#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:30:04 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181172 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/51/2225118.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225118_Fobs loop_ _publ_author_name 'Caracelli, Ignez' 'Moran, Paulo J. S.' 'Hinoue, Luciana' 'Zukerman-Schpector, Julio' 'Tiekink, Edward R. T.' _publ_section_title ; Ethyl (E)-2-methoxyimino-2-(4-nitrobenzoyl)acetate ; _journal_coeditor_code SU2157 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o396 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.264 _cell_angle_beta 73.731 _cell_angle_gamma 68.939 _cell_length_a 7.5197 _cell_length_b 7.5793 _cell_length_c 12.3338 _exptl_crystal_F_000 292.00 _reflns_d_resolution_high 0.7942 _cod_data_source_file su2157Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' moran2 in P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 107.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 22.78 21.27 0.24 o 2 0 0 403.59 422.40 3.19 o 3 0 0 147.40 177.79 1.54 o 4 0 0 711.52 732.74 5.56 o 5 0 0 159.25 158.67 1.90 o 6 0 0 98.37 93.22 1.53 o 7 0 0 19.64 16.87 0.69 o 8 0 0 4.84 4.74 0.62 o -8 1 0 0.09 0.36 0.38 o -7 1 0 25.43 23.73 0.83 o -6 1 0 5.73 6.83 0.48 o -5 1 0 3.45 4.23 0.37 o -4 1 0 0.01 0.01 0.17 o -3 1 0 318.69 297.93 2.48 o -2 1 0 16.43 14.09 0.31 o -1 1 0 36.55 30.17 0.37 o 0 1 0 1593.87 1616.76 11.68 o 1 1 0 260.16 247.03 2.49 o 2 1 0 1185.80 1210.99 11.34 o 3 1 0 967.13 955.67 11.51 o 4 1 0 5.43 5.64 0.19 o 5 1 0 25.47 29.16 0.66 o 6 1 0 50.90 41.00 0.89 o 7 1 0 0.00 -0.13 0.27 o 8 1 0 0.82 0.90 0.51 o -7 2 0 52.17 49.79 1.32 o -6 2 0 8.28 8.73 0.70 o -5 2 0 57.43 54.11 1.07 o -4 2 0 34.28 33.35 1.08 o -3 2 0 260.91 243.76 2.18 o -1 2 0 81.97 81.72 0.84 o 0 2 0 671.78 670.48 4.87 o 1 2 0 2366.86 2372.95 18.56 o 2 2 0 186.14 199.05 1.87 o 3 2 0 430.28 424.96 4.37 o 4 2 0 345.01 412.18 4.01 o 5 2 0 190.67 206.61 2.70 o 6 2 0 1.21 1.51 0.34 o 7 2 0 410.29 392.74 4.43 o 8 2 0 4.02 8.33 0.93 o 9 2 0 0.34 0.38 0.62 o -7 3 0 55.27 55.21 1.70 o -6 3 0 14.96 14.92 0.75 o -5 3 0 30.18 