4 3 0 1498.65 1755.92 31.71 o -3 3 0 7968.17 8569.67 116.40 o -2 3 0 26769.68 28575.07 369.21 o -1 3 0 68.15 166.33 21.08 o 0 3 0 655.93 698.06 12.55 o 1 3 0 3153.22 3569.58 49.41 o 2 3 0 630.60 675.58 12.53 o 3 3 0 627.50 682.26 13.54 o 4 3 0 234.79 298.79 18.10 o 5 3 0 37.58 62.12 7.93 o 6 3 0 10.50 19.48 5.81 o 7 3 0 0.47 -1.68 7.12 o 8 3 0 89.92 81.45 13.60 o 9 3 0 1426.43 1345.54 44.12 o 10 3 0 1141.13 1118.54 42.15 o 11 3 0 35.65 24.89 18.31 o -10 4 0 64.25 89.42 24.93 o -9 4 0 76.20 99.40 16.88 o -8 4 0 14.47 10.20 12.42 o -7 4 0 162.55 164.54 23.73 o -6 4 0 128.08 130.54 10.58 o -5 4 0 552.13 598.54 33.99 o -4 4 0 5809.42 5986.64 86.39 o -3 4 0 3378.85 3563.23 53.53 o -2 4 0 57.97 89.29 8.51 o -1 4 0 11867.35 12824.63 208.76 o 0 4 0 4540.11 4924.74 67.80 o 1 4 0 3365.26 3452.82 49.09 o 2 4 0 6.37 8.34 2.15 o 3 4 0 519.39 549.08 11.76 o 4 4 0 2102.80 2105.47 34.07 o 5 4 0 47.06 40.64 6.50 o 6 4 0 9.37 15.96 5.14 o 7 4 0 523.10 576.05 25.34 o 8 4 0 923.03 954.17 34.84 o 9 4 0 83.67 82.41 15.39 o 10 4 0 535.71 443.85 42.29 o 11 4 0 757.16 747.03 36.88 o -10 5 0 211.25 274.13 26.02 o -9 5 0 88.63 92.11 43.71 o -8 5 0 55.34 48.70 25.84 o -7 5 0 31.53 55.94 23.26 o -6 5 0 852.39 891.09 33.45 o -5 5 0 1575.24 1607.01 72.48 o -4 5 0 46.41 38.75 5.41 o -3 5 0 4751.94 4889.78 93.79 o -2 5 0 10482.99 10521.07 177.62 o -1 5 0 3593.72 3545.70 91.70 o 0 5 0 1307.93 1563.59 25.84 o 1 5 0 4904.23 5080.49 70.88 o 2 5 0 7368.34 6989.13 95.40 o 3 5 0 961.19 808.17 17.84 o 4 5 0 620.22 724.30 15.19 o 5 5 0 313.00 351.15 10.74 o 6 5 0 136.31 173.01 14.52 o 7 5 0 17.70 17.06 9.28 o 8 5 0 269.95 230.78 19.10 o 9 5 0 1707.50 1594.73 49.74 o 10 5 0 945.07 893.24 38.66 o 11 5 0 4.98 10.10 14.00 o -9 6 0 19.79 21.45 14.72 o -8 6 0 5.21 9.89 22.71 o -7 6 0 67.77 72.66 15.57 o -6 6 0 1.80 9.29 10.72 o -5 6 0 939.76 992.23 34.96 o -4 6 0 2789.57 2789.12 63.85 o -3 6 0 1407.58 1313.96 54.42 o -2 6 0 324.73 389.91 18.59 o -1 6 0 3791.83 3507.24 68.92 o 0 6 0 10445.28 10061.06 135.10 o 1 6 0 5374.25 5049.42 71.94 o 2 6 0 600.13 594.45 14.30 o 3 6 0 2922.14 2925.69 45.18 o 4 6 0 2303.82 2318.96 37.50 o 5 6 0 8.29 -13.13 17.60 o 6 6 0 57.82 68.90 11.44 o 7 6 0 484.66 491.81 26.79 o 8 6 0 242.10 221.92 18.98 o 9 6 0 39.30 