#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/50/2225077.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225077_Fobs loop_ _publ_author_name 'Yusnita, Juahir' 'Mohd Ali, Hapipah' 'Abdulla, Mahmood A.' 'Robinson, Ward T.' 'Khaledi, Hamid' _publ_section_title ; Bis(pyridine-\kN){N^2^,N^2'^-[1,1'-(pyridine-2,6-diyl)diethylidyne]benzenesulfonohydrazonato-\k^5^O,N,N',N'',O'}nickel(II) ; _journal_coeditor_code OM2309 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m129 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.823 _cell_angle_gamma 90.000 _cell_length_a 11.6029 _cell_length_b 15.8298 _cell_length_c 16.4156 _exptl_crystal_F_000 1428.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file om2309Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 292.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 103.20 112.31 7.18 o 4 0 0 2276.37 2339.53 29.98 o 6 0 0 19925.47 19587.68 215.76 o 8 0 0 17.26 22.53 5.78 o 10 0 0 9775.25 9605.38 147.50 o 12 0 0 4083.95 4053.35 82.31 o 1 1 0 27695.41 27175.54 428.88 o 2 1 0 15059.96 15290.01 137.51 o 3 1 0 4444.05 4868.37 45.18 o 4 1 0 2325.56 2427.09 24.90 o 5 1 0 2051.56 1919.55 21.98 o 6 1 0 1726.31 1865.25 22.70 o 7 1 0 3389.25 3332.42 35.88 o 8 1 0 10559.51 10724.44 95.66 o 9 1 0 4290.89 4267.50 54.44 o 10 1 0 673.95 622.07 20.00 o 11 1 0 1413.51 1458.81 30.84 o 12 1 0 44.91 56.90 12.08 o 13 1 0 2857.59 2885.58 49.04 o 0 2 0 255.13 272.72 15.21 o 1 2 0 8749.26 9079.03 63.53 o 2 2 0 4452.97 4583.71 29.30 o 3 2 0 1692.19 1678.52 17.74 o 4 2 0 1923.38 1890.18 21.28 o 5 2 0 4.22 18.90 5.10 o 6 2 0 308.59 336.00 9.47 o 7 2 0 9218.71 9233.05 97.50 o 8 2 0 234.54 287.05 10.54 o 9 2 0 2474.95 2449.27 31.53 o 10 2 0 1697.87 1725.47 32.18 o 11 2 0 395.48 416.99 29.21 o 12 2 0 1187.16 1199.13 29.40 o 13 2 0 284.88 321.58 19.14 o 1 3 0 17683.75 18070.33 123.25 o 2 3 0 11202.17 11365.50 83.91 o 3 3 0 45.35 54.68 7.35 o 4 3 0 70.50 77.23 5.27 o 5 3 0 3014.19 3110.14 35.71 o 6 3 0 30.33 27.79 5.74 o 7 3 0 890.26 841.67 15.69 o 8 3 0 7020.14 7020.88 72.92 o 9 3 0 328.03 351.27 18.89 o 10 3 0 219.32 202.06 13.56 o 11 3 0 270.55 288.97 20.48 o 12 3 0 220.46 223.77 16.21 o 13 3 0 342.18 332.58 24.93 o 0 4 0 944.72 801.08 20.13 o 1 4 0 5771.99 5988.31 46.44 