#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/52/2225289.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225289_Fobs loop_ _publ_author_name 'Xie, Bu-Yun' 'Huang, Wei' 'Zhang, Ying' 'Yang, Rui-Qing' 'Xie, Yong-Rong' _publ_section_title ; Pentaaqua(acetonitrile-\kN)zinc(II) 4,6-dihydroxybenzene-1,3-disulfonate trihydrate ; _journal_coeditor_code HY2283 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m341 _journal_volume 66 _journal_year 2010 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.8731 _cell_length_b 6.9972 _cell_length_c 22.9980 _exptl_crystal_F_000 1072.00 _reflns_d_resolution_high 0.7674 _[local]_cod_data_source_file hy2283Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 P n m a R = 0.04 Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 402.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1139.64 1140.88 39.43 o 6 0 0 1899.92 1805.28 42.31 o 8 0 0 434.22 316.14 40.79 o 10 0 0 3048.95 3225.48 107.43 o 12 0 0 531.29 481.37 46.23 o 14 0 0 51.83 12.24 25.84 o 16 0 0 2.21 1.36 31.28 o 2 1 0 12501.03 12311.69 197.11 o 4 1 0 161.04 173.02 14.92 o 6 1 0 2471.41 2870.49 42.89 o 8 1 0 781.63 705.91 20.05 o 10 1 0 3.36 -10.71 11.42 o 12 1 0 645.02 656.79 51.67 o 14 1 0 62.30 122.38 35.36 o 16 1 0 133.24 146.86 39.43 o 0 2 0 162232.16 135520.22 2078.36 o 2 2 0 1424.03 1345.34 34.26 o 4 2 0 2532.76 2589.78 37.83 o 6 2 0 668.34 650.61 23.73 o 8 2 0 530.99 519.73 22.39 o 10 2 0 141.46 152.61 20.12 o 12 2 0 1.95 0.00 19.04 o 14 2 0 13.20 -17.68 23.12 o 16 2 0 6.99 5.44 28.56 o 2 3 0 114.40 202.58 27.57 o 4 3 0 623.21 576.72 21.81 o 6 3 0 51.34 56.53 9.45 o 8 3 0 79.50 81.86 13.56 o 10 3 0 244.07 252.53 20.61 o 12 3 0 177.94 251.72 33.32 o 14 3 0 0.98 -20.40 20.40 o 0 4 0 81891.37 77016.45 1185.09 o 2 4 0 4152.21 4088.48 75.67 o 4 4 0 500.88 482.99 27.95 o 6 4 0 1073.87 1305.66 53.85 o 8 4 0 214.88 163.20 25.96 o 10 4 0 589.58 667.15 30.25 o 12 4 0 19.48 -3.32 43.51 o 14 4 0 12.97 -5.44 20.40 o 2 5 0 2568.15 2474.92 50.86 o 4 5 0 11.64 -4.13 8.98 o 6 5 0 353.65 352.85 35.09 o 8 5 0 337.77 333.51 42.83 o 10 5 0 6.58 14.21 22.58 o 12 5 0 211.06 258.32 38.43 o 0 6 0 23327.69 21654.97 377.38 