29.93 13.04 o 10 6 0 284.09 265.70 23.32 o 11 6 0 890.56 966.66 43.03 o -9 7 0 27.20 29.32 18.22 o -8 7 0 0.08 8.05 21.57 o -7 7 0 46.13 69.05 15.36 o -6 7 0 262.71 262.85 21.94 o -5 7 0 308.77 362.34 41.93 o -4 7 0 122.47 131.10 14.66 o -3 7 0 2625.81 2474.25 58.38 o -2 7 0 4478.96 4594.54 90.42 o -1 7 0 2343.02 2316.15 52.29 o 0 7 0 3144.37 3346.63 51.27 o 1 7 0 8503.17 8198.75 113.20 o 2 7 0 5385.11 5169.60 75.05 o 3 7 0 17.99 24.32 5.40 o 4 7 0 1031.50 994.14 30.49 o 5 7 0 1.29 6.36 7.77 o 6 7 0 47.48 67.37 12.05 o 7 7 0 51.35 65.21 33.53 o 8 7 0 606.47 612.23 29.71 o 9 7 0 1046.80 1040.07 40.44 o 10 7 0 469.89 450.77 28.90 o 11 7 0 0.06 -3.39 12.80 o -8 8 0 4.83 14.91 14.03 o -7 8 0 7.74 1.61 12.19 o -6 8 0 18.16 36.89 18.78 o -5 8 0 875.30 839.79 36.33 o -4 8 0 1293.97 1348.26 43.47 o -3 8 0 339.45 355.20 21.34 o -2 8 0 422.69 371.64 21.11 o -1 8 0 5162.95 5168.20 99.89 o 0 8 0 6219.16 6256.07 114.77 o 1 8 0 913.30 971.91 21.68 o 2 8 0 3153.79 3165.53 50.84 o 3 8 0 2686.11 2745.24 45.50 o 4 8 0 4.75 -2.33 7.17 o 5 8 0 52.26 50.69 13.41 o 6 8 0 70.46 61.32 12.22 o 7 8 0 502.05 504.44 26.21 o 8 8 0 841.44 722.50 32.83 o 9 8 0 3.50 -5.71 12.83 o 10 8 0 525.73 524.12 31.13 o -7 9 0 15.21 6.70 12.88 o -6 9 0 310.98 256.97 33.79 o -5 9 0 244.60 249.07 23.05 o -4 9 0 72.58 39.25 13.77 o -3 9 0 1177.00 1072.20 37.68 o -2 9 0 2030.76 2098.50 72.74 o -1 9 0 732.07 755.37 29.22 o 0 9 0 1524.04 1538.22 42.32 o 1 9 0 4600.12 4753.40 92.57 o 2 9 0 357.64 305.09 17.44 o 3 9 0 60.11 53.25 14.42 o 4 9 0 2.50 -4.00 7.70 o 5 9 0 100.40 132.19 29.76 o 6 9 0 265.95 307.33 21.22 o 7 9 0 4.28 24.18 11.93 o 8 9 0 535.59 525.42 29.23 o 9 9 0 1692.50 1610.22 53.36 o 10 9 0 214.34 233.04 23.79 o -6 10 0 12.22 -3.86 12.50 o -5 10 0 229.42 237.00 22.73 o -4 10 0 1013.97 1044.79 40.93 o -3 10 0 561.88 538.76 28.90 o -2 10 0 1124.31 1076.59 38.43 o -1 10 0 2292.45 2366.03 59.24 o 0 10 0 1794.99 1800.06 48.77 o 1 10 0 96.77 92.40 12.63 o 2 10 0 2.08 0.05 8.27 o 3 10 0 233.79 214.01 16.29 o 4 10 0 120.55 133.33 15.28 o 5 10 0 17.17 18.54 20.51 o 6 10 0 64.64 94.02 15.28 o 7 10 0 696.88 741.77 33.72 o 8 10 0 449.33 377.84 26.33 o 9 10 0 1.20 5.61 17.55 o 10 10 0 525.35 495.71 32.61 o -6 11 0 103.96 114.83 20.19 o -5 11 