#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/49/2224947.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224947_Fobs loop_ _publ_author_name 'Hill, Bj\"orn' 'Lerner, Hans-Wolfram' 'Bolte, Michael' _publ_section_title ; Redetermination of diammonium thiomolybdate ; _journal_coeditor_code FB2179 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i13 _journal_volume 66 _journal_year 2010 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.5867 _cell_length_b 6.9451 _cell_length_c 12.2005 _exptl_crystal_F_000 512.00 _reflns_d_resolution_high 0.8136 _[local]_cod_data_source_file fb2179Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' (I) P n m a R = 0.03' _shelx_refln_list_code 4 _shelx_f_calc_maximum 248.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 26192.91 25927.96 2094.04 o 4 0 0 10554.47 10281.70 344.04 o 6 0 0 1281.96 1305.31 15.39 o 8 0 0 6913.30 7866.68 454.25 o 10 0 0 8432.45 8672.69 677.98 o 2 1 0 5.48 31.31 3.73 o 4 1 0 1461.24 1442.18 36.65 o 6 1 0 643.24 718.96 19.01 o 8 1 0 4138.48 4306.29 158.21 o 10 1 0 232.74 230.82 9.67 o 0 2 0 35259.80 37789.98 916.64 o 2 2 0 8361.02 7484.65 122.50 o 4 2 0 46940.33 50593.79 1282.23 o 6 2 0 13096.19 13739.57 316.78 o 8 2 0 1525.96 1672.58 47.57 o 10 2 0 629.09 665.78 22.96 o 2 3 0 41.59 41.68 3.47 o 4 3 0 1483.35 1407.74 22.08 o 6 3 0 326.10 336.13 9.94 o 8 3 0 2661.99 2756.17 66.71 o 10 3 0 187.88 169.10 6.19 o 0 4 0 61769.14 65965.00 2074.82 o 2 4 0 11099.01 10817.79 221.61 o 4 4 0 5377.25 5187.74 83.73 o 6 4 0 859.56 897.13 20.97 o 8 4 0 4594.17 4916.12 121.90 o 10 4 0 5728.55 5573.01 132.50 o 2 5 0 15.62 26.46 4.28 o 4 5 0 561.21 586.42 7.54 o 6 5 0 305.74 313.32 8.46 o 8 5 0 2030.84 2149.23 68.24 o 0 6 0 5705.20 5560.38 122.60 o 2 6 0 2766.22 2699.33 43.78 o 4 6 0 14426.15 15456.13 344.68 o 6 6 0 5400.48 5496.45 127.84 o 8 6 0 804.73 773.05 23.25 o 2 7 0 59.19 62.83 5.39 o 4 7 0 446.51 435.74 12.15 o 6 7 0 49.47 62.01 6.23 o 0 8 0 12190.97 11757.12 330.86 o 2 8 0 2892.60 2643.84 56.10 o 4 8 0 1271.73 1108.01 41.91 o 1 0 1 89.45 74.33 6.03 o 2 0 1 600.82 617.36 14.97 o 3 0 1 20790.60 19592.38 826.14 o 4 0 1 1841.79 1821.51 32.92 o 5 0 1 393.05 426.10 7.60 o 6 0 1 4820.81 4960.63 128.97 o 7 0 1 5.74 10.58 4.09 o 8 0 1 228.72 242.60 10.26 o 9 0 1 363.16 367.33 18.10 o 10 0 1 60.65 65.09 4.77 o 11 0 1 634.22 571.54 22.81 o 0 1 1 3541.35 3144.71 63.86 o 1 1 1 23503.93 24420.60 383.80 o 2 1 1 939.54 749.93 11.61 o 3 1 1 17599.33 17635.17 378.85 o 4 1 1 1868.70 1698.41 36.06 o 5 1 1 16417.13 16952.73 337.44 o 6 1 1 408.32 417.32 8.65 o 7 1 1 3771.91 4074.08 83.07 o 8 1 1 1244.83 1337.20 29.29 o 9 1 1 4138.50 4519.88 95.69 o 10 1 1 968.52 970.28 28.04 o 11 1 1 399.88 394.40 10.99 o 1 2 1 4063.18 3867.07 38.81 o 2 2 1 11382.11 11021.68 220.53 o 3 2 1 668.92 615.04 9.98 o 4 2 1 412.19 412.40 6.69 o 5 2 1 670.00 667.90 11.43 o 6 2 1 27.53 32.14 2.96 o 7 2 1 3828.31 3854.50 67.37 o 8 2 1 1997.90 2118.26 38.24 o 9 2 1 1324.47 1336.75 23.31 o 10 2 1 276.73 290.25 6.36 o 11 2 1 5.00 10.96 4.06 o 0 3 1 2938.99 2616.70 29.55 o 1 3 1 16055.86 15754.19 201.54 o 2 3 1 600.72 531.79 6.14 o 3 3 1 10563.33 10552.42 165.63 