#------------------------------------------------------------------------------ #$Date: 2010-03-05 20:15:21 +0200 (Fri, 05 Mar 2010) $ #$Revision: 1024 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2225062.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225062_Fobs loop_ _publ_author_name 'Ioannou, Savvas' 'Nicolaides, Athanassios V.' 'Manos, Manolis J.' _publ_section_title ; Tricyclo[3.3.1.0^3,7^]nonane-3,7-diyl bis(methanesulfonate) ; _journal_coeditor_code NC2172 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o409 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.092 _cell_angle_gamma 90.000 _cell_length_a 8.8017 _cell_length_b 10.3107 _cell_length_c 14.4623 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file nc2172Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' OMS in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 223.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1364.94 1357.57 16.55 o 4 0 0 3.22 6.55 8.28 o 6 0 0 734.78 732.64 19.10 o 8 0 0 307.46 347.16 17.69 o 10 0 0 34.58 55.18 40.17 o 1 1 0 734.17 791.35 13.66 o 2 1 0 27010.35 25956.54 132.35 o 3 1 0 4.88 2.51 5.08 o 4 1 0 43.39 42.22 6.16 o 5 1 0 600.45 645.85 11.47 o 6 1 0 89.78 85.19 9.26 o 7 1 0 4.12 6.96 9.26 o 8 1 0 614.91 592.86 17.79 o 9 1 0 11.28 2.59 13.49 o 10 1 0 758.93 852.47 35.98 o 0 2 0 49820.17 51270.48 528.15 o 1 2 0 2003.05 2143.89 14.33 o 2 2 0 834.51 870.83 10.91 o 3 2 0 516.18 599.45 11.15 o 4 2 0 167.21 208.89 9.43 o 5 2 0 837.00 890.32 15.85 o 6 2 0 175.34 177.90 11.53 o 7 2 0 30.31 19.96 10.81 o 8 2 0 237.42 254.89 14.43 o 9 2 0 9.08 17.03 12.51 o 10 2 0 51.51 54.83 21.93 o 1 3 0 4801.06 4975.89 28.26 o 2 3 0 8.78 4.55 4.91 o 3 3 0 100.21 94.57 5.27 o 4 3 0 1125.88 1098.63 16.10 o 5 3 0 195.31 230.71 11.02 o 6 3 0 0.95 0.86 9.87 o 7 3 0 853.20 836.43 19.32 o 8 3 0 1111.64 1113.98 22.93 o 9 3 0 24.49 26.96 12.57 o 10 3 0 437.92 465.05 25.62 o 0 4 0 2159.98 2321.54 29.96 o 1 4 0 8270.29 8590.90 38.41 o 2 4 0 5.51 0.40 6.99 o 3 4 0 761.67 780.38 11.14 o 4 4 0 12.66 6.39 4.20 o 5 4 0 63.49 68.47 10.01 o 6 4 0 1565.77 1535.22 23.21 o 7 4 0 15.10 18.45 11.04 o 8 4 0 817.75 869.31 21.54 o 9 4 0 158.42 169.27 15.38 o 1 5 0 2861.94 3054.36 26.04 o 2 5 0 379.61 353.53 12.29 o 3 5 0 525.58 516.69 11.65 o 4 5 0 871.65 747.74 16.41 o 5 5 0 201.16 