#------------------------------------------------------------------------------ #$Date: 2010-03-05 20:15:21 +0200 (Fri, 05 Mar 2010) $ #$Revision: 1024 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2225045.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225045_Fobs loop_ _publ_author_name 'Duke, III, Charles B.' 'Ross, Charles R.' 'Burkey, Theodore J.' _publ_section_title ; Tricarbonyl(2-methyl-2-\h^6^-phenyl-1,3-dioxolane)chromium(0) ; _journal_coeditor_code KP2246 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m148 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.573 _cell_angle_beta 79.277 _cell_angle_gamma 62.734 _cell_length_a 7.1950 _cell_length_b 7.2120 _cell_length_c 13.9235 _exptl_crystal_F_000 308.00 _reflns_d_resolution_high 0.8274 _[local]_cod_data_source_file kp2246Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' act1 in P1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 92.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7257.34 8027.11 114.16 o 2 0 0 1109.98 1272.33 27.22 o 3 0 0 113.51 145.93 5.00 o 4 0 0 97.81 105.26 1.88 o 5 0 0 253.18 265.02 2.77 o 6 0 0 83.48 85.40 1.77 o 7 0 0 131.92 128.75 2.11 o -7 1 0 72.12 73.88 4.15 o -6 1 0 54.57 57.53 1.56 o -5 1 0 462.44 451.21 4.97 o -4 1 0 2.60 3.65 0.66 o -3 1 0 5.73 9.79 1.13 o -2 1 0 16.11 20.60 1.96 o -1 1 0 158.16 160.97 2.79 o 0 1 0 3273.84 3548.84 65.89 o 1 1 0 1303.46 1474.98 22.05 o 2 1 0 868.25 936.04 14.18 o 3 1 0 44.86 62.69 2.84 o 4 1 0 1605.88 1611.55 14.20 o 5 1 0 374.51 364.98 3.55 o 6 1 0 135.12 135.57 2.05 o 7 1 0 147.93 152.95 2.10 o 8 1 0 179.68 195.50 6.60 o -6 2 0 12.34 10.19 0.98 o -5 2 0 2.41 2.15 1.00 o -4 2 0 134.32 135.35 2.21 o -3 2 0 186.30 177.95 2.75 o -2 2 0 3094.95 3195.99 53.27 o -1 2 0 5011.97 5194.79 73.49 o 0 2 0 21.53 22.52 1.13 o 1 2 0 32.54 35.97 1.19 o 2 2 0 100.46 111.95 3.01 o 3 2 0 11.37 14.51 1.54 o 4 2 0 99.64 79.35 1.68 o 5 2 0 29.98 27.72 1.11 o 6 2 0 788.68 808.73 6.63 o 7 2 0 335.99 330.57 3.06 o 8 2 0 60.73 56.81 3.32 o -5 3 0 239.93 223.79 4.65 o -4 3 0 176.81 168.81 3.02 o -3 3 0 717.18 714.44 7.88 o -2 3 0 642.33 632.89 7.75 o -1 3 0 629.44 588.02 8.24 o 0 3 0 112.32 111.22 3.47 o 1 3 0 817.79 879.29 28.02 o 2 3 0 1415.55 1576.04 46.41 o 3 3 0 2279.97 2414.69 28.56 o 4 3 0 95.52 88.16 1.79 o 5 3 0 238.62 232.07 2.67 o 6 3 0 936.42 