#------------------------------------------------------------------------------ #$Date: 2010-04-11 15:29:29 +0300 (Sun, 11 Apr 2010) $ #$Revision: 1088 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2225201.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225201_Fobs loop_ _publ_author_name 'Saeed, Musabbir A.' 'Fronczek, Frank R.' 'Hossain, Md. Alamgir' _publ_section_title ; 3,3'-Di-tert-butyl-1,1'-[1,3-phenylenebis(methylene)]diurea ; _journal_coeditor_code CI5033 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o656 _journal_page_last o657 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.0700 _cell_length_b 11.7600 _cell_length_c 18.2210 _exptl_crystal_F_000 1456.00 _reflns_d_resolution_high 0.8116 _[local]_cod_data_source_file ci5033Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ORNL1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 335.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 4796.87 3838.51 62.75 o 6 0 0 904.49 1316.94 41.17 o 8 0 0 8581.12 9040.73 168.26 o 10 0 0 2913.74 3215.81 78.74 o 12 0 0 1958.13 1964.02 72.74 o 14 0 0 401.95 352.52 59.55 o 16 0 0 592.97 812.95 79.14 o 18 0 0 835.12 642.68 86.73 o 20 0 0 138.66 -11.99 192.65 o 22 0 0 56.05 67.55 127.90 o 2 1 0 42255.01 39056.19 474.82 o 4 1 0 512.30 364.51 16.79 o 6 1 0 18657.22 18855.24 208.23 o 8 1 0 1016.48 770.18 27.98 o 10 1 0 296.48 331.33 23.18 o 12 1 0 247.43 195.04 28.38 o 14 1 0 2649.37 3173.05 78.34 o 16 1 0 357.28 495.20 59.15 o 18 1 0 141.71 215.03 55.56 o 20 1 0 16.30 135.49 67.55 o 22 1 0 32.70 55.56 71.54 o 0 2 0 17957.64 20831.65 328.54 o 2 2 0 14055.39 10736.57 131.09 o 4 2 0 89584.69 80755.06 862.51 o 6 2 0 452.67 944.04 27.18 o 8 2 0 16.47 43.96 24.38 o 10 2 0 0.03 39.97 23.98 o 12 2 0 162.61 103.52 32.37 o 14 2 0 90.85 107.51 48.36 o 16 2 0 1356.99 1642.28 87.13 o 18 2 0 217.51 139.89 64.35 o 20 2 0 0.03 -31.57 63.15 o 22 2 0 21.58 -31.57 71.94 o 2 3 0 8421.32 10040.73 126.70 o 4 3 0 99.40 115.51 24.38 o 6 3 0 21901.04 19893.60 249.80 o 8 3 0 1768.42 1521.58 39.57 o 10 3 0 2.56 23.58 23.98 o 12 3 0 8.86 71.94 36.37 o 14 3 0 640.16 798.56 71.54 o 16 3 0 1137.26 1249.00 93.92 o 18 3 0 939.06 1019.18 96.72 o 20 3 0 14.58 7.99 68.35 o 0 4 0 13347.25 16437.98 275.78 o 2 