o 2 6 0 1521.88 1374.55 61.89 o 4 6 0 14.39 -5.41 12.17 o 6 6 0 320.34 354.58 43.51 o 8 6 0 100.55 108.70 34.68 o 10 6 0 403.41 430.09 77.51 o 12 6 0 16.39 24.04 26.72 o 2 7 0 402.15 418.09 27.87 o 4 7 0 204.64 202.54 35.09 o 6 7 0 19.66 18.36 21.15 o 8 7 0 48.45 32.49 32.64 o 10 7 0 30.00 48.95 31.73 o 0 8 0 2818.25 2733.98 96.60 o 2 8 0 252.86 290.67 39.89 o 4 8 0 72.70 18.14 27.88 o 6 8 0 94.64 97.39 33.32 o 8 8 0 24.46 50.15 46.23 o 2 9 0 12.81 25.74 26.32 o 2 0 1 4164.94 3746.29 89.75 o 3 0 1 2577.76 2979.76 43.14 o 4 0 1 4921.40 5096.37 71.42 o 5 0 1 5412.43 5916.66 102.83 o 6 0 1 371.61 411.48 18.84 o 7 0 1 1195.06 1162.70 24.43 o 8 0 1 1.99 9.15 6.75 o 9 0 1 1786.73 1708.70 40.57 o 10 0 1 62.98 79.41 23.80 o 11 0 1 1191.63 1288.45 47.12 o 12 0 1 48.53 22.25 31.96 o 13 0 1 7.07 4.78 16.81 o 14 0 1 1.90 1.58 22.44 o 15 0 1 13.91 25.87 20.66 o 16 0 1 1.43 -22.44 22.44 o 0 1 1 207.78 232.87 7.56 o 1 1 1 13513.63 14032.57 180.57 o 2 1 1 166.34 107.61 7.77 o 3 1 1 14538.30 14591.68 147.39 o 4 1 1 7.82 2.28 2.68 o 5 1 1 2399.48 2514.03 35.94 o 6 1 1 611.81 630.82 13.21 o 7 1 1 4418.84 4737.84 48.28 o 8 1 1 4472.59 4335.18 46.64 o 9 1 1 338.71 392.64 14.23 o 10 1 1 2192.84 2204.54 43.15 o 11 1 1 531.83 529.56 54.39 o 12 1 1 483.53 482.56 31.73 o 13 1 1 81.24 59.73 19.16 o 14 1 1 42.68 38.67 19.69 o 15 1 1 2.21 -7.01 20.40 o 16 1 1 15.02 -15.33 21.08 o 1 2 1 4186.27 4540.05 53.85 o 2 2 1 7379.30 7672.73 83.72 o 3 2 1 2692.58 2897.50 27.67 o 4 2 1 7082.21 6847.09 58.63 o 5 2 1 713.63 804.82 13.21 o 6 2 1 11017.30 10962.38 91.53 o 7 2 1 461.30 512.06 13.54 o 8 2 1 347.16 377.16 14.20 o 9 2 1 1821.60 1824.07 37.92 o 10 2 1 54.75 28.66 13.32 o 11 2 1 107.27 110.21 13.53 o 12 2 1 96.54 96.22 44.87 o 13 2 1 18.39 25.31 17.23 o 14 2 1 36.46 31.00 19.16 o 15 2 1 86.15 117.63 25.00 o 16 2 1 1.35 -10.15 19.69 o 0 3 1 11.55 6.80 6.28 o 1 3 1 940.89 939.26 17.51 o 2 3 1 1273.00 1285.94 22.90 o 3 3 1 3671.02 3670.00 42.00 o 4 3 1 21.24 24.00 5.92 o 5 3 1 1016.02 1059.00 21.12 o 6 3 1 1427.81 1401.75 21.33 o 7 3 1 4522.52 4627.49 55.27 o 8 3 1 3058.46 2971.25 43.38 o 9 3 1 4.63 8.11 7.40 o 10 3 1 1278.10 1216.12 29.38 o 11 3 1 529.41 