29.98 0.93 o -4 3 0 51.79 49.43 1.10 o -3 3 0 23.80 22.37 0.62 o -2 3 0 1.68 0.80 0.18 o -1 3 0 6.83 7.24 0.26 o 0 3 0 71.29 61.11 0.65 o 1 3 0 30.27 29.68 0.45 o 2 3 0 596.70 599.15 5.28 o 3 3 0 19.93 18.76 0.47 o 4 3 0 253.52 271.59 2.89 o 5 3 0 37.15 42.13 0.97 o 6 3 0 41.70 48.40 1.87 o 7 3 0 419.01 386.09 6.56 o 8 3 0 11.15 12.56 2.13 o 9 3 0 0.50 1.20 0.70 o -6 4 0 8.16 8.71 0.78 o -5 4 0 2.56 2.81 0.52 o -4 4 0 2.54 2.41 0.49 o -3 4 0 0.00 0.04 0.28 o -2 4 0 3.11 3.71 0.33 o -1 4 0 1488.23 1494.29 10.07 o 0 4 0 154.09 167.07 1.46 o 1 4 0 533.27 547.81 4.21 o 2 4 0 296.31 307.09 2.51 o 3 4 0 143.35 149.94 1.66 o 4 4 0 267.36 245.66 2.81 o 5 4 0 321.15 317.48 3.89 o 6 4 0 48.96 48.95 1.16 o 7 4 0 9.16 9.66 0.93 o -5 5 0 60.80 62.07 1.76 o -4 5 0 3.04 4.03 0.50 o -3 5 0 80.46 75.81 1.33 o -2 5 0 18.37 18.40 0.64 o -1 5 0 6.89 6.41 0.35 o 0 5 0 373.80 364.56 3.17 o 1 5 0 0.09 2.07 0.74 o 2 5 0 316.92 323.54 2.73 o 3 5 0 49.14 47.00 0.82 o 4 5 0 42.05 39.85 0.76 o 5 5 0 58.16 57.77 1.54 o 6 5 0 37.39 38.71 1.97 o 7 5 0 0.01 0.22 0.66 o -4 6 0 38.16 39.56 1.41 o -3 6 0 62.82 62.76 1.30 o -2 6 0 4.04 4.38 0.42 o -1 6 0 0.67 -0.14 0.32 o 0 6 0 4.60 3.92 0.34 o 1 6 0 15.10 14.44 0.55 o 2 6 0 86.26 80.84 1.22 o 3 6 0 0.02 -0.08 0.26 o 4 6 0 21.18 22.91 0.87 o 5 6 0 0.00 -0.44 0.77 o 6 6 0 235.79 232.46 5.90 o 7 6 0 203.07 205.02 5.47 o 8 6 0 36.41 41.55 2.30 o -3 7 0 26.43 28.02 1.20 o -2 7 0 199.10 197.31 2.90 o -1 7 0 10.96 9.97 0.63 o 0 7 0 19.06 19.38 0.66 o 1 7 0 30.37 27.98 0.78 o 2 7 0 8.36 10.60 0.51 o 3 7 0 9.45 9.71 0.55 o 4 7 0 18.81 17.37 1.29 o 5 7 0 202.52 201.66 3.98 o 6 7 0 118.41 129.37 3.05 o 7 7 0 7.68 6.01 1.09 o 8 7 0 109.18 124.87 4.26 o -1 8 0 32.87 30.48 1.24 o 0 8 0 27.14 27.29 1.25 o 1 8 0 6.33 8.62 0.89 o 2 8 0 10.88 9.29 0.54 o 3 8 0 30.59 27.89 0.81 o 4 8 0 98.27 99.97 2.63 o 5 8 0 84.43 90.61 2.55 o 6 8 0 7.54 9.51 1.04 o 7 8 0 0.24 0.30 0.65 o 1 9 0 2.10 1.86 0.54 o 2 9 0 31.26 35.36 0.99 o 3 9 0 1.32 3.52 0.47 o 4 9 0 159.94 177.60 3.90 o 5 9 0 55.75 53.82 3.55 o -5 -9 1 11.52 13.60 1.20 o -4 -9 1 2.19 3.98 0.76 o -3 -9 1 5.21 5.66 0.55 o -2 -9 1 