o 2 4 0 110.45 98.70 4.20 o 3 4 0 298.45 288.33 5.24 o 4 4 0 795.43 897.33 13.36 o 5 4 0 17.20 2.28 4.06 o 6 4 0 389.46 302.71 10.64 o 7 4 0 6398.49 6631.38 63.41 o 8 4 0 125.46 154.16 8.96 o 9 4 0 984.43 958.20 19.17 o 10 4 0 38.52 16.91 7.23 o 11 4 0 201.95 190.66 16.45 o 12 4 0 656.06 712.11 26.60 o 13 4 0 622.59 574.35 27.79 o 1 5 0 64.47 58.25 5.30 o 2 5 0 169.32 161.24 4.23 o 3 5 0 630.04 710.28 9.11 o 4 5 0 926.67 759.93 10.27 o 5 5 0 39.21 65.98 5.15 o 6 5 0 142.25 132.95 8.22 o 7 5 0 2114.55 2185.91 44.36 o 8 5 0 3915.87 3763.11 42.66 o 9 5 0 3.18 3.82 6.63 o 10 5 0 510.69 534.75 16.17 o 11 5 0 820.07 801.07 23.88 o 12 5 0 34.14 36.00 11.85 o 13 5 0 558.10 581.12 37.54 o 0 6 0 3792.61 3704.13 43.58 o 1 6 0 109.71 142.34 4.88 o 2 6 0 6984.07 7178.28 52.05 o 3 6 0 7306.37 7783.59 60.33 o 4 6 0 459.96 358.35 7.44 o 5 6 0 6254.90 6641.41 54.12 o 6 6 0 892.93 861.23 16.67 o 7 6 0 3048.76 2862.51 36.58 o 8 6 0 1.00 -7.00 5.56 o 9 6 0 274.21 267.78 10.60 o 10 6 0 841.66 831.64 17.50 o 11 6 0 81.76 83.35 10.53 o 12 6 0 2189.97 2168.62 39.82 o 13 6 0 1192.66 1191.16 27.09 o 1 7 0 17033.49 17200.77 141.10 o 2 7 0 6797.05 7483.75 54.65 o 3 7 0 9.00 4.37 2.87 o 4 7 0 134.74 193.66 6.58 o 5 7 0 2325.35 2252.33 23.02 o 6 7 0 2.42 2.47 5.20 o 7 7 0 3492.99 3532.13 43.04 o 8 7 0 1226.84 1187.56 22.53 o 9 7 0 505.85 496.37 14.70 o 10 7 0 1661.08 1704.76 27.53 o 11 7 0 3829.52 3847.21 82.55 o 12 7 0 198.27 215.58 36.46 o 0 8 0 17201.09 17246.56 188.66 o 1 8 0 152.49 208.60 7.63 o 2 8 0 2829.19 2996.88 25.34 o 3 8 0 1512.08 1337.54 15.48 o 4 8 0 750.79 814.99 12.94 o 5 8 0 206.82 195.06 7.50 o 6 8 0 9538.94 9472.11 82.67 o 7 8 0 898.64 887.50 18.54 o 8 8 0 1322.66 1361.93 24.50 o 9 8 0 97.64 91.87 9.58 o 10 8 0 5169.85 5274.65 66.85 o 11 8 0 38.68 30.78 10.27 o 12 8 0 224.69 242.79 19.72 o 1 9 0 58.24 106.16 7.60 o 2 9 0 6702.20 6696.82 50.80 o 3 9 0 4581.93 5003.57 46.77 o 4 9 0 4474.85 4642.59 44.40 o 5 9 0 88.68 102.61 6.12 o 6 9 0 383.05 357.59 13.49 o 7 9 0 205.62 203.19 10.33 o 8 9 0 1259.02 1252.98 29.55 o 9 9 0 1156.35 1159.87 29.60 o 10 9 0 40.35 39.68 10.11 o 11 9 0 27.65 29.58 10.20 o 12 9 0 667.84 652.72 29.65 o 0 10 0 43.42 61.11 7.17 o 1 10 0 1358.05 1366.36 16.53 o 2 10 0 1043.24 1087.79 13.27 o 3 