#------------------------------------------------------------------------------
#$Date: 2010-03-05 20:15:21 +0200 (Fri, 05 Mar 2010) $
#$Revision: 1024 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2225095.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2225095_Fobs
loop_
_publ_author_name
'Zhang, Zhong'
'Lu, Jianqi'
'Wu, Difeng'
_publ_section_title
;
Tris(propionitrile-\kN)[1,4,7-tris(cyanomethyl)-1,4,7-triazacyclononane-\k^3^N^1^,N^4^,N^7^]copper(II)
bis(perchlorate) dihydrate
;
_journal_coeditor_code RK2185
_journal_issue 2
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first m235
_journal_page_last m236
_journal_volume 66
_journal_year 2010
_space_group_IT_number 148
_symmetry_space_group_name_Hall '-R 3'
_symmetry_space_group_name_H-M 'R -3 :H'
_cell_angle_alpha 90.000
_cell_angle_beta 90.000
_cell_angle_gamma 120.000
_cell_length_a 9.9618
_cell_length_b 9.9618
_cell_length_c 61.6227
_exptl_crystal_F_000 2214.00
_reflns_d_resolution_high 0.8107
_[local]_cod_data_source_file rk2185Isup2.hkl
_[local]_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' 11 in R-3'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 554.38
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
-1 2 0 232457.72 215181.02 1707.57 o
0 3 0 69415.84 65515.41 504.93 o
-2 4 0 103540.70 98733.43 391.86 o
-4 5 0 47726.07 46167.02 342.65 o
-1 5 0 97388.25 93059.78 596.81 o
-3 6 0 64006.57 59143.08 2012.49 o
0 6 0 61720.26 57525.77 273.09 o
-5 7 0 44618.71 41981.50 286.87 o
-2 7 0 51925.68 48724.61 229.58 o
-7 8 0 34616.46 31915.37 96.38 o
-4 8 0 29450.67 28678.46 218.82 o
-1 8 0 32263.75 30602.35 111.00 o
-6 9 0 16576.94 16154.20 145.33 o
-3 9 0 11519.54 11169.56 431.41 o
0 9 0 8845.42 8083.45 304.12 o
-8 10 0 7323.28 7378.70 351.68 o
-5 10 0 20208.41 18747.35 535.02 o
-2 10 0 13141.49 13081.20 407.89 o
-10 11 0 2474.44 2521.49 323.21 o
-7 11 0 7837.12 7682.57 220.16 o
-4 11 0 3915.62 3764.70 128.63 o
-1 11 0 1833.43 1880.66 267.85 o
-6 12 0 7988.27 7410.07 58.69 o
-1 1 1 2094.14 2815.62 362.90 o
-3 2 1 1594.19 2538.59 264.56 o
0 2 1 26150.61 24848.77 211.32 o
-5 3 1 3768.87 3924.62 182.68 o
-2 3 1 45087.83 43086.03 199.87 o
1 3 1 1128.67 1328.15 107.00 o
-7 4 1 1434.07 1520.55 102.40 o
-4 4 1 8885.96 8415.02 149.32 o
-1 4 1 3145.17 3435.77 206.48 o
2 4 1 293.50 421.31 214.32 o
-9 5 1 1965.91 2009.65 117.62 o
-6 5 1 500.03 702.70 209.99 o