538.84 29.47 o 12 3 1 379.26 343.91 23.40 o 13 3 1 2.72 -4.41 13.92 o 14 3 1 31.48 38.58 18.19 o 15 3 1 0.61 -16.35 16.35 o 1 4 1 280.39 258.55 11.22 o 2 4 1 2293.57 2264.97 42.01 o 3 4 1 55.34 60.55 7.53 o 4 4 1 766.91 783.40 18.37 o 5 4 1 520.78 541.05 15.58 o 6 4 1 1523.94 1549.61 41.27 o 7 4 1 22.16 27.14 12.06 o 8 4 1 36.23 73.74 14.51 o 9 4 1 1148.16 1139.97 23.06 o 10 4 1 6.64 14.77 8.12 o 11 4 1 160.17 175.41 14.11 o 12 4 1 63.29 48.48 11.23 o 13 4 1 10.17 8.85 12.36 o 14 4 1 17.71 4.12 34.68 o 15 4 1 38.90 17.87 17.23 o 0 5 1 260.48 245.87 17.92 o 1 5 1 2561.30 2604.17 36.94 o 2 5 1 284.97 266.84 13.94 o 3 5 1 1808.04 1703.65 40.92 o 4 5 1 46.05 60.23 8.18 o 5 5 1 524.26 492.06 42.59 o 6 5 1 500.20 537.57 34.22 o 7 5 1 713.88 724.25 36.70 o 8 5 1 1072.10 1160.03 58.46 o 9 5 1 186.23 230.11 31.60 o 10 5 1 553.27 624.92 34.33 o 11 5 1 180.35 159.47 22.71 o 12 5 1 150.93 172.09 27.97 o 13 5 1 40.72 56.79 26.32 o 1 6 1 153.54 159.65 12.67 o 2 6 1 170.81 204.95 13.56 o 3 6 1 139.70 133.49 15.80 o 4 6 1 112.44 116.62 13.65 o 5 6 1 260.01 247.45 47.30 o 6 6 1 591.38 600.04 42.50 o 7 6 1 24.51 12.60 16.68 o 8 6 1 52.07 51.63 17.29 o 9 6 1 265.30 339.74 30.08 o 10 6 1 6.62 28.01 17.28 o 11 6 1 89.31 120.26 23.11 o 12 6 1 3.23 7.31 17.44 o 0 7 1 88.82 77.54 16.23 o 1 7 1 415.44 396.17 19.40 o 2 7 1 3.40 6.69 8.86 o 3 7 1 448.28 411.44 26.15 o 4 7 1 2.41 14.19 13.94 o 5 7 1 1.48 -15.54 22.77 o 6 7 1 162.89 153.21 22.75 o 7 7 1 302.03 328.16 30.08 o 8 7 1 210.37 243.39 28.67 o 9 7 1 28.09 42.87 19.13 o 10 7 1 74.77 87.62 30.62 o 1 8 1 3.72 14.37 10.56 o 2 8 1 124.55 109.70 16.46 o 3 8 1 1.65 -14.25 14.25 o 4 8 1 186.24 137.19 23.90 o 5 8 1 24.96 9.37 17.44 o 6 8 1 251.15 287.32 30.20 o 7 8 1 7.91 8.95 18.34 o 8 8 1 22.72 29.31 19.92 o 0 9 1 18.02 8.27 17.19 o 1 9 1 89.36 58.96 20.73 o 2 9 1 32.24 58.77 20.66 o 1 0 2 136.87 201.25 12.24 o 3 0 2 4583.00 4577.33 75.96 o 4 0 2 7739.58 8200.78 109.57 o 5 0 2 3848.27 3839.16 57.69 o 6 0 2 2710.21 2948.67 42.56 o 7 0 2 117.39 99.19 9.03 o 8 0 2 1468.77 1464.49 38.86 o 9 0 2 18.28 17.02 9.92 o 10 0 2 126.79 112.10 17.77 o 11 0 2 68.63 56.96 16.81 o 12 0 2 3.09 12.94 21.76 o 13 0 2 