#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/49/2224906.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224906_Fobs loop_ _publ_author_name 'Wang, Chen-Yi' 'Ye, Jin-Yun' 'Wu, Xiang' 'Yuan, Cai-Jun' _publ_section_title ; Bis{2-ethoxy-6-[2-(isopropylammonio)ethyliminomethyl]phenolato}dithiocyanatonickel(II) ; _journal_coeditor_code CI5007 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m118 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.730 _cell_angle_gamma 90.000 _cell_length_a 24.9578 _cell_length_b 14.0161 _cell_length_c 9.6126 _exptl_crystal_F_000 1432.00 _reflns_d_resolution_high 0.7875 _[local]_cod_data_source_file ci5007Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2c in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 404.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 109074.48 94693.84 1797.20 o 6 0 0 6541.04 5732.65 154.18 o 8 0 0 3492.45 2903.81 114.47 o 10 0 0 7849.40 7499.60 163.52 o 12 0 0 8658.72 8621.85 479.67 o 14 0 0 8441.42 8281.01 181.61 o 16 0 0 25843.35 26724.44 545.86 o 18 0 0 1056.10 1095.82 140.94 o 20 0 0 106.15 146.26 45.69 o 22 0 0 457.31 532.62 104.34 o 24 0 0 494.39 744.42 121.47 o 26 0 0 103.47 91.88 90.33 o 28 0 0 386.82 552.86 129.26 o 30 0 0 1081.60 1298.84 183.77 o 1 1 0 3226.40 2871.85 126.26 o 3 1 0 7401.96 7121.42 112.18 o 5 1 0 2529.06 2449.03 49.06 o 7 1 0 6732.00 6172.45 120.89 o 9 1 0 3910.41 4024.20 69.33 o 11 1 0 3613.53 3519.07 91.71 o 13 1 0 1706.19 1769.72 52.09 o 15 1 0 37.33 14.31 18.66 o 17 1 0 890.38 958.08 49.59 o 19 1 0 757.27 666.83 55.13 o 21 1 0 176.84 140.99 67.74 o 23 1 0 60.35 140.16 57.26 o 25 1 0 316.75 320.45 73.78 o 27 1 0 726.57 1015.71 205.57 o 29 1 0 754.54 895.37 110.11 o 31 1 0 0.70 38.46 75.96 o 0 2 0 10202.85 10618.09 228.93 o 2 2 0 914.88 981.08 25.09 o 4 2 0 8346.46 8909.57 150.76 o 6 2 0 2010.82 1771.80 48.10 o 8 2 0 171.08 322.49 20.50 o 10 2 0 1772.42 1654.41 66.54 o 12 2 0 159.95 131.83 20.42 o 14 2 0 7660.04 7497.49 122.44 o 16 2 0 14192.38 14592.78 209.14 o 18 2 0 1802.78 1933.78 66.29 o 20 2 0 2286.77 2312.26 93.14 o 22 2 0 1256.80 1327.70 115.24 o 24 2 0 434.23 553.54 81.29 o 26 2 0 990.79 1137.08 109.02 o 28 2 0 188.24 179.75 75.53 o 30 2 0 27.09 -9.68 71.17 o 1 3 0 36765.79 38583.42 324.98 o 3 3 0 41055.38 41110.89 504.87 o 5 3 0 1776.67 1532.60 38.44 o 7 3 0 1573.55 1494.08 29.51 o 9 3 0 10363.63 10489.95 136.83 o 11 