#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/51/2225106.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225106_Fobs loop_ _publ_author_name 'Wu, Yiming' 'Meng, Qinglong' 'Zhang, Chi' _publ_section_title ; Poly[(\m~2~-3,6-di-4-pyridyl-1,2,4,5-tetrazine)(\m~2~-thiocyanato)copper(I)] ; _journal_coeditor_code SI2230 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m217 _journal_volume 66 _journal_year 2010 _space_group_IT_number 11 _symmetry_space_group_name_Hall '-P 2yb' _symmetry_space_group_name_H-M 'P 1 21/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.420 _cell_angle_gamma 90.000 _cell_length_a 5.8640 _cell_length_b 18.5100 _cell_length_c 6.3993 _exptl_crystal_F_000 359.88 _reflns_d_resolution_high 0.7997 _[local]_cod_data_source_file si2230Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s in P2(1)/m P21/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 126.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 15961.94 14677.73 159.55 o 2 0 0 4.85 5.90 0.67 o 3 0 0 1670.39 1588.47 89.83 o 4 0 0 2609.26 2654.84 35.80 o 5 0 0 2215.76 1881.39 329.66 o 6 0 0 1095.99 1073.24 190.96 o 1 1 0 37.13 38.94 0.87 o 2 1 0 82.59 77.17 2.28 o 3 1 0 77.51 78.84 1.95 o 4 1 0 496.26 493.03 5.54 o 5 1 0 0.29 15.24 2.94 o 6 1 0 110.85 104.69 6.83 o 1 2 0 12.97 14.32 0.32 o 2 2 0 2562.06 2524.15 9.74 o 3 2 0 3938.29 3939.34 44.75 o 4 2 0 138.49 136.75 2.45 o 5 2 0 2.96 3.44 2.94 o 6 2 0 290.80 295.60 6.69 o 1 3 0 71.95 68.18 0.74 o 2 3 0 1.03 3.80 0.60 o 3 3 0 49.73 54.86 1.15 o 4 3 0 159.09 150.94 2.38 o 5 3 0 106.60 104.34 3.05 o 6 3 0 32.77 38.24 2.39 o 0 4 0 3342.27 3401.42 23.48 o 1 4 0 188.10 136.18 2.58 o 2 4 0 1388.73 1339.48 8.64 o 3 4 0 2658.22 2674.77 15.80 o 4 4 0 317.62 317.43 4.09 o 5 4 0 14.61 22.31 6.83 o 6 4 0 237.99 255.45 6.07 o 1 5 0 117.08 98.01 0.96 o 2 5 0 16.42 10.87 0.59 o 3 5 0 47.68 48.61 1.23 o 4 5 0 176.03 179.08 2.70 o 5 5 0 67.57 59.51 2.96 o 6 5 0 41.91 48.68 6.02 o 0 6 0 3405.60 3423.02 25.10 o 1 6 0 144.38 124.46 1.01 o 2 6 0 1028.10 1031.36 4.66 o 3 6 0 2409.45 2434.58 14.42 o 4 6 0 328.17 335.00 7.48 o 5 6 0 35.00 34.28 4.18 o 6 6 0 187.01 197.45 8.15 o 1 7 0 684.25 671.16 3.03 o 2 7 0 15.48 16.00 1.04 o 3 7 0 19.48 22.27 1.50 o 4 7 0 15.37 12.90 0.89 o 5 7 0 30.04 24.62 4.70 o 6 7 0 77.20 75.48 2.84 o 0 8 0 6204.14 6401.24 150.96 o 1 8 0 243.02 205.14 2.54 o 2 8 0 26.19 44.72 1.38 o 3 8 0 259.79 205.74 2.64 o 4 8 0 215.07 205.03 6.31 o 5 8 