181.70 12.63 o 6 5 0 326.53 346.24 15.99 o 7 5 0 143.96 136.93 14.86 o 8 5 0 1133.74 1194.24 30.89 o 9 5 0 1.69 7.47 15.17 o 0 6 0 2733.58 2600.36 60.18 o 1 6 0 2677.65 2897.75 27.80 o 2 6 0 54.16 88.15 9.90 o 3 6 0 619.24 642.88 20.99 o 4 6 0 1560.80 1501.56 27.95 o 5 6 0 109.79 113.55 15.35 o 6 6 0 478.32 491.87 21.51 o 7 6 0 11.47 10.35 14.90 o 8 6 0 1023.86 994.56 30.15 o 9 6 0 20.14 10.45 20.45 o 1 7 0 0.83 2.84 8.89 o 2 7 0 157.81 150.96 11.55 o 3 7 0 13.45 10.31 12.59 o 4 7 0 2742.80 2626.77 57.34 o 5 7 0 878.63 856.16 25.33 o 6 7 0 0.08 1.24 14.94 o 7 7 0 699.25 742.89 26.99 o 8 7 0 230.27 238.16 20.73 o 0 8 0 856.69 860.67 49.45 o 1 8 0 1408.69 1365.55 27.21 o 2 8 0 337.87 364.55 36.12 o 3 8 0 745.20 699.34 27.75 o 4 8 0 1320.06 1298.26 29.39 o 5 8 0 932.73 951.26 27.42 o 6 8 0 147.51 150.49 18.70 o 7 8 0 158.69 163.01 19.40 o 1 9 0 363.61 374.76 23.72 o 2 9 0 434.43 392.70 24.60 o 3 9 0 204.97 205.34 22.30 o 4 9 0 672.09 691.80 30.15 o 5 9 0 635.01 607.11 31.11 o 6 9 0 66.37 81.23 20.84 o 7 9 0 946.48 1048.53 33.12 o 0 10 0 1177.38 1079.35 39.95 o 1 10 0 816.18 717.27 30.42 o 2 10 0 5.18 13.35 18.49 o 3 10 0 295.39 277.92 24.90 o 4 10 0 114.29 90.75 21.13 o 5 10 0 198.07 205.48 24.08 o 6 10 0 0.05 0.00 21.39 o 1 11 0 4.41 14.95 19.99 o 2 11 0 922.32 861.88 35.15 o 3 11 0 55.00 44.35 19.15 o 4 11 0 9.13 13.89 20.94 o 0 12 0 1618.60 1551.58 81.80 o 1 12 0 49.24 51.35 27.22 o 2 12 0 21.94 13.31 22.40 o -9 0 1 2.51 0.00 22.42 o -7 0 1 1020.18 936.10 27.13 o -5 0 1 746.59 721.42 16.94 o -3 0 1 416.40 545.46 18.28 o 3 0 1 8464.03 8891.67 39.13 o 5 0 1 660.44 670.47 16.64 o 7 0 1 704.39 731.68 20.98 o 9 0 1 21.14 10.12 17.28 o -10 1 1 168.51 143.76 23.55 o -9 1 1 1019.24 1000.64 37.58 o -8 1 1 3.48 2.35 9.98 o -7 1 1 819.61 850.39 17.12 o -6 1 1 205.48 196.73 10.39 o -5 1 1 923.87 1055.48 18.52 o -4 1 1 1425.89 1474.66 26.70 o -3 1 1 7343.47 7199.74 27.63 o -2 1 1 2332.31 2291.46 13.51 o -1 1 1 11137.78 11694.35 50.04 o 1 1 1 2942.30 2976.31 19.54 o 2 1 1 746.00 756.68 11.54 o 3 1 1 539.38 644.87 32.29 o 4 1 1 101.71 103.50 7.09 o 5 1 1 4400.85 4574.52 28.92 o 6 1 1 21.72 21.07 8.22 o 7 1 1 18.33 24.25 10.52 o 8 1 1 86.26 71.12 12.19 o 9 1 1 1173.59 1188.90 27.63 o 10 1 1 63.63 49.43 20.89 o -10 2 1 497.70 555.63 31.07 o -9 2 1 3.57 0.00 15.60 o -8 2 1 71.20 