314.13 355.60 30.77 o 14 0 2 0.01 -5.44 17.31 o 15 0 2 194.40 267.65 32.20 o 16 0 2 24.43 19.10 22.46 o 1 1 2 33905.14 32217.49 348.79 o 2 1 2 2.08 9.99 7.85 o 3 1 2 22175.07 21898.81 217.09 o 4 1 2 408.58 365.64 11.57 o 5 1 2 30.56 41.18 4.96 o 6 1 2 2978.34 2992.80 54.12 o 7 1 2 233.08 254.87 9.63 o 8 1 2 343.73 334.02 10.73 o 9 1 2 757.45 725.69 18.50 o 10 1 2 214.89 231.48 18.24 o 11 1 2 180.63 181.98 22.44 o 12 1 2 0.37 -4.08 14.42 o 13 1 2 61.63 56.43 19.23 o 14 1 2 407.66 436.68 44.19 o 15 1 2 50.31 58.47 22.12 o 16 1 2 0.22 10.04 20.12 o 0 2 2 2305.51 2509.87 43.44 o 1 2 2 1421.88 1568.45 23.82 o 2 2 2 100.92 78.56 6.02 o 3 2 2 2786.02 2660.34 24.38 o 5 2 2 13242.93 12907.64 112.77 o 6 2 2 187.45 227.77 9.34 o 7 2 2 360.63 309.32 11.16 o 8 2 2 475.53 489.10 31.60 o 9 2 2 56.20 52.43 9.80 o 10 2 2 333.77 351.53 19.92 o 11 2 2 10.44 2.68 8.90 o 12 2 2 4.10 33.29 15.84 o 13 2 2 262.33 308.84 29.31 o 14 2 2 25.58 18.86 21.08 o 15 2 2 188.30 178.51 28.85 o 16 2 2 61.57 27.05 23.02 o 1 3 2 4172.80 4011.70 53.11 o 2 3 2 1367.71 1470.60 28.27 o 3 3 2 8496.45 8572.73 82.45 o 4 3 2 1.76 0.99 4.46 o 5 3 2 46.98 57.40 4.91 o 6 3 2 6.59 -0.70 4.80 o 7 3 2 60.85 43.51 7.57 o 8 3 2 202.91 208.71 12.26 o 9 3 2 47.13 25.67 8.31 o 10 3 2 18.07 -3.39 8.33 o 11 3 2 38.62 39.79 10.92 o 12 3 2 6.34 30.36 13.32 o 13 3 2 44.04 58.90 18.19 o 14 3 2 428.77 390.97 31.24 o 15 3 2 44.89 -11.17 17.77 o 0 4 2 24.16 18.15 17.74 o 1 4 2 4.50 0.43 6.21 o 2 4 2 1438.88 1493.22 26.00 o 3 4 2 843.74 799.06 21.40 o 4 4 2 380.66 359.59 13.11 o 5 4 2 1706.91 1792.23 31.95 o 6 4 2 111.49 97.81 14.76 o 7 4 2 4.29 -1.98 10.81 o 8 4 2 51.37 55.76 13.19 o 9 4 2 3.35 -0.61 8.31 o 10 4 2 125.56 130.90 11.07 o 11 4 2 1.82 -1.65 9.00 o 12 4 2 15.56 26.11 11.26 o 13 4 2 145.64 183.90 18.34 o 14 4 2 0.05 16.32 15.38 o 1 5 2 6584.79 6413.65 73.94 o 2 5 2 107.42 119.46 12.05 o 3 5 2 3385.68 3313.52 50.20 o 4 5 2 182.53 173.05 11.90 o 5 5 2 92.20 66.90 11.80 o 6 5 2 393.41 393.82 25.32 o 7 5 2 104.24 100.88 17.66 o 8 5 2 0.45 1.10 13.19 o 9 5 2 283.30 271.95 36.31 o 10 5 2 22.75 34.36 15.79 o 11 5 2 99.83 156.77 25.73 o 12 5 2 4.80 -10.66 17.92 o 13 5 2 21.85 10.11 