-3 5 1 548.41 685.13 296.64 o
0 5 1 6875.44 7142.04 248.37 o
3 5 1 4092.81 4184.50 124.07 o
-11 6 1 1.91 213.17 213.80 o
-8 6 1 1144.17 1244.91 180.43 o
-5 6 1 8377.47 8192.30 184.83 o
-2 6 1 18.61 38.57 129.49 o
1 6 1 1419.61 1776.48 158.23 o
4 6 1 321.18 389.00 139.30 o
-10 7 1 1508.84 1557.61 169.15 o
-7 7 1 20.59 33.99 140.36 o
-4 7 1 672.96 851.08 135.09 o
-1 7 1 273.36 564.24 174.94 o
2 7 1 10.27 190.63 253.87 o
5 7 1 40.80 66.86 53.53 o
-12 8 1 596.76 621.91 94.78 o
-9 8 1 1214.03 1629.32 308.04 o
-6 8 1 162.52 739.90 337.91 o
-3 8 1 1435.81 1630.59 276.20 o
0 8 1 2481.26 2442.93 35.63 o
3 8 1 33.93 66.58 207.77 o
-11 9 1 10.43 193.04 142.00 o
-8 9 1 3204.99 3396.92 314.28 o
-5 9 1 892.71 947.30 105.96 o
-2 9 1 3.26 168.09 383.18 o
1 9 1 13.92 63.16 49.91 o
-10 10 1 22.15 294.46 511.06 o
-7 10 1 443.85 924.73 217.61 o
-4 10 1 1025.11 1130.86 256.41 o
-1 10 1 63.33 418.17 188.89 o
-9 11 1 62.10 442.22 680.46 o
-6 11 1 83.42 175.43 202.63 o
-3 11 1 330.35 336.44 46.61 o
-8 12 1 7.28 327.65 454.47 o
-5 12 1 2.09 132.29 269.17 o
0 1 2 40988.39 37739.39 526.82 o
-2 2 2 37259.46 35834.48 266.65 o
1 2 2 64228.73 60276.48 436.58 o
-4 3 2 12322.84 11362.67 365.08 o
-1 3 2 792.01 944.67 465.01 o
2 3 2 191.58 1075.99 479.43 o
-6 4 2 1880.35 2276.14 321.78 o
-3 4 2 2081.02 2926.55 214.83 o
0 4 2 38.29 476.51 172.13 o
3 4 2 330.27 526.05 78.80 o
-8 5 2 297.94 323.93 174.85 o
-5 5 2 50.32 101.80 68.79 o
-2 5 2 7874.91 7417.47 864.42 o
1 5 2 1653.31 1753.02 203.83 o
4 5 2 416.09 432.39 32.01 o
-10 6 2 11.46 384.49 93.66 o
-7 6 2 3994.82 3964.75 142.32 o
-4 6 2 2729.05 3002.16 493.67 o
-1 6 2 17948.39 18188.69 277.25 o
2 6 2 2006.41 2129.43 101.88 o
5 6 2 522.34 589.36 180.74 o
-12 7 2 137.64 359.25 101.22 o
-9 7 2 2248.86 2349.06 487.96 o
-6 7 2 1530.15 1406.33 392.01 o
-3 7 2 49.33 448.64 191.90 o
0 7 2 100.06 372.52 258.39 o
3 7 2 25.82 175.44 87.64 o
-11 8 2 242.45 444.72 412.85 o
-8 8 2 314.33 980.82 407.68 o
-5 8 2 171.30 326.39 108.21 o
-2 8 2 232.05 544.14 243.24 o
1 8 2 2288.74 2207.26 103.38 o
4 8 2 162.59 111.32 566.54 o
-10 9 2 84.34 125.31 58.93 o
-7 9 2 330.37 812.00 216.30 o
-4 9 2 931.97 1063.84 190.36 o
-1 9 2 906.13 918.19 220.08 o
2 9 2 306.71 570.97 448.38 o
-9 10 2 768.94 918.14 391.94 o
-6 10 2 68.30 596.76 238.68 o
-3 10 2 145.82 336.30 541.37 o
0 10 2 213.97 274.43 482.02 o
-8 11 2 105.46 108.93 31.74 o