4 0 525.16 652.28 29.18 o 4 4 0 8415.93 7878.46 112.31 o 6 4 0 14747.58 15073.48 186.25 o 8 4 0 3156.28 2826.93 67.15 o 10 4 0 63.73 7.99 27.98 o 12 4 0 237.18 195.04 47.56 o 14 4 0 5886.91 6446.42 182.65 o 16 4 0 1.26 28.38 56.35 o 18 4 0 20.47 -28.38 72.34 o 20 4 0 176.22 251.80 100.32 o 2 5 0 6.53 7.99 23.98 o 4 5 0 333.65 304.56 28.78 o 6 5 0 1353.95 1581.13 40.37 o 8 5 0 1260.21 1127.09 38.37 o 10 5 0 691.18 607.91 53.16 o 12 5 0 336.88 359.71 59.95 o 14 5 0 1045.83 1068.34 78.34 o 16 5 0 27.87 71.94 71.94 o 18 5 0 6.89 0.00 39.97 o 20 5 0 513.59 718.62 91.53 o 0 6 0 1474.97 1367.70 51.56 o 2 6 0 1131.54 875.30 33.57 o 4 6 0 2514.08 2194.64 53.16 o 6 6 0 213.86 204.24 27.18 o 8 6 0 2917.66 2615.90 64.75 o 10 6 0 863.64 698.24 46.76 o 12 6 0 620.80 586.33 64.35 o 14 6 0 3595.67 4567.53 145.08 o 16 6 0 62.29 28.38 56.35 o 18 6 0 190.35 215.03 63.15 o 20 6 0 79.02 19.98 71.94 o 2 7 0 165.07 200.64 32.37 o 4 7 0 385.72 326.94 31.97 o 6 7 0 219.33 211.43 36.77 o 8 7 0 1623.27 1496.80 73.54 o 10 7 0 136.53 243.80 51.16 o 12 7 0 7.66 51.96 63.95 o 14 7 0 84.13 79.54 67.55 o 16 7 0 5.10 48.36 59.95 o 18 7 0 34.78 220.62 67.55 o 0 8 0 0.14 0.00 39.97 o 2 8 0 81.64 39.97 35.97 o 4 8 0 384.64 440.45 39.97 o 6 8 0 968.01 721.82 54.36 o 8 8 0 272.34 191.85 55.96 o 10 8 0 844.27 805.75 68.35 o 12 8 0 463.34 424.86 65.15 o 14 8 0 4.92 19.98 60.35 o 16 8 0 148.57 215.03 68.74 o 18 8 0 11.77 -11.99 68.35 o 2 9 0 210.20 179.46 47.56 o 4 9 0 939.66 1076.73 57.95 o 6 9 0 1113.36 1084.73 70.74 o 8 9 0 4283.26 3877.68 125.90 o 10 9 0 77.43 99.92 55.56 o 12 9 0 0.02 35.97 71.94 o 14 9 0 1.01 -35.97 63.95 o 16 9 0 406.04 506.39 76.74 o 0 10 0 3164.04 3087.92 140.69 o 2 10 0 18.07 59.55 47.96 o 4 10 0 7.96 35.97 47.96 o 6 10 0 2793.37 2740.20 112.71 o 8 10 0 1985.33 2083.52 97.92 o 10 10 0 781.85 780.97 91.93 o 12 10 0 268.63 286.97 64.35 o 14 10 0 72.42 87.53 72.34 o 16 10 0 246.78 232.21 71.14 o 2 11 0 2658.82 3087.92 105.52 o 4 11 0 879.93 875.30 71.14 o 6 11 0 34.46 28.38 48.36 o 8 11 0 0.38 31.57 63.15 o 10 11 0 0.98 -7.99 64.35 o 12 11 0 57.49 51.96 63.95 o 14 11 0 30.52 39.97 67.95 o 0 12 0 842.24 916.86 114.71 o 2 12 0 1148.89 1405.27 89.93 o 4 12 0 173.16 251.80 64.35 o 6 12 0 53.99 132.29 56.75 o 8 