19.23 o 0 6 2 99.95 98.51 16.42 o 1 6 2 32.88 6.14 8.72 o 2 6 2 704.83 706.95 21.52 o 3 6 2 350.45 334.32 17.28 o 4 6 2 523.55 507.51 22.07 o 5 6 2 1428.59 1437.59 45.52 o 6 6 2 142.56 126.66 19.28 o 7 6 2 90.09 79.60 18.44 o 8 6 2 60.87 45.69 17.17 o 9 6 2 7.23 -15.29 15.29 o 10 6 2 43.34 41.36 18.47 o 11 6 2 6.99 4.16 17.93 o 12 6 2 2.48 -20.17 32.32 o 1 7 2 624.17 582.23 21.74 o 2 7 2 15.82 7.06 9.75 o 3 7 2 883.08 875.15 30.09 o 4 7 2 141.85 122.80 20.15 o 5 7 2 42.29 38.49 19.11 o 6 7 2 123.90 127.75 21.53 o 7 7 2 84.42 64.91 23.16 o 8 7 2 0.36 -13.26 15.76 o 9 7 2 31.71 48.68 19.97 o 10 7 2 3.91 9.40 19.14 o 0 8 2 19.22 16.29 16.21 o 1 8 2 23.32 7.39 11.36 o 2 8 2 59.65 85.89 15.55 o 3 8 2 88.62 106.95 21.21 o 4 8 2 19.18 48.90 18.95 o 5 8 2 296.22 310.05 30.95 o 6 8 2 3.78 14.55 18.44 o 7 8 2 0.70 -6.02 17.60 o 1 9 2 273.10 287.14 24.63 o 2 9 2 2.08 11.94 17.87 o 1 0 3 1173.58 1230.63 39.43 o 2 0 3 5696.81 6656.29 159.10 o 3 0 3 540.84 543.35 17.31 o 4 0 3 1116.44 1054.11 24.04 o 6 0 3 4903.86 5511.50 61.80 o 7 0 3 5962.56 5721.19 73.77 o 8 0 3 1.39 -3.05 6.59 o 9 0 3 636.32 614.53 24.57 o 10 0 3 127.63 137.79 16.45 o 11 0 3 1292.08 1261.65 76.83 o 12 0 3 341.39 291.13 40.79 o 13 0 3 351.32 336.59 30.77 o 14 0 3 178.67 230.01 65.95 o 15 0 3 7.03 23.72 20.52 o 16 0 3 0.38 -3.15 21.09 o 0 1 3 652.50 762.86 29.92 o 1 1 3 1886.34 1747.32 26.21 o 2 1 3 8180.64 8195.92 362.74 o 3 1 3 9961.32 10199.85 115.87 o 4 1 3 9639.64 9009.97 201.95 o 5 1 3 13392.99 12958.25 120.06 o 6 1 3 1607.27 1708.31 28.42 o 7 1 3 348.18 319.08 11.41 o 8 1 3 1227.21 1291.29 27.01 o 9 1 3 118.75 125.46 8.86 o 10 1 3 3.42 -7.79 9.92 o 11 1 3 18.26 18.78 17.25 o 12 1 3 33.65 40.48 16.81 o 13 1 3 12.22 7.73 16.81 o 14 1 3 2.99 -13.83 16.81 o 15 1 3 110.96 162.77 27.83 o 16 1 3 39.04 43.25 40.79 o 1 2 3 303.09 337.71 12.70 o 2 2 3 20141.79 20061.26 200.85 o 3 2 3 229.09 293.61 6.55 o 4 2 3 42.65 33.58 4.51 o 5 2 3 348.25 346.22 10.66 o 6 2 3 1707.77 1745.83 26.71 o 7 2 3 2641.82 2456.33 72.80 o 8 2 3 523.03 482.90 18.83 o 9 2 3 67.20 64.54 13.13 o 10 2 3 73.75 70.64 11.35 o 11 2 3 1506.59 1576.17 53.71 o 12 2 3 149.97 113.22 16.67 o 13 2 3 329.45 