#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:27:41 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181169 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/48/2224891.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224891_Fobs loop_ _publ_author_name 'Loh, Wan-Sin' 'Fun, Hoong-Kun' 'Sarveswari, S.' 'Vijayakumar, V.' 'Reddy, B. Palakshi' _publ_section_title ; 2,4,6,8-Tetrakis(4-bromophenyl)-3,7-diazabicyclo[3.3.1]nonan-9-one ; _journal_coeditor_code CI2986 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o265 _journal_page_last o266 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.067 _cell_angle_gamma 90.000 _cell_length_a 14.7409 _cell_length_b 27.7762 _cell_length_c 7.1538 _exptl_crystal_F_000 1488.00 _reflns_d_resolution_high 0.7097 _cod_data_source_file ci2986Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 4br_0m in P2(1)/c (RT)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 429.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 23106.26 26001.88 407.26 o 3 0 0 733.00 780.02 17.42 o 4 0 0 145.31 139.45 15.95 o 5 0 0 7043.90 7460.63 112.13 o 6 0 0 21541.61 23084.46 378.34 o 7 0 0 5949.03 6291.76 99.01 o 8 0 0 35465.55 38352.32 546.09 o 9 0 0 84.88 141.25 20.20 o 10 0 0 21645.96 23145.13 338.08 o 11 0 0 2319.48 2427.17 56.66 o 12 0 0 2610.30 2867.92 64.17 o 13 0 0 115.62 88.31 38.50 o 14 0 0 850.09 905.05 71.29 o 15 0 0 0.14 -18.79 59.92 o 16 0 0 1230.34 1253.69 90.49 o 17 0 0 267.32 204.97 101.68 o 18 0 0 1915.53 2066.57 159.20 o 19 0 0 503.89 540.66 86.61 o 20 0 0 247.59 143.30 87.24 o 2 1 0 761.24 850.09 11.80 o 3 1 0 1390.66 1432.32 17.88 o 4 1 0 1620.14 1767.94 24.45 o 5 1 0 287.58 338.52 10.73 o 6 1 0 962.73 1049.20 18.66 o 7 1 0 9252.96 10414.13 110.32 o 8 1 0 1153.38 1187.09 23.33 o 9 1 0 13459.12 14108.46 149.06 o 10 1 0 1339.73 1338.43 28.41 o 11 1 0 9679.61 10268.99 113.94 o 12 1 0 4380.54 4587.90 60.87 o 13 1 0 945.21 1021.78 46.98 o 14 1 0 10.59 59.58 37.88 o 15 1 0 1.52 29.49 41.63 o 16 1 0 211.36 139.47 46.92 o 17 1 0 639.57 704.55 59.18 o 18 1 0 230.68 222.93 56.22 o 19 1 0 507.26 637.46 79.04 o 20 1 0 68.44 -29.47 58.57 o 1 2 0 17.19 18.33 3.47 o 2 2 0 1392.41 1485.81 18.22 o 3 2 0 3.55 10.74 4.39 o 4 2 0 10561.88 11325.66 115.99 o 5 2 0 7410.97 8497.39 89.30 o 6 2 0 5243.27 5249.25 58.72 o 7 2 0 11542.99 12604.70 131.82 o 8 2 0 6.03 7.16 11.27 o 9 2 0 847.72 902.02 22.01 o 10 2 0 2599.79 2547.26 38.84 o 11 2 0 5792.92 6151.25 74.29 o 12 2 0 116.55 104.53 19.10 o 13 2 0 2221.28 2393.57 61.78 o 14 2 0 380.30 