o 4 3 1 1157.14 1120.80 18.19 o 5 3 1 10608.54 10998.65 184.26 o 6 3 1 268.85 292.70 5.07 o 7 3 1 2844.20 2937.30 58.24 o 8 3 1 1040.79 1095.25 16.80 o 9 3 1 3605.00 3689.93 72.74 o 10 3 1 895.33 834.94 15.54 o 11 3 1 435.73 468.72 20.32 o 1 4 1 52.74 50.55 2.60 o 2 4 1 587.13 527.60 7.42 o 3 4 1 6533.22 6329.00 83.18 o 4 4 1 794.72 797.20 10.69 o 5 4 1 146.42 147.35 3.31 o 6 4 1 2481.62 2515.20 39.52 o 7 4 1 1.23 5.07 3.42 o 8 4 1 147.79 152.59 4.16 o 9 4 1 216.88 216.18 5.98 o 10 4 1 24.07 25.41 4.40 o 0 5 1 1051.70 1000.55 21.30 o 1 5 1 7261.15 7460.55 82.60 o 2 5 1 237.02 236.79 3.75 o 3 5 1 5992.62 6113.22 91.12 o 4 5 1 1067.28 1103.51 11.64 o 5 5 1 7168.00 7259.87 80.09 o 6 5 1 339.87 359.78 6.75 o 7 5 1 2019.05 2112.81 43.52 o 8 5 1 625.45 646.98 15.69 o 9 5 1 2126.82 2092.08 41.07 o 1 6 1 773.01 757.51 7.64 o 2 6 1 2163.55 2128.84 31.41 o 3 6 1 41.16 43.34 3.20 o 4 6 1 135.06 151.77 6.14 o 5 6 1 197.74 201.95 4.11 o 6 6 1 0.82 9.05 3.83 o 7 6 1 1403.72 1447.47 38.13 o 8 6 1 825.62 840.43 23.09 o 0 7 1 965.29 930.37 15.82 o 1 7 1 4330.52 4335.74 54.32 o 2 7 1 212.83 219.17 4.01 o 3 7 1 2771.07 2730.19 55.02 o 4 7 1 374.43 379.98 6.83 o 5 7 1 2951.46 2912.66 43.13 o 6 7 1 103.58 109.91 4.64 o 1 8 1 24.96 27.72 3.49 o 2 8 1 212.85 197.15 6.42 o 3 8 1 1245.33 1167.55 20.63 o 4 8 1 208.72 193.51 5.93 o 0 0 2 6641.52 5851.58 157.96 o 1 0 2 19761.09 19518.27 307.43 o 2 0 2 9027.14 7687.66 178.21 o 3 0 2 70.67 88.90 4.90 o 4 0 2 7943.99 7538.52 253.65 o 5 0 2 2482.02 2445.38 70.44 o 6 0 2 3778.59 3861.24 124.03 o 7 0 2 770.36 797.99 23.36 o 8 0 2 1646.98 1715.49 64.21 o 9 0 2 12822.96 13634.95 539.10 o 10 0 2 505.34 516.77 15.84 o 11 0 2 2313.16 2244.34 66.53 o 1 1 2 360.20 391.22 6.84 o 2 1 2 15.23 22.85 3.09 o 3 1 2 609.32 619.84 12.04 o 4 1 2 465.22 481.75 8.73 o 5 1 2 953.42 893.54 8.75 o 6 1 2 60.48 68.01 2.97 o 7 1 2 38.98 41.03 3.10 o 8 1 2 466.38 486.97 10.18 o 9 1 2 147.66 161.55 4.79 o 10 1 2 88.21 88.82 3.88 o 11 1 2 34.01 38.69 3.85 o 0 2 2 12230.78 11783.24 152.46 o 1 2 2 332.32 358.46 5.58 o 2 2 2 8448.88 8227.73 117.08 o 3 2 2 3180.72 2934.02 39.62 o 4 2 2 3194.44 3168.83 26.78 o 5 2 2 26116.88 27284.70 501.65 o 6 2 2 1523.63 1556.24 23.66 o 7 2 2 1653.86 1742.29 28.41 o 8 2 2 1982.20 2108.07 37.54 o 9 2 2 1820.88 1889.88 36.35 o 10 2 2 1256.82 1292.27 28.47 o 11 2 2 165.40 149.61 4.79 o 1 3 2 259.75 244.01 3.52 o 2 3 2 2.02 5.41 2.29 o 3 3 2 535.79 499.02 7.52 o 4 3 2 309.76 308.98 4.88 o 5 3 2 599.71 627.70 10.47 o 6 3 2 41.63 50.32 3.09 o 7 3 2 77.43 87.28 3.29 o 8 3 2 346.80 369.89 7.47 o 9 3 2 136.65 141.19 4.25 o 10 3 2 76.49 75.24 4.38 o 0 4 2 2792.56 2746.97 49.47 o 1 4 2 9038.26 8833.85 124.10 o 2 4 2 3461.80 3473.59 44.13 o 3 4 2 71.14 80.43 2.88 o 4 4 2 4161.46 4254.03 61.61 o 5 4 2 1144.88 1150.67 20.02 o 6 4 2 2361.14 2436.23 49.69 o 7 4 2 537.79 572.87 10.50 o 8 4 2 1086.43 1104.56 19.40 o 9 4 2 8164.36 8098.12 127.58 o 10 4 2 368.37 357.93 8.30 o 1 5 2 381.75 374.11 5.34 o 2 5 2 0.87 15.73 3.27 o 3 5 2 56.56 60.27 3.06 o 4 5 2 156.36 164.94 3.42 o 5 5 2 295.77 297.53 5.22 o 6 5 2 34.18 39.10 3.44 o 7 5 2 1.59 6.77 3.39 o 8 5 2 212.66 216.96 4.67 o 