82.15 12.13 o -7 2 1 737.50 761.86 17.97 o -6 2 1 169.90 166.75 11.13 o -5 2 1 1376.54 1295.08 18.14 o -4 2 1 2318.81 2269.52 20.65 o -3 2 1 41.31 25.40 6.72 o -2 2 1 1.98 17.47 6.49 o -1 2 1 2371.94 2292.39 28.27 o 0 2 1 4952.15 5305.50 35.00 o 1 2 1 2046.15 2143.77 15.50 o 2 2 1 1150.88 1153.49 12.77 o 3 2 1 156.19 172.60 8.34 o 4 2 1 60.05 70.04 8.20 o 5 2 1 233.47 244.23 11.06 o 6 2 1 2137.26 2090.92 25.00 o 7 2 1 616.26 628.22 17.40 o 8 2 1 89.55 86.69 12.31 o 9 2 1 63.47 45.90 12.80 o 10 2 1 21.61 10.60 19.99 o -10 3 1 883.90 961.84 32.15 o -9 3 1 119.02 127.03 18.48 o -8 3 1 15.54 7.60 11.44 o -7 3 1 353.03 357.65 14.78 o -6 3 1 83.29 76.49 10.52 o -5 3 1 113.27 94.17 9.71 o -4 3 1 103.77 121.74 8.76 o -3 3 1 1146.92 1105.27 12.97 o -2 3 1 1073.25 951.91 11.43 o -1 3 1 0.81 3.15 7.24 o 0 3 1 2275.79 2345.66 18.28 o 1 3 1 1294.37 1347.20 14.18 o 2 3 1 298.27 308.94 10.33 o 3 3 1 3111.15 2937.01 30.34 o 4 3 1 75.94 56.03 8.49 o 5 3 1 126.97 143.24 10.44 o 6 3 1 23.35 24.85 10.10 o 7 3 1 229.00 241.86 13.82 o 8 3 1 957.23 970.87 23.50 o 9 3 1 436.32 408.64 18.22 o 10 3 1 654.79 637.27 32.29 o -9 4 1 175.19 162.20 18.96 o -8 4 1 412.19 419.72 17.03 o -7 4 1 477.51 461.98 16.34 o -6 4 1 248.11 244.74 12.98 o -5 4 1 505.68 480.17 13.90 o -4 4 1 1115.44 1111.97 19.13 o -3 4 1 121.90 121.31 7.06 o -2 4 1 256.56 237.67 14.75 o -1 4 1 1929.73 1958.21 20.33 o 0 4 1 1114.33 1304.39 12.07 o 1 4 1 2003.90 1844.27 19.32 o 2 4 1 380.72 384.80 10.23 o 3 4 1 4.25 7.16 8.69 o 4 4 1 1.93 0.00 8.13 o 5 4 1 3667.26 3665.14 31.14 o 6 4 1 2305.82 2279.28 27.45 o 7 4 1 179.02 191.99 13.70 o 8 4 1 18.68 32.21 12.30 o 9 4 1 1.77 8.69 13.28 o -9 5 1 0.25 0.40 19.98 o -8 5 1 4.36 0.00 15.72 o -7 5 1 2.53 0.00 13.76 o -6 5 1 129.66 127.08 13.16 o -5 5 1 1047.74 955.70 22.96 o -4 5 1 295.37 287.15 11.86 o -3 5 1 754.51 777.34 15.52 o -2 5 1 25.41 24.42 8.58 o -1 5 1 93.68 55.03 8.72 o 0 5 1 1615.91 1806.29 14.92 o 1 5 1 205.59 187.43 7.18 o 2 5 1 100.09 88.17 7.85 o 3 5 1 4480.24 4468.72 38.98 o 4 5 1 23.58 19.08 11.71 o 5 5 1 408.16 391.61 14.08 o 6 5 1 226.22 211.65 13.46 o 7 5 1 2720.18 2711.71 36.94 o 8 5 1 769.89 791.83 24.14 o 9 5 1 4.04 0.00 14.98 o -9 6 1 404.25 451.40 29.26 o -8 6 1 8.48 10.00 16.42 o -7 6 1 604.34 549.59 23.64 o -6 6 1 67.93 70.32 15.71 o -5 6 1 106.99 85.80 14.88 