3 0 6985.83 7058.72 162.30 o 13 3 0 34.03 41.86 17.70 o 15 3 0 19.17 36.11 19.71 o 17 3 0 41.34 55.84 22.32 o 19 3 0 1.49 17.08 26.08 o 21 3 0 1139.22 1311.73 138.65 o 23 3 0 130.59 89.27 60.74 o 25 3 0 252.93 294.89 182.99 o 27 3 0 7.56 -10.90 61.67 o 29 3 0 293.79 283.86 125.37 o 31 3 0 231.14 232.05 130.82 o 0 4 0 18929.50 20813.34 412.70 o 2 4 0 193.68 267.47 19.11 o 4 4 0 24917.00 24968.60 227.64 o 6 4 0 23979.53 23397.64 274.51 o 8 4 0 1532.04 1367.56 33.97 o 10 4 0 9953.77 9568.21 114.51 o 12 4 0 19437.66 18484.93 281.82 o 14 4 0 517.56 418.50 33.94 o 16 4 0 260.06 249.31 30.69 o 18 4 0 874.87 948.54 78.95 o 20 4 0 6050.41 6168.93 153.46 o 22 4 0 1562.29 1852.42 115.43 o 24 4 0 392.78 393.44 117.58 o 26 4 0 834.03 919.94 203.24 o 28 4 0 717.12 841.99 107.90 o 30 4 0 507.21 552.86 146.39 o 1 5 0 218.87 242.92 16.79 o 3 5 0 4589.31 4903.33 79.18 o 5 5 0 843.91 796.68 29.07 o 7 5 0 1655.74 1857.22 57.71 o 9 5 0 67.06 74.50 13.98 o 11 5 0 809.69 780.20 31.36 o 13 5 0 918.09 1016.99 45.95 o 15 5 0 887.65 962.08 47.67 o 17 5 0 312.86 294.10 33.45 o 19 5 0 305.15 291.97 44.96 o 21 5 0 0.22 33.61 32.41 o 23 5 0 586.14 669.57 64.98 o 25 5 0 24.91 -3.07 54.76 o 27 5 0 0.09 4.67 91.88 o 29 5 0 20.46 26.48 104.34 o 0 6 0 1667.45 1599.17 113.69 o 2 6 0 242.53 416.95 26.56 o 4 6 0 5183.66 5140.68 77.46 o 6 6 0 14226.55 14490.85 168.24 o 8 6 0 16100.96 15760.18 171.83 o 10 6 0 13640.05 13322.59 173.30 o 12 6 0 946.14 887.22 36.69 o 14 6 0 3217.75 3094.61 79.10 o 16 6 0 2239.85 2262.19 111.01 o 18 6 0 565.31 561.21 51.84 o 20 6 0 1493.39 1482.45 82.36 o 22 6 0 1401.48 1373.46 115.66 o 24 6 0 1539.88 1411.34 309.14 o 26 6 0 652.20 889.25 155.74 o 28 6 0 479.54 643.19 152.62 o 1 7 0 1564.75 1765.17 61.12 o 3 7 0 3605.03 3836.29 78.47 o 5 7 0 29.86 23.65 13.30 o 7 7 0 2309.88 2258.84 52.98 o 9 7 0 1482.12 1564.58 45.42 o 11 7 0 1572.04 1577.29 47.52 o 13 7 0 40.97 29.51 21.28 o 15 7 0 2.29 25.12 21.09 o 17 7 0 18.60 -30.05 20.03 o 19 7 0 44.84 10.13 45.33 o 21 7 0 273.37 196.06 91.11 o 23 7 0 427.82 469.45 73.18 o 25 7 0 17.27 74.75 88.77 o 27 7 0 1.50 66.97 101.23 o 0 8 0 2701.52 2733.17 151.06 o 2 8 0 290.57 290.27 33.38 o 4 8 0 2288.53 2450.80 58.31 o 6 8 0 4809.92 4669.03 117.89 o 8 8 0 8290.73 8483.42 120.06 o 10 8 0 6318.55 6621.11 104.45 o 12 8 0 677.97 645.33 43.09 o 14 8 0 872.12 887.56 51.58 o 16 8 0 428.83 564.87 52.02 o 18 8 0 126.91 89.70 