429.73 44.52 o 15 2 0 623.48 738.25 56.12 o 16 2 0 9.25 -19.27 45.99 o 17 2 0 33.26 65.54 49.52 o 18 2 0 17.41 41.96 54.65 o 19 2 0 79.61 45.39 55.95 o 20 2 0 0.65 59.24 74.38 o 1 3 0 922.75 816.72 13.02 o 2 3 0 2399.97 2531.92 29.41 o 3 3 0 7.04 -5.08 5.08 o 4 3 0 839.06 770.47 14.12 o 5 3 0 666.53 730.13 14.89 o 6 3 0 238.53 275.09 13.61 o 7 3 0 203.01 286.11 14.90 o 8 3 0 2484.00 2647.27 36.61 o 9 3 0 1860.31 1778.38 30.03 o 10 3 0 1074.14 1094.47 28.27 o 11 3 0 109.62 86.06 17.54 o 12 3 0 720.81 787.97 31.29 o 13 3 0 46.00 65.49 31.56 o 14 3 0 2.08 43.41 38.08 o 15 3 0 80.60 156.09 43.99 o 16 3 0 3.77 35.56 45.14 o 17 3 0 17.72 -26.44 47.88 o 18 3 0 76.00 20.54 53.65 o 19 3 0 5.62 54.42 56.95 o 20 3 0 9.72 34.24 59.53 o 0 4 0 868.12 848.36 19.04 o 1 4 0 2.79 12.60 3.86 o 2 4 0 80.21 102.38 5.03 o 3 4 0 84.25 106.65 9.58 o 4 4 0 2378.30 2409.99 30.99 o 5 4 0 2386.28 2521.33 31.43 o 6 4 0 1888.11 1683.43 24.86 o 7 4 0 3941.21 4101.72 49.19 o 8 4 0 143.57 102.89 12.64 o 9 4 0 353.17 473.37 17.74 o 10 4 0 91.28 88.11 15.85 o 11 4 0 3228.83 3094.07 45.87 o 12 4 0 5.11 -0.39 18.05 o 13 4 0 952.46 951.47 59.90 o 14 4 0 0.16 -39.21 39.21 o 15 4 0 79.33 129.77 46.03 o 16 4 0 6.94 27.67 44.30 o 17 4 0 50.23 99.74 52.35 o 18 4 0 14.54 10.68 53.89 o 19 4 0 23.61 20.35 56.74 o 20 4 0 0.88 -55.64 55.64 o 1 5 0 2252.33 2323.85 25.67 o 2 5 0 16050.98 17562.38 180.85 o 3 5 0 17700.94 18629.79 197.42 o 4 5 0 15254.20 16479.16 176.12 o 5 5 0 1831.26 1919.11 27.64 o 6 5 0 499.00 557.47 14.67 o 7 5 0 6559.30 7163.73 79.07 o 8 5 0 3134.86 3226.64 42.63 o 9 5 0 13391.73 14100.46 149.32 o 10 5 0 4560.11 4673.79 59.12 o 11 5 0 10754.97 11479.08 139.47 o 12 5 0 201.19 226.42 20.33 o 13 5 0 3.99 9.16 31.34 o 14 5 0 231.67 245.27 50.66 o 15 5 0 834.20 940.58 55.99 o 16 5 0 20.70 42.90 47.00 o 17 5 0 663.12 733.25 59.84 o 18 5 0 251.61 247.53 57.69 o 19 5 0 176.11 228.43 58.72 o 20 5 0 95.78 144.57 61.17 o 0 6 0 184605.56 144393.53 3888.12 o 1 6 0 8066.52 8708.87 97.19 o 2 6 0 68900.30 70852.20 929.92 o 3 6 0 3722.54 4117.82 45.61 o 4 6 0 629.83 664.47 15.87 o 5 6 0 5312.99 5593.38 68.12 o 6 6 0 12459.53 13219.35 137.49 o 7 6 0 2321.58 2461.78 36.69 o 8 6 0 27818.60 30512.04 326.08 o 9 6 0 322.41 301.31 18.05 o 10 6 0 13401.12 14009.00 158.27 o 11 6 0 2752.09 2728.87 51.84 o 12 6 0 1139.89 1195.75 39.53 o 13 6 0 562.27 564.59 38.24 o 14 6 0 78.29 133.70 54.60 o 15 6 0 43.81 6.14 43.03 o 16 6 0 1062.36 1149.88 63.45 o 17 6 0 285.55 276.40 52.58 o 18 6 0 1482.98 1650.01 75.62 o 19 6 0 153.47 175.64 