o -4 6 1 28.00 27.91 13.11 o -3 6 1 11.26 4.17 8.70 o -2 6 1 432.89 398.57 13.91 o -1 6 1 0.07 0.00 8.80 o 0 6 1 407.35 451.58 10.64 o 1 6 1 4164.83 3958.66 54.45 o 2 6 1 86.51 64.03 8.87 o 3 6 1 355.26 357.23 16.13 o 4 6 1 309.06 298.90 16.90 o 5 6 1 6294.79 6203.83 75.83 o 6 6 1 337.67 337.67 19.16 o 7 6 1 17.15 11.58 14.97 o 8 6 1 48.32 52.08 16.96 o 9 6 1 47.85 76.27 18.11 o -8 7 1 83.16 84.11 18.00 o -7 7 1 112.54 98.01 17.55 o -6 7 1 0.79 6.26 14.87 o -5 7 1 1879.64 1834.96 68.06 o -4 7 1 348.53 343.12 18.47 o -3 7 1 84.47 98.85 13.97 o -2 7 1 663.82 641.55 17.39 o -1 7 1 1420.72 1387.19 22.21 o 0 7 1 183.40 163.43 13.52 o 1 7 1 48.66 43.16 11.80 o 2 7 1 17.80 12.65 9.16 o 3 7 1 1913.71 1908.07 30.36 o 4 7 1 581.26 545.14 20.71 o 5 7 1 37.78 26.59 14.39 o 6 7 1 252.47 261.30 19.31 o 7 7 1 703.63 662.45 25.67 o 8 7 1 81.38 59.41 17.65 o -7 8 1 137.28 114.04 18.19 o -6 8 1 8.62 13.73 15.71 o -5 8 1 2.88 9.77 14.64 o -4 8 1 65.24 71.88 14.98 o -3 8 1 1.96 0.00 14.53 o -2 8 1 304.68 316.20 26.97 o -1 8 1 0.20 2.85 12.52 o 0 8 1 802.01 754.19 22.08 o 1 8 1 1761.85 1678.78 31.77 o 2 8 1 1010.82 1024.70 36.16 o 3 8 1 698.84 674.17 27.71 o 4 8 1 501.54 498.70 21.02 o 5 8 1 856.63 785.71 25.75 o 6 8 1 125.29 127.15 17.68 o 7 8 1 16.50 21.45 16.70 o -7 9 1 238.40 219.13 21.36 o -6 9 1 335.93 349.37 30.97 o -5 9 1 607.84 614.94 29.71 o -4 9 1 207.15 203.15 22.46 o -3 9 1 603.28 659.98 28.62 o -2 9 1 900.46 775.70 35.49 o -1 9 1 268.06 280.58 17.77 o 0 9 1 1540.51 1533.86 30.55 o 1 9 1 0.79 0.00 17.43 o 2 9 1 796.06 815.03 30.06 o 3 9 1 102.68 86.20 19.97 o 4 9 1 1532.89 1580.09 68.80 o 5 9 1 11.13 18.69 18.00 o 6 9 1 346.70 350.56 26.45 o 7 9 1 10.46 7.33 23.46 o -6 10 1 31.69 23.81 21.08 o -5 10 1 437.90 463.28 28.81 o -4 10 1 106.58 112.43 22.13 o -3 10 1 174.57 188.16 22.41 o -2 10 1 94.18 111.97 20.80 o -1 10 1 187.31 201.22 21.45 o 0 10 1 216.69 215.97 21.61 o 1 10 1 50.67 48.81 18.93 o 2 10 1 495.77 536.89 28.66 o 3 10 1 51.14 41.68 20.33 o 4 10 1 956.01 1054.36 50.83 o 5 10 1 32.87 28.17 20.31 o 6 10 1 731.70 762.66 34.54 o -4 11 1 7.76 11.34 21.94 o -3 11 1 800.00 814.62 31.09 o -2 11 1 217.12 243.43 24.76 o -1 11 1 244.65 268.70 23.88 o 0 11 1 615.36 586.89 52.49 o 1 11 1 76.89 65.95 21.02 o 2 11 1 318.09 310.88 26.33 o 3 11 1 3.63 2.98 20.61 o 4 11 1 50.48 