12 0 4.57 87.53 63.95 o 10 12 0 91.82 235.81 87.53 o 12 12 0 96.45 55.56 63.95 o 2 13 0 952.92 924.86 73.14 o 4 13 0 2.47 0.00 39.97 o 6 13 0 0.09 -67.55 67.55 o 8 13 0 1.94 43.96 63.95 o 0 14 0 621.11 852.91 147.88 o 2 14 0 171.22 95.92 59.55 o 4 14 0 0.20 95.92 64.35 o 2 1 1 10021.00 8299.28 73.20 o 3 1 1 2182.26 1831.92 26.98 o 4 1 1 12653.69 10858.81 98.72 o 5 1 1 1543.23 1837.39 27.18 o 6 1 1 425.18 585.46 16.10 o 7 1 1 617.17 604.88 17.66 o 8 1 1 473.31 496.18 16.89 o 9 1 1 2879.15 3053.26 34.77 o 10 1 1 900.21 866.11 23.74 o 11 1 1 0.00 7.99 17.24 o 12 1 1 191.67 216.89 22.89 o 13 1 1 402.22 515.15 26.98 o 14 1 1 23.17 53.22 43.76 o 15 1 1 8.06 -26.19 45.96 o 16 1 1 23.18 7.85 35.68 o 17 1 1 94.85 45.19 38.10 o 18 1 1 2.54 11.31 33.32 o 19 1 1 12.02 37.77 39.28 o 20 1 1 21.99 79.04 49.09 o 21 1 1 30.87 -1.94 50.16 o 22 1 1 3.00 45.61 77.54 o 0 2 1 4653.65 6314.92 80.34 o 1 2 1 11508.37 12649.43 100.61 o 2 2 1 37268.36 35018.24 267.64 o 3 2 1 929.57 854.71 16.84 o 4 2 1 8580.06 6959.40 63.10 o 5 2 1 598.71 831.08 19.17 o 6 2 1 1255.97 995.95 23.98 o 7 2 1 676.56 796.72 20.21 o 8 2 1 275.53 278.59 16.39 o 9 2 1 86.78 75.35 13.99 o 10 2 1 865.34 912.90 22.88 o 11 2 1 20.51 18.19 16.96 o 12 2 1 311.72 213.95 26.00 o 13 2 1 155.10 134.76 30.70 o 14 2 1 187.08 208.41 39.02 o 15 2 1 77.02 102.82 40.12 o 16 2 1 289.29 311.12 55.95 o 17 2 1 533.77 474.91 47.96 o 18 2 1 348.04 423.38 54.36 o 19 2 1 53.71 107.17 41.94 o 20 2 1 8.51 78.11 71.74 o 21 2 1 40.02 32.30 53.76 o 22 2 1 17.84 19.98 59.07 o 1 3 1 936.64 752.97 17.10 o 2 3 1 6754.72 5013.53 50.73 o 3 3 1 96.25 272.18 16.03 o 4 3 1 149.67 174.98 17.10 o 5 3 1 5328.24 5212.58 54.76 o 6 3 1 6.37 60.17 21.78 o 7 3 1 1623.04 1701.61 29.53 o 8 3 1 1168.58 1163.27 24.30 o 9 3 1 352.90 339.49 19.78 o 10 3 1 82.28 69.39 13.23 o 11 3 1 2.85 16.25 21.06 o 12 3 1 81.26 45.76 57.75 o 13 3 1 1242.72 1128.39 52.96 o 14 3 1 0.04 24.54 79.74 o 15 3 1 99.75 144.63 40.87 o 16 3 1 2404.92 2547.83 188.45 o 17 3 1 10.27 50.25 43.58 o 18 3 1 10.01 -9.47 33.19 o 19 3 1 264.29 243.14 70.74 o 20 3 1 61.04 -45.96 53.70 o 21 3 1 6.41 20.18 79.74 o 0 4 1 3903.76 2793.35 46.76 o 1 4 1 705.07 932.88 54.36 o 2 4 1 287.61 307.29 21.98 o 3 4 1 1193.44 983.17 22.47 o 4 4 1 