-5 11 2 305.24 685.41 258.96 o
-2 11 2 917.36 1062.06 213.76 o
-7 12 2 1369.58 1391.16 229.94 o
-4 12 2 264.74 384.99 114.90 o
1 1 3 1530.92 2175.81 461.72 o
-1 2 3 126.25 1807.74 186.51 o
2 2 3 937.88 1032.17 149.13 o
-3 3 3 23924.44 23382.40 162.34 o
0 3 3 48.65 201.21 193.18 o
3 3 3 1284.50 1282.20 442.22 o
-5 4 3 1012.72 1197.36 625.54 o
-2 4 3 497.80 590.19 194.26 o
1 4 3 7455.53 7700.93 481.13 o
4 4 3 15.83 119.84 86.73 o
-7 5 3 40.88 469.14 135.52 o
-4 5 3 715.52 1285.89 176.82 o
-1 5 3 13135.65 13374.58 554.79 o
2 5 3 139.63 838.59 220.38 o
5 5 3 1655.72 2053.51 255.61 o
-9 6 3 148.31 157.32 14.70 o
-6 6 3 1197.38 1450.15 81.27 o
-3 6 3 7789.38 7719.06 547.10 o
0 6 3 149.68 573.58 156.01 o
3 6 3 564.01 668.00 216.69 o
6 6 3 112.13 263.95 174.22 o
-11 7 3 1180.87 1228.17 353.74 o
-8 7 3 569.75 1053.05 280.81 o
-5 7 3 788.89 861.87 147.79 o
-2 7 3 1778.20 1886.75 135.88 o
1 7 3 338.80 1031.49 327.25 o
4 7 3 14.13 265.81 119.87 o
-10 8 3 9.70 32.88 48.69 o
-7 8 3 153.44 229.33 45.55 o
-4 8 3 737.04 1023.03 238.82 o
-1 8 3 1663.41 1745.65 113.29 o
2 8 3 380.87 471.47 229.06 o
-9 9 3 2772.80 2542.27 41.86 o
-6 9 3 323.82 338.47 84.95 o
-3 9 3 103.74 274.09 108.39 o
0 9 3 68.95 181.08 217.48 o
-11 10 3 789.76 816.63 35.83 o
-8 10 3 140.46 165.60 513.14 o
-5 10 3 356.87 598.19 115.47 o
-2 10 3 293.87 328.20 414.75 o
1 10 3 212.07 237.61 321.52 o
-10 11 3 144.63 149.96 85.27 o
-7 11 3 91.99 76.36 642.97 o
-4 11 3 78.48 135.35 152.81 o
-1 11 3 625.43 617.62 532.23 o
-6 12 3 53.15 131.57 155.58 o
-1 1 4 16703.73 15693.84 204.19 o
-3 2 4 41842.43 38827.90 208.47 o
0 2 4 42436.55 39480.76 177.23 o
-5 3 4 11015.50 10304.65 119.45 o
-2 3 4 1692.12 3117.93 291.62 o
1 3 4 823.27 999.73 316.01 o
-7 4 4 4027.10 4703.53 210.26 o
-4 4 4 29.81 88.44 195.07 o
-1 4 4 3284.49 3655.96 185.98 o
2 4 4 15116.81 16008.51 371.01 o
-9 5 4 100.70 352.68 142.50 o
-6 5 4 9718.81 9615.88 267.79 o
-3 5 4 6590.96 6550.29 206.35 o
0 5 4 32477.23 30143.37 340.17 o
3 5 4 420.95 512.23 212.94 o
-11 6 4 33.61 138.28 210.78 o
-8 6 4 17830.35 16092.12 406.79 o
-5 6 4 1483.63 2352.90 283.59 o
-2 6 4 1252.04 1524.40 635.34 o
1 6 4 1022.87 1506.20 279.47 o
4 6 4 91.22 73.22 32.01 o
-10 7 4 1315.22 1234.54 171.32 o
-7 7 4 1173.54 1286.67 175.00 o
-4 7 4 3914.94 3604.08 534.99 o
-1 7 4 9482.87 9520.48 503.52 o
2 7 4 776.06 766.62 148.77 o