9.93 15.44 0.72 o -1 -9 1 4.52 6.06 0.57 o -6 -8 1 9.51 10.25 1.59 o -5 -8 1 266.24 268.24 5.19 o -4 -8 1 42.18 46.17 1.36 o -3 -8 1 6.62 7.76 0.51 o -2 -8 1 12.61 12.01 0.60 o -1 -8 1 72.50 67.28 1.29 o 0 -8 1 0.24 0.19 0.35 o 1 -8 1 26.54 21.19 1.34 o -7 -7 1 105.15 117.32 4.05 o -6 -7 1 112.72 117.37 4.76 o -5 -7 1 290.39 290.76 4.07 o -4 -7 1 119.91 117.76 2.14 o -3 -7 1 21.21 22.12 1.01 o -2 -7 1 20.72 20.91 0.67 o -1 -7 1 45.03 43.56 0.96 o 0 -7 1 0.18 -0.24 0.24 o 1 -7 1 158.02 152.22 2.36 o 2 -7 1 13.93 10.76 0.69 o 3 -7 1 27.46 28.43 1.21 o -7 -6 1 16.52 19.68 1.64 o -6 -6 1 0.27 1.20 0.77 o -5 -6 1 219.94 215.62 3.17 o -4 -6 1 1197.67 1182.97 12.84 o -3 -6 1 3.51 2.74 0.42 o -2 -6 1 0.33 0.00 0.38 o -1 -6 1 136.87 139.99 1.77 o 0 -6 1 136.68 126.15 1.69 o 1 -6 1 5.70 5.65 0.37 o 2 -6 1 53.75 51.16 1.25 o 3 -6 1 0.01 -0.06 0.29 o 4 -6 1 9.64 8.96 0.80 o -7 -5 1 53.83 51.94 2.30 o -6 -5 1 164.39 167.83 5.90 o -5 -5 1 19.33 18.85 1.09 o -4 -5 1 397.58 399.78 6.91 o -3 -5 1 132.38 128.33 1.65 o -2 -5 1 722.94 709.97 5.95 o -1 -5 1 553.05 588.52 5.61 o 0 -5 1 10.72 10.48 0.41 o 1 -5 1 54.00 52.76 0.85 o 2 -5 1 279.07 274.22 2.94 o 3 -5 1 9.98 9.93 0.50 o 4 -5 1 0.67 0.62 0.33 o 5 -5 1 230.35 238.98 3.87 o -6 -4 1 60.83 60.34 1.13 o -5 -4 1 4.80 4.13 0.42 o -4 -4 1 9.12 9.39 0.46 o -3 -4 1 29.35 26.21 0.55 o -2 -4 1 333.62 344.10 2.78 o -1 -4 1 102.01 104.15 1.09 o 0 -4 1 129.52 135.55 1.26 o 1 -4 1 2.08 2.59 0.21 o 2 -4 1 100.76 104.23 1.23 o 3 -4 1 512.25 507.97 6.53 o 4 -4 1 7.87 7.29 0.48 o 5 -4 1 4.69 5.09 0.53 o 6 -4 1 14.70 14.88 0.92 o -8 -3 1 10.66 10.87 0.96 o -7 -3 1 4.56 7.12 0.52 o -6 -3 1 18.29 18.05 0.66 o -5 -3 1 27.13 28.58 0.82 o -4 -3 1 141.71 129.71 1.47 o -3 -3 1 2.86 3.28 0.24 o -2 -3 1 196.03 197.60 1.97 o -1 -3 1 89.53 102.04 0.99 o 0 -3 1 2370.74 2341.80 17.58 o 1 -3 1 2.23 2.00 0.16 o 2 -3 1 57.40 61.90 0.73 o 3 -3 1 216.19 209.87 1.87 o 4 -3 1 0.67 0.60 0.27 o 5 -3 1 2.35 2.44 0.58 o 6 -3 1 350.57 347.06 4.30 o 7 -3 1 3.29 2.77 0.92 o -8 -2 1 51.37 40.44 1.66 o -7 -2 1 20.25 17.78 1.01 o -6 -2 1 1.52 1.45 0.33 o -5 -2 1 45.71 40.36 0.75 o -4 -2 