346.71 30.28 o 14 2 3 146.33 168.58 26.43 o 15 2 3 10.80 6.17 19.69 o 16 2 3 2.75 -8.51 20.66 o 0 3 3 2027.45 2160.38 44.19 o 1 3 3 611.45 720.68 21.21 o 2 3 3 2720.80 2851.81 37.81 o 3 3 3 18560.12 18485.12 175.54 o 4 3 3 4024.38 3868.51 44.06 o 5 3 3 10792.05 11139.20 94.32 o 6 3 3 1070.36 1077.35 22.18 o 7 3 3 533.70 525.47 14.45 o 8 3 3 193.80 209.45 11.88 o 9 3 3 441.80 493.36 18.64 o 10 3 3 52.22 52.52 10.40 o 11 3 3 1.36 -6.80 7.99 o 12 3 3 57.16 65.33 15.24 o 13 3 3 160.06 151.87 22.12 o 14 3 3 1.70 10.20 16.35 o 15 3 3 142.55 179.31 26.92 o 1 4 3 3375.20 3258.66 45.45 o 2 4 3 1259.05 1244.97 23.70 o 3 4 3 57.87 66.35 8.54 o 4 4 3 158.88 169.97 10.04 o 5 4 3 333.40 368.59 18.10 o 6 4 3 412.11 434.45 19.80 o 7 4 3 1793.62 1829.36 53.78 o 8 4 3 115.22 149.11 18.28 o 9 4 3 153.94 154.18 10.20 o 10 4 3 0.04 2.70 7.58 o 11 4 3 978.48 957.36 26.29 o 12 4 3 62.02 43.48 11.37 o 13 4 3 244.19 180.88 18.50 o 14 4 3 106.68 176.33 46.91 o 0 5 3 15.12 16.03 10.16 o 1 5 3 80.11 73.51 10.08 o 2 5 3 1071.49 1054.63 24.31 o 3 5 3 951.07 958.78 23.06 o 4 5 3 1012.40 956.71 25.56 o 5 5 3 1884.31 1935.10 42.83 o 6 5 3 219.81 224.01 27.28 o 7 5 3 54.42 45.41 14.28 o 8 5 3 63.94 46.08 15.23 o 9 5 3 0.16 4.79 14.08 o 10 5 3 2.67 -5.58 15.08 o 11 5 3 1.66 -0.09 16.86 o 12 5 3 26.93 40.53 20.74 o 13 5 3 1.27 -14.65 23.54 o 1 6 3 5.29 -7.77 7.77 o 2 6 3 290.36 310.10 16.80 o 3 6 3 67.48 59.32 9.83 o 4 6 3 180.74 201.56 19.69 o 5 6 3 22.56 31.56 14.39 o 6 6 3 417.01 404.59 29.03 o 7 6 3 828.69 910.32 41.09 o 8 6 3 59.35 53.23 17.58 o 9 6 3 59.84 103.51 21.33 o 10 6 3 23.96 30.44 17.96 o 11 6 3 132.80 133.70 26.75 o 12 6 3 25.97 37.90 21.54 o 0 7 3 75.37 45.03 15.55 o 1 7 3 3.69 2.57 9.21 o 2 7 3 418.63 397.63 22.42 o 3 7 3 504.98 523.99 25.11 o 4 7 3 422.98 356.45 31.65 o 5 7 3 1228.82 1255.98 46.89 o 6 7 3 162.63 171.75 23.93 o 7 7 3 170.50 149.70 24.10 o 8 7 3 33.46 25.08 18.26 o 9 7 3 11.93 21.44 18.59 o 10 7 3 3.14 21.45 19.06 o 1 8 3 44.84 71.63 12.93 o 2 8 3 42.59 37.84 14.05 o 3 8 3 7.49 19.16 15.63 o 4 8 3 22.21 9.07 17.00 o 5 8 3 31.10 48.84 19.31 o 6 8 3 20.41 16.56 17.88 o 7 8 3 101.18 98.40 23.22 o 0 9 3 20.52 18.07 20.11 o 