9 5 2 22.04 21.57 3.79 o 0 6 2 3370.70 3312.70 46.92 o 1 6 2 10.84 54.29 7.65 o 2 6 2 2269.83 2246.71 33.96 o 3 6 2 1580.28 1626.21 22.81 o 4 6 2 1141.76 1155.02 13.76 o 5 6 2 9056.13 9497.73 102.63 o 6 6 2 657.23 663.00 15.44 o 7 6 2 869.76 857.35 22.40 o 8 6 2 922.61 931.66 28.67 o 1 7 2 42.79 46.15 3.30 o 2 7 2 1.51 7.28 3.22 o 3 7 2 233.98 227.41 3.80 o 4 7 2 69.25 80.07 3.74 o 5 7 2 107.35 104.24 4.13 o 6 7 2 13.65 18.25 4.02 o 0 8 2 708.86 675.46 10.79 o 1 8 2 2728.24 2533.35 22.10 o 2 8 2 863.03 814.20 11.31 o 3 8 2 119.13 106.48 4.15 o 1 0 3 139.72 150.23 5.66 o 2 0 3 63.50 59.55 4.54 o 3 0 3 13193.28 12396.77 282.24 o 4 0 3 139.41 142.17 4.98 o 5 0 3 23.39 24.74 4.28 o 6 0 3 2866.45 2528.74 124.67 o 7 0 3 1493.72 1491.02 46.35 o 8 0 3 13.76 17.76 4.19 o 9 0 3 45.03 44.79 5.14 o 10 0 3 44.10 49.26 5.60 o 11 0 3 96.08 89.67 5.82 o 0 1 3 21721.61 23052.68 687.06 o 1 1 3 580.34 510.69 9.80 o 2 1 3 3746.32 3293.16 44.49 o 3 1 3 53.11 67.05 3.15 o 4 1 3 10080.84 9628.14 195.06 o 5 1 3 30.17 43.35 2.91 o 6 1 3 3471.63 3577.99 48.32 o 7 1 3 330.23 351.32 8.63 o 8 1 3 4749.02 4920.39 114.23 o 9 1 3 40.69 46.55 3.55 o 10 1 3 4353.81 4566.48 97.09 o 11 1 3 506.79 483.80 14.15 o 1 2 3 5877.88 5803.31 65.36 o 2 2 3 4756.13 4745.06 49.94 o 3 2 3 460.45 461.89 6.68 o 4 2 3 204.61 211.81 3.77 o 5 2 3 17.72 28.75 3.30 o 6 2 3 236.41 231.18 4.17 o 7 2 3 1979.63 2080.75 39.12 o 8 2 3 1087.40 1159.87 20.43 o 9 2 3 469.95 509.75 11.20 o 10 2 3 213.89 219.80 5.61 o 11 2 3 611.51 608.11 20.18 o 0 3 3 14101.63 13946.27 151.83 o 1 3 3 166.88 183.31 3.43 o 2 3 3 2970.29 2759.11 44.58 o 3 3 3 134.67 137.18 3.28 o 4 3 3 6846.51 6865.66 104.68 o 5 3 3 61.96 65.91 3.30 o 6 3 3 2574.97 2745.21 47.21 o 7 3 3 291.74 314.03 7.35 o 8 3 3 3996.20 4101.25 86.86 o 9 3 3 18.32 19.98 3.74 o 10 3 3 3810.23 3740.93 86.32 o 1 4 3 180.84 169.41 3.18 o 2 4 3 8.57 10.34 2.43 o 3 4 3 5228.42 5052.51 64.33 o 4 4 3 141.96 143.38 3.52 o 5 4 3 22.70 29.92 3.26 o 6 4 3 1459.87 1444.39 24.67 o 7 4 3 952.22 982.35 18.84 o 8 4 3 10.85 15.85 3.56 o 9 4 3 37.61 41.28 4.11 o 10 4 3 11.25 14.35 4.61 o 0 5 3 6055.24 6113.61 79.60 o 1 5 3 204.12 200.57 3.32 o 2 5 3 1702.70 1732.44 19.70 o 3 5 3 72.23 67.84 2.98 o 4 5 3 5012.27 5104.35 76.73 o 5 5 3 0.48 6.28 3.61 o 6 5 3 2196.23 2307.28 41.94 o 7 5 3 146.57 151.96 4.10 o 8 5 3 2490.41 2457.88 35.90 o 9 5 3 46.78 45.59 4.61 o 1 6 3 1269.69 1271.31 16.39 o 2 6 3 944.23 918.68 13.13 o 3 6 3 294.54 290.81 5.02 o 4 6 3 29.15 33.90 3.20 o 5 6 3 4.78 10.45 3.34 o 6 6 3 28.51 27.31 3.77 o 7 6 3 759.33 744.94 18.93 o 8 6 3 480.67 484.34 14.76 o 0 7 3 4176.95 4130.10 48.24 o 1 7 3 19.62 22.75 3.23 o 2 7 3 1254.00 1271.80 19.56 o 3 7 3 78.68 80.74 3.44 o 4 7 3 2157.23 2147.70 27.95 o 5 7 3 59.33 59.37 3.91 o 6 7 3 1035.56 990.75 21.94 o 1 8 3 66.40 66.66 3.94 o 2 8 3 16.91 17.66 3.84 o 3 8 3 1075.00 1007.43 14.38 o 0 0 4 57048.21 65300.31 1584.02 o 1 0 4 3610.80 3285.10 54.27 o 2 0 4 2138.53 1969.05 40.58 o 3 0 4 12004.30 10817.72 251.78 o 4 0 4 202.59 201.79 6.61 o 5 0 4 12747.48 12248.77 254.71 o 6 0 4 509.43 521.34 18.20 o 7 0 4 6013.42 6098.45 124.75 o 8 0 4 786.81 833.59 23.09 o 9 0 4 