5 7 4 2327.79 2293.76 287.32 o
-12 8 4 205.47 179.27 92.75 o
-9 8 4 11.58 79.22 67.19 o
-6 8 4 5698.27 5259.58 166.96 o
-3 8 4 444.82 444.41 314.08 o
0 8 4 340.53 557.61 189.78 o
3 8 4 1317.59 1379.74 231.66 o
-11 9 4 62.77 185.31 257.66 o
-8 9 4 530.78 501.63 30.85 o
-5 9 4 3189.93 2984.80 149.40 o
-2 9 4 1602.88 1609.84 165.62 o
1 9 4 822.05 1025.00 513.26 o
-10 10 4 1272.71 1135.06 73.46 o
-7 10 4 1233.12 1609.47 474.20 o
-4 10 4 588.47 573.94 17.45 o
-1 10 4 60.58 183.53 279.73 o
-9 11 4 56.65 305.70 252.99 o
-6 11 4 826.85 1300.75 499.48 o
-3 11 4 1001.83 1479.71 364.66 o
-8 12 4 597.71 648.21 141.97 o
-5 12 4 268.67 344.73 96.34 o
0 1 5 35347.20 33705.36 1517.62 o
-2 2 5 22246.02 22002.69 210.11 o
1 2 5 3377.97 4281.36 362.38 o
-4 3 5 7739.72 7217.04 348.37 o
-1 3 5 11525.12 11140.07 561.19 o
2 3 5 8692.48 8846.22 285.57 o
-6 4 5 14639.45 14392.71 191.12 o
-3 4 5 524.80 905.86 164.69 o
0 4 5 645.68 649.09 201.81 o
3 4 5 1467.70 1679.71 154.88 o
-8 5 5 4653.19 4245.19 188.59 o
-5 5 5 1328.96 1488.01 130.77 o
-2 5 5 1119.63 1469.27 574.03 o
1 5 5 1705.91 3032.28 227.14 o
4 5 5 425.59 551.58 205.94 o
-10 6 5 289.09 366.98 137.46 o
-7 6 5 3642.72 3637.12 755.71 o
-4 6 5 6122.41 6214.14 363.84 o
-1 6 5 115.79 1979.39 290.83 o
2 6 5 213.00 836.90 317.98 o
5 6 5 755.67 781.09 71.11 o
-12 7 5 167.14 661.74 381.32 o
-9 7 5 234.23 483.59 134.74 o
-6 7 5 2915.42 3550.49 314.00 o
-3 7 5 788.47 1127.24 208.86 o
0 7 5 3836.15 3986.56 247.17 o
3 7 5 864.19 1137.91 175.23 o
-11 8 5 536.72 647.46 376.70 o
-8 8 5 152.37 402.39 149.85 o
-5 8 5 738.04 1004.37 216.36 o
-2 8 5 2166.52 2314.10 223.77 o
1 8 5 621.04 744.82 208.53 o
4 8 5 609.40 918.29 606.02 o
-10 9 5 5.25 117.26 208.24 o
-7 9 5 551.58 923.98 176.02 o
-4 9 5 213.02 294.58 372.34 o
-1 9 5 60.47 66.14 91.39 o
2 9 5 611.24 606.15 187.81 o
-9 10 5 79.40 129.84 338.09 o
-6 10 5 2152.33 2034.73 141.21 o
-3 10 5 874.35 1170.84 377.75 o
0 10 5 10.57 96.32 261.34 o
-8 11 5 198.88 478.98 324.14 o
-5 11 5 1710.09 1823.88 259.29 o
-2 11 5 1473.84 1382.12 77.95 o
-7 12 5 1375.81 1194.11 76.82 o
-4 12 5 31.65 459.51 235.77 o
0 0 6 307340.41 290095.38 862.94 o
1 1 6 286588.91 267722.03 854.96 o
-1 2 6 26145.04 25549.36 358.77 o
2 2 6 5218.40 4783.01 209.66 o
-3 3 6 43903.50 40924.06 453.13 o
0 3 6 87382.83 82654.28 464.32 o
3 3 6 2504.05 2681.74 299.73 o
-5 4 6 26424.41 25223.13 270.29 o