41.54 o 20 8 0 4.22 35.56 42.83 o 22 8 0 146.62 129.16 50.33 o 24 8 0 778.22 939.46 138.61 o 26 8 0 529.51 557.54 119.92 o 28 8 0 209.42 451.64 147.95 o 1 9 0 464.38 533.21 62.15 o 3 9 0 0.12 5.08 17.14 o 5 9 0 1707.36 1792.06 66.45 o 7 9 0 851.40 846.26 40.66 o 9 9 0 221.35 246.46 26.56 o 11 9 0 58.23 51.43 22.93 o 13 9 0 1688.14 1768.77 66.65 o 15 9 0 384.25 326.85 57.20 o 17 9 0 1.53 36.21 33.13 o 19 9 0 159.12 157.08 105.90 o 21 9 0 128.97 117.25 48.59 o 23 9 0 8.45 7.27 46.72 o 25 9 0 23.03 45.76 45.28 o 27 9 0 72.57 60.74 70.08 o 0 10 0 2517.21 2968.33 180.65 o 2 10 0 7967.58 8555.73 253.07 o 4 10 0 4717.94 4830.69 93.69 o 6 10 0 1208.37 1292.77 51.13 o 8 10 0 1119.80 1118.70 49.16 o 10 10 0 1406.25 1421.79 76.11 o 12 10 0 5500.99 5648.68 233.86 o 14 10 0 1674.66 1696.47 172.09 o 16 10 0 679.37 604.79 102.01 o 18 10 0 2195.05 2480.38 151.84 o 20 10 0 498.43 530.84 87.21 o 22 10 0 66.79 85.53 47.52 o 24 10 0 171.16 183.77 58.37 o 26 10 0 210.02 295.90 85.65 o 1 11 0 134.41 141.19 52.17 o 3 11 0 393.59 482.48 84.88 o 5 11 0 110.10 101.14 25.55 o 7 11 0 165.03 140.00 30.23 o 9 11 0 929.53 888.17 105.10 o 11 11 0 1033.45 908.00 68.90 o 13 11 0 230.48 228.88 115.24 o 15 11 0 237.82 227.22 55.41 o 17 11 0 432.09 451.94 72.07 o 19 11 0 0.46 45.93 37.71 o 21 11 0 282.21 205.38 55.03 o 23 11 0 7.90 -8.13 44.38 o 0 12 0 2851.41 2988.58 204.01 o 2 12 0 6481.55 6843.74 408.81 o 4 12 0 2875.53 2969.44 111.30 o 6 12 0 39.18 71.70 26.51 o 8 12 0 62.20 39.00 30.48 o 10 12 0 492.22 512.93 56.01 o 12 12 0 1370.60 1175.36 111.12 o 14 12 0 532.50 481.18 73.08 o 16 12 0 131.81 118.25 76.31 o 18 12 0 665.01 704.27 87.42 o 20 12 0 554.55 596.52 123.03 o 22 12 0 47.17 90.60 47.14 o 1 13 0 699.24 770.70 126.15 o 3 13 0 502.09 467.66 62.14 o 5 13 0 9.81 79.07 43.88 o 7 13 0 53.99 61.64 43.47 o 9 13 0 306.68 307.36 94.94 o 11 13 0 95.24 37.80 32.93 o 13 13 0 1187.90 1058.96 233.60 o 15 13 0 266.01 186.99 74.75 o 17 13 0 27.81 2.84 41.28 o 19 13 0 1.71 110.04 50.88 o 21 13 0 21.78 -20.66 44.90 o 0 14 0 119.27 210.24 95.00 o 2 14 0 291.67 339.65 76.75 o 4 14 0 691.67 674.72 73.23 o 6 14 0 373.84 544.35 140.42 o 8 14 0 198.62 176.62 99.67 o 10 14 0 226.95 267.63 50.39 o 12 14 0 426.51 496.66 75.28 o 14 14 0 437.92 360.41 98.11 o 16 14 0 324.20 232.09 97.34 o 18 14 0 1083.57 952.68 104.64 o 1 15 0 35.58 42.09 55.07 o 3 15 0 44.67 43.94 46.01 o 5 15 0 261.09 222.71 