#------------------------------------------------------------------------------ #$Date: 2010-04-11 15:29:29 +0300 (Sun, 11 Apr 2010) $ #$Revision: 1088 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2225210.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225210_Fobs loop_ _publ_author_name 'Znovjyak, Kateryna O.' 'Ovchynnikov, Vladimir A.' 'Sliva, Tetyana Yu.' 'Shishkina, Svitlana V.' 'Amirkhanov, Vladimir M.' _publ_section_title ; Bis(N-{bis[methyl(phenyl)amino]phosphoryl}-2,2,2-trichloroacetamide)dinitratodioxidouranium(VI) ; _journal_coeditor_code CV2695 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m306 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.421 _cell_angle_gamma 90.000 _cell_length_a 10.2180 _cell_length_b 16.2228 _cell_length_c 28.4327 _exptl_crystal_F_000 2408.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file cv2695Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kiev10 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 466.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2051.05 2052.26 80.99 o 4 0 0 5578.29 5030.93 132.35 o 6 0 0 31.02 139.40 105.11 o 10 0 0 719.65 534.59 105.56 o 12 0 0 4242.42 4629.35 257.24 o 2 1 0 48639.44 48924.00 436.02 o 3 1 0 6489.48 5771.63 99.63 o 4 1 0 829.32 717.49 83.59 o 5 1 0 5890.33 4616.49 123.61 o 6 1 0 30566.20 28073.82 283.76 o 7 1 0 23444.19 23689.72 574.27 o 8 1 0 111.80 236.09 134.41 o 9 1 0 709.38 778.73 99.33 o 10 1 0 2362.36 2453.95 148.86 o 11 1 0 1733.12 1382.46 120.62 o 12 1 0 174.19 165.71 86.20 o 13 1 0 590.35 496.38 120.64 o 1 2 0 18015.68 22699.61 994.29 o 2 2 0 18444.88 18635.19 115.26 o 3 2 0 22233.27 20733.93 365.51 o 4 2 0 317.21 443.93 70.01 o 5 2 0 54621.43 47907.65 291.87 o 6 2 0 312.08 293.87 107.53 o 7 2 0 13701.56 13049.78 540.37 o 8 2 0 3.72 62.15 56.96 o 9 2 0 6963.06 7029.61 200.35 o 10 2 0 44.55 45.38 53.58 o 11 2 0 1453.52 1506.46 130.95 o 12 2 0 9.58 158.52 82.16 o 13 2 0 3357.37 3715.08 192.69 o 1 3 0 39744.07 44736.82 457.09 o 2 3 0 48591.50 42789.71 2977.41 o 3 3 0 13815.34 14122.23 253.22 o 4 3 0 2075.70 2191.21 89.44 o 5 3 0 16724.54 14180.02 396.21 o 6 3 0 18686.36 17440.86 605.46 o 7 3 0 9477.66 9553.80 208.34 o 8 3 0 10.97 46.81 44.33 o 9 3 0 938.66 628.51 94.85 o 10 3 0 2046.60 2243.05 164.05 o 11 3 0 1574.94 1385.46 152.26 o 12 3 0 605.19 523.02 118.31 o 13 3 0 159.57 177.32 96.57 o 1 4 0 13624.98 16421.38 131.07 o 2 4 0 2793.51 3244.94 81.88 o 3 4 0 18207.66 17592.45 1322.39 o 4 4 0 28834.79 30184.78 2598.85 o 5 4 0 2745.12 3003.65 109.11 o 6 4 0 19.43 189.50 80.98 o 7 4 0 273.04 296.39 103.05 o 8 4 0 18213.22 18169.17 262.10 o 9 4 0 31.68 94.11 72.13 o 10 4 0 596.23 471.52 126.04 o 11 4 0 22.41 137.60 94.15 o 12 4 0 3803.09 4103.07 185.68 o 1 5 0 1243.00 1476.93 49.95 o 2 5 0 23382.49 25111.98 