0 190.01 204.56 33.84 o -4 11 0 9.02 5.44 15.51 o -3 11 0 514.34 491.28 29.78 o -2 11 0 1173.85 1240.81 70.41 o -1 11 0 119.52 100.94 15.40 o 0 11 0 3.29 10.55 9.89 o 1 11 0 798.29 806.98 31.04 o 2 11 0 1295.19 1313.79 64.23 o 3 11 0 157.67 153.79 26.56 o 4 11 0 66.74 73.42 14.32 o 5 11 0 81.26 81.17 35.20 o 6 11 0 12.52 -1.47 11.04 o 7 11 0 15.23 9.15 12.36 o 8 11 0 549.08 509.45 36.08 o 9 11 0 559.71 524.14 31.79 o -4 12 0 303.42 316.07 39.06 o -3 12 0 52.66 54.17 15.96 o -2 12 0 174.21 177.13 25.27 o -1 12 0 973.25 1017.55 39.80 o 0 12 0 338.00 380.79 44.37 o 1 12 0 563.45 582.17 44.53 o 2 12 0 66.20 66.26 22.84 o 3 12 0 448.04 473.88 41.47 o 4 12 0 0.07 9.50 18.15 o 5 12 0 11.36 0.61 17.81 o 6 12 0 248.27 232.23 21.25 o 7 12 0 399.02 330.69 25.72 o 8 12 0 146.74 125.53 19.28 o -3 13 0 170.99 156.91 32.19 o -2 13 0 413.87 462.48 30.32 o -1 13 0 122.48 146.46 20.46 o 0 13 0 109.88 120.46 27.64 o 1 13 0 340.58 400.60 42.29 o 2 13 0 55.13 71.84 24.93 o 3 13 0 331.80 360.34 39.63 o 4 13 0 2.78 10.88 19.90 o 5 13 0 3.90 8.69 18.62 o 6 13 0 92.84 85.81 26.19 o 7 13 0 13.53 2.76 21.06 o -1 14 0 332.14 341.50 41.47 o 0 14 0 180.87 204.00 33.76 o 1 14 0 1.33 5.32 20.52 o 2 14 0 126.83 163.65 32.36 o 3 14 0 28.04 -0.12 18.98 o 4 14 0 14.80 24.12 22.08 o 5 14 0 23.00 3.81 19.49 o 6 14 0 173.61 185.94 34.36 o -5 -14 1 208.65 183.47 33.38 o -4 -14 1 26.44 18.18 22.06 o -3 -14 1 25.01 2.85 20.00 o -2 -14 1 539.69 549.16 49.79 o -1 -14 1 282.11 297.71 38.85 o 0 -14 1 13.47 22.79 22.22 o 1 -14 1 14.57 -5.38 19.28 o -7 -13 1 229.33 270.61 39.12 o -6 -13 1 146.89 120.81 29.15 o -5 -13 1 158.96 126.86 29.08 o -4 -13 1 1103.36 1085.12 64.37 o -3 -13 1 433.70 461.87 42.53 o -2 -13 1 208.07 215.72 33.41 o -1 -13 1 98.35 100.87 26.14 o 0 -13 1 305.51 350.51 39.16 o 1 -13 1 110.51 122.52 18.72 o 2 -13 1 0.10 -12.06 12.67 o 3 -13 1 23.51 33.45 15.59 o -8 -12 1 9.03 -0.54 13.11 o -7 -12 1 9.73 1.37 13.07 o -6 -12 1 449.06 430.34 26.91 o -5 -12 1 720.30 773.56 52.49 o -4 -12 1 105.61 132.29 27.12 o -3 -12 1 666.78 677.34 48.42 o -2 -12 1 758.37 901.35 54.61 o -1 -12 1 483.97 509.51 42.01 o 0 -12 1 15.62 1.53 12.81 o 1 -12 1 240.26 282.11 23.08 o 2 -12 1 73.28 73.28 16.29 o 3 -12 1 1.87 -2.43 12.70 o 4 -12 1 4.83 -14.49 19.56 o -9 -11 1 0.53 -6.00 15.00 o -8 -11 1 145.58 180.32 21.09 o -7 -11 1 321.02 354.01 25.71 o -6 -11 1 122.25 121.28 16.50 o -5 -11 1 292.50 276.80 21.26 o -4 -11 1 3260.07 3370.07 75.95 o -3 -11 1 1269.57 1373.91 66.30 o -2 -11 1 0.95 -0.90 15.10 o -1 -11 1 390.08 437.85 34.74 o 0 -11 1 214.79 242.34 19.06 o 1 -11 1 2.25 12.57 11.16 o 2 -11 1 6.19 8.14 14.55 o 3 -11 1 40.35 26.07 13.98 o 4 -11 1 274.34 293.12 31.07 o 5 -11 1 33.44 34.32 15.54 o 6 -11 1 14.30 28.11 20.96 o -9 -10 1 188.86 187.85 22.52 o -8 -10 1 76.33 73.65 16.93 o -7 -10 1 363.32 312.39 23.36 o -6 -10 1 1299.37 1236.66 41.74 o -5 -10 1 1455.57 1441.37 78.57 o -4 -10 1 61.05 74.78 13.06 o -3 -10 1 1707.82 1642.94 43.93 o -2 -10 1 1750.30 1779.44 45.52 o -1 -10 1 15.13 35.07 10.44 o 0 -10 1 362.94 363.00 27.00 o 1 -10 1 37.16 25.77 10.97 o 2 -10 1 12.22 27.92 12.02 o 3 -10 1 41.52 27.90 13.16 o 4 -10 1 91.20 114.71 18.02 o 5 -10 1 430.99 418.53 28.28 o 6 -10 1 302.57 271.66 24.90 o -10 -9 1 89.73 119.39 19.75 o -9 -9 1 31.41 58.25 16.05 o -8 -9 1 557.75 499.47 28.63 o -7 -9 1 2517.96 2393.53 65.17 o -6 -9 1 136.26 171.96 17.49 o -5 -9 1 5497.15 5298.33 105.82 o -4 -9 1 2622.88 2597.74 60.29 o -3 -9 1 2344.08 2418.51 55.65 o -2 -9 1 15.98 8.12 7.23 o -1 -9 1 609.30 669.71 29.58 o 0 -9 1 435.55 446.48 29.34 o 1 -9 1 0.52 0.93 9.65 o 2 -9 1 68.85 88.85 13.44 o 3 -9 1 344.41 387.27 24.26 o 4 -9 1 387.46 455.37 45.22 o 5 -9 1 16.96 35.30 13.36 o 6 -9 1 61.40 52.38 16.10 o 7 -9 1 434.44 474.14 45.91 o -10 -8 1 37.69 42.35 15.18 o -9 -8 1 899.82 936.37 39.51 o -8 -8 1 486.11 513.65 29.00 o -7 -8 1 1447.00 1354.00 51.77 o -6 -8 1 4136.44 4084.06 141.64 o -5 -8 1 2886.24 2972.20 67.00 o -4 -8 1 216.67 207.48 15.32 o -3 -8 1 2278.44 2359.90 40.89 o -2 -8 1 3121.09 3175.90 51.27 o -1 -8 1 1005.96 1052.66 23.16 o 0 -8 1 15.80 6.36 8.14 o 1 -8 1 64.39 57.93 11.33 o 2 -8 1 172.82 151.89 15.58 o 3 -8 1 163.84 172.36 15.91 o 4 -8 1 380.39 358.99 22.67 o 5 -8 1 1434.76 1349.76 45.17 o 6 -8 1 609.17 607.01 31.71 o 7 -8 1 5.66 3.34 17.95 o 8 -8 1 213.27 230.58 24.04 o -11 -7 1 9.97 16.55 15.61 o -10 -7 1 69.59 59.98 15.90 o -9 -7 1 2.67 28.06 13.51 o -8 -7 1 1715.82 1702.54 73.69 o -7 -7 1 2156.88 2261.71 58.28 o -6 -7 1 15.74 0.26 8.43 