2754.45 2932.87 41.50 o 10 0 4 1830.03 1873.42 44.03 o 11 0 4 1202.49 1154.22 43.56 o 1 1 4 737.34 765.71 10.31 o 2 1 4 62.16 65.74 3.16 o 3 1 4 419.28 375.02 5.87 o 4 1 4 832.82 759.33 16.58 o 5 1 4 35.18 35.17 3.13 o 6 1 4 55.71 56.75 3.19 o 7 1 4 0.07 3.09 3.13 o 8 1 4 2159.30 2183.08 39.71 o 9 1 4 47.40 49.55 3.81 o 10 1 4 6.80 11.14 3.90 o 11 1 4 11.57 12.90 4.64 o 0 2 4 3360.45 3297.79 75.86 o 1 2 4 12739.93 12588.11 130.37 o 2 2 4 54.96 50.34 3.17 o 3 2 4 6427.98 6348.10 83.50 o 4 2 4 11679.97 11596.40 149.71 o 5 2 4 3279.42 3269.70 51.49 o 6 2 4 1759.00 1842.02 37.45 o 7 2 4 3858.85 4114.53 80.93 o 8 2 4 57.86 64.45 3.69 o 9 2 4 5471.18 5698.76 133.53 o 10 2 4 99.59 106.28 4.45 o 11 2 4 2505.60 2263.75 79.23 o 1 3 4 332.16 341.20 5.12 o 2 3 4 0.03 6.70 2.60 o 3 3 4 218.72 204.95 3.46 o 4 3 4 818.20 799.62 8.31 o 5 3 4 35.11 36.53 3.27 o 6 3 4 8.66 13.74 3.23 o 7 3 4 0.40 3.91 3.37 o 8 3 4 1308.19 1334.90 28.27 o 9 3 4 50.04 55.76 3.91 o 10 3 4 5.93 9.32 4.17 o 0 4 4 19059.25 19733.86 279.93 o 1 4 4 2646.72 2626.49 29.56 o 2 4 4 999.27 948.36 14.55 o 3 4 4 6057.93 6104.46 103.12 o 4 4 4 95.83 95.68 3.20 o 5 4 4 7423.73 7535.36 125.07 o 6 4 4 290.02 287.52 6.76 o 7 4 4 3801.25 3956.22 93.41 o 8 4 4 540.44 551.16 10.58 o 9 4 4 1847.63 1807.40 31.79 o 1 5 4 144.28 145.09 3.45 o 2 5 4 79.71 82.92 3.09 o 3 5 4 95.35 98.54 3.26 o 4 5 4 259.25 270.04 5.38 o 5 5 4 8.30 9.77 3.47 o 6 5 4 42.83 39.61 3.96 o 7 5 4 5.25 10.32 3.77 o 8 5 4 1093.36 1057.91 23.34 o 9 5 4 36.93 45.37 5.92 o 0 6 4 418.52 416.56 7.52 o 1 6 4 4598.15 4728.80 75.54 o 2 6 4 16.81 38.10 4.19 o 3 6 4 2325.95 2344.18 41.03 o 4 6 4 3835.90 3978.41 47.72 o 5 6 4 1377.62 1372.59 24.54 o 6 6 4 748.07 745.26 16.17 o 7 6 4 1754.55 1592.15 41.30 o 1 7 4 43.90 45.12 3.32 o 2 7 4 21.62 24.26 3.44 o 3 7 4 56.17 57.85 3.95 o 4 7 4 252.86 247.54 4.65 o 5 7 4 2.43 4.74 4.04 o 0 8 4 3762.27 3765.97 77.85 o 1 8 4 872.91 810.06 11.51 o 2 8 4 247.25 237.31 4.74 o 1 0 5 1.34 9.26 4.32 o 2 0 5 1764.18 1598.01 21.84 o 3 0 5 6179.41 5955.69 175.10 o 4 0 5 1425.70 1262.14 23.45 o 5 0 5 298.44 301.13 8.19 o 6 0 5 3900.55 3824.27 81.45 o 7 0 5 607.61 645.27 13.53 o 8 0 5 1127.07 1100.16 24.97 o 9 0 5 457.45 456.97 15.19 o 10 0 5 161.65 169.67 6.48 o 11 0 5 286.27 279.59 15.45 o 0 1 5 7952.48 7692.55 188.01 o 1 1 5 11331.22 11468.35 164.46 o 2 1 5 7690.31 7109.35 110.59 o 3 1 5 5603.34 5293.31 78.14 o 4 1 5 4941.86 4716.40 84.04 o 5 1 5 10798.50 10255.04 220.29 o 6 1 5 4586.75 4591.36 64.81 o 7 1 5 854.60 875.23 16.44 o 8 1 5 2080.71 2143.32 32.15 o 9 1 5 2321.50 2444.85 45.98 o 10 1 5 1426.70 1427.38 28.99 o 11 1 5 13.52 22.65 6.53 o 1 2 5 492.98 485.97 9.17 o 2 2 5 6948.94 6885.51 117.36 o 3 2 5 1951.04 1812.05 29.36 o 4 2 5 602.63 611.05 13.09 o 5 2 5 533.21 520.64 10.77 o 6 2 5 5.22 9.13 2.85 o 7 2 5 1795.23 1782.71 35.82 o 8 2 5 992.67 1004.29 17.37 o 9 2 5 439.44 431.34 10.07 o 10 2 5 482.44 499.04 11.21 o 0 3 5 4369.99 4678.97 93.53 o 1 3 5 8574.17 8837.60 111.83 o 2 3 5 5351.81 5511.39 80.14 o 3 3 5 3824.92 3833.38 41.53 o 4 3 5 4200.93 4232.27 70.58 o 5 3 5 7083.65 7242.80 118.67 o 6 3 5 3904.80 4003.00 64.38 o 7 3 5 679.02 710.10 