946.04 7.64 o 7 3 0 236.69 228.38 2.87 o 8 3 0 0.86 0.54 0.97 o -5 4 0 3.72 5.59 1.89 o -4 4 0 15.21 12.26 1.82 o -3 4 0 727.37 713.34 8.31 o -2 4 0 1305.74 1290.79 12.02 o -1 4 0 14.80 11.48 0.94 o 0 4 0 8.09 8.30 1.49 o 1 4 0 303.77 339.63 7.57 o 2 4 0 212.70 254.35 3.54 o 3 4 0 308.68 264.59 3.30 o 4 4 0 77.79 68.01 1.79 o 5 4 0 465.94 467.23 4.25 o 6 4 0 88.56 94.03 1.96 o 7 4 0 76.29 75.62 2.22 o 8 4 0 2.04 1.84 1.15 o -3 5 0 13.76 16.90 2.09 o -2 5 0 91.58 94.67 3.07 o -1 5 0 31.41 38.60 2.26 o 0 5 0 43.15 42.38 1.74 o 1 5 0 345.43 338.09 4.69 o 2 5 0 346.04 326.12 4.66 o 3 5 0 783.85 776.78 6.58 o 4 5 0 447.30 465.50 4.87 o 5 5 0 650.58 629.88 5.70 o 6 5 0 201.01 185.99 2.59 o 7 5 0 116.24 122.39 2.13 o 8 5 0 31.08 33.01 1.55 o -2 6 0 104.01 102.88 3.68 o -1 6 0 4.67 3.05 1.57 o 0 6 0 53.27 54.11 2.09 o 1 6 0 27.74 32.94 1.65 o 2 6 0 47.70 55.17 2.54 o 3 6 0 115.31 133.63 2.86 o 4 6 0 426.20 443.34 4.47 o 5 6 0 69.32 74.51 1.98 o 6 6 0 3.03 3.79 1.46 o 7 6 0 9.35 10.56 1.26 o 8 6 0 17.35 16.72 2.08 o -1 7 0 15.13 11.94 4.53 o 0 7 0 133.49 139.18 3.46 o 1 7 0 129.16 127.46 3.66 o 2 7 0 99.65 96.94 2.64 o 3 7 0 139.06 145.02 2.67 o 4 7 0 317.55 344.55 4.42 o 5 7 0 2.52 3.00 1.17 o 6 7 0 8.95 9.22 1.45 o 7 7 0 6.55 6.27 2.07 o 2 8 0 322.03 317.86 7.76 o 3 8 0 140.12 124.98 9.97 o 4 8 0 6.60 5.87 4.15 o 5 8 0 10.45 6.19 2.39 o -4 -8 1 18.86 13.57 5.04 o -3 -8 1 27.73 31.88 5.44 o -2 -8 1 125.70 125.53 7.32 o -7 -7 1 110.10 110.55 4.26 o -6 -7 1 168.59 179.17 3.20 o -5 -7 1 365.87 363.67 3.97 o -4 -7 1 50.63 55.73 1.78 o -3 -7 1 14.25 11.48 1.37 o -2 -7 1 2.40 1.04 1.42 o -1 -7 1 1.95 1.09 1.95 o 0 -7 1 19.83 19.17 1.99 o 1 -7 1 74.56 78.53 5.86 o -7 -6 1 150.58 154.51 3.96 o -6 -6 1 261.86 253.32 3.54 o -5 -6 1 185.87 171.46 2.41 o -4 -6 1 511.52 505.47 4.90 o -3 -6 1 209.68 226.79 3.05 o -2 -6 1 100.65 109.92 2.68 o -1 -6 1 30.03 32.11 1.95 o 0 -6 1 91.96 97.86 2.65 o 1 -6 1 378.94 389.30 5.31 o 2 -6 1 33.88 37.20 2.54 o -8 -5 1 95.32 97.71 5.90 o -7 -5 1 61.83 59.79 1.62 o -6 -5 1 52.61 58.96 1.92 o -5 -5 1 50.46 56.13 1.80 o -4 -5 1 471.33 471.44 4.87 o -3 -5 1 16.63 19.66 1.38 o -2 -5 1 212.30 224.55 2.92 o -1 -5 1 155.50 156.69 2.76 o 0 -5 1 406.87 403.65 5.00 o 1 -5 1 1595.59 1602.67 15.81 o 2 -5 1 1036.41 1050.31 12.62 o 3 -5 1 100.19 92.85 2.35 o -8 -4 1 13.31 16.17 1.35 o -7 -4 1 76.82 77.35 2.07 o -6 -4 1 136.17 140.94 2.47 o -5 -4 1 93.36 89.63 1.90 o -4 -4 1 293.66 305.55 3.42 o -3 -4 1 432.68 499.52 5.10 o -2 -4 1 72.35 56.90 1.63 o -1 -4 1 171.75 156.09 2.71 o 0 -4 1 871.98 843.08 23.61 o 1 -4 1 332.47 331.28 4.27 o 2 -4 1 331.63 347.54 5.78 o 3 -4 1 35.79 36.45 2.53 o 4 -4 1 26.47 27.85 2.26 o -8 -3 1 12.48 13.06 1.31 o -7 -3 1 437.12 436.23 4.57 o -6 -3 1 288.77 279.22 3.09 o -5 -3 1 3.97 4.56 0.89 o -4 -3 1 200.88 196.75 2.50 o -3 -3 1 174.21 196.13 2.72 o -2 -3 1 210.95 179.43 3.43 o -1 -3 1 714.74 666.37 20.32 o 0 -3 1 2057.76 1960.26 43.96 o 1 -3 1 665.35 628.23 11.59 o 2 -3 1 584.95 568.11 6.84 o 3 -3 1 0.19 0.20 0.95 o 4 -3 1 259.04 243.95 3.43 o 5 -3 1 231.01 220.39 4.85 o -8 -2 1 18.95 20.12 2.24 o -7 -2 1 173.40 179.42 2.44 o -6 -2 1 109.79 113.50 1.99 o -5 -2 1 40.67 48.87 1.49 o -4 -2 1 217.24 198.91 2.59 o -3 -2 1 1688.27 1746.29 23.54 o -2 -2 1 2468.18 2675.16 49.02 o -1 -2 1 437.83 457.45 7.21 o 0 -2 1 121.05 149.18 4.40 o 1 -2 1 598.61 553.35 9.62 o 2 -2 1 82.94 69.32 3.02 o 3 -2 1 212.10 214.54 3.08 o 4 -2 1 1092.98 1034.45 9.33 o 5 -2 1 225.45 219.55 3.54 o 6 -2 1 288.90 300.29 5.87 o -8 -1 1 36.41 42.96 2.36 o -7 -1 1 28.91 35.28 1.27 o -6 -1 1 392.53 400.28 4.05 o -5 -1 1 85.59 94.28 1.73 o -4 -1 1 218.81 208.91 2.74 o -3 -1 1 2496.17 2612.70 79.41 o -2 -1 1 244.52 239.21 7.64 o -1 -1 1 6720.17 7303.02 111.59 o 0 -1 1 4591.27 4914.27 75.96 o 1 -1 1 1339.27 1469.09 19.44 o 2 -1 1 204.69 236.62 4.38 o 3 -1 1 8.94 16.83 1.22 o 4 -1 1 23.10 21.25 1.04 o 5 -1 1 14.63 15.79 1.45 o 6 -1 1 214.78 209.00 3.35 o 7 -1 1 143.11 129.41 7.69 o -7 0 1 29.42 26.54 1.18 o -6 0 1 36.56 44.08 1.35 o -5 0 1 195.22 201.02 2.56 o -4 0 1 1127.83 1155.96 9.54 o -3 0 1 733.84 681.22 8.99 o -2 0 1 670.29 826.01 16.65 o -1 0 1 279.81 320.89 4.38 o 0 0 1 102.98 118.82 1.75 o 1 0 1 277.67 320.16 4.62 o 2 0 1 501.77 570.46 9.81 o 3 0 1 888.42 876.09 19.36 o 4 0 1 304.13 286.30 3.41 o 5 0 1 369.75 364.20 3.65 o 6 0 1 222.08 224.24 3.03 o 7 0 1 307.81 302.55 4.15 o -7 1 1 0.95 -0.05 2.05 o -6 1 1 67.61 71.43 1.85 o -5 1 1 228.29 231.90 2.68 o -4 1 1 977.81 943.07 7.34 o -3 1 1 946.84 935.61 9.13 o -2 1 1 816.51 868.15 23.30 o -1 1 1 504.12 586.62 10.81 o 0 1 1 579.47 583.78 7.87 o 1 1 1 479.81 565.29 7.93 o 2 1 1 81.71 105.25 2.23 o 3 1 1 1186.68 1241.25 28.67 