100.21 o 7 15 0 6.34 -3.75 52.30 o 9 15 0 158.99 44.34 60.09 o 11 15 0 88.61 60.95 44.99 o 13 15 0 3.80 70.97 46.09 o 15 15 0 11.43 22.82 47.31 o 0 16 0 492.83 505.91 90.43 o 2 16 0 624.08 480.84 114.99 o 4 16 0 442.07 286.54 64.69 o 6 16 0 456.59 394.23 70.50 o 8 16 0 635.04 537.87 99.92 o 10 16 0 79.05 24.92 84.10 o 12 16 0 112.49 60.74 85.65 o 1 17 0 5.39 17.25 44.92 o 3 17 0 25.28 -9.76 54.83 o 5 17 0 0.79 101.98 57.46 o 7 17 0 3.38 -14.02 85.65 o -31 1 1 435.29 695.75 112.26 o -29 1 1 462.88 581.10 99.62 o -27 1 1 531.66 762.51 101.75 o -25 1 1 577.08 576.47 85.21 o -23 1 1 113.90 103.96 53.93 o -21 1 1 804.02 965.25 88.60 o -19 1 1 841.17 909.46 78.73 o -17 1 1 1771.39 1887.01 59.98 o -15 1 1 11113.53 11242.86 157.89 o -13 1 1 3451.55 3181.78 67.52 o -11 1 1 992.58 798.65 37.99 o -9 1 1 593.26 564.71 49.28 o -7 1 1 551.81 682.31 21.92 o -5 1 1 34609.83 31508.78 353.05 o -3 1 1 3671.72 3880.95 98.11 o -1 1 1 26941.67 26296.64 346.96 o 1 1 1 59760.05 58668.86 1230.32 o 3 1 1 4924.32 4950.00 95.79 o 5 1 1 29738.05 29716.59 389.33 o 7 1 1 5264.19 4594.72 114.27 o 9 1 1 14277.80 13053.71 195.34 o 11 1 1 7533.12 7510.56 114.31 o 13 1 1 2278.47 1879.64 55.92 o 15 1 1 8716.46 8878.90 143.15 o 17 1 1 3794.84 3855.45 106.37 o 19 1 1 4356.13 4804.36 109.53 o 21 1 1 3446.71 3624.32 100.51 o 23 1 1 575.80 550.80 61.10 o 25 1 1 17.16 -28.29 53.12 o 27 1 1 35.59 -31.40 105.90 o 29 1 1 94.24 120.16 87.99 o 31 1 1 187.24 230.38 92.81 o -30 2 1 1.04 5.89 73.18 o -28 2 1 273.33 352.89 86.91 o -26 2 1 38.33 128.87 63.26 o -24 2 1 755.58 828.26 91.40 o -22 2 1 137.98 166.27 56.13 o -20 2 1 83.52 78.66 45.61 o -18 2 1 48.84 13.89 25.85 o -16 2 1 210.33 172.90 26.35 o -14 2 1 699.27 630.90 35.97 o -12 2 1 8914.12 8459.99 151.28 o -10 2 1 3135.76 3100.20 59.11 o -8 2 1 35.27 40.96 11.05 o -6 2 1 17513.63 16815.08 226.96 o -4 2 1 4167.71 4211.48 72.26 o -2 2 1 7817.04 7078.08 160.08 o 0 2 1 4001.87 4727.05 61.46 o 2 2 1 851.41 917.82 22.19 o 4 2 1 25791.16 25909.28 428.89 o 6 2 1 12682.29 12528.10 208.80 o 8 2 1 12.54 8.74 9.55 o 10 2 1 183.74 158.35 19.74 o 12 2 1 794.35 850.43 52.82 o 14 2 1 4662.49 4487.13 104.53 o 16 2 1 2388.50 2432.97 71.51 o 18 2 1 1701.75 1918.91 75.82 o 20 2 1 666.90 682.84 50.03 o 22 2 1 531.77 603.27 117.23 o 24 2 1 605.79 657.95 89.55 o 26 2 1 32.79 66.19 61.67 o 28 2 1 10.06 80.29 112.13 o 30 2 1 56.83 186.05 80.93 o -31 3 1 703.20 