0 157.14 170.04 7.56 o 6 8 0 177.79 173.44 6.90 o 1 9 0 50.10 56.08 0.76 o 2 9 0 106.56 113.63 1.49 o 3 9 0 85.72 72.06 1.42 o 4 9 0 298.41 297.57 4.99 o 5 9 0 11.26 10.00 2.50 o 6 9 0 12.33 11.76 3.96 o 0 10 0 3342.73 3491.34 27.40 o 1 10 0 825.55 858.20 6.44 o 2 10 0 1124.88 1202.02 9.86 o 3 10 0 1449.22 1534.41 16.05 o 4 10 0 258.04 250.56 6.92 o 5 10 0 85.61 86.48 3.58 o 6 10 0 246.79 254.74 6.02 o 1 11 0 78.98 66.46 4.68 o 2 11 0 0.07 0.95 0.61 o 3 11 0 15.09 13.15 1.32 o 4 11 0 91.61 79.32 3.65 o 5 11 0 1.14 3.89 1.32 o 6 11 0 52.33 52.22 4.36 o 0 12 0 2541.53 2685.45 58.56 o 1 12 0 636.87 650.70 9.78 o 2 12 0 583.20 592.62 6.54 o 3 12 0 894.68 925.09 11.42 o 4 12 0 274.96 252.82 16.42 o 5 12 0 89.73 91.84 4.26 o 6 12 0 144.25 154.19 13.36 o 1 13 0 0.39 1.39 0.64 o 2 13 0 0.03 1.15 1.40 o 3 13 0 15.29 12.74 2.02 o 4 13 0 76.12 66.60 3.57 o 5 13 0 0.10 0.70 1.39 o 0 14 0 1139.23 1176.72 17.12 o 1 14 0 274.46 275.55 3.95 o 2 14 0 316.92 318.22 5.34 o 3 14 0 485.93 474.53 5.92 o 4 14 0 138.74 136.93 4.67 o 5 14 0 44.19 35.85 3.55 o 1 15 0 9.87 8.10 0.55 o 2 15 0 5.72 5.44 0.57 o 3 15 0 15.20 13.96 1.44 o 4 15 0 40.68 36.00 2.35 o 5 15 0 10.47 8.95 2.13 o 0 16 0 189.30 193.53 3.97 o 1 16 0 4.54 6.81 0.66 o 2 16 0 34.13 36.54 2.14 o 3 16 0 120.88 114.16 5.90 o 4 16 0 19.40 20.11 1.71 o 5 16 0 1.13 2.57 0.95 o 1 17 0 121.20 115.93 4.03 o 2 17 0 24.59 19.60 2.01 o 3 17 0 8.33 7.78 1.83 o 4 17 0 4.49 3.75 0.95 o 0 18 0 354.09 359.30 6.02 o 1 18 0 86.72 87.58 2.05 o 2 18 0 86.54 76.70 5.06 o 3 18 0 139.50 139.29 3.42 o 4 18 0 73.29 60.79 10.20 o 1 19 0 0.22 1.97 0.61 o 2 19 0 0.00 0.59 0.88 o 3 19 0 0.53 0.70 0.38 o 4 19 0 6.19 3.08 1.17 o 0 20 0 88.60 88.51 4.84 o 1 20 0 9.45 15.31 0.98 o 2 20 0 10.98 18.20 2.35 o -7 0 1 176.38 186.85 6.90 o -6 0 1 62.81 82.93 5.28 o -5 0 1 28.84 25.25 2.35 o -4 0 1 1272.12 1292.06 18.06 o -3 0 1 1657.37 1669.58 10.22 o -2 0 1 699.53 624.39 4.36 o -1 0 1 921.17 875.68 4.88 o 0 0 1 1765.57 1879.34 13.36 o 1 0 1 338.62 286.79 2.57 o 2 0 1 3267.60 3289.10 17.64 o 3 0 1 1534.48 1590.52 14.01 o 4 0 1 117.75 111.10 2.95 o 5 0 1 382.35 394.98 11.01 o 6 0 1 147.89 150.59 6.16 o -7 1 1 93.96 102.27 11.52 o -6 1 1 36.09 36.61 4.11 o -5 1 1 196.43 193.26 4.46 o -4 1 1 609.14 625.97 6.71 o -3 1 1 36.00 35.53 0.90 o -2 1 1 1246.58 1255.36 5.25 o -1 1 1 2455.08 2428.30 8.75 o 0 1 1 97.30 84.39 0.95 o 2 1 1 109.44 91.06 1.86 o 3 1 1 70.58 72.15 1.35 o 4 1 1 186.59 162.51 3.88 