1 0.27 1.12 0.22 o -3 -2 1 2.74 3.68 0.20 o -2 -2 1 854.48 888.30 8.24 o -1 -2 1 1591.31 1646.59 12.68 o 0 -2 1 170.64 184.92 1.65 o 1 -2 1 369.20 365.78 3.36 o 2 -2 1 328.02 319.11 2.40 o 3 -2 1 1.14 -0.06 0.29 o 4 -2 1 13.41 12.55 0.46 o 5 -2 1 3.66 4.25 0.40 o 6 -2 1 2.63 3.39 0.43 o 7 -2 1 60.99 63.17 1.33 o -8 -1 1 5.53 5.03 0.56 o -7 -1 1 268.45 253.69 2.94 o -6 -1 1 5.35 9.76 0.50 o -5 -1 1 10.14 9.97 0.43 o -4 -1 1 72.85 76.12 0.79 o -3 -1 1 768.90 748.86 5.98 o -2 -1 1 1355.70 1299.58 12.12 o -1 -1 1 492.21 476.58 6.54 o 0 -1 1 1222.18 1230.17 11.99 o 1 -1 1 394.09 364.40 2.74 o 2 -1 1 38.65 29.00 0.42 o 3 -1 1 154.82 158.18 1.46 o 4 -1 1 228.08 217.13 1.98 o 5 -1 1 97.83 96.93 1.42 o 6 -1 1 33.24 32.65 0.85 o 7 -1 1 91.63 89.00 1.53 o 8 -1 1 21.59 22.63 1.18 o -8 0 1 0.54 0.05 0.47 o -7 0 1 39.38 34.89 0.96 o -6 0 1 38.43 34.47 0.86 o -5 0 1 26.27 25.94 0.67 o -4 0 1 402.21 443.86 3.56 o -3 0 1 1276.51 1229.88 8.95 o -2 0 1 117.60 117.93 1.14 o -1 0 1 3568.05 3424.31 28.66 o 0 0 1 115.66 108.76 3.16 o 1 0 1 169.27 178.24 1.35 o 2 0 1 7043.15 6444.81 55.19 o 3 0 1 87.65 103.40 1.07 o 4 0 1 77.48 77.49 0.88 o 5 0 1 49.47 45.37 0.86 o 6 0 1 30.75 29.96 0.77 o 7 0 1 46.16 47.10 1.05 o 8 0 1 2.62 2.47 0.59 o -8 1 1 24.19 21.89 1.11 o -7 1 1 0.12 0.12 0.38 o -6 1 1 144.40 135.35 1.91 o -5 1 1 154.55 152.48 1.92 o -4 1 1 61.09 66.22 0.90 o -3 1 1 8.16 6.72 0.42 o -2 1 1 2.31 3.74 0.19 o -1 1 1 2.94 4.07 0.21 o 0 1 1 14.62 24.17 0.28 o 1 1 1 258.14 277.87 2.28 o 2 1 1 1108.81 1063.51 13.43 o 3 1 1 294.03 284.42 2.88 o 4 1 1 1205.42 1246.40 9.00 o 5 1 1 767.64 765.40 7.26 o 6 1 1 13.66 10.47 0.70 o 7 1 1 0.18 -0.14 0.27 o 8 1 1 0.05 -0.42 0.42 o -7 2 1 5.97 6.63 0.64 o -6 2 1 163.60 155.30 2.40 o -5 2 1 94.58 86.49 1.91 o -4 2 1 152.76 152.47 2.28 o -3 2 1 70.81 82.71 1.11 o -2 2 1 2.77 2.40 0.22 o -1 2 1 37.02 34.34 0.50 o 0 2 1 11517.91 10411.71 108.35 o 1 2 1 3171.71 3106.60 25.36 o 2 2 1 354.01 360.92 3.20 o 3 2 1 12.86 13.61 0.33 o 4 2 1 844.42 939.26 9.83 o 5 2 1 64.86 64.05 1.03 o 6 2 1 93.42 82.67 1.55 o 7 2 1 4.95 3.21 0.71 o 8 2 1 1.93 2.27 0.65 o 9 2 1 4.15 5.96 