10 0 913.68 911.94 16.79 o 4 10 0 2416.82 2404.90 27.40 o 5 10 0 3263.57 3372.10 38.87 o 6 10 0 1183.88 1227.70 50.62 o 7 10 0 2050.16 2119.89 47.66 o 8 10 0 637.28 608.90 21.78 o 9 10 0 1247.31 1257.16 32.47 o 10 10 0 37.29 27.78 13.69 o 11 10 0 369.13 370.43 31.71 o 1 11 0 1197.50 1117.86 17.53 o 2 11 0 2.78 0.67 3.90 o 3 11 0 2210.37 2225.67 26.99 o 4 11 0 1253.28 1323.99 26.43 o 5 11 0 77.34 91.85 14.41 o 6 11 0 65.43 87.29 13.57 o 7 11 0 1501.88 1465.14 48.31 o 8 11 0 889.11 882.74 57.18 o 9 11 0 296.89 303.46 22.19 o 10 11 0 115.30 102.33 20.02 o 11 11 0 95.11 108.83 23.80 o 0 12 0 9.37 14.34 7.79 o 1 12 0 2109.81 2239.89 27.78 o 2 12 0 2063.20 2029.13 30.06 o 3 12 0 711.65 684.06 28.42 o 4 12 0 4486.10 4385.83 59.49 o 5 12 0 19.05 23.60 8.24 o 6 12 0 121.32 105.94 14.94 o 7 12 0 8.19 -1.79 22.95 o 8 12 0 147.04 159.44 18.27 o 9 12 0 427.78 452.13 26.22 o 10 12 0 328.92 345.78 25.26 o 1 13 0 1096.93 1058.67 24.20 o 2 13 0 90.87 107.02 10.58 o 3 13 0 1567.53 1600.46 31.06 o 4 13 0 536.25 496.75 18.00 o 5 13 0 2460.68 2437.09 52.88 o 6 13 0 553.51 587.97 26.49 o 7 13 0 52.22 64.32 14.68 o 8 13 0 319.03 314.02 23.39 o 9 13 0 214.39 237.11 21.98 o 0 14 0 2267.30 2172.29 67.24 o 1 14 0 238.06 306.48 19.63 o 2 14 0 339.46 317.51 15.48 o 3 14 0 3356.33 3212.99 50.24 o 4 14 0 279.95 332.53 16.39 o 5 14 0 338.75 359.16 22.15 o 6 14 0 1399.98 1399.25 60.72 o 7 14 0 28.76 12.17 12.94 o 8 14 0 147.56 160.35 19.68 o 9 14 0 187.37 192.31 21.51 o 1 15 0 2644.35 2483.42 123.33 o 2 15 0 327.83 275.46 15.53 o 3 15 0 322.18 299.04 16.16 o 4 15 0 2599.05 2494.02 43.72 o 5 15 0 505.98 570.88 27.02 o 6 15 0 81.67 94.16 16.33 o 7 15 0 777.88 821.62 52.90 o 8 15 0 394.65 436.45 27.88 o 0 16 0 2933.78 2842.82 84.29 o 1 16 0 834.36 844.39 24.71 o 2 16 0 6.85 -5.11 9.01 o 3 16 0 4525.32 4618.60 96.18 o 4 16 0 19.96 32.95 10.63 o 5 16 0 110.54 115.16 17.07 o 6 16 0 0.28 5.05 16.13 o 7 16 0 379.71 375.54 26.47 o 1 17 0 193.13 183.05 15.00 o 2 17 0 646.49 649.38 23.23 o 3 17 0 4.05 6.71 10.37 o 4 17 0 557.58 631.05 30.07 o 5 17 0 1066.73 1120.62 52.02 o 0 18 0 62.09 34.36 22.30 o 1 18 0 185.45 177.90 15.62 o 2 18 0 29.54 14.69 11.06 o 3 18 0 394.71 436.82 21.48 o 4 18 0 72.90 88.77 17.37 o -13 0 1 1339.23 1420.75 47.80 o -11 0 1 