58.32 o 20 6 0 129.45 68.43 62.29 o 1 7 0 26132.59 27895.76 310.55 o 2 7 0 25776.66 27380.32 262.94 o 3 7 0 618.47 574.14 12.94 o 4 7 0 17172.58 18226.53 194.95 o 5 7 0 8719.38 10014.02 111.11 o 6 7 0 3010.94 3209.72 40.39 o 7 7 0 6331.74 6728.34 75.57 o 8 7 0 124.19 192.02 14.94 o 9 7 0 3455.38 3710.04 52.04 o 10 7 0 217.16 214.03 19.45 o 11 7 0 1734.89 1805.78 37.76 o 12 7 0 349.66 278.65 27.00 o 13 7 0 793.16 822.42 57.47 o 14 7 0 12.07 11.33 34.25 o 15 7 0 140.64 174.03 45.54 o 16 7 0 449.95 488.74 53.68 o 17 7 0 58.08 20.00 49.41 o 18 7 0 61.88 58.24 55.66 o 19 7 0 440.85 455.68 61.88 o 20 7 0 31.35 136.04 96.35 o 0 8 0 90673.17 90102.20 1510.82 o 1 8 0 19977.40 22171.80 213.26 o 2 8 0 1602.85 1548.34 20.97 o 3 8 0 3611.13 4128.42 46.88 o 4 8 0 99.77 59.90 7.59 o 5 8 0 14521.08 16476.31 178.25 o 6 8 0 11230.23 13420.54 147.69 o 7 8 0 2523.84 2589.08 36.48 o 8 8 0 1682.15 1844.18 30.96 o 9 8 0 48.34 26.40 15.39 o 10 8 0 825.82 808.74 24.15 o 11 8 0 2886.13 3165.15 47.87 o 12 8 0 79.52 70.90 24.96 o 13 8 0 2032.76 2279.27 91.50 o 14 8 0 385.86 459.62 43.05 o 15 8 0 1543.49 1782.24 71.22 o 16 8 0 95.21 140.38 48.03 o 17 8 0 183.81 131.31 49.53 o 18 8 0 133.43 78.54 53.89 o 19 8 0 32.84 -9.53 56.56 o 1 9 0 3579.09 4369.41 53.57 o 2 9 0 8878.81 8993.01 90.52 o 3 9 0 131.14 111.86 8.47 o 4 9 0 537.38 497.40 13.64 o 5 9 0 826.29 783.19 18.12 o 6 9 0 6961.78 7832.10 90.60 o 7 9 0 2442.75 2665.31 48.78 o 8 9 0 7126.86 7314.15 83.10 o 9 9 0 8753.21 8588.16 96.70 o 10 9 0 1455.69 1406.34 33.42 o 11 9 0 3251.65 3176.48 66.07 o 12 9 0 557.60 451.02 28.88 o 13 9 0 109.55 72.24 33.06 o 14 9 0 185.99 241.37 36.86 o 15 9 0 175.99 198.76 47.33 o 16 9 0 88.01 73.80 48.83 o 17 9 0 178.45 138.90 51.94 o 18 9 0 40.49 27.03 54.61 o 19 9 0 22.53 4.29 58.33 o 0 10 0 9326.63 10778.21 134.50 o 1 10 0 1126.72 1205.47 19.38 o 2 10 0 1729.81 2032.29 26.86 o 3 10 0 839.94 903.12 16.65 o 4 10 0 2531.62 2721.44 49.12 o 5 10 0 2483.29 2812.09 39.20 o 6 10 0 148.32 150.95 14.64 o 7 10 0 722.46 772.15 21.09 o 8 10 0 3.98 5.73 13.84 o 9 10 0 469.24 455.78 19.63 o 10 10 0 1348.67 1326.27 30.74 o 11 10 0 407.90 494.95 28.33 o 12 10 0 346.98 341.47 28.66 o 13 10 0 5.44 45.26 33.13 o 14 10 0 20.55 -11.13 34.86 o 15 10 0 60.74 60.37 46.35 o 16 10 0 0.49 40.49 49.04 o 17 10 0 68.38 92.67 52.71 o 18 10 0 21.49 38.07 56.12 o 19 10 0 0.75 -54.92 54.92 o 1 11 0 8792.75 9051.58 88.58 o 2 11 0 21046.60 21594.63 209.74 o 3 11 0 10734.37 11008.57 110.89 o 4 11 0 22102.13 22922.72 213.13 o 5 11 0 24.62 96.02 11.28 o 6 11 