o 5 1 1 288.97 275.72 11.67 o 6 1 1 54.22 50.63 2.74 o -7 2 1 141.73 146.19 6.02 o -6 2 1 65.24 70.61 4.70 o -5 2 1 42.53 34.40 3.16 o -4 2 1 1227.53 1199.14 26.86 o -3 2 1 2322.80 2353.48 59.22 o -2 2 1 672.18 642.61 5.04 o -1 2 1 807.08 783.26 3.81 o 0 2 1 1802.58 1815.46 16.00 o 1 2 1 230.86 209.10 1.92 o 2 2 1 4728.05 4710.16 45.72 o 3 2 1 2087.68 2079.90 22.71 o 4 2 1 113.73 112.76 2.09 o 5 2 1 409.32 417.02 8.20 o 6 2 1 147.35 153.92 11.74 o -7 3 1 133.31 123.73 5.58 o -6 3 1 158.81 159.11 4.41 o -5 3 1 357.94 358.73 8.95 o -4 3 1 554.32 565.97 6.53 o -3 3 1 100.21 109.14 3.37 o -2 3 1 3051.23 3182.80 11.85 o -1 3 1 4824.30 4955.06 32.01 o 0 3 1 52.34 57.97 2.28 o 1 3 1 1619.11 1625.72 6.92 o 2 3 1 662.37 692.91 4.12 o 3 3 1 61.61 75.06 1.55 o 4 3 1 221.00 204.13 3.06 o 5 3 1 105.47 101.13 4.62 o 6 3 1 67.73 71.34 2.90 o -7 4 1 113.02 106.71 4.99 o -6 4 1 601.26 613.00 11.78 o -5 4 1 426.60 457.06 8.45 o -4 4 1 1208.19 1240.36 12.29 o -3 4 1 12.09 5.42 1.02 o -2 4 1 19.70 13.02 0.81 o -1 4 1 13922.39 14310.18 82.78 o 1 4 1 67.53 60.62 1.78 o 2 4 1 92.73 64.93 0.99 o 3 4 1 755.05 687.84 5.02 o 4 4 1 866.96 803.46 17.76 o 5 4 1 1124.50 1157.44 23.63 o 6 4 1 82.54 86.30 4.33 o -7 5 1 9.11 9.39 2.94 o -6 5 1 35.15 34.88 2.38 o -5 5 1 3.11 4.48 1.91 o -4 5 1 295.56 274.03 3.69 o -3 5 1 1.07 2.77 0.49 o -2 5 1 5.13 14.58 0.70 o -1 5 1 2271.58 2431.16 8.84 o 0 5 1 4325.95 4557.50 42.57 o 1 5 1 856.07 844.52 5.12 o 2 5 1 107.16 80.69 1.13 o 3 5 1 586.97 589.74 6.24 o 4 5 1 222.53 216.64 3.92 o 5 5 1 13.05 14.91 3.16 o 6 5 1 95.66 91.47 4.77 o -7 6 1 168.88 166.15 6.46 o -6 6 1 109.22 120.15 4.72 o -5 6 1 4.94 4.91 1.09 o -4 6 1 1070.88 1106.54 16.78 o -3 6 1 1728.53 1781.11 10.93 o -2 6 1 404.01 397.27 2.30 o -1 6 1 171.24 130.40 2.33 o 0 6 1 919.08 851.95 4.65 o 1 6 1 646.38 604.94 2.88 o 2 6 1 2864.16 2867.44 19.01 o 3 6 1 651.68 644.08 7.84 o 4 6 1 10.35 9.33 0.99 o 5 6 1 133.10 140.71 3.88 o 6 6 1 125.26 140.17 10.05 o -6 7 1 13.61 15.64 1.98 o -5 7 1 79.50 78.52 3.48 o -4 7 1 218.01 225.01 3.37 o -3 7 1 1.04 2.94 0.85 o -2 7 1 515.07 502.23 4.41 o -1 7 1 544.84 535.20 2.86 o 0 7 1 153.90 163.19 2.25 o 1 7 1 297.75 283.27 1.99 o 2 7 1 7.40 7.92 0.53 o 3 7 1 46.09 46.47 1.17 o 4 7 1 70.99 70.26 4.61 o 5 7 1 62.84 66.59 4.46 o 6 7 1 90.64 86.19 9.54 o -6 8 1 85.32 78.61 3.48 o -5 8 1 9.39 7.70 1.40 o -4 8 1 895.59 882.47 12.84 o -3 8 1 1044.32 1078.26 10.67 o -2 8 1 409.09 400.39 2.90 o -1 8 1 1094.71 1075.30 6.95 o 0 8 1 2854.66 2873.52 18.29 o 1 8 1 500.10 470.74 2.46 o 2 8 1 1470.04 1521.74 11.10 o 3 8 1 959.50 965.84 10.44 o 4 8 1 126.82 126.01 3.36 o 5 8 1 291.54 309.70 10.93 o 6 8 1 105.51 103.41 8.73 o -6 9 1 53.96 45.10 9.25 o -5 9 1 141.61 141.55 3.91 o -4 9 1 220.22 213.67 3.94 o -3 9 1 5.64 5.37 0.46 o -2 9 1 384.99 394.40 5.00 o -1 9 1 590.91 570.64 6.01 o 0 9 1 10.92 8.69 0.30 o 1 9 1 403.11 401.34 3.00 o 2 9 1 25.65 18.97 0.70 o 3 9 1 23.52 21.37 1.06 o 4 9 1 40.38 36.98 2.15 o 5 9 1 60.55 63.94 2.96 o 6 9 1 47.90 48.41 4.25 o -6 10 1 56.20 58.25 4.98 o -5 10 1 10.33 9.93 2.13 o -4 10 1 688.13 682.47 10.35 o -3 10 1 579.59 579.94 6.69 o -2 10 1 187.28 186.14 1.76 o -1 10 1 937.08 894.36 5.43 o 0 10 1 2038.09 2142.86 13.77 o 1 10 1 453.27 434.18 3.05 o 2 10 1 976.53 983.18 9.65 o 3 10 1 591.74 597.07 6.78 o 4 10 1 188.15 192.21 7.27 o 5 10 1 345.10 359.86 7.63 o 6 10 1 80.70 74.15 2.99 o -6 11 1 50.65 45.91 5.21 o -5 11 1 111.68 103.99 4.86 o -4 11 1 171.47 161.66 5.18 o -3 11 1 14.62 12.11 0.70 o -2 11 1 419.45 402.45 4.43 o -1 11 1 720.43 700.16 7.79 o 0 11 1 212.51 227.71 2.76 o 1 11 1 600.18 616.71 6.27 o 2 11 1 44.34 36.08 2.21 o 3 11 1 0.45 1.91 0.62 o 4 11 1 86.29 90.00 2.84 o 5 11 1 129.62 127.03 4.26 o -6 12 1 53.31 56.62 5.18 o -5 12 1 20.78 12.92 1.69 o -4 12 1 26.60 33.17 1.66 o -3 12 1 67.79 59.81 2.20 o -2 12 1 253.51 248.28 3.17 o -1 12 1 738.02 721.52 7.01 o 0 12 1 210.05 184.55 2.10 o 1 12 1 100.13 105.35 4.89 o 2 12 1 256.41 236.43 3.04 o 3 12 1 523.91 515.16 6.95 o 4 12 1 124.05 124.05 3.34 o 5 12 1 70.55 76.64 7.12 o -6 13 1 12.86 10.81 1.68 o -5 13 1 12.94 16.59 2.86 o -4 13 1 133.60 123.18 7.43 o -3 13 1 121.77 119.49 3.71 o -2 13 1 380.60 380.10 4.33 o -1 13 1 140.92 123.02 4.62 o 0 13 1 18.94 16.27 0.74 o 1 13 1 278.71 290.34 3.47 o 2 13 1 194.68 191.82 4.70 o 3 13 1 5.00 4.11 0.74 o 4 13 1 4.88 2.98 1.69 o 5 13 1 12.93 11.41 2.86 o -5 14 1 30.67 26.93 2.67 o -4 14 1 411.45 408.38 11.96 o -3 14 1 287.96 272.36 7.38 o -2 14 1 85.29 81.68 2.56 o -1 14 1 333.89 327.70 3.68 o 0 14 1 963.03 993.02 17.08 o 1 14 1 447.27 467.63 5.76 o 2 14 1 559.17 589.96 8.53 o 3 14 1 214.32 211.04 8.40 o 4 14 1 55.38 58.08 3.44 o 5 14 1 155.12 167.80 9.03 o -5 15 1 30.20 26.95 3.45 o -4 15 1 69.69 66.26 5.28 o -3 15 1 19.26 17.18 1.97 o -2 15 1 145.54 150.50 3.15 o -1 15 1 113.40 102.96 3.20 o 0 15 1 1.60 1.81 0.47 o 1 15 1 67.80 56.59 2.84 o 2 15 1 30.30 27.51 