1206.90 1111.21 38.39 o -9 0 1 1190.09 1201.12 35.58 o -7 0 1 118.68 145.11 8.41 o -5 0 1 1954.57 1683.96 20.54 o -3 0 1 8701.00 8641.32 80.47 o -1 0 1 5236.51 5017.48 186.50 o 1 0 1 26578.13 14615.35 279.96 o 3 0 1 6606.02 6739.56 91.65 o 5 0 1 4899.83 5203.09 97.00 o 7 0 1 709.07 711.21 15.70 o 9 0 1 2572.79 2564.01 54.20 o 11 0 1 318.26 318.78 37.07 o 13 0 1 8.79 7.08 15.77 o -13 1 1 248.75 265.25 18.87 o -12 1 1 1139.84 1148.83 29.13 o -11 1 1 80.10 81.34 11.92 o -10 1 1 1205.53 1165.29 26.28 o -9 1 1 209.78 256.99 20.78 o -8 1 1 11.34 18.27 6.29 o -7 1 1 2709.35 2746.37 31.30 o -6 1 1 2611.78 2723.10 26.65 o -5 1 1 2649.64 2480.52 23.88 o -4 1 1 1019.44 1169.59 13.32 o -3 1 1 129.99 146.20 4.80 o -2 1 1 3064.65 3171.33 28.08 o -1 1 1 18813.05 18311.11 136.56 o 0 1 1 42.83 5.75 2.40 o 1 1 1 24167.23 24521.75 215.48 o 2 1 1 1319.34 1363.11 18.16 o 3 1 1 5547.83 5520.53 62.76 o 4 1 1 2603.09 2442.57 24.90 o 5 1 1 185.50 183.02 5.12 o 6 1 1 1874.39 2084.94 23.74 o 7 1 1 6570.10 6701.42 62.24 o 8 1 1 458.57 478.87 16.17 o 9 1 1 1365.24 1387.32 26.80 o 10 1 1 3276.60 3290.20 47.07 o 11 1 1 408.23 397.33 17.86 o 12 1 1 1395.29 1379.74 37.90 o 13 1 1 583.93 619.61 23.42 o -13 2 1 460.51 454.39 21.57 o -12 2 1 1169.38 1200.11 29.63 o -11 2 1 120.43 118.56 12.72 o -10 2 1 44.21 44.50 9.92 o -9 2 1 32.63 21.64 6.51 o -8 2 1 161.50 158.06 11.10 o -7 2 1 5062.41 5166.55 51.14 o -6 2 1 12088.04 11746.34 92.17 o -5 2 1 1695.57 1774.35 19.10 o -4 2 1 175.46 191.07 6.47 o -3 2 1 46.59 73.53 5.30 o -2 2 1 2002.31 2099.14 26.36 o -1 2 1 16763.82 17231.92 152.40 o 0 2 1 41806.76 41602.01 1069.40 o 1 2 1 2995.21 3064.32 29.22 o 2 2 1 4953.25 5133.95 36.51 o 3 2 1 2491.49 2284.17 25.20 o 4 2 1 215.53 277.37 7.44 o 5 2 1 1779.45 1880.46 22.23 o 6 2 1 5538.39 5624.10 52.96 o 7 2 1 9536.45 9782.82 87.02 o 8 2 1 7.86 18.07 5.64 o 9 2 1 1251.68 1196.78 20.53 o 10 2 1 2861.45 2713.53 41.73 o 11 2 1 32.20 8.90 12.50 o 12 2 1 58.19 65.31 12.25 o 13 2 1 37.72 41.95 13.84 o -13 3 1 357.02 348.72 19.82 o -12 3 1 310.45 300.21 23.08 o -11 3 1 325.67 313.86 16.94 o -10 3 1 453.92 431.46 17.65 o -9 3 1 29.04 33.65 6.99 o -8 3 1 12796.69 12744.50 112.63 o -7 3 1 2065.59 2029.23 23.35 o -6 3 1 3390.39 3563.66 33.76 o -5 3 1 62.76 35.03 