41.49 21.25 o -2 12 1 132.72 122.36 23.73 o -1 12 1 27.82 21.35 27.88 o 0 12 1 133.07 143.55 29.73 o 1 12 1 7.06 0.83 25.75 o 2 12 1 34.42 67.46 19.79 o -10 0 2 61.18 41.43 24.40 o -8 0 2 1361.68 1321.96 77.11 o -6 0 2 77.09 85.90 13.72 o -4 0 2 3950.06 4006.42 34.95 o -2 0 2 245.13 288.45 7.96 o 2 0 2 6023.97 5589.79 27.20 o 4 0 2 3633.84 3481.69 29.45 o 6 0 2 76.59 48.59 11.18 o 8 0 2 607.34 620.87 34.41 o 10 0 2 251.33 238.65 32.24 o -10 1 2 711.23 748.46 34.91 o -9 1 2 40.27 23.12 16.23 o -8 1 2 361.80 307.98 20.03 o -7 1 2 325.95 353.27 12.79 o -6 1 2 1273.72 1253.49 17.80 o -5 1 2 1435.32 1472.52 17.03 o -4 1 2 224.46 215.04 8.18 o -3 1 2 1414.63 1537.74 13.35 o -2 1 2 2246.91 2393.47 13.56 o -1 1 2 2464.34 2480.94 17.84 o 1 1 2 2359.71 2496.03 17.91 o 2 1 2 3812.02 3414.41 18.68 o 3 1 2 626.98 606.20 9.46 o 4 1 2 204.94 272.71 8.46 o 5 1 2 968.78 1012.59 14.58 o 6 1 2 695.82 697.92 14.23 o 7 1 2 74.57 66.88 11.31 o 8 1 2 3711.14 3559.92 45.27 o 9 1 2 151.95 157.07 16.39 o 10 1 2 68.76 62.82 19.60 o -10 2 2 0.69 0.00 21.42 o -9 2 2 124.68 95.88 20.95 o -8 2 2 2110.50 2062.61 54.25 o -7 2 2 1582.54 1497.64 22.80 o -6 2 2 79.00 87.00 9.36 o -5 2 2 3163.57 3388.85 25.45 o -4 2 2 757.68 828.07 12.67 o -3 2 2 212.75 250.01 8.45 o -2 2 2 154.40 148.08 7.69 o -1 2 2 2470.06 2621.38 19.35 o 0 2 2 6272.93 6551.68 50.93 o 1 2 2 3503.63 3563.97 19.96 o 2 2 2 592.54 518.04 10.69 o 3 2 2 331.46 374.03 9.92 o 4 2 2 118.64 101.51 6.24 o 5 2 2 143.62 126.90 7.87 o 6 2 2 723.43 711.40 16.77 o 7 2 2 1025.17 1055.33 21.03 o 8 2 2 70.92 73.07 12.46 o 9 2 2 229.55 185.03 15.13 o 10 2 2 229.08 197.31 18.22 o -10 3 2 879.21 949.46 37.21 o -9 3 2 127.45 95.85 18.20 o -8 3 2 232.67 213.32 18.60 o -7 3 2 529.97 570.22 16.77 o -6 3 2 507.48 515.42 14.85 o -5 3 2 4851.43 4833.81 33.37 o -4 3 2 163.63 149.58 10.05 o -3 3 2 16.88 13.65 7.53 o -2 3 2 295.44 278.34 8.48 o -1 3 2 1440.06 1663.45 13.15 o 0 3 2 604.20 625.92 12.17 o 1 3 2 159.60 119.77 6.97 o 2 3 2 191.45 153.13 8.92 o 3 3 2 82.44 72.55 8.75 o 4 3 2 805.45 805.58 14.87 o 5 3 2 234.99 232.82 11.53 o 6 3 2 61.26 50.19 10.50 o 7 3 2 1388.51 1350.43 29.18 o 8 3 2 1044.60 1056.10 23.03 o 9 3 2 782.78 778.05 22.42 o 10 3 2 153.35 136.98 18.12 o -9 4 2 158.39 141.79 22.40 o -8 4 2 475.92 449.76 22.24 o -7 4 2 2281.55 2222.78 28.48 o -6 