197.17 o 3 5 0 14103.28 16463.50 1414.81 o 4 5 0 635.97 589.12 108.57 o 5 5 0 3471.41 3317.82 267.23 o 6 5 0 20242.88 19866.91 1365.56 o 7 5 0 10002.26 10409.35 457.40 o 8 5 0 5275.21 4801.13 210.18 o 9 5 0 2403.99 2671.53 167.95 o 10 5 0 1832.40 1971.83 198.43 o 11 5 0 1715.71 1769.43 361.24 o 12 5 0 7.53 221.55 130.47 o 0 6 0 422.24 546.26 94.97 o 1 6 0 94865.70 105492.52 1253.93 o 2 6 0 314.77 287.95 41.69 o 3 6 0 20872.10 20356.80 978.84 o 4 6 0 136.37 275.99 111.89 o 5 6 0 19361.68 18943.94 1276.73 o 6 6 0 203.25 360.90 146.80 o 7 6 0 5589.45 6245.29 236.46 o 8 6 0 1907.83 2103.31 215.27 o 9 6 0 10345.54 10364.06 280.74 o 10 6 0 54.73 66.54 68.95 o 11 6 0 1342.37 1398.54 331.78 o 12 6 0 3.99 151.70 132.39 o 1 7 0 4163.60 5390.38 72.31 o 2 7 0 76818.66 76512.56 641.90 o 3 7 0 23283.45 23672.94 207.04 o 4 7 0 2584.57 2921.53 159.96 o 5 7 0 17653.27 16668.57 705.19 o 6 7 0 9968.69 10113.92 1092.31 o 7 7 0 5417.28 5930.12 238.09 o 8 7 0 320.55 344.31 149.26 o 9 7 0 355.76 327.86 136.82 o 10 7 0 2413.59 2600.06 254.21 o 11 7 0 1195.28 1257.01 226.93 o 12 7 0 320.24 181.85 154.76 o 0 8 0 66373.39 69953.52 923.34 o 1 8 0 3818.06 4582.06 122.12 o 2 8 0 2782.33 2920.19 66.22 o 3 8 0 58.81 162.93 98.28 o 4 8 0 24140.89 25041.17 1160.54 o 5 8 0 7416.13 8612.89 715.78 o 6 8 0 92.38 253.33 131.23 o 7 8 0 2640.84 2570.08 378.86 o 8 8 0 13802.53 13975.26 704.34 o 9 8 0 6.94 199.19 160.70 o 10 8 0 533.92 432.66 151.86 o 11 8 0 13.91 142.00 129.70 o 12 8 0 1368.77 1806.85 238.48 o 1 9 0 11392.24 12872.65 100.77 o 2 9 0 16097.37 14776.57 270.44 o 3 9 0 16590.29 17993.89 173.81 o 4 9 0 1106.68 1052.34 161.92 o 5 9 0 2261.24 2065.69 352.55 o 6 9 0 6686.89 6389.48 219.29 o 7 9 0 3574.64 3632.13 352.93 o 8 9 0 1136.68 827.66 155.36 o 9 9 0 1476.46 1175.98 170.14 o 10 9 0 1667.62 1403.63 216.65 o 11 9 0 1409.84 1553.67 248.17 o 0 10 0 5220.02 5081.11 197.56 o 1 10 0 13678.80 15351.42 135.06 o 2 10 0 1604.78 1544.76 65.67 o 3 10 0 22274.60 22093.97 340.36 o 4 10 0 61.59 204.78 87.79 o 5 10 0 8309.11 8396.91 818.25 o 6 10 0 1352.18 1086.22 193.93 o 7 10 0 1834.08 2135.92 214.17 o 8 10 0 31.34 81.98 75.16 o 9 10 0 3793.77 4076.47 262.01 o 10 10 0 0.84 128.36 111.81 o 11 10 0 810.19 873.75 223.64 o 1 11 0 139.07 188.93 51.61 o 2 11 0 14730.41 15060.54 133.70 o 3 11 0 13262.32 15059.06 268.05 o 4 11 0 81.22 62.77 45.41 o 5 11 0 4106.27 3914.19 155.30 o 6 11 0 3220.80 3201.00 259.12 o 7 11 0 1290.08 1161.54 158.22 o 8 11 0 3.41 82.05 77.08 o 9 11 0 247.31 346.01 165.49 o 10 11 0 2407.97 2824.80 334.48 o 11 11 0 497.38 358.88 173.57 o 0 12 0 8385.17 9265.35 170.87 o 1 12 0 178.54 67.74 36.49 o 2 12 0 801.71 563.47 82.06 o 3 12 0 15.75 147.80 89.55 o 4 12 0 15829.17 16335.58 327.96 o 5 12 0 2269.29 2349.53 156.94 o 6 12 0 144.82 91.70 74.34 o 7 12 0 933.46 