4.72 o -4 3 1 7299.48 7036.44 61.50 o -3 3 1 2784.81 2742.29 23.85 o -2 3 1 6898.01 6680.93 56.20 o -1 3 1 4815.19 5015.71 42.07 o 0 3 1 20749.15 21169.84 170.34 o 1 3 1 312.45 331.27 5.72 o 2 3 1 33811.80 33398.24 225.80 o 3 3 1 174.84 268.46 5.39 o 4 3 1 3427.23 3513.49 37.77 o 5 3 1 538.00 594.63 22.22 o 6 3 1 200.07 212.56 8.09 o 7 3 1 298.83 385.52 11.08 o 8 3 1 12904.91 12830.99 112.94 o 9 3 1 543.99 549.53 14.64 o 10 3 1 2555.58 2540.84 40.30 o 11 3 1 388.40 385.23 17.62 o 12 3 1 881.63 853.06 25.29 o 13 3 1 1237.40 1242.75 39.21 o -13 4 1 5179.69 5149.71 71.71 o -12 4 1 224.77 190.97 15.60 o -11 4 1 3206.19 3090.03 47.94 o -10 4 1 5.08 -8.97 6.57 o -9 4 1 2607.79 2743.24 35.25 o -8 4 1 243.40 253.00 12.26 o -7 4 1 3655.08 3418.59 34.34 o -6 4 1 4495.95 4821.76 47.10 o -5 4 1 285.12 213.52 7.95 o -4 4 1 5.52 13.21 4.54 o -3 4 1 3128.29 3043.13 29.01 o -2 4 1 2322.34 2404.76 22.54 o -1 4 1 1518.77 1289.92 12.37 o 0 4 1 1874.79 2091.09 20.43 o 1 4 1 16409.74 16149.14 373.88 o 2 4 1 6824.19 7211.73 60.46 o 3 4 1 767.33 554.03 7.76 o 4 4 1 1365.94 1474.83 13.87 o 5 4 1 502.56 444.55 10.02 o 6 4 1 2313.06 2250.32 32.89 o 7 4 1 1330.05 1206.59 20.59 o 8 4 1 340.96 357.34 14.10 o 9 4 1 6020.00 6068.06 61.89 o 10 4 1 642.25 621.02 16.67 o 11 4 1 15.66 4.96 9.80 o 12 4 1 132.42 121.19 13.90 o 13 4 1 12.55 -8.72 11.15 o -13 5 1 955.83 997.81 29.27 o -12 5 1 208.32 204.17 15.98 o -11 5 1 725.41 747.60 23.35 o -10 5 1 765.44 789.76 24.59 o -9 5 1 558.47 561.18 15.66 o -8 5 1 5715.63 5762.04 58.89 o -7 5 1 1482.13 1379.86 20.82 o -6 5 1 5.49 7.99 4.85 o -5 5 1 12133.77 12250.45 117.46 o -4 5 1 31.49 15.80 3.56 o -3 5 1 5590.85 5867.50 50.84 o -2 5 1 1685.50 1655.76 17.06 o -1 5 1 1560.35 1576.19 14.69 o 0 5 1 11856.27 12315.41 101.71 o 1 5 1 5663.70 5291.31 51.17 o 2 5 1 4718.88 4479.81 36.26 o 3 5 1 640.90 567.33 10.66 o 4 5 1 1258.14 1285.86 13.94 o 5 5 1 1692.22 1558.79 18.39 o 6 5 1 2060.11 2085.78 25.26 o 7 5 1 1796.33 1688.56 21.29 o 8 5 1 3425.67 3390.49 39.38 o 9 5 1 493.66 474.47 14.63 o 10 5 1 229.77 244.82 12.18 o 11 5 1 4175.59 4209.11 58.39 o 12 5 1 471.52 451.93 26.81 o 13 5 1 2.03 -1.07 9.90 o -13 6 1 44.60 31.68 12.96 o -12 6 1 2697.54 2767.45 47.31 o -11 6 1 58.70 59.29 11.58 o -10 6 1 2338.76 