0 308.89 267.08 14.85 o 7 11 0 9451.09 9995.37 109.04 o 8 11 0 232.75 296.17 16.64 o 9 11 0 8496.90 8706.85 99.00 o 10 11 0 810.53 877.76 25.71 o 11 11 0 2210.43 2324.99 50.29 o 12 11 0 800.67 867.42 42.01 o 13 11 0 282.03 258.07 38.21 o 14 11 0 257.78 262.70 39.62 o 15 11 0 1093.42 1056.79 59.15 o 16 11 0 3.70 27.17 55.17 o 17 11 0 221.04 204.17 53.06 o 18 11 0 6.68 -7.53 55.14 o 19 11 0 19.46 14.76 57.17 o 0 12 0 21992.62 24543.81 297.19 o 1 12 0 4157.44 4628.94 47.54 o 2 12 0 8891.32 9607.99 98.26 o 3 12 0 11459.54 12190.15 122.53 o 4 12 0 4415.47 4530.92 49.60 o 5 12 0 5790.64 6022.29 65.71 o 6 12 0 17.17 24.47 12.07 o 7 12 0 0.35 1.87 11.28 o 8 12 0 5135.88 5256.81 64.72 o 9 12 0 1636.90 1681.61 33.71 o 10 12 0 8721.46 8896.46 101.90 o 11 12 0 66.96 36.22 22.75 o 12 12 0 594.65 705.63 40.48 o 13 12 0 101.22 92.89 35.72 o 14 12 0 29.83 55.48 37.89 o 15 12 0 13.93 36.56 46.38 o 16 12 0 893.15 995.08 63.51 o 17 12 0 13.79 67.15 52.84 o 18 12 0 506.69 459.00 60.88 o 19 12 0 85.87 126.68 58.51 o 1 13 0 90.90 84.56 10.52 o 2 13 0 6281.00 6478.51 69.90 o 3 13 0 458.37 485.81 15.22 o 4 13 0 10897.54 11287.53 110.22 o 5 13 0 842.04 961.94 20.32 o 6 13 0 1017.49 1084.27 24.40 o 7 13 0 554.33 621.97 20.51 o 8 13 0 0.17 -14.82 14.82 o 9 13 0 1.47 -14.01 14.01 o 10 13 0 181.67 152.41 22.53 o 11 13 0 2174.58 2135.50 47.74 o 12 13 0 116.22 219.64 35.53 o 13 13 0 739.23 724.01 44.20 o 14 13 0 94.40 85.74 37.97 o 15 13 0 154.85 181.25 47.05 o 16 13 0 96.92 138.48 50.61 o 17 13 0 8.65 40.01 53.14 o 18 13 0 20.19 52.08 57.06 o 19 13 0 76.17 110.44 72.60 o 0 14 0 14278.32 16206.99 200.92 o 1 14 0 5616.71 6039.69 60.80 o 2 14 0 12717.17 13741.07 138.21 o 3 14 0 10450.56 10900.82 118.99 o 4 14 0 1319.90 1494.76 25.34 o 5 14 0 9834.14 10339.77 102.74 o 6 14 0 1722.80 1772.38 29.84 o 7 14 0 132.04 142.33 15.82 o 8 14 0 1158.25 1282.78 29.32 o 9 14 0 0.69 -11.53 14.10 o 10 14 0 415.93 503.26 28.72 o 11 14 0 401.44 448.55 27.03 o 12 14 0 8.14 50.48 33.53 o 13 14 0 355.08 451.96 42.26 o 14 14 0 4.98 21.47 38.38 o 15 14 0 917.67 1045.31 62.45 o 16 14 0 181.55 222.84 50.96 o 17 14 0 281.16 378.55 58.62 o 18 14 0 67.37 40.39 67.11 o 19 14 0 48.31 154.45 149.53 o 1 15 0 5441.60 5735.16 60.92 o 2 15 0 2.85 -11.06 12.05 o 3 15 0 1979.71 2020.43 36.21 o 4 15 0 46.67 29.11 12.93 o 5 15 0 117.29 143.42 14.18 o 6 15 0 1511.02 1498.54 40.92 o 7 15 0 3296.49 3394.50 48.01 o 8 15 0 1398.37 1534.55 31.13 o 9 15 0 4760.84 4865.85 76.24 o 10 15 0 972.15 1023.09 35.10 o 11 15 0 1314.20 1329.21 49.14 o 12 15 0 0.78 