6783.96 5406.01 59.06 o 5 4 1 1318.24 1458.99 38.77 o 6 4 1 368.10 351.26 54.76 o 7 4 1 1213.84 1253.91 53.76 o 8 4 1 1327.17 1003.52 26.78 o 9 4 1 508.97 651.47 40.37 o 10 4 1 37.58 17.39 41.57 o 11 4 1 216.84 208.88 27.84 o 12 4 1 29.56 7.23 28.38 o 13 4 1 11.53 17.15 75.74 o 14 4 1 378.28 345.50 43.17 o 15 4 1 0.33 13.19 41.06 o 16 4 1 27.09 -25.09 45.56 o 17 4 1 187.82 286.97 45.50 o 18 4 1 515.49 566.91 55.29 o 19 4 1 57.22 176.37 60.35 o 20 4 1 72.03 -20.50 50.16 o 21 4 1 11.33 75.60 53.56 o 1 5 1 896.86 705.29 19.07 o 2 5 1 884.85 475.86 17.52 o 3 5 1 536.31 786.36 30.18 o 4 5 1 65.95 198.26 16.96 o 5 5 1 72.45 93.07 41.97 o 6 5 1 78.76 28.38 23.98 o 7 5 1 85.49 40.51 31.97 o 8 5 1 418.96 306.64 62.15 o 9 5 1 481.92 460.76 43.17 o 10 5 1 1072.75 1144.78 37.79 o 11 5 1 1446.72 1357.11 92.93 o 12 5 1 1097.07 1219.96 59.34 o 13 5 1 92.92 185.54 48.36 o 14 5 1 408.09 401.02 101.72 o 15 5 1 360.42 420.86 47.44 o 16 5 1 127.41 201.67 45.78 o 17 5 1 806.44 657.17 53.70 o 18 5 1 48.97 1.00 49.24 o 19 5 1 150.47 202.36 51.79 o 20 5 1 50.84 115.83 56.05 o 0 6 1 242.45 526.78 31.97 o 1 6 1 12.02 51.76 16.96 o 2 6 1 120.06 93.59 15.42 o 3 6 1 1063.66 991.36 31.77 o 4 6 1 4.08 94.95 16.95 o 5 6 1 161.95 170.82 19.63 o 6 6 1 46.04 43.91 19.92 o 7 6 1 168.69 162.47 20.99 o 8 6 1 2226.13 2240.90 44.76 o 9 6 1 676.12 625.88 34.52 o 10 6 1 554.66 708.97 37.92 o 11 6 1 2465.40 2393.01 63.31 o 12 6 1 1993.41 2211.82 69.32 o 13 6 1 685.74 547.30 49.96 o 14 6 1 751.22 802.81 53.23 o 15 6 1 658.10 870.46 51.29 o 16 6 1 0.11 35.49 43.71 o 17 6 1 12.72 38.69 88.13 o 18 6 1 19.87 121.04 48.81 o 19 6 1 11.92 9.06 46.41 o 20 6 1 0.89 55.07 50.64 o 1 7 1 1353.21 1387.07 28.11 o 2 7 1 72.08 47.96 16.95 o 3 7 1 0.41 -19.64 19.64 o 4 7 1 218.25 274.70 20.49 o 5 7 1 661.66 734.49 66.55 o 6 7 1 147.03 177.85 25.01 o 7 7 1 864.29 751.65 57.35 o 8 7 1 88.10 121.41 31.37 o 9 7 1 269.63 263.79 34.68 o 10 7 1 2525.76 2372.90 65.28 o 11 7 1 863.09 939.45 50.57 o 12 7 1 5.77 2.00 37.02 o 13 7 1 28.17 119.39 39.28 o 14 7 1 61.02 123.61 85.73 o 15 7 1 3.36 63.66 46.16 o 16 7 1 0.09 21.78 61.95 o 17 7 1 27.48 21.79 42.39 o 18 7 1 1.20 2.44 55.76 o 19 7 1 35.97 -4.29 49.74 o 0 8 1 285.29 204.24 32.37 o 1 8 1 145.34 151.88 23.17 