o -5 -7 1 2358.33 2280.33 54.39 o -4 -7 1 9928.76 9905.65 136.00 o -3 -7 1 4580.89 4780.56 70.82 o -2 -7 1 36.54 32.37 5.35 o -1 -7 1 2451.91 2456.12 40.33 o 0 -7 1 995.20 996.89 20.40 o 1 -7 1 398.44 385.33 18.51 o 2 -7 1 127.15 106.85 13.53 o 3 -7 1 6.34 -5.41 9.96 o 4 -7 1 656.21 620.99 26.89 o 5 -7 1 464.55 438.44 26.50 o 6 -7 1 478.85 434.03 26.68 o 7 -7 1 1273.71 1195.94 64.07 o 8 -7 1 529.30 561.96 31.96 o 9 -7 1 3.31 2.34 13.35 o -11 -6 1 0.81 -10.79 13.37 o -10 -6 1 206.83 234.47 22.39 o -9 -6 1 735.59 762.96 47.12 o -8 -6 1 24.00 19.12 10.91 o -7 -6 1 1187.02 1190.08 38.60 o -6 -6 1 7269.18 7269.25 135.31 o -5 -6 1 3540.47 3398.05 71.18 o -4 -6 1 1025.22 995.84 20.50 o -3 -6 1 3039.76 3107.03 47.96 o -2 -6 1 3536.96 3484.35 52.53 o -1 -6 1 1365.98 1336.62 24.56 o 0 -6 1 4.13 -1.25 3.20 o 1 -6 1 409.00 417.55 17.66 o 2 -6 1 1.36 9.99 6.53 o 3 -6 1 200.24 196.37 28.29 o 4 -6 1 346.36 330.71 19.73 o 5 -6 1 2499.53 2454.23 89.01 o 6 -6 1 2341.66 2242.74 93.06 o 7 -6 1 24.86 7.17 21.35 o 8 -6 1 633.69 654.51 33.60 o 9 -6 1 511.44 580.47 33.77 o -11 -5 1 53.84 70.71 17.49 o -10 -5 1 10.65 12.76 13.05 o -9 -5 1 566.62 603.04 30.16 o -8 -5 1 1421.41 1428.47 44.17 o -7 -5 1 794.79 771.12 29.68 o -6 -5 1 0.75 -2.29 18.96 o -5 -5 1 5647.45 5360.50 77.96 o -4 -5 1 9354.68 9191.98 125.09 o -3 -5 1 3198.06 3256.97 48.82 o -2 -5 1 449.39 400.90 10.76 o -1 -5 1 1673.78 1595.81 26.69 o 0 -5 1 1096.78 1057.90 19.31 o 1 -5 1 166.85 155.48 10.58 o 2 -5 1 1811.39 1848.71 71.01 o 3 -5 1 684.62 645.67 23.21 o 4 -5 1 2464.32 2273.62 43.41 o 5 -5 1 278.40 291.43 19.09 o 6 -5 1 363.17 386.01 22.67 o 7 -5 1 1906.82 1796.13 57.75 o 8 -5 1 1224.54 1211.75 44.43 o 9 -5 1 38.62 50.81 15.19 o 10 -5 1 300.50 319.00 27.08 o -11 -4 1 2.96 -4.43 12.53 o -10 -4 1 505.33 507.64 29.35 o -9 -4 1 658.54 587.40 29.59 o -8 -4 1 0.72 -8.96 10.06 o -7 -4 1 2139.27 2156.28 78.48 o -6 -4 1 5173.72 5113.72 76.67 o -5 -4 1 4051.63 3878.47 58.84 o -4 -4 1 498.54 526.00 17.71 o -3 -4 1 2773.78 2765.54 41.68 o -2 -4 1 3549.33 3565.42 51.20 o -1 -4 1 1038.38 1120.78 19.47 o 0 -4 1 305.31 286.94 7.70 o 1 -4 1 2.67 25.05 5.17 o 2 -4 1 779.34 638.47 28.00 o 3 -4 1 326.33 245.32 25.33 o 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