o 4 1 1 216.89 179.97 3.38 o 5 1 1 122.37 110.82 1.75 o 6 1 1 10.56 13.81 1.02 o 7 1 1 188.36 191.72 2.48 o 8 1 1 1.66 2.41 2.08 o -6 2 1 348.97 337.34 7.13 o -5 2 1 602.13 585.87 5.92 o -4 2 1 1109.83 1132.52 9.85 o -3 2 1 608.73 592.21 5.28 o -2 2 1 1081.96 1080.78 20.91 o -1 2 1 63.01 66.28 1.90 o 0 2 1 55.30 54.80 1.64 o 1 2 1 244.35 269.72 4.59 o 2 2 1 51.43 51.05 1.54 o 3 2 1 499.85 492.38 12.42 o 4 2 1 1573.86 1568.49 15.23 o 5 2 1 1188.61 1181.95 8.69 o 6 2 1 86.95 85.18 1.71 o 7 2 1 56.26 57.48 2.22 o 8 2 1 13.52 14.36 1.34 o -5 3 1 155.28 147.27 2.76 o -4 3 1 122.67 125.88 2.36 o -3 3 1 221.33 234.58 3.05 o -2 3 1 4.59 8.03 1.09 o -1 3 1 687.14 717.59 12.16 o 0 3 1 622.22 578.67 11.01 o 1 3 1 18.15 31.75 1.38 o 2 3 1 359.87 310.33 9.37 o 3 3 1 18.89 23.47 1.44 o 4 3 1 605.55 573.34 5.76 o 5 3 1 166.93 169.12 2.28 o 6 3 1 9.15 10.70 1.10 o 7 3 1 178.89 172.48 2.27 o 8 3 1 81.82 84.77 2.27 o -5 4 1 113.17 121.96 6.30 o -4 4 1 123.51 110.12 6.26 o -3 4 1 564.04 545.36 7.26 o -2 4 1 66.94 62.35 1.94 o -1 4 1 438.49 426.29 4.59 o 0 4 1 460.37 470.73 8.25 o 1 4 1 27.42 24.21 2.12 o 2 4 1 1362.10 1229.13 17.53 o 3 4 1 854.85 791.37 7.40 o 4 4 1 829.51 827.56 8.01 o 5 4 1 13.67 13.66 1.05 o 6 4 1 64.16 73.79 1.86 o 7 4 1 13.73 15.51 1.14 o 8 4 1 35.72 37.58 2.02 o -4 5 1 84.03 79.33 3.06 o -3 5 1 1.94 1.80 1.84 o -2 5 1 128.57 131.04 3.39 o -1 5 1 13.97 14.89 1.88 o 0 5 1 194.99 196.45 2.95 o 1 5 1 1069.38 1043.38 11.14 o 2 5 1 666.16 655.43 6.88 o 3 5 1 122.19 120.24 2.14 o 4 5 1 23.52 22.04 1.32 o 5 5 1 0.90 -0.07 0.99 o 6 5 1 755.58 728.45 6.00 o 7 5 1 693.60 691.68 6.14 o 8 5 1 103.60 110.89 2.74 o -2 6 1 6.05 4.04 1.73 o -1 6 1 12.38 11.28 2.25 o 0 6 1 57.81 64.20 2.68 o 1 6 1 469.89 468.42 5.93 o 2 6 1 326.50 320.47 4.23 o 3 6 1 466.95 464.95 6.10 o 4 6 1 58.73 63.24 1.91 o 5 6 1 278.67 273.41 3.11 o 6 6 1 253.30 259.24 3.17 o 7 6 1 120.64 127.77 2.39 o 8 6 1 153.02 155.09 4.28 o -1 7 1 390.13 407.56 14.38 o 0 7 1 295.55 307.37 5.67 o 1 7 1 70.68 73.22 5.40 o 2 7 1 226.03 216.93 3.80 o 3 7 1 545.50 524.51 6.83 o 4 7 1 18.61 19.94 1.62 o 5 7 1 470.56 462.36 5.52 o 6 7 1 121.90 128.09 2.94 o 7 7 1 127.98 140.05 5.10 o 1 8 1 32.53 35.23 2.17 o 2 8 1 1.12 1.31 1.79 o 3 8 1 118.39 126.18 4.47 o 4 8 1 92.05 108.24 3.93 o 5 8 1 37.98 28.13 2.44 o -4 -8 2 10.29 1.86 4.34 o -3 -8 2 10.51 