o 2 8 1 410.43 427.14 25.98 o 3 8 1 165.29 84.17 22.89 o 4 8 1 25.79 9.87 23.90 o 5 8 1 353.35 350.55 30.95 o 6 8 1 431.68 565.10 37.77 o 7 8 1 2.14 -30.91 30.91 o 8 8 1 675.03 676.88 144.68 o 9 8 1 946.46 955.99 47.02 o 10 8 1 332.79 337.54 42.66 o 11 8 1 661.82 621.85 90.73 o 12 8 1 548.22 641.05 45.21 o 13 8 1 100.09 142.20 43.19 o 14 8 1 4.25 32.21 49.76 o 15 8 1 135.07 144.08 49.40 o 16 8 1 101.74 156.67 46.26 o 17 8 1 24.92 114.20 92.13 o 18 8 1 21.62 28.07 45.35 o 1 9 1 691.72 663.91 32.20 o 2 9 1 889.87 909.11 87.93 o 3 9 1 2445.78 2446.32 65.75 o 4 9 1 135.83 236.98 56.75 o 5 9 1 260.64 220.94 42.28 o 6 9 1 604.06 608.54 46.13 o 7 9 1 289.58 290.67 43.89 o 8 9 1 131.03 167.16 84.33 o 9 9 1 857.93 968.14 48.60 o 10 9 1 193.39 246.39 42.77 o 11 9 1 157.60 152.70 45.01 o 12 9 1 1.76 35.16 43.76 o 13 9 1 41.20 -41.83 42.11 o 14 9 1 421.88 541.12 51.85 o 15 9 1 88.72 199.62 52.40 o 16 9 1 11.75 92.64 48.96 o 17 9 1 553.55 641.84 82.33 o 0 10 1 22.71 195.04 47.56 o 1 10 1 31.85 61.80 89.33 o 2 10 1 377.24 331.96 35.81 o 3 10 1 82.43 62.69 32.65 o 4 10 1 596.31 528.35 38.00 o 5 10 1 295.36 333.20 37.30 o 6 10 1 712.15 635.89 73.94 o 7 10 1 546.22 590.32 46.63 o 8 10 1 8.89 12.25 37.16 o 9 10 1 136.57 90.88 45.87 o 10 10 1 47.91 12.60 42.28 o 11 10 1 0.75 1.59 33.39 o 12 10 1 18.91 -24.02 42.53 o 13 10 1 16.57 39.92 47.76 o 14 10 1 9.97 -27.95 48.19 o 15 10 1 198.07 224.25 49.81 o 16 10 1 54.76 52.37 57.75 o 1 11 1 183.86 202.52 44.36 o 2 11 1 92.11 32.08 49.96 o 3 11 1 254.69 256.43 36.60 o 4 11 1 524.19 558.91 43.24 o 5 11 1 16.23 75.74 39.85 o 6 11 1 85.07 138.10 40.59 o 7 11 1 1304.77 1359.34 54.24 o 8 11 1 10.52 33.03 47.84 o 9 11 1 10.05 42.61 53.96 o 10 11 1 63.37 22.42 47.46 o 11 11 1 0.43 14.73 49.40 o 12 11 1 6.02 30.19 61.95 o 13 11 1 222.13 165.50 48.32 o 14 11 1 6.27 51.58 52.38 o 0 12 1 95.12 35.97 52.36 o 1 12 1 405.68 548.39 44.93 o 2 12 1 229.05 267.68 49.36 o 3 12 1 111.35 66.47 37.82 o 4 12 1 0.00 38.22 41.77 o 5 12 1 5.67 26.08 42.53 o 6 12 1 29.00 20.18 42.67 o 7 12 1 76.94 121.78 42.82 o 8 12 1 4.55 81.45 45.36 o 9 12 1 82.47 128.20 46.24 o 10 12 1 94.37 115.51 52.23 o 11 12 1 33.37 59.46 90.13 o 12 12 1 3.21 29.78 50.87 o 1 13 1 30.15 71.98 75.74 o 2 13 1 12.91 8.50 