1.65 o 3 15 1 7.53 6.91 1.07 o 4 15 1 12.65 9.79 1.09 o 5 15 1 2.96 1.17 0.66 o -5 16 1 13.97 10.12 1.69 o -4 16 1 162.00 154.94 15.12 o -3 16 1 78.80 80.27 2.47 o -2 16 1 31.73 28.68 1.46 o -1 16 1 160.85 160.62 3.69 o 0 16 1 374.46 369.37 4.56 o 1 16 1 96.47 95.08 2.07 o 2 16 1 149.85 147.81 5.91 o 3 16 1 70.90 63.09 5.53 o 4 16 1 18.94 21.39 8.22 o -4 17 1 29.20 23.87 2.44 o -3 17 1 1.00 0.15 0.42 o -2 17 1 0.48 0.81 0.24 o -1 17 1 1.47 2.06 0.32 o 0 17 1 1.28 1.68 0.38 o 1 17 1 32.57 31.12 2.99 o 2 17 1 1.05 0.38 0.34 o 3 17 1 15.46 15.18 1.40 o 4 17 1 0.41 1.17 0.59 o -4 18 1 89.78 82.20 4.70 o -3 18 1 83.62 71.19 9.39 o -2 18 1 35.68 35.62 2.00 o -1 18 1 53.48 52.94 4.73 o 0 18 1 166.32 154.24 5.02 o 1 18 1 65.58 81.36 12.40 o 2 18 1 101.46 97.31 10.41 o 3 18 1 28.06 26.61 4.40 o 4 18 1 1.28 4.26 1.91 o -4 19 1 20.00 11.89 2.50 o -3 19 1 0.24 1.76 0.59 o -2 19 1 12.71 11.74 1.61 o -1 19 1 22.57 11.80 1.98 o 0 19 1 5.58 2.08 0.52 o 1 19 1 37.43 34.90 5.94 o 2 19 1 3.05 1.17 0.88 o 3 19 1 61.03 47.70 5.43 o -3 20 1 28.04 17.61 3.67 o -2 20 1 88.75 100.40 3.96 o -1 20 1 149.93 182.44 5.72 o 0 20 1 111.95 110.08 5.43 o 1 20 1 5.86 7.19 1.32 o 2 20 1 56.28 64.44 7.05 o 3 20 1 120.14 109.50 4.40 o -2 21 1 195.67 201.38 6.31 o -1 21 1 182.77 174.81 5.43 o 0 21 1 5.07 9.25 2.05 o 1 21 1 2.03 1.76 1.03 o -7 0 2 34.97 38.02 4.99 o -6 0 2 21.95 26.13 5.14 o -5 0 2 71.78 77.35 5.14 o -4 0 2 127.54 104.27 2.48 o -3 0 2 1040.94 1228.82 15.41 o -2 0 2 28.98 20.48 1.07 o -1 0 2 2474.10 2466.13 16.29 o 0 0 2 472.49 479.92 6.24 o 1 0 2 24.15 39.19 1.04 o 2 0 2 10.85 40.14 1.34 o 3 0 2 20.86 10.80 0.92 o 4 0 2 433.88 425.95 11.89 o 5 0 2 287.24 286.80 8.81 o 6 0 2 21.86 18.93 3.23 o -7 1 2 3.73 5.57 1.91 o -6 1 2 66.88 74.47 3.27 o -5 1 2 546.94 542.06 10.07 o -4 1 2 177.53 173.38 2.46 o -3 1 2 912.55 922.09 6.05 o -2 1 2 2323.14 2391.20 17.77 o -1 1 2 7.91 11.52 1.46 o 0 1 2 9.07 4.87 0.34 o 1 1 2 4985.05 5126.46 26.74 o 2 1 2 279.83 286.71 3.96 o 3 1 2 131.23 119.59 1.90 o 4 1 2 288.31 265.40 10.35 o 5 1 2 1.88 7.23 1.93 o 6 1 2 7.11 9.46 3.52 o -7 2 2 105.80 112.58 4.84 o -6 2 2 1.32 1.81 1.39 o -5 2 2 14.21 26.41 2.79 o -4 2 2 1209.55 1276.43 12.57 o -3 2 2 410.90 423.90 5.78 o -2 2 2 878.93 862.49 3.92 o -1 2 2 278.37 273.45 1.57 o 0 2 2 128.99 125.78 1.00 o 1 2 2 2435.70 2411.78 20.74 o 2 2 2 2235.29 2237.38 13.15 o 3 2 2 174.23 184.15 3.22 o 4 2 2 137.85 141.17 6.38 o 5 2 2 272.92 292.38 6.28 o 