7.19 4.37 o -6 -7 2 109.04 109.93 2.59 o -5 -7 2 47.49 33.55 2.11 o -4 -7 2 0.98 1.83 1.23 o -3 -7 2 9.55 7.30 1.30 o -2 -7 2 97.34 102.36 2.58 o -1 -7 2 102.61 107.26 3.47 o 0 -7 2 121.20 125.87 3.25 o -7 -6 2 88.15 92.81 2.38 o -6 -6 2 70.13 63.01 2.30 o -5 -6 2 28.69 27.85 1.97 o -4 -6 2 155.63 156.38 2.53 o -3 -6 2 59.44 67.78 1.95 o -2 -6 2 1070.80 1097.06 10.40 o -1 -6 2 527.46 554.11 6.88 o 0 -6 2 168.58 174.07 3.04 o 1 -6 2 137.48 141.92 3.75 o 2 -6 2 116.57 113.92 3.24 o -8 -5 2 96.41 104.28 6.64 o -7 -5 2 26.22 31.69 1.67 o -6 -5 2 6.37 6.86 1.26 o -5 -5 2 27.56 28.54 1.68 o -4 -5 2 9.51 8.32 1.25 o -3 -5 2 897.90 877.79 7.82 o -2 -5 2 278.28 264.40 3.31 o -1 -5 2 370.01 356.24 4.44 o 0 -5 2 170.02 170.03 2.80 o 1 -5 2 16.80 18.75 1.43 o 2 -5 2 364.81 376.81 5.83 o 3 -5 2 23.05 24.80 1.54 o -8 -4 2 65.39 67.38 2.08 o -7 -4 2 3.80 4.48 1.14 o -6 -4 2 135.31 129.17 2.32 o -5 -4 2 17.69 15.27 1.39 o -4 -4 2 273.93 273.01 3.15 o -3 -4 2 1724.45 1726.29 15.51 o -2 -4 2 219.09 197.36 2.75 o -1 -4 2 711.96 653.37 6.37 o 0 -4 2 54.09 49.37 2.34 o 1 -4 2 244.55 251.10 3.62 o 2 -4 2 192.72 196.81 3.62 o 3 -4 2 6.90 6.90 1.65 o 4 -4 2 156.85 153.55 3.71 o -8 -3 2 92.55 92.76 2.72 o -7 -3 2 0.48 0.62 1.10 o -6 -3 2 34.70 43.61 1.84 o -5 -3 2 635.23 594.92 5.73 o -4 -3 2 1547.05 1565.44 13.64 o -3 -3 2 1831.86 1846.00 17.39 o -2 -3 2 2113.96 2096.03 25.95 o -1 -3 2 637.95 611.17 8.58 o 0 -3 2 45.24 52.54 2.26 o 1 -3 2 504.44 484.06 9.31 o 2 -3 2 9.04 8.70 0.96 o 3 -3 2 281.33 271.84 4.28 o 4 -3 2 333.09 335.36 5.39 o 5 -3 2 516.94 522.16 9.39 o -8 -2 2 4.56 6.64 1.40 o -7 -2 2 125.32 125.29 2.19 o -6 -2 2 25.68 31.28 1.46 o -5 -2 2 211.22 190.45 2.45 o -4 -2 2 1779.73 1693.86 14.61 o -3 -2 2 846.26 777.95 9.62 o -2 -2 2 978.29 1019.72 18.03 o -1 -2 2 1356.50 1458.83 21.53 o 0 -2 2 129.67 133.78 3.12 o 1 -2 2 78.16 91.13 3.03 o 2 -2 2 11.97 20.82 1.25 o 3 -2 2 604.24 538.66 5.96 o 4 -2 2 15.00 16.14 1.25 o 5 -2 2 19.22 20.65 1.48 o 6 -2 2 103.64 101.97 3.11 o -7 -1 2 18.38 21.18 1.16 o -6 -1 2 414.92 416.17 4.46 o -5 -1 2 675.30 680.45 5.94 o -4 -1 2 970.75 942.95 8.24 o -3 -1 2 881.34 875.19 17.34 o -2 -1 2 1619.34 1762.73 30.48 o -1 -1 2 1483.24 1692.53 34.76 o 0 -1 2 3577.60 3756.63 105.28 o 1 -1 2 361.41 365.40 7.15 o 2 -1 2 1282.55 1292.23 20.31 o 3 -1 2 639.77 585.11 8.29 o 4 -1 2 