#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/51/2225120.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225120_Fobs loop_ _publ_author_name 'bin Shawkataly, Omar' 'Khan, Imthyaz Ahmed' 'Yeap, Chin Sing' 'Fun, Hoong-Kun' _publ_section_title ; Bis{[\m-bis(diphenylarsino)methane-1:2\k^2^As:As']nonacarbonyl-1\k^3^C,2\k^3^C,3\k^3^C-[tris(4-methoxyphenyl)arsine-3\kAs]-triangulo-triruthenium(0)} dichloromethane solvate ; _journal_coeditor_code TK2594 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m180 _journal_page_last m181 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 95.997 _cell_angle_beta 101.259 _cell_angle_gamma 103.451 _cell_length_a 10.7669 _cell_length_b 12.8159 _cell_length_c 20.7167 _exptl_crystal_F_000 1442.00 _reflns_d_resolution_high 0.6614 _[local]_cod_data_source_file tk2594Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' iak25m in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 365.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1512.18 1274.43 33.43 o 2 0 0 4039.32 4664.21 101.98 o 3 0 0 267.03 326.88 15.59 o 4 0 0 36.03 44.16 9.02 o 5 0 0 13240.16 13046.82 118.87 o 6 0 0 9073.96 9476.03 90.96 o 7 0 0 635.64 703.86 22.45 o 8 0 0 550.97 532.46 22.53 o 9 0 0 5.89 8.21 8.81 o 10 0 0 551.89 568.30 23.88 o 11 0 0 1646.49 1606.78 39.49 o 12 0 0 943.58 916.70 33.05 o 13 0 0 8798.07 8732.52 182.59 o 14 0 0 865.36 823.84 39.05 o 15 0 0 0.45 61.35 39.04 o 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o -10 3 0 2982.16 3009.58 60.09 o -9 3 0 680.01 690.42 30.64 o -8 3 0 5753.45 5836.35 68.08 o -7 3 0 2681.63 2942.24 47.30 o -6 3 0 15937.64 16771.75 190.66 o -5 3 0 468.00 432.01 12.31 o -4 3 0 3686.62 3606.99 55.62 o -3 3 0 71.29 111.98 7.14 o -2 3 0 4527.26 4696.96 54.68 o -1 3 0 15552.72 16782.79 152.69 o 0 3 0 1662.67 1964.95 21.25 o 1 3 0 19081.81 21245.96 177.98 o 2 3 0 15693.97 16284.63 119.32 o 3 3 0 11745.14 12011.83 114.86 o 4 3 0 50.04 84.12 12.49 o 5 3 0 24387.16 24669.10 193.66 o 6 3 0 468.86 466.60 15.38 o 7 3 0 16002.65 15896.48 202.09 o 8 3 0 1655.53 1636.68 40.88 o 9 3 0 1141.38 1004.64 39.61 o 10 3 0 4759.78 4682.78 86.34 o 11 3 0 167.50 140.80 26.06 o 12 3 0 3838.15 3900.83 106.58 o 13 3 0 660.40 707.73 50.17 o 14 3 0 446.94 493.52 74.43 o -15 4 0 5220.18 5456.27 95.34 o -14 4 0 45.49 40.24 25.94 o -13 4 0 31.18 5.67 17.71 o -12 4 0 279.30 300.02 23.28 o -11 4 0 4231.81 4258.52 71.45 o -10 4 0 2548.78 2674.23 49.81 o -9 4 0 2080.36 2149.37 34.61 o -8 4 0 1263.55 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9902.45 9842.90 84.41 o -4 5 0 15515.93 15817.22 139.03 o -3 5 0 1752.52 2063.32 20.63 o -2 5 0 1260.83 1311.63 16.33 o -1 5 0 9918.40 10052.01 78.66 o 0 5 0 2151.63 2315.63 21.60 o 1 5 0 60800.30 61449.31 429.74 o 2 5 0 2477.30 2082.39 23.79 o 3 5 0 37.84 54.61 8.93 o 4 5 0 298.35 238.74 11.74 o 5 5 0 407.62 441.69 21.72 o 6 5 0 20856.50 20156.02 191.68 o 7 5 0 2040.44 2094.59 47.64 o 8 5 0 4803.62 4535.70 78.74 o 9 5 0 864.68 841.28 38.73 o 10 5 0 162.84 188.86 23.97 o 11 5 0 175.47 175.70 28.64 o 12 5 0 996.65 990.68 59.56 o 13 5 0 1118.17 1240.30 123.77 o -15 6 0 94.64 39.30 18.34 o -14 6 0 670.05 734.29 70.55 o -13 6 0 46.77 81.23 21.25 o -12 6 0 1019.90 1055.90 46.33 o -11 6 0 264.80 275.60 18.54 o -10 6 0 12708.49 13118.13 150.67 o -9 6 0 66.00 81.47 18.93 o -8 6 0 3520.55 3628.26 53.21 o -7 6 0 13304.61 12922.10 109.15 o -6 6 0 1690.15 1651.90 22.00 o -5 6 0 23205.67 23365.66 234.99 o -4 6 0 31210.51 31834.73 221.80 o -3 6 0 18439.34 17909.10 137.66 o -2 6 0 9164.40 9350.39 66.78 o -1 6 0 4064.17 4521.24 40.57 o 0 6 0 1104.60 1315.05 16.96 o 1 6 0 27945.70 28161.02 203.59 o 2 6 0 84.92 112.47 6.56 o 3 6 0 6369.45 6143.59 53.39 o 4 6 0 1187.34 1213.64 25.49 o 5 6 0 1032.30 1132.93 25.94 o 6 6 0 4474.32 4186.54 72.01 o 7 6 0 4652.68 4751.76 64.21 o 8 6 0 8242.01 7910.99 118.32 o 9 6 0 82.45 53.76 19.29 o 10 6 0 11551.72 11111.77 159.31 o 11 6 0 46.99 53.75 25.73 o 12 6 0 14.72 62.11 49.74 o 13 6 0 175.76 217.32 42.79 o -15 7 0 26.16 13.51 27.13 o -14 7 0 5699.70 6047.49 246.79 o -13 7 0 4819.12 5074.18 100.96 o -12 7 0 72.44 64.79 20.11 o -11 7 0 2.30 7.89 16.39 o -10 7 0 1474.33 1556.79 36.03 o -9 7 0 379.13 333.88 27.63 o -8 7 0 16793.92 16893.23 205.98 o -7 7 0 2588.29 2597.22 39.68 o -6 7 0 502.74 509.52 17.31 o -5 7 0 3521.98 3706.30 39.84 o -4 7 0 24894.35 24990.70 198.66 o -3 7 0 9556.85 9504.14 83.34 o -2 7 0 4824.74 4691.56 37.86 o -1 7 0 10319.59 10406.42 72.17 o 0 7 0 6881.02 6803.37 52.92 o 1 7 0 945.86 911.66 20.26 o 2 7 0 114.36 144.88 9.58 o 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