770.89 172.87 o -29 3 1 148.94 149.13 77.63 o -27 3 1 415.10 391.50 83.04 o -25 3 1 1549.84 1726.45 125.02 o -23 3 1 926.17 1201.77 101.11 o -21 3 1 3321.25 3385.14 145.54 o -19 3 1 341.47 347.46 45.33 o -17 3 1 2033.94 1909.56 74.82 o -15 3 1 6188.78 5990.22 107.06 o -13 3 1 173.64 146.88 21.65 o -11 3 1 5726.21 5890.17 93.61 o -9 3 1 9470.86 8781.25 117.31 o -7 3 1 28354.45 25833.72 251.11 o -5 3 1 9667.16 9652.64 92.04 o -3 3 1 2571.36 2669.99 50.80 o -1 3 1 39898.83 42391.32 467.78 o 1 3 1 16895.30 17480.75 183.87 o 3 3 1 519.18 629.06 25.05 o 5 3 1 4269.98 4096.16 100.72 o 7 3 1 405.85 431.01 23.74 o 9 3 1 5095.04 4703.31 95.33 o 11 3 1 3498.87 3400.21 73.20 o 13 3 1 73.00 81.97 20.14 o 15 3 1 2932.09 2828.53 75.15 o 17 3 1 1437.28 1523.89 58.97 o 19 3 1 58.71 45.70 25.65 o 21 3 1 674.01 776.17 63.36 o 23 3 1 612.62 688.34 80.76 o 25 3 1 1393.98 1755.15 125.37 o 27 3 1 228.44 232.10 98.11 o 29 3 1 161.88 264.75 119.92 o -30 4 1 2.99 -37.85 81.76 o -28 4 1 120.66 139.04 115.24 o -26 4 1 63.99 60.02 60.45 o -24 4 1 20.74 -31.04 47.14 o -22 4 1 269.85 375.36 90.33 o -20 4 1 1308.93 1227.46 94.03 o -18 4 1 88.96 84.48 37.69 o -16 4 1 413.53 419.00 85.91 o -14 4 1 1671.42 1838.37 64.96 o -12 4 1 4864.79 4734.12 92.39 o -10 4 1 24.14 41.38 12.44 o -8 4 1 3597.30 3830.93 61.70 o -6 4 1 40.31 30.11 8.37 o -4 4 1 3681.04 3535.69 64.51 o -2 4 1 263.58 338.32 20.18 o 0 4 1 7869.81 8382.55 127.15 o 2 4 1 8390.38 8372.28 98.57 o 4 4 1 9919.83 10076.65 130.04 o 6 4 1 8636.19 8475.18 113.67 o 8 4 1 112.56 129.02 17.38 o 10 4 1 2023.37 2085.44 54.95 o 12 4 1 1795.26 1768.01 42.25 o 14 4 1 587.17 553.35 37.39 o 16 4 1 885.55 931.51 50.05 o 18 4 1 617.01 648.49 47.74 o 20 4 1 37.88 89.71 30.26 o 22 4 1 145.63 55.98 48.11 o 24 4 1 67.38 53.32 41.72 o 26 4 1 21.46 74.75 95.00 o 28 4 1 53.78 -96.56 82.54 o 30 4 1 284.17 422.05 140.16 o -29 5 1 266.00 388.36 94.63 o -27 5 1 25.65 96.27 68.04 o -25 5 1 37.06 -65.94 46.64 o -23 5 1 1216.30 1340.35 107.31 o -21 5 1 4035.78 4058.70 199.00 o -19 5 1 969.30 1096.49 68.12 o -17 5 1 1632.27 1579.52 117.18 o -15 5 1 6425.41 6533.99 128.80 o -13 5 1 3588.47 3447.72 99.18 o -11 5 1 8030.39 8284.32 118.91 o -9 5 1 7031.62 6712.18 93.58 o -7 5 1 14768.01 13621.63 149.27 o -5 5 1 17209.51 17723.77 204.04 o -3 5 1 80.45 110.35 15.76 o -1 5 1 5016.86 5266.56 124.76 o 1 5 1 21858.45 22749.74 246.71 o 3 5 1 6024.10 6135.41 85.62 