20.52 33.66 o 13 15 0 28.71 18.69 36.08 o 14 15 0 10.88 -31.13 38.15 o 15 15 0 255.88 288.45 52.13 o 16 15 0 248.22 248.83 54.15 o 17 15 0 122.33 95.35 67.03 o 18 15 0 164.88 240.23 70.24 o 0 16 0 1320.80 1302.68 34.83 o 1 16 0 6.68 19.33 11.55 o 2 16 0 1389.51 1626.81 26.49 o 3 16 0 296.92 343.66 16.48 o 4 16 0 1728.18 1710.91 31.85 o 5 16 0 20.72 25.73 13.74 o 6 16 0 4762.84 5048.80 57.92 o 7 16 0 3623.40 3624.92 62.85 o 8 16 0 962.92 1006.06 26.15 o 9 16 0 95.28 87.97 22.37 o 10 16 0 1077.78 1164.43 41.90 o 11 16 0 286.69 361.65 37.22 o 12 16 0 1089.31 1122.77 55.70 o 13 16 0 291.04 275.91 36.91 o 14 16 0 16.23 42.26 39.56 o 15 16 0 75.26 85.53 41.96 o 16 16 0 2.85 -49.88 49.88 o 17 16 0 26.21 50.69 77.72 o 18 16 0 9.18 50.37 91.98 o 1 17 0 8020.15 8125.02 83.32 o 2 17 0 2535.62 2690.31 35.98 o 3 17 0 1756.73 1774.82 30.68 o 4 17 0 4768.48 4864.84 55.96 o 5 17 0 284.88 326.14 17.23 o 6 17 0 6071.06 6328.55 69.73 o 7 17 0 2517.04 2602.98 42.11 o 8 17 0 591.27 583.74 27.64 o 9 17 0 1561.51 1630.03 40.57 o 10 17 0 286.83 396.16 28.54 o 11 17 0 168.56 233.93 32.92 o 12 17 0 695.89 807.06 52.91 o 13 17 0 238.29 281.00 47.57 o 14 17 0 571.56 619.69 54.91 o 15 17 0 452.25 497.37 70.68 o 16 17 0 87.00 186.78 128.85 o 17 17 0 224.86 322.34 131.47 o 18 17 0 145.78 101.05 118.88 o 0 18 0 81.56 74.17 19.90 o 1 18 0 221.18 266.83 14.96 o 2 18 0 149.58 229.39 14.91 o 3 18 0 3631.30 4014.15 51.04 o 4 18 0 1801.48 1803.00 32.21 o 5 18 0 157.11 168.87 16.61 o 6 18 0 1019.43 1201.50 26.81 o 7 18 0 467.93 538.19 32.95 o 8 18 0 1453.42 1598.87 42.54 o 9 18 0 11.55 22.38 23.60 o 10 18 0 1527.51 1604.25 49.04 o 11 18 0 17.77 0.92 31.83 o 12 18 0 711.92 815.86 54.54 o 13 18 0 9.29 -17.58 35.76 o 14 18 0 69.17 69.72 34.98 o 15 18 0 71.70 85.91 61.15 o 16 18 0 231.98 357.38 93.33 o 17 18 0 207.78 250.95 90.03 o 18 18 0 2.58 -47.25 137.47 o 1 19 0 224.54 155.15 17.18 o 2 19 0 97.62 166.95 26.43 o 3 19 0 76.72 54.43 16.27 o 4 19 0 591.13 598.31 21.18 o 5 19 0 1904.63 1969.22 33.82 o 6 19 0 1718.31 1716.53 39.63 o 7 19 0 982.25 1038.45 33.41 o 8 19 0 181.09 170.05 26.01 o 9 19 0 108.54 99.68 25.53 o 10 19 0 14.21 -23.62 33.43 o 11 19 0 4.20 28.68 43.91 o 12 19 0 923.51 1041.51 59.41 o 13 19 0 71.92 89.10 46.94 o 14 19 0 417.66 473.92 66.79 o 15 19 0 61.08 126.51 64.31 o 16 19 0 54.20 58.84 88.02 o 17 19 0 0.07 -57.16 89.92 o 0 20 0 2238.17 2794.57 55.64 o 1 20 0 366.67 340.31 26.07 o 2 20 0 769.43 949.62 25.96 o 3 20 0 1655.50 1595.13 40.07 o 4 20 0 846.80 908.40 27.46 o 5 20 0 1092.38 1104.12 