0.93 o -6 3 1 1.20 0.79 0.39 o -5 3 1 6.51 5.97 0.52 o -4 3 1 19.38 21.18 0.77 o -3 3 1 29.13 26.68 0.76 o -2 3 1 4.81 5.63 0.28 o -1 3 1 649.71 648.96 5.57 o 0 3 1 632.36 693.73 4.76 o 1 3 1 57.63 61.59 0.64 o 2 3 1 1187.58 1212.50 9.40 o 3 3 1 0.00 -0.13 0.20 o 4 3 1 400.75 369.17 3.75 o 5 3 1 0.53 1.21 0.29 o 6 3 1 20.56 26.96 0.72 o 7 3 1 28.78 22.20 1.64 o 8 3 1 0.76 0.87 0.54 o 9 3 1 66.97 84.73 4.37 o -6 4 1 11.14 11.50 0.90 o -5 4 1 0.28 0.19 0.38 o -4 4 1 21.38 21.41 0.82 o -3 4 1 14.16 14.32 0.64 o -2 4 1 6.83 8.35 0.42 o -1 4 1 89.13 93.91 1.47 o 0 4 1 9.03 10.87 0.33 o 1 4 1 26.26 34.52 0.52 o 2 4 1 173.00 197.59 1.88 o 3 4 1 119.47 123.81 1.42 o 4 4 1 191.57 202.04 2.09 o 5 4 1 1.32 3.96 0.53 o 6 4 1 17.75 17.41 2.02 o 7 4 1 16.57 15.77 0.96 o 8 4 1 18.57 13.55 1.01 o 9 4 1 1.14 2.44 0.73 o -5 5 1 5.56 6.53 0.72 o -4 5 1 11.50 13.03 0.73 o -3 5 1 1.09 1.13 0.32 o -2 5 1 15.15 16.20 0.61 o -1 5 1 37.92 40.48 0.74 o 0 5 1 152.36 158.24 1.65 o 1 5 1 0.85 1.12 0.21 o 2 5 1 151.92 159.63 1.45 o 3 5 1 216.90 243.93 2.17 o 4 5 1 399.66 389.99 3.78 o 5 5 1 6.69 6.32 0.45 o 6 5 1 289.66 295.04 4.83 o 7 5 1 102.72 96.22 3.17 o -4 6 1 101.62 110.21 4.38 o -3 6 1 52.64 50.72 1.16 o -2 6 1 1.23 0.81 0.48 o -1 6 1 171.68 170.40 2.14 o 0 6 1 0.09 0.15 0.25 o 1 6 1 0.19 -0.14 0.23 o 2 6 1 0.18 0.35 0.23 o 3 6 1 0.19 0.25 0.26 o 4 6 1 129.32 123.20 2.06 o 5 6 1 113.22 111.42 3.50 o 6 6 1 341.34 340.38 7.76 o 7 6 1 17.42 20.01 1.64 o 8 6 1 2.77 5.25 1.09 o -3 7 1 0.22 0.65 0.44 o -2 7 1 4.56 3.41 0.45 o -1 7 1 60.02 57.51 1.20 o 0 7 1 1.42 1.54 0.38 o 1 7 1 381.33 366.12 3.71 o 2 7 1 13.99 11.23 0.55 o 3 7 1 107.63 108.25 1.52 o 4 7 1 82.20 87.23 1.75 o 5 7 1 43.11 45.06 2.30 o 6 7 1 3.09 3.37 0.68 o 7 7 1 0.85 0.98 0.77 o 8 7 1 23.06 27.34 1.97 o -1 8 1 9.00 9.31 0.75 o 0 8 1 0.09 -0.05 0.37 o 1 8 1 85.42 74.45 1.35 o 2 8 1 0.42 0.10 0.28 o 3 8 1 34.41 29.99 0.83 o 4 8 1 97.17 97.19 2.58 o 5 8 1 2.92 3.49 0.73 o 6 8 1 1.34 0.72 0.60 o 7 8 1 0.01 0.49 0.68 o 1 9 1 4.26 6.34 0.72 o 2 9 1 36.47 34.63 0.98 o 3 9 1 0.22 0.71 0.82 o 4 9 1 4.55 4.61 0.81 o 5 9 1 233.83 240.40 4.86 o -4 -9 2 0.27 1.01 0.98 o -3 -9 2 1.16 1.60 0.43 o -2 -9 2 56.02 69.12 1.55 o -1 -9 2 0.39 0.62 0.42 o -6 -8 2 11.73 11.48 1.53 o -5 -8 2 134.29 140.15 2.60 o -4 -8 2 8.01 7.70 1.48 o -3 -8 2 0.17 -0.01 0.40 o -2 -8 2 47.09 47.54 1.08 o -1 -8 2 17.42 16.89 0.97 o 0 -8 2 0.33 0.49 0.32 o 1 -8 2 16.52 19.45 0.99 o -7 -7 2 0.24 -0.44 0.87 o -6 -7 2 0.86 0.23 0.58 o -5 -7 2 2.85 3.65 0.54 o -4 -7 2 51.35 51.60 1.36 o -3 -7 2 6.40 5.70 0.56 o -2 -7 2 12.83 12.93 0.63 o -1 -7 2 9.59 9.66 0.51 o 0 -7 2 2.10 2.73 0.36 o 1 -7 2 20.21 19.03 0.84 o 2 -7 2 8.09 8.81 0.71 o 3 -7 2 9.41 9.34 0.80 o -7 -6 2 27.28 30.83 2.08 o -6 -6 2 33.65 38.16 1.69 o -5 -6 2 1054.51 1039.88 11.54 o -4 -6 2 27.19 30.61 1.03 o -3 -6 2 197.49 183.46 3.66 o -2 -6 2 478.98 477.93 5.06 o -1 -6 2 186.09 183.52 3.00 o 0 -6 2 0.49 0.29 0.26 o 1 -6 2 0.26 0.32 0.29 o 2 -6 2 77.61 73.91 1.48 o 3 -6 2 5.43 4.54 0.52 o 4 -6 2 0.63 0.88 0.42 o -7 -5 2 4.00 4.26 0.98 o -6 -5 2 16.46 16.43 0.96 o -5 -5 2 260.53 260.68 4.25 o -4 -5 2 42.61 43.40 1.13 o -3 -5 2 171.82 170.89 2.62 o -2 -5 2 150.44 158.38 2.92 o -1 -5 2 714.38 710.49 6.97 o 0 -5 2 730.91 736.25 5.83 o 1 -5 2 0.87 0.69 0.24 o 2 -5 2 169.44 169.33 5.46 o 3 -5 2 3.09 3.56 0.39 o 4 -5 2 12.65 12.99 0.62 o 5 -5 2 119.02 127.70 2.26 o -7 -4 2 18.80 16.07 1.42 o -6 -4 2 50.87 46.62 2.13 o -5 -4 2 31.18 31.01 1.16 o -4 -4 2 217.89 215.40 2.99 o -3 -4 2 141.19 135.79 1.85 o -2 -4 2 175.81 162.73 1.61 o -1 -4 2 498.14 531.97 4.11 o 0 -4 2 25.41 21.71 0.46 o 1 -4 2 62.24 54.30 0.80 o 2 -4 2 463.69 455.81 3.83 o 3 -4 2 46.18 41.31 0.88 o 4 -4 2 0.01 -0.08 0.25 o 5 -4 2 24.41 25.50 1.07 o 6 -4 2 101.60 103.80 3.50 o -7 -3 2 5.90 5.63 0.50 o -6 -3 2 5.50 4.72 0.62 o -5 -3 2 195.73 198.37 2.34 o -4 -3 2 212.03 200.81 1.92 o -3 -3 2 2.40 2.30 0.22 o -2 -3 2 20.59 20.68 0.42 o -1 -3 2 694.41 703.82 5.20 o 0 -3 2 47.08 44.41 0.59 o 1 -3 2 80.01 77.80 0.81 o 2 -3 2 477.74 519.74 3.54 o 3 -3 2 95.37 97.02 1.08 o 4 -3 2 25.56 28.61 0.71 o 5 -3 2 237.92 234.95 2.75 o 6 -3 2 396.71 404.03 4.30 o 7 -3 2 2.40 2.25 0.47 o -8 -2 2 17.98 16.87 0.92 o -7 -2 2 5.69 6.23 0.52 o -6 -2 2 