38.04 o 3 13 1 194.35 239.75 43.45 o 4 13 1 3.39 14.08 39.71 o 5 13 1 0.01 40.94 46.85 o 6 13 1 60.78 19.98 39.85 o 7 13 1 27.86 -15.03 41.19 o 8 13 1 218.57 260.48 47.80 o 9 13 1 22.57 -11.75 42.16 o 0 14 1 180.74 243.80 67.15 o 1 14 1 48.47 63.55 46.28 o 2 14 1 190.77 233.48 50.35 o 3 14 1 31.82 51.64 42.53 o 4 14 1 0.54 -13.44 43.61 o 5 14 1 15.48 25.89 46.54 o 2 0 2 14423.54 12479.17 113.11 o 3 0 2 42138.66 38881.54 348.92 o 4 0 2 1294.03 1182.65 25.98 o 5 0 2 5244.42 4414.85 58.75 o 6 0 2 6162.96 5230.59 63.95 o 7 0 2 3719.80 3660.26 53.56 o 8 0 2 20.74 11.99 20.38 o 9 0 2 261.82 239.81 19.58 o 10 0 2 2660.02 2248.19 41.97 o 11 0 2 274.54 204.24 19.98 o 12 0 2 15.50 11.99 27.98 o 13 0 2 0.32 -35.97 35.97 o 14 0 2 2710.62 2746.59 86.33 o 15 0 2 741.83 823.74 54.36 o 16 0 2 141.49 -7.99 48.36 o 17 0 2 91.71 83.93 47.56 o 18 0 2 234.97 220.62 52.76 o 19 0 2 204.97 276.58 61.15 o 20 0 2 79.25 75.94 63.95 o 21 0 2 9.87 -7.99 76.34 o 22 0 2 24.81 -83.93 87.93 o 1 1 2 3598.90 3485.20 44.76 o 2 1 2 191.74 152.74 7.79 o 3 1 2 4713.02 4507.72 41.97 o 4 1 2 1459.64 1301.15 16.11 o 5 1 2 793.34 1040.28 52.96 o 6 1 2 26.17 44.45 13.59 o 7 1 2 3.86 -12.48 12.48 o 8 1 2 8661.68 7633.46 70.37 o 9 1 2 2422.74 2761.75 35.11 o 10 1 2 0.24 2.14 14.27 o 11 1 2 512.60 499.65 20.06 o 12 1 2 3351.45 3063.98 66.55 o 13 1 2 526.20 522.77 29.19 o 14 1 2 237.31 104.46 32.31 o 15 1 2 2.84 -30.60 30.60 o 16 1 2 45.87 123.07 54.36 o 17 1 2 25.44 36.78 38.23 o 18 1 2 217.00 143.68 42.39 o 19 1 2 303.55 366.65 53.96 o 20 1 2 202.32 287.04 49.11 o 21 1 2 289.28 401.59 57.99 o 22 1 2 6.48 -94.20 115.71 o 0 2 2 752.24 512.39 11.59 o 1 2 2 3332.95 4078.17 48.56 o 2 2 2 134.31 59.54 9.59 o 3 2 2 3270.94 5053.97 50.87 o 4 2 2 2139.68 2541.91 31.51 o 5 2 2 555.47 799.45 21.38 o 6 2 2 3794.66 2974.87 36.36 o 7 2 2 3031.76 3095.23 35.17 o 8 2 2 1202.33 1093.60 29.18 o 9 2 2 687.09 539.50 30.78 o 10 2 2 4289.39 3945.07 50.45 o 11 2 2 164.02 185.25 20.06 o 12 2 2 263.41 145.73 26.49 o 13 2 2 192.83 140.34 66.15 o 14 2 2 942.82 904.22 44.22 o 15 2 2 91.80 55.56 31.48 o 16 2 2 15.46 30.79 43.96 o 17 2 2 11.45 25.52 33.19 o 18 2 2 370.13 397.10 45.34 o 19 2 2 440.72 456.13 48.18 o 20 2 2 152.50 95.62 42.25 o 21 2 2 0.07 -9.94 