13.08 o 8 3 5 1670.28 1715.44 36.57 o 9 3 5 2114.48 2037.25 47.78 o 10 3 5 1060.61 1000.64 22.47 o 1 4 5 7.22 14.42 2.97 o 2 4 5 1050.20 1064.59 13.05 o 3 4 5 2619.61 2609.58 33.04 o 4 4 5 628.12 626.22 9.06 o 5 4 5 134.16 135.99 3.78 o 6 4 5 2285.64 2336.27 38.43 o 7 4 5 331.26 329.33 6.47 o 8 4 5 748.95 762.22 13.21 o 9 4 5 272.20 270.08 7.35 o 0 5 5 3332.74 3469.80 49.39 o 1 5 5 3928.54 4138.36 47.86 o 2 5 5 3486.46 3576.42 50.46 o 3 5 5 2535.11 2617.76 31.88 o 4 5 5 2110.56 2172.72 30.17 o 5 5 5 5050.91 5192.17 85.25 o 6 5 5 2076.07 2086.26 38.14 o 7 5 5 537.95 536.09 16.27 o 8 5 5 1233.20 1144.33 19.82 o 1 6 5 163.04 165.29 3.80 o 2 6 5 2069.84 2113.12 32.04 o 3 6 5 458.53 464.77 5.71 o 4 6 5 279.09 293.97 5.80 o 5 6 5 157.35 166.70 4.42 o 6 6 5 9.64 12.82 4.27 o 7 6 5 606.09 572.73 13.07 o 0 7 5 1232.90 1215.64 34.18 o 1 7 5 2587.12 2625.27 48.20 o 2 7 5 1669.08 1675.23 30.32 o 3 7 5 1121.32 1106.49 15.79 o 4 7 5 1582.13 1544.17 20.42 o 5 7 5 1900.25 1803.73 32.57 o 1 8 5 0.98 2.80 4.35 o 0 0 6 8528.63 8501.33 106.53 o 1 0 6 816.89 755.50 18.57 o 2 0 6 10688.01 10525.23 155.95 o 3 0 6 8948.10 8505.29 183.95 o 4 0 6 16896.59 16647.49 315.40 o 5 0 6 2896.27 2732.76 59.66 o 6 0 6 7080.63 7002.60 125.35 o 7 0 6 2304.09 2284.96 49.49 o 8 0 6 2509.89 2546.60 69.68 o 9 0 6 514.18 508.82 14.82 o 10 0 6 408.69 424.45 11.43 o 1 1 6 864.25 800.72 12.35 o 2 1 6 11.31 17.19 3.12 o 3 1 6 166.68 170.08 4.09 o 4 1 6 1433.40 1359.86 27.40 o 5 1 6 1023.91 930.26 14.79 o 6 1 6 115.49 119.31 4.05 o 7 1 6 282.10 273.52 6.56 o 8 1 6 1615.77 1672.86 26.62 o 9 1 6 346.33 353.60 7.87 o 10 1 6 167.65 166.24 4.80 o 0 2 6 25820.80 27359.30 549.98 o 1 2 6 10408.42 10413.58 176.91 o 2 2 6 13231.91 13363.45 232.03 o 3 2 6 2634.59 2581.28 29.90 o 4 2 6 4660.77 4602.79 89.10 o 5 2 6 517.97 487.55 9.73 o 6 2 6 1464.96 1453.55 30.94 o 7 2 6 1541.72 1541.40 37.86 o 8 2 6 3898.68 3929.87 84.46 o 9 2 6 534.30 534.32 9.91 o 10 2 6 2663.16 2590.93 49.83 o 1 3 6 414.45 440.18 7.96 o 2 3 6 0.13 4.37 2.65 o 3 3 6 273.25 256.41 3.94 o 4 3 6 986.79 983.06 15.35 o 5 3 6 739.87 738.38 14.88 o 6 3 6 77.61 92.15 3.40 o 7 3 6 359.07 357.22 6.98 o 8 3 6 1239.83 1228.35 28.73 o 9 3 6 328.93 321.94 8.80 o 0 4 6 4455.35 4800.25 80.85 o 1 4 6 377.20 393.43 7.03 o 2 4 6 5413.10 5662.56 58.81 o 3 4 6 4620.50 4728.74 51.05 o 4 4 6 9803.34 10161.54 152.78 o 5 4 6 1834.38 1860.56 31.92 o 6 4 6 4736.74 4826.70 81.17 o 7 4 6 1426.87 1414.43 29.73 o 8 4 6 1717.84 1668.03 39.78 o 9 4 6 272.48 262.10 7.42 o 1 5 6 457.95 479.68 7.63 o 2 5 6 0.08 7.84 3.08 o 3 5 6 6.17 11.97 3.14 o 4 5 6 561.00 567.31 11.12 o 5 5 6 394.57 420.15 7.86 o 6 5 6 64.67 68.63 3.85 o 7 5 6 53.87 55.45 4.11 o 8 5 6 729.46 686.37 15.27 o 0 6 6 8889.05 9436.34 231.87 o 1 6 6 3256.90 3437.20 58.05 o 2 6 6 4604.52 4932.27 78.83 o 3 6 6 823.05 836.01 11.57 o 4 6 6 1777.32 1804.31 36.19 o 5 6 6 150.51 170.73 4.30 o 6 6 6 739.15 728.34 13.15 o 1 7 6 54.86 64.35 3.94 o 2 7 6 0.52 7.44 3.72 o 3 7 6 129.66 131.41 4.41 o 4 7 6 235.42 228.81 4.93 o 1 0 7 342.27 332.93 5.92 o 2 0 7 708.79 668.33 12.35 o 3 0 7 2542.24 2457.58 70.79 o 4 0 7 319.62 319.49 9.21 o 5 0 7 378.64 