4 2 1801.61 1813.56 34.53 o -5 4 2 1405.69 1352.07 21.81 o -4 4 2 647.46 595.64 13.44 o -3 4 2 358.20 403.48 9.81 o -2 4 2 1442.05 1349.46 21.27 o -1 4 2 8450.37 8594.31 58.85 o 0 4 2 145.41 123.57 9.04 o 1 4 2 56.42 55.53 7.40 o 2 4 2 0.20 0.00 8.69 o 3 4 2 1538.08 1712.80 21.65 o 4 4 2 2.00 13.13 9.50 o 5 4 2 199.57 189.34 11.59 o 6 4 2 154.52 147.98 12.42 o 7 4 2 1030.91 1011.97 21.81 o 8 4 2 1073.92 1118.41 24.09 o 9 4 2 58.83 49.24 13.50 o -9 5 2 48.96 27.07 19.84 o -8 5 2 539.97 504.40 27.94 o -7 5 2 0.06 0.10 14.04 o -6 5 2 1353.48 1304.36 28.42 o -5 5 2 822.18 793.25 18.32 o -4 5 2 2948.80 2902.95 26.41 o -3 5 2 243.73 251.66 8.96 o -2 5 2 357.52 344.39 13.07 o -1 5 2 2067.42 2203.17 24.62 o 0 5 2 2442.06 2441.83 22.48 o 1 5 2 2.77 11.97 6.38 o 2 5 2 359.59 319.77 9.82 o 3 5 2 1111.09 1071.58 21.27 o 4 5 2 288.58 305.76 14.21 o 5 5 2 65.18 49.82 11.74 o 6 5 2 1447.82 1397.03 26.77 o 7 5 2 506.96 503.02 17.76 o 8 5 2 50.87 49.52 14.25 o 9 5 2 176.96 159.10 21.32 o -9 6 2 14.34 19.55 20.70 o -8 6 2 15.16 15.85 19.95 o -7 6 2 140.71 132.09 17.42 o -6 6 2 1406.97 1378.42 30.41 o -5 6 2 299.97 323.78 24.33 o -4 6 2 1630.41 1610.41 28.97 o -3 6 2 183.87 191.41 12.68 o -2 6 2 616.76 615.84 16.44 o -1 6 2 549.72 519.73 15.16 o 0 6 2 323.26 288.88 11.19 o 1 6 2 150.06 136.13 7.79 o 2 6 2 120.95 110.42 9.04 o 3 6 2 143.58 130.92 13.20 o 4 6 2 574.64 552.82 19.52 o 5 6 2 377.39 347.71 18.49 o 6 6 2 8.06 0.06 13.75 o 7 6 2 36.90 38.15 13.53 o 8 6 2 1046.15 1113.28 28.34 o -8 7 2 105.63 117.78 22.35 o -7 7 2 19.08 23.60 17.06 o -6 7 2 1130.85 1044.35 30.30 o -5 7 2 62.72 67.34 15.34 o -4 7 2 596.99 585.66 21.18 o -3 7 2 3.86 0.00 14.17 o -2 7 2 2936.08 2969.15 33.41 o -1 7 2 71.07 64.81 11.02 o 0 7 2 2524.81 2477.71 32.84 o 1 7 2 53.20 63.46 12.07 o 2 7 2 654.81 609.16 18.36 o 3 7 2 1073.21 1070.14 24.21 o 4 7 2 6.13 0.00 13.09 o 5 7 2 188.22 183.94 16.94 o 6 7 2 713.88 694.08 26.52 o 7 7 2 0.38 0.00 15.64 o 8 7 2 46.56 49.22 22.23 o -7 8 2 166.21 176.64 19.35 o -6 8 2 17.09 14.15 15.68 o -5 8 2 79.33 65.49 16.11 o -4 8 2 239.30 197.97 17.57 o -3 8 2 832.18 831.01 26.95 o -2 8 2 0.15 0.00 14.15 o -1 8 2 401.64 400.75 18.52 o 0 8 2 1335.45 1295.82 26.96 o 1 8 2 1190.67 1174.29 25.37 o 2 8 2 151.76 146.68 17.25 o 3 8 2 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