52.38 o 1 3 2 1836.53 1951.57 61.35 o 2 3 2 1693.84 1759.64 29.18 o 3 3 2 37.49 165.43 13.84 o 4 3 2 1527.33 1145.21 22.48 o 5 3 2 942.05 662.35 22.78 o 6 3 2 468.99 467.48 19.18 o 7 3 2 820.68 803.55 26.78 o 8 3 2 5217.69 4866.88 56.10 o 9 3 2 220.10 317.67 17.52 o 10 3 2 96.41 61.17 16.12 o 11 3 2 360.43 400.15 21.34 o 12 3 2 251.76 191.94 29.64 o 13 3 2 66.82 -2.56 30.99 o 14 3 2 20.27 17.14 89.73 o 15 3 2 765.03 833.58 47.74 o 16 3 2 600.16 630.26 153.88 o 17 3 2 286.86 272.01 97.92 o 18 3 2 181.98 211.14 50.03 o 19 3 2 0.15 -13.89 45.08 o 20 3 2 25.87 -17.38 47.56 o 21 3 2 24.53 58.09 50.03 o 0 4 2 4.21 103.52 20.78 o 1 4 2 516.19 759.81 17.24 o 2 4 2 1463.78 1367.87 24.52 o 3 4 2 1843.82 1670.82 54.16 o 4 4 2 1153.29 1228.14 26.58 o 5 4 2 441.78 520.97 20.49 o 6 4 2 731.49 664.11 30.98 o 7 4 2 107.79 131.32 23.78 o 8 4 2 268.79 223.71 20.06 o 9 4 2 1842.14 1925.11 35.33 o 10 4 2 321.26 226.43 25.58 o 11 4 2 130.86 52.46 35.97 o 12 4 2 338.96 223.81 36.74 o 13 4 2 648.78 850.21 34.50 o 14 4 2 1604.42 1549.47 67.55 o 15 4 2 391.05 258.79 43.78 o 16 4 2 571.35 533.42 80.14 o 17 4 2 174.46 111.51 44.95 o 18 4 2 16.73 -30.50 37.97 o 19 4 2 46.23 89.33 65.75 o 20 4 2 14.30 64.64 51.84 o 21 4 2 46.31 17.75 55.96 o 1 5 2 738.03 721.88 19.22 o 2 5 2 116.94 167.87 15.36 o 3 5 2 2366.03 2275.13 34.05 o 4 5 2 2409.04 2481.86 35.61 o 5 5 2 6513.11 7144.43 75.60 o 6 5 2 937.16 733.85 21.76 o 7 5 2 0.06 7.40 23.78 o 8 5 2 287.95 249.13 33.97 o 9 5 2 49.20 94.64 25.98 o 10 5 2 306.09 398.42 30.38 o 11 5 2 352.59 305.77 55.95 o 12 5 2 39.40 65.57 32.15 o 13 5 2 4405.74 4713.81 100.07 o 14 5 2 917.00 798.70 50.30 o 15 5 2 106.63 40.78 71.54 o 16 5 2 255.61 218.87 41.97 o 17 5 2 1004.50 1120.49 62.88 o 18 5 2 132.49 153.83 50.40 o 19 5 2 42.49 115.02 51.96 o 20 5 2 18.35 32.59 55.03 o 0 6 2 2033.26 1880.89 43.96 o 1 6 2 1.88 45.64 15.59 o 2 6 2 122.27 139.54 16.81 o 3 6 2 13.51 41.72 17.99 o 4 6 2 927.78 928.67 24.59 o 5 6 2 0.25 -2.25 19.78 o 6 6 2 6.23 18.17 25.98 o 7 6 2 38.41 35.57 27.78 o 8 6 2 319.08 361.49 84.13 o 9 6 2 77.46 41.09 27.74 o 10 6 2 632.41 609.40 39.44 o 11 6 2 0.63 -48.16 48.16 o 12 6 2 837.75 800.36 45.50 o 13 6 2 791.74 749.79 46.30 o 14 6 2 0.13 6.96 38.36 o 15 6 2 11.45 -1.15 38.10 