o 5 5 1 1409.81 1408.07 34.95 o 7 5 1 4412.76 4354.12 64.77 o 9 5 1 11339.72 10768.37 260.08 o 11 5 1 1860.89 1699.63 140.11 o 13 5 1 632.23 590.47 40.84 o 15 5 1 8946.08 9077.67 308.18 o 17 5 1 4286.34 4347.42 102.21 o 19 5 1 896.02 897.91 56.22 o 21 5 1 531.47 636.57 61.07 o 23 5 1 925.18 881.35 95.33 o 25 5 1 2533.04 2408.86 288.89 o 27 5 1 658.69 822.29 152.62 o 29 5 1 259.92 285.00 130.82 o -28 6 1 35.57 115.73 73.76 o -26 6 1 478.56 264.27 86.43 o -24 6 1 352.50 426.25 69.77 o -22 6 1 34.85 39.77 31.34 o -20 6 1 490.38 444.30 53.49 o -18 6 1 2.23 -31.78 21.19 o -16 6 1 1432.24 1529.69 71.89 o -14 6 1 114.64 102.89 23.41 o -12 6 1 1427.45 1363.15 43.77 o -10 6 1 2693.11 2494.60 56.24 o -8 6 1 4114.68 4104.93 71.75 o -6 6 1 5619.57 5845.10 89.52 o -4 6 1 3160.10 3439.11 69.88 o -2 6 1 51.31 13.61 12.60 o 0 6 1 2004.65 2004.38 61.67 o 2 6 1 2717.63 2658.38 61.91 o 4 6 1 3.60 1.11 9.88 o 6 6 1 11920.06 12559.98 140.27 o 8 6 1 432.47 455.60 24.39 o 10 6 1 0.91 17.82 11.82 o 12 6 1 534.87 552.69 36.66 o 14 6 1 2717.30 2846.25 122.73 o 16 6 1 1764.83 1796.50 123.88 o 18 6 1 2108.53 1903.11 138.92 o 20 6 1 37.90 33.51 40.41 o 22 6 1 595.58 540.67 98.11 o 24 6 1 1.58 53.62 48.59 o 26 6 1 134.19 185.33 99.67 o 28 6 1 110.24 66.97 107.46 o -27 7 1 494.96 546.63 123.03 o -25 7 1 1159.43 1306.30 112.18 o -23 7 1 785.70 711.08 82.50 o -21 7 1 1187.33 1238.33 80.31 o -19 7 1 5116.82 4882.71 183.99 o -17 7 1 485.21 495.01 49.44 o -15 7 1 168.09 326.74 63.06 o -13 7 1 4631.84 4500.09 84.82 o -11 7 1 6159.42 5862.30 95.98 o -9 7 1 7927.80 7828.14 112.39 o -7 7 1 961.53 993.08 36.61 o -5 7 1 4361.34 4423.71 86.24 o -3 7 1 7281.75 7430.14 117.41 o -1 7 1 14.35 37.63 15.48 o 1 7 1 7143.86 9031.61 159.54 o 3 7 1 25.71 90.41 17.22 o 5 7 1 19218.88 19210.40 230.38 o 7 7 1 6524.17 6369.94 106.18 o 9 7 1 2227.12 2246.47 51.78 o 11 7 1 3852.03 3806.90 85.33 o 13 7 1 5773.27 5882.58 114.19 o 15 7 1 1192.16 1192.93 70.26 o 17 7 1 184.46 134.25 34.80 o 19 7 1 689.90 971.38 95.78 o 21 7 1 360.69 345.07 70.72 o 23 7 1 999.26 967.58 198.56 o 25 7 1 320.13 358.62 76.93 o 27 7 1 594.21 974.91 175.98 o -28 8 1 67.45 141.72 73.20 o -26 8 1 116.96 9.34 51.39 o -24 8 1 78.11 133.93 71.64 o -22 8 1 323.48 327.57 53.00 o -20 8 1 14.17 41.91 33.69 o -18 8 1 110.34 105.78 35.42 o -16 8 1 209.52 141.96 32.78 o -14 8 1 36.55 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