29.67 o 6 20 0 73.81 45.80 27.86 o 7 20 0 123.45 194.98 27.12 o 8 20 0 86.30 163.25 29.75 o 9 20 0 252.85 278.42 51.00 o 10 20 0 39.32 68.30 36.93 o 11 20 0 116.12 103.70 42.95 o 12 20 0 2.05 -21.20 47.51 o 13 20 0 5.90 -27.96 55.11 o 14 20 0 11.21 -58.88 58.88 o 15 20 0 426.54 462.68 71.48 o 16 20 0 9.85 15.07 85.07 o 17 20 0 239.20 374.11 156.94 o 1 21 0 8268.10 9634.21 110.83 o 2 21 0 748.57 759.77 34.89 o 3 21 0 711.84 778.71 36.12 o 4 21 0 621.44 533.18 31.74 o 5 21 0 5184.89 5623.75 109.80 o 6 21 0 35.26 -27.12 34.51 o 7 21 0 4977.50 5864.76 91.83 o 8 21 0 33.22 91.40 30.18 o 9 21 0 770.79 956.98 103.26 o 10 21 0 52.52 72.00 37.93 o 11 21 0 178.05 243.78 68.06 o 12 21 0 74.29 43.25 57.99 o 13 21 0 7.95 -57.68 60.13 o 14 21 0 20.14 -60.41 60.41 o 15 21 0 12.32 63.70 65.21 o 16 21 0 5.21 -46.57 81.17 o 17 21 0 8.52 59.01 124.48 o 0 22 0 1.40 -14.68 27.40 o 1 22 0 241.72 342.93 42.28 o 2 22 0 218.57 262.85 32.03 o 3 22 0 833.80 978.10 37.61 o 4 22 0 3207.56 3340.24 85.14 o 5 22 0 344.84 387.22 34.44 o 6 22 0 198.84 222.67 28.62 o 7 22 0 1062.07 1262.95 41.03 o 8 22 0 39.46 56.98 39.59 o 9 22 0 37.83 7.23 48.21 o 10 22 0 304.13 465.84 61.70 o 11 22 0 368.94 450.57 62.90 o 12 22 0 361.03 409.70 64.74 o 13 22 0 137.19 190.13 64.32 o 14 22 0 16.44 15.76 63.33 o 15 22 0 18.73 40.28 67.57 o 16 22 0 0.95 -23.32 95.62 o 1 23 0 2299.17 2579.86 67.25 o 2 23 0 218.74 252.22 36.37 o 3 23 0 38.45 56.39 55.38 o 4 23 0 1856.08 1979.51 64.11 o 5 23 0 954.73 1066.44 38.68 o 6 23 0 2794.84 3013.25 66.25 o 7 23 0 395.38 564.59 47.64 o 8 23 0 1203.59 1372.09 112.97 o 9 23 0 19.16 36.73 60.13 o 10 23 0 105.38 158.35 53.61 o 11 23 0 64.02 161.03 75.91 o 12 23 0 903.48 1157.84 79.41 o 13 23 0 63.96 150.25 67.23 o 14 23 0 410.17 562.39 74.22 o 15 23 0 44.66 153.69 69.65 o 16 23 0 1.49 53.15 88.75 o 0 24 0 30.71 23.13 39.86 o 1 24 0 220.63 234.15 36.44 o 2 24 0 52.57 40.56 32.25 o 3 24 0 0.30 -30.34 30.34 o 4 24 0 383.94 487.49 45.16 o 5 24 0 11.12 22.94 45.77 o 6 24 0 89.33 150.41 48.23 o 7 24 0 184.15 203.75 43.06 o 8 24 0 7.85 85.23 51.41 o 9 24 0 301.39 290.36 45.82 o 10 24 0 130.74 145.99 57.86 o 11 24 0 213.86 257.62 85.67 o 12 24 0 1.63 95.94 77.68 o 13 24 0 53.02 19.13 89.36 o 14 24 0 2.65 -30.91 65.74 o 15 24 0 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62.11 o -3 1 10 0.07 43.58 63.49 o -2 1 10 8.09 176.97 143.47 o -5 2 10 0.50 142.09 63.60 o -4 2 10 34.09 -6.00 61.39 o -3 2 10 7.34 34.32 62.38 o -5 3 10 5.22 -47.79 132.35 o -4 3 10 7.49 -0.47 71.79 o -3 3 10 1.23 -86.97 86.97 o