350.70 8.81 o 6 0 7 1688.05 1663.59 39.62 o 7 0 7 2861.19 2874.84 72.49 o 8 0 7 13.37 19.10 6.09 o 9 0 7 498.10 476.77 14.61 o 10 0 7 372.94 362.80 11.38 o 0 1 7 397.61 455.75 11.97 o 1 1 7 10792.92 10793.17 128.77 o 2 1 7 2650.30 2568.21 37.21 o 3 1 7 7863.25 7706.19 99.65 o 4 1 7 23.36 36.33 3.47 o 5 1 7 5694.69 5553.70 83.13 o 6 1 7 278.90 275.84 4.63 o 7 1 7 3978.58 3984.68 47.23 o 8 1 7 4.92 7.62 4.04 o 9 1 7 2264.22 2279.95 49.35 o 10 1 7 345.03 343.19 9.60 o 1 2 7 2235.93 2260.77 38.77 o 2 2 7 693.27 664.28 10.28 o 3 2 7 2057.80 2045.45 34.83 o 4 2 7 135.11 125.43 3.59 o 5 2 7 86.91 92.55 3.55 o 6 2 7 1054.35 1023.50 22.85 o 7 2 7 359.61 375.03 7.00 o 8 2 7 0.59 5.81 3.89 o 9 2 7 4.02 8.59 4.07 o 10 2 7 607.86 590.48 13.67 o 0 3 7 425.49 419.31 18.46 o 1 3 7 7265.50 7540.30 124.51 o 2 3 7 1696.77 1730.55 27.63 o 3 3 7 6308.68 6374.12 118.61 o 4 3 7 1.36 6.00 3.01 o 5 3 7 4949.30 4962.41 92.56 o 6 3 7 275.26 262.15 6.16 o 7 3 7 3378.82 3503.14 71.21 o 8 3 7 13.42 19.52 3.99 o 9 3 7 1752.22 1600.69 37.82 o 1 4 7 254.43 277.26 7.47 o 2 4 7 366.30 376.14 6.02 o 3 4 7 1517.96 1496.73 32.25 o 4 4 7 136.49 141.57 3.55 o 5 4 7 239.32 249.94 4.99 o 6 4 7 913.13 923.71 15.34 o 7 4 7 1837.86 1780.51 36.69 o 8 4 7 12.33 15.14 3.76 o 0 5 7 60.81 64.31 4.61 o 1 5 7 5240.38 5595.00 76.82 o 2 5 7 984.93 1022.44 14.73 o 3 5 7 3793.94 3999.10 89.40 o 4 5 7 55.38 68.49 3.98 o 5 5 7 2600.41 2509.69 45.40 o 6 5 7 68.86 68.52 3.92 o 7 5 7 2140.57 2034.68 55.59 o 1 6 7 777.67 822.60 13.75 o 2 6 7 173.33 190.36 4.20 o 3 6 7 846.87 879.16 14.57 o 4 6 7 21.07 25.51 3.68 o 5 6 7 33.73 39.10 3.96 o 6 6 7 314.78 293.92 7.24 o 0 7 7 193.70 201.35 6.73 o 1 7 7 2219.57 2176.82 34.67 o 2 7 7 321.78 316.68 7.00 o 3 7 7 2352.58 2251.50 33.51 o 0 0 8 2.77 9.84 5.55 o 1 0 8 329.98 348.60 7.91 o 2 0 8 4893.51 4657.35 79.87 o 3 0 8 1094.45 1066.73 23.74 o 4 0 8 5292.65 5105.21 150.79 o 5 0 8 4319.92 4151.62 73.19 o 6 0 8 6435.46 6102.41 132.33 o 7 0 8 983.22 951.06 15.95 o 8 0 8 1416.47 1475.16 30.46 o 9 0 8 388.32 388.46 13.82 o 1 1 8 718.70 710.14 10.14 o 2 1 8 215.89 208.22 4.45 o 3 1 8 132.46 127.63 4.02 o 4 1 8 157.94 157.65 3.81 o 5 1 8 416.82 386.25 9.50 o 6 1 8 229.89 232.04 4.78 o 7 1 8 150.67 153.74 4.37 o 8 1 8 328.43 334.85 6.30 o 9 1 8 30.82 32.68 4.77 o 0 2 8 4032.29 4091.13 71.85 o 1 2 8 1971.90 2009.77 25.62 o 2 2 8 6226.72 6500.22 100.09 o 3 2 8 63.66 64.65 3.36 o 4 2 8 449.85 450.06 8.87 o 5 2 8 3.83 11.02 3.22 o 6 2 8 2209.90 2134.50 46.96 o 7 2 8 292.11 306.41 7.87 o 8 2 8 3361.70 3288.07 73.14 o 9 2 8 2674.94 2633.48 52.21 o 1 3 8 477.30 509.32 6.62 o 2 3 8 44.83 48.78 3.36 o 3 3 8 89.68 75.03 3.35 o 4 3 8 179.41 187.39 3.93 o 5 3 8 335.12 319.53 6.13 o 6 3 8 280.43 284.20 6.67 o 7 3 8 102.06 95.48 3.89 o 8 3 8 135.93 136.72 4.40 o 9 3 8 13.03 17.85 4.88 o 0 4 8 18.87 32.94 4.98 o 1 4 8 121.66 126.19 4.57 o 2 4 8 3031.04 3179.37 49.32 o 3 4 8 710.56 734.25 14.04 o 4 4 8 3496.33 3480.62 67.70 o 5 4 8 2845.33 2837.39 51.78 o 6 4 8 4210.21 4159.77 75.47 o 7 4 8 685.85 649.19 11.63 o 8 4 8 1004.14 921.96 26.17 o 1 5 8 253.41 258.59 4.78 o 2 5 8 208.82 220.32 5.15 o 3 5 8 62.90 67.64 3.48 o 4 5 8 