o 16 6 2 0.96 8.03 42.82 o 17 6 2 37.77 45.33 91.93 o 18 6 2 0.01 92.15 52.23 o 19 6 2 7.72 47.71 121.30 o 20 6 2 50.02 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42.97 o 4 9 9 319.93 339.35 32.03 o 5 9 9 211.99 169.38 28.11 o 6 9 9 344.61 325.02 39.97 o 7 9 9 3.88 41.61 30.99 o 8 9 9 294.20 335.86 47.56 o 9 9 9 0.24 3.07 40.12 o 10 9 9 151.35 180.56 66.15 o 11 9 9 194.72 193.83 46.14 o 12 9 9 21.84 32.49 88.13 o 13 9 9 84.16 107.74 61.95 o 14 9 9 7.78 117.62 50.64 o 0 10 9 8.76 -23.58 43.56 o 1 10 9 112.82 144.11 55.56 o 2 10 9 28.46 6.70 32.17 o 3 10 9 3.59 -3.98 28.40 o 4 10 9 22.73 73.74 30.81 o 5 10 9 3.59 -29.53 29.53 o 6 10 9 0.01 19.30 45.56 o 7 10 9 88.20 111.01 64.15 o 8 10 9 80.81 61.45 55.96 o 9 10 9 8.78 29.29 39.33 o 10 10 9 74.14 160.87 129.90 o 11 10 9 96.61 72.98 45.62 o 12 10 9 47.34 133.37 63.98 o 13 10 9 0.37 71.75 66.77 o 1 11 9 45.59 78.01 42.81 o 2 11 9 0.00 25.82 34.47 o 3 11 9 538.00 430.26 44.55 o 4 11 9 45.69 19.31 41.97 o 5 11 9 123.62 130.06 38.57 o 6 11 9 27.95 43.71 43.74 o 7 11 9 118.18 100.55 53.47 o 8 11 9 27.54 31.82 54.51 o 9 11 9 143.15 176.07 56.65 o 10 11 9 43.96 93.09 60.38 o 11 11 9 24.03 32.20 56.66 o 0 12 9 1.68 55.56 59.55 o 1 12 9 32.34 -47.96 47.96 o 2 12 9 62.34 24.30 77.74 o 3 12 9 72.01 13.74 44.17 o 4 12 9 99.73 4.70 47.06 o 5 12 9 6.54 -22.79 43.11 o 6 12 9 15.22 108.06 46.66 o 7 12 9 104.02 135.25 55.49 o 8 12 9 53.86 81.93 77.94 o 1 13 9 60.14 83.64 48.04 o 2 13 9 8.26 30.51 110.11 o 3 13 9 87.64 127.01 46.59 o 1 0 10 1335.09 1506.79 19.58 o 2 0 10 3932.35 4696.62 60.75 o 3 0 10 1454.55 1652.27 25.58 o 4 0 10 324.72 411.67 12.79 o 5 0 10 46.28 48.36 12.39 o 6 0 10 4.01 0.00 39.97 o 7 0 10 1.75 23.58 15.99 o 8 0 10 65.36 59.55 15.59 o 9 0 10 100.78 79.54 20.38 o 10 0 10 621.43 535.57 29.18 o 11 0 10 3315.55 3404.86 73.94 o 12 0 10 0.74 -23.58 27.58 o 13 0 10 484.65 456.43 40.37 o 14 0 10 255.83 263.79 43.17 o 15 0 10 77.00 19.98 44.36 o 16 0 10 2.81 4.00 48.76 o 17 0 10 26.91 48.36 59.95 o 18 0 10 62.26 -31.57 63.15 o 19 0 10 348.56 506.39 99.52 o 1 1 10 0.09 -2.40 11.99 o 2 1 10 254.48 287.50 10.17 o 3 1 10 933.05 884.97 17.07 o 4 1 10 8196.45 8308.66 77.04 o 5 1 10 292.78 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