6 2 2 18.22 17.80 2.07 o -7 3 2 13.59 15.16 1.90 o -6 3 2 126.39 143.91 3.94 o -5 3 2 593.62 597.77 10.58 o -4 3 2 44.90 45.71 1.50 o -3 3 2 287.12 255.99 3.65 o -2 3 2 2519.69 2497.85 12.52 o -1 3 2 317.95 263.02 5.00 o 0 3 2 84.75 61.20 1.00 o 1 3 2 2199.05 2161.70 8.38 o 2 3 2 64.18 89.70 1.92 o 3 3 2 47.42 45.51 1.20 o 4 3 2 505.89 469.63 48.80 o 5 3 2 7.07 8.17 1.90 o 6 3 2 5.84 11.16 2.57 o -7 4 2 89.26 102.16 4.84 o -6 4 2 1.99 3.21 0.98 o -5 4 2 46.38 42.07 3.38 o -4 4 2 989.54 1000.49 20.12 o -3 4 2 214.78 221.30 3.30 o -2 4 2 907.12 896.37 4.18 o -1 4 2 1641.10 1633.07 9.85 o 0 4 2 968.53 968.57 8.15 o 1 4 2 1260.09 1237.12 6.18 o 2 4 2 1268.31 1261.86 11.16 o 3 4 2 267.12 262.83 3.32 o 4 4 2 332.44 329.70 17.39 o 5 4 2 384.44 421.46 8.77 o 6 4 2 11.07 11.68 2.94 o -7 5 2 31.62 30.82 4.40 o -6 5 2 242.80 251.46 6.70 o -5 5 2 646.41 677.09 20.11 o -4 5 2 86.77 83.07 1.77 o -3 5 2 404.93 385.34 3.15 o -2 5 2 2289.11 2328.46 12.25 o -1 5 2 861.74 802.21 4.85 o 0 5 2 295.97 230.27 5.21 o 1 5 2 2105.81 2164.65 8.47 o 2 5 2 3.43 4.34 0.63 o 3 5 2 61.15 56.71 1.37 o 4 5 2 385.45 398.04 7.88 o 5 5 2 10.10 16.31 2.15 o 6 5 2 1.32 1.01 0.87 o -7 6 2 57.90 52.69 6.31 o -6 6 2 5.48 8.04 1.76 o -5 6 2 87.15 91.30 11.83 o -4 6 2 959.56 939.90 22.22 o -3 6 2 117.84 118.20 2.30 o -2 6 2 770.39 723.85 4.66 o -1 6 2 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520.36 5.82 o -2 9 2 196.58 166.78 5.73 o -1 9 2 779.95 820.78 10.71 o 0 9 2 105.82 138.56 2.22 o 1 9 2 1731.22 1727.62 12.32 o 2 9 2 67.12 57.79 2.20 o 3 9 2 13.42 10.96 0.98 o 4 9 2 1.31 1.95 1.98 o 5 9 2 8.03 4.16 1.44 o -6 10 2 4.09 1.70 1.61 o -5 10 2 15.40 15.80 2.33 o -4 10 2 490.77 474.52 6.86 o -3 10 2 24.77 19.82 1.21 o -2 10 2 1.30 0.66 0.64 o -1 10 2 2.46 1.57 0.53 o 0 10 2 198.92 180.10 5.14 o 1 10 2 906.97 902.38 9.07 o 2 10 2 425.03 439.52 5.93 o 3 10 2 2.24 2.32 0.80 o 4 10 2 2.34 3.17 2.13 o 5 10 2 102.36 101.40 11.30 o -6 11 2 79.94 84.08 5.50 o -5 11 2 212.11 213.36 4.85 o -4 11 2 53.67 53.31 2.24 o -3 11 2 319.17 328.38 4.52 o -2 11 2 1278.02 1324.54 12.61 o -1 11 2 412.90 413.51 6.75 o 0 11 2 68.98 65.85 2.42 o 1 11 2 691.89 697.56 7.14 o 2 11 2 108.37 105.03 2.75 o 3 11 2 299.54 324.01 8.46 o 4 11 2 300.90 291.21 6.32 o 5 11 2 3.03 2.58 1.16 o -6 12 2 0.37 2.28 0.92 o -5 12 2 20.09 15.97 1.34 o -4 12 2 187.34 180.44 5.25 o -3 12 2 0.66 2.12 0.44 o -2 12 2 46.15 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