-2 4 6 19646.36 18913.18 124.27 o
1 4 6 6965.28 6648.82 270.71 o
4 4 6 6100.43 6142.45 154.09 o
-7 5 6 49728.77 46204.15 277.21 o
-4 5 6 19181.43 18751.47 238.47 o
-1 5 6 40366.91 38363.24 264.79 o
2 5 6 11593.46 11190.65 308.47 o
5 5 6 2727.11 2844.01 182.40 o
-9 6 6 19170.53 17870.86 293.14 o
-6 6 6 17884.21 18037.56 269.60 o
-3 6 6 17226.36 17469.22 341.36 o
0 6 6 24856.65 23610.11 135.64 o
3 6 6 10724.36 10111.28 155.63 o
6 6 6 2007.77 2143.30 411.69 o
-11 7 6 2352.16 2113.19 176.94 o
-8 7 6 7925.77 8598.20 217.64 o
-5 7 6 24463.83 22749.67 326.83 o
-2 7 6 14879.63 14508.89 322.14 o
1 7 6 14021.80 13189.06 666.28 o
4 7 6 3038.75 3247.82 277.59 o
-10 8 6 4727.62 4490.67 70.42 o
-7 8 6 6366.10 5962.71 158.44 o
-4 8 6 18991.67 18499.38 452.25 o
-1 8 6 15633.43 15988.56 610.77 o
2 8 6 6254.34 5965.89 155.62 o
-9 9 6 1999.72 1959.35 160.99 o
-6 9 6 10777.25 11300.67 319.35 o
-3 9 6 3680.13 3714.05 173.88 o
0 9 6 3072.42 2815.19 195.05 o
-11 10 6 636.07 698.73 252.60 o
-8 10 6 2470.34 2803.08 547.10 o
-5 10 6 6409.71 6135.00 118.70 o
-2 10 6 3214.68 3100.70 193.08 o
1 10 6 4649.25 4368.66 546.35 o
-10 11 6 531.01 726.69 373.87 o
-7 11 6 5085.71 4734.93 300.01 o
-4 11 6 951.55 936.91 53.82 o
-1 11 6 1903.39 1947.24 329.99 o
-6 12 6 1546.99 1465.08 224.29 o
-1 1 7 26134.35 24314.33 124.58 o
-3 2 7 7083.19 6643.42 114.89 o
0 2 7 19994.17 18768.86 495.61 o
-5 3 7 594.93 1734.89 192.43 o
-2 3 7 85.32 892.64 486.28 o
1 3 7 20112.10 19186.74 189.94 o
-7 4 7 3040.75 3507.25 490.91 o
-4 4 7 2380.56 2377.31 113.04 o
-1 4 7 5441.24 5869.70 209.35 o
2 4 7 3349.53 3358.22 211.05 o
-9 5 7 112.39 157.75 52.21 o
-6 5 7 1171.75 1671.10 376.33 o
-3 5 7 2189.80 2143.78 492.40 o
0 5 7 16095.44 15104.21 533.61 o
3 5 7 139.12 684.59 255.72 o
-11 6 7 468.66 454.03 109.89 o
-8 6 7 5611.64 5682.02 114.46 o
-5 6 7 12994.62 12994.28 766.06 o
-2 6 7 1021.98 1007.36 67.24 o
1 6 7 14525.63 13879.33 37.40 o
4 6 7 71.92 159.29 188.82 o
-10 7 7 107.77 444.37 147.18 o
-7 7 7 4640.62 4404.37 106.86 o
-4 7 7 5656.60 5582.10 342.96 o
-1 7 7 7811.73 7629.00 365.02 o
2 7 7 259.70 297.16 72.39 o
5 7 7 712.57 703.18 151.09 o
-12 8 7 1213.22 1209.06 246.26 o
-9 8 7 9.43 7.36 292.73 o
-6 8 7 4255.54 4755.84 316.30 o
-3 8 7 209.74 848.87 419.72 o
0 8 7 2230.51 2301.74 69.67 o
3 8 7 1604.22 1752.23 198.54 o
-11 9 7 1276.37 1237.51 379.17 o
-8 9 7 1904.91 1945.61 327.73 o