21.58 26.19 3.53 o 5 5 8 148.47 140.15 4.14 o 6 5 8 71.50 72.83 4.45 o 7 5 8 47.88 45.25 4.30 o 0 6 8 1999.45 2086.23 52.00 o 1 6 8 1034.49 1080.69 20.30 o 2 6 8 2669.23 2743.75 55.50 o 3 6 8 56.01 72.83 4.29 o 4 6 8 305.65 294.17 8.35 o 5 6 8 5.43 14.65 4.09 o 1 7 8 108.32 114.42 4.58 o 2 7 8 0.06 1.45 4.30 o 1 0 9 234.74 243.98 8.39 o 2 0 9 1560.74 1520.99 21.84 o 3 0 9 598.65 617.22 16.06 o 4 0 9 593.29 572.88 18.31 o 5 0 9 0.47 5.92 5.75 o 6 0 9 742.91 696.67 12.97 o 7 0 9 442.87 434.29 9.33 o 8 0 9 574.37 550.41 13.83 o 9 0 9 51.99 58.31 8.19 o 0 1 9 3364.98 3650.37 79.42 o 1 1 9 425.07 459.47 11.38 o 2 1 9 3010.70 3078.69 44.12 o 3 1 9 1700.42 1719.78 22.97 o 4 1 9 2669.68 2611.68 48.55 o 5 1 9 2.26 9.53 3.28 o 6 1 9 2316.15 2276.45 35.92 o 7 1 9 2301.71 2245.43 30.09 o 8 1 9 1939.09 1841.85 31.02 o 9 1 9 211.66 199.60 5.84 o 1 2 9 25.85 33.87 3.14 o 2 2 9 1681.86 1715.87 24.81 o 3 2 9 1547.80 1550.03 24.89 o 4 2 9 204.30 201.11 5.35 o 5 2 9 27.69 31.01 3.67 o 6 2 9 320.67 321.42 6.43 o 7 2 9 76.12 83.31 4.71 o 8 2 9 432.71 412.11 8.53 o 9 2 9 17.57 32.06 12.63 o 0 3 9 2167.22 2279.86 30.87 o 1 3 9 274.22 294.57 4.78 o 2 3 9 2275.80 2348.69 32.83 o 3 3 9 1465.70 1427.54 22.55 o 4 3 9 2511.38 2530.52 45.76 o 5 3 9 14.48 26.25 3.69 o 6 3 9 2192.62 2136.67 38.72 o 7 3 9 1853.52 1669.24 55.90 o 8 3 9 1557.85 1462.31 18.07 o 1 4 9 157.91 175.61 4.08 o 2 4 9 975.58 1007.65 12.99 o 3 4 9 277.47 284.18 4.51 o 4 4 9 334.32 340.14 6.07 o 5 4 9 0.07 4.55 3.48 o 6 4 9 509.00 474.64 10.18 o 7 4 9 240.58 225.80 6.48 o 0 5 9 2141.64 2304.18 60.74 o 1 5 9 408.58 433.85 9.23 o 2 5 9 1770.57 1850.67 27.21 o 3 5 9 841.87 865.43 16.44 o 4 5 9 1320.82 1275.26 31.70 o 5 5 9 0.61 7.05 3.72 o 6 5 9 1170.86 1088.98 19.06 o 1 6 9 6.58 10.26 3.98 o 2 6 9 705.15 733.84 13.80 o 3 6 9 505.81 511.88 8.00 o 4 6 9 110.04 111.33 4.44 o 0 0 10 53.85 62.22 7.08 o 1 0 10 4563.19 4861.18 107.57 o 2 0 10 68.49 80.06 5.29 o 3 0 10 7650.42 7655.79 184.42 o 4 0 10 1429.95 1431.63 41.89 o 5 0 10 4536.61 4320.78 75.17 o 6 0 10 39.55 41.35 6.50 o 7 0 10 3405.12 3270.17 93.83 o 8 0 10 223.16 215.95 7.71 o 1 1 10 472.91 471.16 8.28 o 2 1 10 10.97 14.35 3.19 o 3 1 10 72.96 71.31 3.64 o 4 1 10 647.29 647.92 12.19 o 5 1 10 333.87 322.69 6.73 o 6 1 10 0.52 5.64 4.08 o 7 1 10 181.53 176.54 4.77 o 8 1 10 737.49 732.37 14.83 o 0 2 10 3590.53 3699.04 55.36 o 1 2 10 7980.11 8386.08 108.78 o 2 2 10 110.34 128.44 3.81 o 3 2 10 4548.53 4748.63 83.52 o 4 2 10 199.26 198.17 5.94 o 5 2 10 1386.90 1424.42 28.71 o 6 2 10 1086.17 994.10 14.88 o 7 2 10 3399.44 3137.02 43.07 o 8 2 10 3.39 9.69 4.34 o 1 3 10 229.05 230.42 4.24 o 2 3 10 11.94 17.40 3.32 o 3 3 10 151.92 145.83 4.02 o 4 3 10 429.38 428.28 7.06 o 5 3 10 275.34 274.02 4.74 o 6 3 10 0.01 2.54 3.83 o 7 3 10 257.04 249.22 7.53 o 0 4 10 69.18 69.83 4.89 o 1 4 10 2921.91 3154.40 38.86 o 2 4 10 65.63 74.03 3.77 o 3 4 10 4942.37 5073.77 72.45 o 4 4 10 837.87 835.53 18.09 o 5 4 10 3080.17 2980.97 47.01 o 6 4 10 28.02 32.03 3.84 o 1 5 10 288.37 303.67 6.79 o 2 5 10 2.84 6.23 4.01 o 3 5 10 1.12 6.07 4.18 o 4 5 10 280.09 273.35 7.27 o 5 5 10 150.94 148.05 4.57 o 0 6 10 1245.66 1224.24 34.76 