675.97 138.97 o 8 12 0 6001.45 6079.34 277.86 o 9 12 0 30.72 158.00 113.82 o 10 12 0 295.66 332.00 181.64 o 1 13 0 6071.19 6593.15 220.43 o 2 13 0 5914.74 6422.08 275.53 o 3 13 0 10710.15 10317.69 299.64 o 4 13 0 225.25 217.47 82.97 o 5 13 0 2217.18 2511.45 160.81 o 6 13 0 956.24 1050.38 148.67 o 7 13 0 1110.98 1026.50 148.13 o 8 13 0 710.28 466.66 151.21 o 9 13 0 1574.86 1416.54 201.30 o 10 13 0 924.40 928.72 204.09 o 0 14 0 3196.62 2954.26 195.25 o 1 14 0 2454.31 2846.61 134.23 o 2 14 0 36.79 131.37 74.22 o 3 14 0 7494.99 7500.28 195.07 o 4 14 0 86.58 213.12 91.60 o 5 14 0 5757.94 5749.10 169.02 o 6 14 0 10.43 43.93 55.79 o 7 14 0 884.30 990.39 151.79 o 8 14 0 183.00 170.22 91.47 o 9 14 0 2124.06 2348.46 252.84 o 1 15 0 640.25 437.90 103.09 o 2 15 0 6631.04 6864.48 192.28 o 3 15 0 2500.14 2717.37 261.14 o 4 15 0 359.27 560.42 116.49 o 5 15 0 645.18 513.13 116.74 o 6 15 0 1781.23 1749.32 157.88 o 7 15 0 232.64 331.04 113.99 o 8 15 0 112.21 127.13 81.10 o 9 15 0 58.93 100.71 96.53 o 0 16 0 3783.33 3533.98 288.04 o 1 16 0 47.71 51.33 71.36 o 2 16 0 1.98 103.16 107.38 o 3 16 0 336.13 380.67 95.72 o 4 16 0 5001.76 5075.56 236.89 o 5 16 0 358.85 387.57 93.03 o 6 16 0 28.81 43.54 63.06 o 7 16 0 14.19 84.22 82.46 o 8 16 0 2093.75 2457.25 212.53 o 1 17 0 1025.95 858.66 130.51 o 2 17 0 1025.10 1005.87 174.52 o 3 17 0 1431.92 1331.63 183.60 o 4 17 0 173.11 259.18 109.08 o 5 17 0 1687.74 1821.82 145.42 o 6 17 0 464.82 570.06 96.90 o 7 17 0 787.01 772.59 150.28 o 0 18 0 81.45 53.47 96.77 o 1 18 0 1058.20 985.40 143.78 o 2 18 0 557.37 359.68 154.41 o 3 18 0 1254.57 1278.88 184.53 o 4 18 0 171.31 216.62 126.34 o 5 18 0 1620.40 1460.57 176.54 o 6 18 0 32.72 76.10 54.15 o 1 19 0 554.36 367.14 129.05 o 2 19 0 1856.69 1755.65 207.78 o 3 19 0 356.42 420.08 161.90 o 4 19 0 0.49 120.73 99.97 o 5 19 0 9.33 66.15 80.11 o 0 20 0 643.31 498.36 205.98 o 1 20 0 513.95 388.89 133.40 o 2 20 0 79.04 103.89 107.44 o 3 20 0 136.49 233.80 193.09 o 4 20 0 2183.65 2528.58 254.67 o 1 21 0 119.26 123.79 103.42 o -13 0 1 558.39 398.01 139.92 o -11 0 1 2469.74 2356.10 199.98 o -9 0 1 2460.46 1920.61 192.72 o -5 0 1 704.17 405.19 134.73 o -3 0 1 22236.29 17861.73 170.42 o 3 0 1 1585.52 1544.27 100.69 o 7 0 1 11.70 77.60 117.67 o 9 0 1 17965.26 17711.35 431.69 o 11 0 1 304.43 229.47 117.66 o 13 0 1 2458.02 2696.93 277.81 o -13 1 1 1476.92 1741.94 169.35 o -12 1 1 185.06 163.79 81.89 o -11 1 1 94.33 60.80 52.95 o -10 1 1 954.01 766.75 147.01 o -9 1 1 4745.88 5159.72 229.53 o -8 1 1 1670.15 1544.70 140.97 o -7 1 1 2985.20 3689.10 237.30 o -6 1 1 19935.61 18906.14 190.96 o -5 1 1 3065.31 3106.82 88.91 o -4 1 1 12942.49 9225.18 107.57 o -3 1 1 640.62 454.77 60.89 o -2 1 1 45484.30 44271.41 600.28 o 2 1 1 48736.24 47345.20 512.94 o 3 1 1 4015.07 3677.52 115.25 o 4 1 1 2950.82 