217.67 211.06 2.69 o -5 -2 2 79.77 90.43 1.34 o -4 -2 2 107.01 115.96 1.56 o -3 -2 2 734.18 771.98 6.11 o -2 -2 2 160.95 196.02 1.84 o -1 -2 2 203.39 224.63 2.16 o 0 -2 2 50.62 52.57 0.57 o 1 -2 2 281.54 266.73 1.85 o 2 -2 2 27.31 23.02 0.37 o 3 -2 2 160.58 156.95 1.30 o 4 -2 2 23.49 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1.89 0.53 o 6 5 13 10.97 9.55 0.83 o 3 6 13 12.32 13.91 2.13 o 4 6 13 1.25 0.43 0.60 o 1 -3 14 39.81 43.36 1.43 o -1 -2 14 11.79 12.37 1.14 o 0 -2 14 3.12 4.34 0.60 o 1 -2 14 37.81 43.08 1.70 o 2 -2 14 21.69 21.60 1.24 o 3 -2 14 47.15 52.14 2.19 o -1 -1 14 60.07 59.87 1.66 o 0 -1 14 32.05 33.44 1.22 o 1 -1 14 10.28 12.20 1.01 o 2 -1 14 0.64 0.31 0.50 o 3 -1 14 0.01 1.22 0.60 o 4 -1 14 267.10 261.19 4.95 o -1 0 14 3.28 4.12 1.37 o 0 0 14 4.02 5.61 0.79 o 1 0 14 102.85 103.68 2.66 o 2 0 14 0.36 -0.33 0.66 o 3 0 14 0.04 1.31 0.87 o 4 0 14 34.34 46.36 2.62 o 5 0 14 18.17 26.79 2.19 o -1 1 14 35.71 43.17 1.60 o 0 1 14 9.85 10.22 0.92 o 1 1 14 8.82 13.45 1.53 o 2 1 14 11.04 9.73 1.42 o 3 1 14 66.74 62.65 2.95 o 4 1 14 1.35 0.40 0.55 o 5 1 14 0.00 0.77 0.58 o 6 1 14 2.14 4.16 0.85 o 0 2 14 64.82 72.28 3.28 o 1 2 14 143.39 164.47 5.52 o 2 2 14 0.89 1.22 0.71 o 3 2 14 6.97 8.44 0.93 o 4 2 14 11.85 11.76 1.42 o 5 2 14 1.15 1.60 0.66 o 6 2 14 6.59 8.86 1.01 o 0 3 14 3.74 5.84 2.46 o 1 3 14 188.08 194.65 4.17 o 2 3 14 43.10 44.98 2.02 o 3 3 14 24.95 22.19 1.35 o 4 3 14 0.20 0.40 0.58 o 5 3 14 2.52 4.17 1.26 o 6 3 14 4.56 4.72 0.89 o 1 4 14 24.70 26.51 1.80 o 2 4 14 13.69 13.12 1.12 o 3 4 14 1.05 0.71 0.87 o 4 4 14 51.25 51.37 1.97 o 5 4 14 16.40 15.81 1.23 o 3 5 14 1.04 0.87 1.09 o 4 5 14 0.84 0.55 0.54 o 1 -1 15 5.18 5.02 0.81 o 2 -1 15 4.15 4.87 0.81 o 3 -1 15 0.01 -0.22 0.54 o 1 0 15 23.74 23.39 2.35 o 2 0 15 9.03 10.49 1.00 o 3 0 15 10.57 11.59 1.53 o 4 0 15 160.61 185.88 5.90 o 1 1 15 34.03 41.24 1.70 o 2 1 15 7.60 7.98 1.42 o 3 1 15 25.10 25.37 2.08 o 4 1 15 45.64 49.53 2.84 o 1 2 15 20.89 25.59 2.19 o 2 2 15 25.15 28.54 2.19 o 3 2 15 17.04 17.38 1.20 o 4 2 15 2.50 2.07 0.73 o 2 3 15 0.35 -0.03 0.65 o 3 3 15 30.57 32.26 2.35 o 4 3 15 2.59 2.99 0.82 o