o 1 6 10 3440.61 3493.56 59.17 o 2 6 10 25.07 31.84 4.25 o 1 0 11 323.99 346.96 7.54 o 2 0 11 1028.74 1032.56 22.75 o 3 0 11 218.63 213.63 5.86 o 4 0 11 525.72 554.43 16.24 o 5 0 11 191.67 187.03 6.73 o 6 0 11 725.85 701.47 18.77 o 7 0 11 1174.05 1146.37 32.59 o 8 0 11 9.80 11.67 12.61 o 0 1 11 2526.34 2737.87 68.95 o 1 1 11 1106.40 1180.79 21.54 o 2 1 11 9628.43 10055.75 157.99 o 3 1 11 798.59 790.56 12.35 o 4 1 11 2855.88 2934.09 46.27 o 5 1 11 447.43 434.44 9.44 o 6 1 11 3969.38 3726.93 69.35 o 7 1 11 195.31 192.95 7.37 o 1 2 11 366.30 394.65 7.72 o 2 2 11 28.75 31.53 3.64 o 3 2 11 1344.45 1341.41 23.01 o 4 2 11 23.65 51.90 5.81 o 5 2 11 26.76 31.04 3.92 o 6 2 11 1214.89 1167.04 27.49 o 7 2 11 72.99 72.04 5.08 o 0 3 11 1824.97 1987.32 29.92 o 1 3 11 655.23 687.48 11.10 o 2 3 11 7471.14 7901.54 126.54 o 3 3 11 696.08 693.16 10.88 o 4 3 11 2598.79 2579.30 46.76 o 5 3 11 522.37 511.34 10.99 o 6 3 11 3397.39 3208.29 67.15 o 1 4 11 212.65 213.28 4.68 o 2 4 11 651.29 675.61 7.26 o 3 4 11 159.02 162.64 4.57 o 4 4 11 327.86 314.93 5.15 o 5 4 11 113.41 115.12 4.57 o 0 5 11 1658.96 1662.18 19.36 o 1 5 11 690.36 711.89 11.65 o 2 5 11 4908.05 5025.04 77.91 o 3 5 11 362.97 344.05 6.68 o 4 5 11 1482.94 1355.28 37.96 o 0 0 12 668.01 746.89 38.91 o 1 0 12 7675.03 8304.74 219.18 o 2 0 12 1929.38 1978.03 45.03 o 3 0 12 2756.97 2862.61 84.88 o 4 0 12 1590.66 1538.95 32.06 o 5 0 12 105.38 137.39 13.02 o 6 0 12 1560.53 1450.03 36.46 o 7 0 12 1308.05 1171.70 54.20 o 1 1 12 409.60 428.30 7.49 o 2 1 12 148.34 165.70 4.23 o 3 1 12 6.05 11.94 3.76 o 4 1 12 22.12 24.66 3.75 o 5 1 12 688.75 639.02 11.60 o 6 1 12 246.44 223.02 5.48 o 0 2 12 1470.27 1570.85 40.70 o 1 2 12 1534.75 1684.45 24.66 o 2 2 12 1830.89 1843.21 29.46 o 3 2 12 4571.15 4623.28 85.03 o 4 2 12 643.71 606.40 11.74 o 5 2 12 3052.52 2950.69 56.43 o 6 2 12 1186.06 1075.61 15.11 o 1 3 12 330.20 349.80 5.75 o 2 3 12 37.27 42.65 4.31 o 3 3 12 0.69 7.95 4.05 o 4 3 12 36.79 37.37 4.40 o 5 3 12 548.43 510.36 11.72 o 0 4 12 504.79 503.85 9.78 o 1 4 12 4943.73 5197.04 80.99 o 2 4 12 1322.05 1281.53 15.34 o 3 4 12 1755.88 1717.63 26.99 o 4 4 12 1118.15 1009.27 13.73 o 1 5 12 158.41 147.18 4.93 o 1 0 13 309.47 310.54 15.15 o 2 0 13 875.35 905.94 25.54 o 3 0 13 6.95 10.50 5.46 o 4 0 13 282.96 274.50 7.87 o 5 0 13 17.68 17.83 6.61 o 0 1 13 839.96 948.05 22.66 o 1 1 13 1507.60 1564.47 25.00 o 2 1 13 983.81 1079.59 18.37 o 3 1 13 2510.81 2493.26 51.39 o 4 1 13 569.40 570.99 13.25 o 5 1 13 446.18 413.31 8.89 o 1 2 13 0.04 3.51 4.00 o 2 2 13 69.54 71.08 4.17 o 3 2 13 820.52 800.81 13.83 o 4 2 13 0.39 3.95 4.26 o 5 2 13 5.95 10.58 4.51 o 0 3 13 895.38 974.09 19.03 o 1 3 13 1212.43 1215.46 18.65 o 2 3 13 847.20 877.15 15.08 o 3 3 13 2201.23 2022.14 39.64 o 4 3 13 340.10 317.03 5.93 o 1 4 13 199.45 191.73 5.21 o 2 4 13 546.35 472.78 25.10 o 0 0 14 1468.40 1504.16 52.59 o 1 0 14 8.08 13.61 5.73 o 2 0 14 2496.17 2371.94 51.81 o 3 0 14 27.19 36.02 6.71 o 4 0 14 132.21 116.94 7.33 o 1 1 14 83.91 84.27 4.30 o 2 1 14 7.94 9.11 4.08 o 3 1 14 98.69 95.63 4.33 o 0 2 14 12.15 21.39 5.70 o 1 2 14 7.84 11.96 4.12 o 2 2 14 1392.99 1323.89 22.07 o 3 2 14 2.66 14.72 4.58 o