2591.08 84.35 o 5 1 1 382.34 265.76 83.04 o 6 1 1 9154.87 7973.77 168.85 o 7 1 1 22720.58 22710.49 309.45 o 8 1 1 5387.94 4967.34 164.16 o 9 1 1 51.71 102.72 82.10 o 10 1 1 1307.82 1226.29 109.96 o 11 1 1 2830.64 2869.32 155.13 o 12 1 1 1985.61 1938.62 150.71 o 13 1 1 12.76 121.50 79.29 o -13 2 1 0.21 119.68 89.61 o -12 2 1 3377.29 3780.56 196.77 o -11 2 1 3.34 75.66 78.95 o -10 2 1 905.32 847.50 104.64 o -9 2 1 75.80 78.62 55.85 o -8 2 1 16993.69 16810.40 256.69 o -7 2 1 46.64 170.35 100.50 o -6 2 1 8484.59 7674.66 168.80 o -5 2 1 3578.19 3157.63 109.45 o -4 2 1 35239.09 31457.61 237.85 o -3 2 1 73.17 103.01 59.31 o -2 2 1 25435.21 24856.03 191.39 o -1 2 1 2008.91 1855.84 150.04 o 1 2 1 2.33 164.95 39.71 o 2 2 1 89749.55 91859.98 5337.74 o 3 2 1 22152.04 20078.26 650.67 o 4 2 1 19314.13 16064.02 276.48 o 5 2 1 904.42 828.79 89.28 o 6 2 1 38249.25 36505.48 280.37 o 7 2 1 660.03 661.97 98.01 o 8 2 1 6241.02 6396.53 184.32 o 9 2 1 116.93 122.31 72.21 o 10 2 1 5600.61 4904.67 205.86 o 11 2 1 61.65 135.15 63.28 o 12 2 1 2536.49 2696.97 168.77 o 13 2 1 7.98 166.21 85.65 o -13 3 1 1882.17 1837.17 165.74 o -12 3 1 334.75 166.33 95.26 o -11 3 1 169.38 103.09 71.16 o -10 3 1 1051.87 878.55 132.85 o -9 3 1 3740.53 4039.96 178.74 o -8 3 1 782.28 912.96 108.77 o -7 3 1 1757.82 1532.44 129.72 o -6 3 1 9714.21 9425.94 171.80 o -5 3 1 3703.99 4278.66 181.44 o -4 3 1 14943.29 13243.40 477.85 o -3 3 1 100.31 420.72 60.95 o -2 3 1 25326.99 22867.27 501.23 o -1 3 1 123110.99 134523.70 1067.59 o 0 3 1 37591.22 51091.51 496.89 o 1 3 1 7288.44 8148.31 80.82 o 2 3 1 26496.26 25535.36 1556.76 o 3 3 1 14145.34 14860.16 1238.06 o 4 3 1 967.67 926.97 75.17 o 5 3 1 233.87 333.84 69.45 o 6 3 1 7048.97 6194.73 186.02 o 7 3 1 12016.18 12404.76 205.45 o 8 3 1 2631.32 2553.60 126.02 o 9 3 1 201.14 231.34 96.45 o 10 3 1 1580.44 1557.77 165.56 o 11 3 1 3302.49 3388.36 195.99 o 12 3 1 2009.70 2152.46 186.57 o -12 4 1 113.74 199.09 108.90 o -11 4 1 2734.76 2976.72 192.44 o -10 4 1 283.35 231.25 80.41 o -9 4 1 992.10 781.48 90.77 o -8 4 1 9.87 222.40 94.76 o -7 4 1 37514.16 43028.62 519.18 o -6 4 1 1244.04 1128.40 106.82 o -5 4 1 466.07 442.58 76.57 o -4 4 1 1256.54 825.62 104.67 o -3 4 1 27588.26 27944.63 2163.95 o -2 4 1 28040.49 28622.95 225.85 o -1 4 1 7753.82 9395.14 112.62 o 0 4 1 17847.77 21833.11 1241.37 o 1 4 1 144023.33 142791.59 6889.40 o 2 4 1 15612.72 15274.98 725.05 o 3 4 1 613.75 697.15 91.53 o 4 4 1 2011.21 2096.71 200.01 o 5 4 1 32732.86 32200.21 648.75 o 6 4 1 161.73 232.15 74.97 o 7 4 1 260.23 141.14 66.83 o 8 4 1 173.03 288.54 98.86 o 9 4 1 9618.73 10589.49 218.82 o 10 4 1 27.64 152.29 86.89 o 11 4 1 499.98 447.10 126.02 o 12 4 1 286.28 400.28 113.88 o -12 5 1 31.47 102.96 117.64 o -11 5 1 340.80 334.36 157.74 o -10 5 1 968.36 1154.48 154.68 o -9 5 1 2693.55 2786.59 170.01 o -8 5 1 6037.80 5374.61 191.98 o -7 5 1 910.32 965.91 121.74 o -6 5 1 29799.54 28946.96 1794.99 o -5 5 1 6737.98 5936.49 174.36 o -4 5 1 6681.07 6658.90 408.87 o -3 5 1 1592.75 1598.79 141.97 o -2 5 1 3546.03 4147.01 86.15 o -1 5 1 11430.30 11043.08 219.14 o 0 5 1 7668.24 10015.47 195.47 o 1 5 1 3428.78 3670.96 120.25 o 2 5 1 9033.29 10749.98 589.36 o 3 5 1 20070.94 19769.70 940.94 o 4 5 1 18838.24 18061.56 1437.47 o 5 5 1 885.21 1027.37 188.53 o 6 5 1 10646.49 9809.31 379.97 o 7 5 1 11730.66 10904.21 797.90 o 8 5 1 2098.12 2175.18 195.64 o 9 5 1 187.34 132.12 96.76 o 10 5 1 1174.54 1242.70 175.34 o 11 5 1 2314.63 2932.64 277.87 o 12 5 1 1488.02 1524.50 158.89 o -12 6 1 1499.78 1576.93 464.40 o -11 6 1 24.98 117.96 115.81 o -10 6 1 909.03 804.56 189.05 o -9 6 1 1378.82 1492.28 248.27 o -8 6 1 8898.48 8819.94 612.72 o -7 6 1 143.70 209.00 106.32 o -6 6 1 6194.04 6196.61 292.82 o -5 6 1 8277.90 7664.89 592.15 o -4 6 1 15925.72 18023.68 1224.51 o -3 6 1 474.64 586.79 64.82 o -2 6 1 47484.87 51734.44 564.52 o -1 6 1 23638.74 26152.05 159.72 o 0 6 1 106576.10 107048.54 687.87 o 1 6 1 7961.57 8494.22 146.67 o 2 6 1 11044.90 10658.38 154.36 o 3 6 1 3067.54 2654.16 127.59 o 4 6 1 18118.84 15237.31 1151.80 o 5 6 1 919.09 910.48 152.33 o 6 6 1 20526.37 20811.40 1423.53 o 7 6 1 6675.20 6281.23 245.72 o 8 6 1 8165.66 8758.56 458.80 o 9 6 1 81.26 266.42 148.74 o 10 6 1 4100.10 4269.54 297.22 o 11 6 1 301.38 448.56 185.26 o 12 6 1 994.66 938.51 205.36 o -12 7 1 433.56 422.69 185.88 o -11 7 1 411.62 505.61 183.32 o -10 7 1 1743.45 1984.74 216.81 o -9 7 1 6900.70 7089.30 254.67 o -8 7 1 107.28 75.53 63.87 o -7 7 1 609.48 724.23 153.78 o -6 7 1 1926.01 2301.55 287.12 o -5 7 1 4075.45 4195.77 359.84 o -4 7 1 4783.92 5103.46 385.52 o -3 7 1 6541.79 6905.30 98.45 o -2 7 1 58146.57 68994.13 597.91 o -1 7 1 80218.94 92667.62 882.38 o 0 7 1 59039.75 69193.27 2562.67 o 1 7 1 34582.98 41292.61 205.28 o 2 7 1 4024.87 3560.53 93.57 o 3 7 1 15233.76 15595.04 859.10 o 4 7 1 2253.91 2494.13 177.28 o 5 7 1 1165.81 1554.83 324.53 o 6 7 1 3322.04 3593.54 392.74 o 7 7 1 13250.48 12797.56 694.87 o 8 7 1 8343.00 8626.44 1131.23 o 9 7 1 6.23 162.69 89.58 o 10 7 1 1522.42 1736.48 215.27 o 11 7 1 1477.16 1688.53 241.54 o 12 7 1 404.95 652.60 205.73 o -12 8 1 135.85 171.93 148.83 o -11 8 1 2863.41 2951.23 237.58 o -10 8 1 184.00 218.38 149.50 o -9 8 1 863.62 854.32 169.12 o -8 8 1 47.70 119.79 90.74 o -7 8 1 14345.37 14327.36 280.24 o -6 8 1 1180.24 1293.50 167.73 o -5 8 1 1963.87 2081.61 311.07 o -4 8 1 3890.96 3707.55 387.68 o -3 8 1 26256.92 27636.39 208.34 o -2 8 1 7773.80 8103.12 87.83 o -1 8 1 1441.17 1846.30 63.09 o 0 8 1 9106.34 10145.85 317.31 o 1 8 1 71710.74 74449.85 2551.62 o 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