269.23 243.45 3.21 o 5 -1 2 182.99 177.28 2.46 o 6 -1 2 280.84 267.70 3.81 o -7 0 2 78.83 74.49 2.22 o -6 0 2 455.91 459.36 4.13 o -5 0 2 523.23 531.47 4.87 o -4 0 2 155.05 139.84 2.32 o -3 0 2 802.49 830.75 10.55 o -2 0 2 60.04 64.94 2.01 o -1 0 2 447.19 517.89 12.03 o 0 0 2 3386.33 3643.96 54.52 o 1 0 2 1015.42 1164.25 15.43 o 2 0 2 6527.58 7205.00 151.10 o 3 0 2 777.51 821.62 14.80 o 4 0 2 86.54 80.41 2.27 o 5 0 2 44.31 49.87 1.43 o 6 0 2 11.72 15.15 1.16 o 7 0 2 52.35 54.71 1.72 o -7 1 2 308.89 317.23 6.35 o -6 1 2 140.66 145.33 2.19 o -5 1 2 244.55 251.30 2.82 o -4 1 2 189.88 193.48 2.45 o -3 1 2 836.35 895.47 8.46 o -2 1 2 248.66 317.99 14.12 o -1 1 2 1373.32 1619.68 30.12 o 0 1 2 114.58 130.98 2.06 o 1 1 2 1376.70 1537.94 21.82 o 2 1 2 1492.03 1658.43 24.72 o 3 1 2 1260.39 1285.71 25.27 o 4 1 2 1176.80 1204.20 13.94 o 5 1 2 0.65 3.39 0.75 o 6 1 2 580.52 571.61 5.53 o 7 1 2 245.81 243.83 2.93 o 8 1 2 143.56 140.15 7.90 o -6 2 2 73.01 71.09 2.09 o -5 2 2 33.07 36.05 1.38 o -4 2 2 57.16 59.11 1.51 o -3 2 2 553.87 585.43 5.18 o -2 2 2 27.17 25.30 1.49 o -1 2 2 26.09 27.28 7.25 o 0 2 2 4024.98 3958.84 59.67 o 1 2 2 8467.17 8851.71 126.69 o 2 2 2 267.98 319.52 5.45 o 3 2 2 336.30 329.83 12.54 o 4 2 2 1094.27 1139.56 15.35 o 5 2 2 76.90 78.10 1.64 o 6 2 2 873.30 874.08 6.84 o 7 2 2 463.36 455.85 4.66 o 8 2 2 533.18 550.20 7.90 o -5 3 2 5.20 7.34 1.20 o -4 3 2 192.64 188.75 2.93 o -3 3 2 3.45 3.27 0.84 o -2 3 2 10.65 18.93 1.91 o -1 3 2 893.44 840.46 13.64 o 0 3 2 1100.32 1091.88 19.20 o 1 3 2 1613.43 1610.47 23.52 o 2 3 2 26.96 24.01 1.21 o 3 3 2 500.48 517.93 12.83 o 4 3 2 36.09 32.91 1.24 o 5 3 2 448.98 438.42 4.66 o 6 3 2 214.21 212.55 2.59 o 7 3 2 34.86 37.98 1.50 o 8 3 2 72.13 74.00 1.85 o -5 4 2 22.53 26.74 4.03 o -4 4 2 56.56 52.32 2.30 o -3 4 2 9.36 10.54 1.34 o -2 4 2 182.36 172.78 2.75 o -1 4 2 968.50 916.19 9.49 o 0 4 2 1061.37 1026.39 15.43 o 1 4 2 1136.41 1122.39 29.77 o 2 4 2 679.43 720.23 15.34 o 3 4 2 33.95 35.03 1.64 o 4 4 2 110.81 120.21 2.02 o 5 4 2 445.63 425.57 4.06 o 6 4 2 540.24 531.91 4.67 o 7 4 2 889.46 899.65 7.39 o 8 4 2 41.72 44.34 1.92 o -4 5 2 7.68 10.12 1.89 o -3 5 2 15.85 14.49 1.82 o -2 5 2 167.41 164.15 3.15 o -1 5 2 61.43 60.47 2.76 o 0 5 2 255.22 231.30 3.32 o 1 5 2 229.57 221.00 3.30 o 2 5 2 117.69 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