2318.02 33.90 o -9 6 1 1600.48 1613.19 26.35 o -8 6 1 634.53 643.91 17.52 o -7 6 1 26.65 23.26 6.75 o -6 6 1 16426.38 16238.63 154.58 o -5 6 1 441.04 390.40 8.42 o -4 6 1 152.40 127.11 4.90 o -3 6 1 44.13 85.39 4.92 o -2 6 1 322.89 344.49 7.52 o -1 6 1 1039.93 1048.88 11.24 o 0 6 1 3271.62 2956.64 28.79 o 1 6 1 99.97 117.45 5.17 o 2 6 1 979.49 937.72 11.20 o 3 6 1 6841.50 7431.25 70.04 o 4 6 1 3869.36 3860.54 33.22 o 5 6 1 88.96 115.56 4.72 o 6 6 1 2328.67 2287.82 30.34 o 7 6 1 2080.93 2152.64 32.70 o 8 6 1 67.29 72.87 6.83 o 9 6 1 1377.56 1357.90 21.15 o 10 6 1 4036.55 4023.07 43.02 o 11 6 1 116.39 120.35 11.39 o 12 6 1 549.53 564.59 20.61 o 13 6 1 228.86 233.48 17.67 o -12 7 1 209.74 181.94 20.15 o -11 7 1 606.56 598.28 25.08 o -10 7 1 1414.62 1374.31 24.39 o -9 7 1 20.47 28.13 7.71 o -8 7 1 58.23 61.05 8.01 o -7 7 1 2183.30 2090.70 26.78 o -6 7 1 400.18 372.46 14.92 o -5 7 1 1527.37 1616.24 18.10 o -4 7 1 1276.63 1128.99 13.82 o -3 7 1 1827.75 1897.38 20.58 o -2 7 1 67.01 52.22 3.10 o -1 7 1 1017.24 1092.64 14.00 o 0 7 1 540.40 437.98 9.04 o 1 7 1 376.77 561.20 13.12 o 2 7 1 2018.83 1810.26 18.25 o 3 7 1 1476.91 1468.14 15.91 o 4 7 1 148.24 155.95 5.69 o 5 7 1 5.72 18.86 3.37 o 6 7 1 472.29 479.51 10.27 o 7 7 1 134.41 191.14 12.35 o 8 7 1 1371.11 1395.25 24.76 o 9 7 1 119.59 118.30 9.13 o 10 7 1 198.36 210.37 11.61 o 11 7 1 149.35 170.87 13.41 o 12 7 1 420.89 513.74 20.55 o -12 8 1 1047.84 1066.86 33.98 o -11 8 1 325.12 370.05 25.39 o -10 8 1 255.37 229.53 14.28 o -9 8 1 995.16 950.09 26.22 o -8 8 1 1266.40 1295.08 23.55 o -7 8 1 5314.96 5504.58 54.77 o -6 8 1 2413.07 2598.55 26.54 o -5 8 1 3786.81 3670.93 33.77 o -4 8 1 1965.61 1975.57 22.24 o -3 8 1 2782.99 3249.73 32.00 o -2 8 1 3950.39 4046.69 34.48 o -1 8 1 2.51 8.59 3.80 o 0 8 1 3602.57 3795.85 37.01 o 1 8 1 287.68 466.56 10.36 o 2 8 1 3459.58 3710.36 32.69 o 3 8 1 2708.90 2881.86 26.81 o 4 8 1 1820.97 1761.09 20.59 o 5 8 1 21.99 24.48 4.04 o 6 8 1 918.13 878.75 17.75 o 7 8 1 854.35 860.00 18.62 o 8 8 1 620.48 649.41 17.23 o 9 8 1 2427.02 2421.05 36.14 o 10 8 1 1322.95 1320.30 24.34 o 11 8 1 96.00 106.21 12.05 o 12 8 1 1483.27 1478.96 39.48 o -12 9 1 364.68 364.06 24.13 o -11 9 1 312.79 338.02 17.41 o -10 9 1 777.95 778.64 25.53 o -9 9 1 346.11 