-5 9 7 467.69 606.06 75.62 o
-2 9 7 843.07 868.17 113.98 o
1 9 7 2809.17 2788.87 346.92 o
-10 10 7 20.56 66.26 190.35 o
-7 10 7 2331.77 2439.61 292.50 o
-4 10 7 11.61 475.85 160.54 o
-1 10 7 1018.35 1135.13 406.35 o
-9 11 7 510.03 496.24 32.28 o
-6 11 7 1352.34 1238.42 120.10 o
-3 11 7 728.46 787.98 384.09 o
-8 12 7 92.60 473.36 329.01 o
-5 12 7 35.68 188.52 237.02 o
0 1 8 32722.78 31237.72 271.94 o
-2 2 8 94741.45 89943.82 1402.53 o
1 2 8 297.37 651.74 331.87 o
-4 3 8 12903.72 12505.23 168.72 o
-1 3 8 11034.13 10531.88 154.10 o
2 3 8 1896.97 1805.46 85.70 o
-6 4 8 3720.49 3753.28 90.95 o
-3 4 8 50.93 1335.42 351.44 o
0 4 8 11262.55 11504.01 218.45 o
3 4 8 8773.40 8439.10 177.85 o
-8 5 8 380.85 471.19 124.88 o
-5 5 8 558.21 620.93 302.86 o
-2 5 8 28.95 351.97 484.08 o
1 5 8 6162.38 5956.39 96.30 o
4 5 8 1075.71 1165.27 222.25 o
-10 6 8 507.67 850.32 322.08 o
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-4 6 8 2232.53 2350.52 169.05 o
-1 6 8 297.39 457.56 101.86 o
2 6 8 1031.17 981.05 65.67 o
5 6 8 309.31 348.51 76.58 o
-12 7 8 351.91 571.83 423.20 o
-9 7 8 12.80 34.07 32.14 o
-6 7 8 1386.89 1465.52 309.73 o
-3 7 8 811.82 1102.89 207.99 o
0 7 8 563.06 788.77 186.20 o
3 7 8 1405.74 1499.08 94.17 o
-11 8 8 39.94 34.04 52.74 o
-8 8 8 684.16 920.53 389.68 o
-5 8 8 1045.54 1179.44 208.60 o
-2 8 8 1437.75 1687.08 291.61 o
1 8 8 821.03 1073.88 115.68 o
4 8 8 28.56 106.26 81.59 o
-10 9 8 15.63 130.94 207.68 o
-7 9 8 1888.40 1908.95 341.81 o
-4 9 8 6.07 289.81 97.60 o
-1 9 8 163.47 585.12 183.07 o
2 9 8 126.18 110.40 151.00 o
-9 10 8 1101.03 1146.18 187.84 o
-6 10 8 90.24 275.60 306.52 o
-3 10 8 1415.48 1674.62 208.99 o
0 10 8 73.85 150.04 188.67 o
-8 11 8 78.93 238.85 173.77 o
-5 11 8 349.26 411.32 325.03 o
-2 11 8 2.97 76.11 231.37 o
-7 12 8 367.18 443.46 247.96 o
-4 12 8 864.56 1201.53 548.46 o
0 0 9 20224.27 24845.97 499.55 o
1 1 9 44346.89 42248.63 1237.64 o
-1 2 9 6194.94 10062.02 900.34 o
2 2 9 29441.11 28156.40 614.36 o
-3 3 9 5475.29 5336.12 117.83 o
0 3 9 67296.57 63074.73 1088.91 o
3 3 9 3917.53 3936.76 138.41 o
-5 4 9 4437.03 4540.35 231.91 o
-2 4 9 477.38 1606.80 244.11 o
1 4 9 7872.93 7319.94 130.10 o
4 4 9 2836.77 2887.82 178.29 o
-7 5 9 17451.99 16860.46 104.85 o
-4 5 9 2455.37 3367.78 206.53 o
-1 5 9 24372.21 22403.13 234.94 o
2 5 9 2124.18 2554.42 186.90 o
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