313.45 37.14 o -8 9 1 1194.11 1105.72 49.80 o -7 9 1 2343.23 2344.13 35.54 o -6 9 1 73.08 65.69 6.40 o -5 9 1 3081.92 2965.10 31.32 o -4 9 1 20.10 30.99 4.41 o -3 9 1 23.06 11.19 3.72 o -2 9 1 3836.04 3770.73 32.98 o -1 9 1 5149.93 5061.80 53.85 o 0 9 1 123.18 124.29 7.60 o 1 9 1 6274.75 6394.02 64.28 o 2 9 1 12.35 12.63 3.62 o 3 9 1 927.68 955.80 15.58 o 4 9 1 2934.24 2984.04 31.04 o 5 9 1 3658.55 3653.49 41.04 o 6 9 1 1183.97 1209.46 24.09 o 7 9 1 4507.48 4563.62 53.59 o 8 9 1 146.93 135.88 10.19 o 9 9 1 6805.59 6796.26 91.13 o 10 9 1 405.18 435.17 18.15 o 11 9 1 594.21 593.84 37.37 o 12 9 1 638.48 623.59 39.08 o -11 10 1 165.64 156.08 19.79 o -10 10 1 0.51 -5.10 9.91 o -9 10 1 876.55 962.76 27.81 o -8 10 1 598.95 610.85 21.85 o -7 10 1 17.07 9.78 10.83 o -6 10 1 2480.65 2438.49 50.45 o -5 10 1 2.88 -3.14 5.49 o -4 10 1 1935.41 1973.11 28.35 o -3 10 1 5569.58 5504.52 51.02 o -2 10 1 477.89 460.69 10.07 o -1 10 1 2190.51 2308.61 29.60 o 0 10 1 195.86 187.02 6.70 o 1 10 1 2180.75 2148.85 24.85 o 2 10 1 104.50 87.76 5.49 o 3 10 1 16047.07 16071.49 122.61 o 4 10 1 1680.95 1604.30 20.73 o 5 10 1 161.16 185.17 8.59 o 6 10 1 60.91 75.05 14.41 o 7 10 1 3615.29 3569.74 66.71 o 8 10 1 8.39 6.97 11.23 o 9 10 1 1252.03 1309.44 32.24 o 10 10 1 1050.72 1041.49 30.07 o 11 10 1 1.65 -7.00 9.35 o -11 11 1 311.56 328.35 21.34 o -10 11 1 81.75 135.84 14.92 o -9 11 1 102.95 102.26 16.29 o -8 11 1 1715.81 1849.05 46.68 o -7 11 1 476.79 492.13 32.48 o -6 11 1 318.13 290.37 15.66 o -5 11 1 314.44 317.67 14.07 o -4 11 1 4858.63 4927.17 56.00 o -3 11 1 668.60 565.87 15.12 o -2 11 1 10415.34 10411.27 102.96 o -1 11 1 2117.88 2064.86 25.41 o 0 11 1 21.70 21.25 5.19 o 1 11 1 40.16 77.10 5.99 o 2 11 1 11888.06 11650.70 91.74 o 3 11 1 612.37 658.39 11.69 o 4 11 1 910.65 966.93 16.04 o 5 11 1 14152.84 14245.04 165.21 o 6 11 1 123.06 169.15 24.96 o 7 11 1 45.87 36.56 12.58 o 8 11 1 8062.13 7790.32 122.90 o 9 11 1 8.08 8.76 12.82 o 10 11 1 1205.80 1123.75 39.56 o 11 11 1 494.00 505.25 31.35 o -10 12 1 1546.01 1583.85 46.96 o -9 12 1 640.85 626.96 36.33 o -8 12 1 609.92 553.10 27.23 o -7 12 1 1780.48 1768.16 45.22 o -6 12 1 2067.37 2102.19 49.44 o -5 12 1 446.33 428.53 18.72 o -4 12 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