1 9 3 4.31 12.96 14.19 o 2 9 3 53.20 51.65 19.87 o 0 0 4 4645.64 4374.52 107.43 o 1 0 4 4915.86 5583.40 131.90 o 2 0 4 10134.57 9873.34 159.48 o 3 0 4 1075.59 1356.34 31.04 o 4 0 4 477.77 503.44 27.20 o 5 0 4 1212.47 1202.13 21.08 o 6 0 4 1540.67 1531.87 49.55 o 7 0 4 819.34 858.35 19.75 o 8 0 4 3716.76 3638.84 87.17 o 9 0 4 379.79 319.58 21.16 o 10 0 4 484.49 462.26 23.53 o 11 0 4 910.39 847.66 38.46 o 12 0 4 158.89 176.69 29.92 o 13 0 4 523.84 449.44 33.16 o 14 0 4 16.34 -2.57 17.77 o 15 0 4 1.47 1.05 18.73 o 16 0 4 20.58 7.78 48.27 o 1 1 4 11088.56 11346.02 149.39 o 2 1 4 829.17 882.28 21.95 o 3 1 4 506.58 452.07 16.41 o 4 1 4 5609.30 5405.42 76.00 o 5 1 4 26.88 50.75 5.60 o 6 1 4 356.47 313.87 12.43 o 7 1 4 732.59 760.57 15.73 o 8 1 4 6.97 4.63 5.01 o 9 1 4 1486.39 1459.42 24.44 o 10 1 4 32.82 21.61 11.45 o 11 1 4 1.78 -6.36 10.59 o 12 1 4 127.49 180.73 23.54 o 13 1 4 106.76 90.96 21.15 o 14 1 4 166.21 161.28 50.99 o 15 1 4 0.27 5.67 19.69 o 16 1 4 5.11 -10.55 19.69 o 0 2 4 2007.78 2275.56 41.84 o 1 2 4 4946.41 5174.42 55.37 o 2 2 4 10051.91 10760.09 103.97 o 3 2 4 1893.37 1823.48 28.07 o 4 2 4 624.92 549.42 13.89 o 5 2 4 1662.38 1610.45 24.58 o 6 2 4 2391.06 2337.58 32.50 o 7 2 4 1513.96 1455.19 27.52 o 8 2 4 1807.48 1903.18 33.77 o 9 2 4 271.01 263.52 14.85 o 10 2 4 396.31 419.22 18.13 o 11 2 4 725.83 753.07 31.01 o 12 2 4 366.29 359.81 70.03 o 13 2 4 298.83 272.58 32.64 o 14 2 4 3.46 5.65 18.19 o 15 2 4 1.00 2.26 19.69 o 16 2 4 51.88 62.87 24.39 o 1 3 4 57.09 20.90 7.60 o 2 3 4 2258.09 2347.84 33.55 o 3 3 4 103.01 126.65 8.35 o 4 3 4 6059.52 5891.24 61.12 o 5 3 4 173.80 151.09 6.17 o 6 3 4 103.00 101.82 7.44 o 7 3 4 1266.65 1272.61 23.57 o 8 3 4 33.20 34.38 8.43 o 9 3 4 294.57 264.77 14.74 o 10 3 4 284.98 275.59 16.05 o 11 3 4 121.11 115.14 14.57 o 12 3 4 30.01 25.65 13.83 o 13 3 4 137.03 122.53 19.26 o 14 3 4 267.12 202.56 25.47 o 15 3 4 9.10 2.54 21.08 o 0 4 4 4538.38 4417.99 79.78 o 1 4 4 759.27 795.93 22.19 o 2 4 4 3680.80 3719.64 49.76 o 3 4 4 8.89 1.64 5.55 o 4 4 4 2.14 2.29 5.50 o 5 4 4 24.39 33.48 9.36 o 6 4 4 930.48 882.42 26.67 o 7 4 4 342.47 361.83 23.25 o 8 4 4 633.45 638.95 19.87 o 9 4 4 45.02 47.45 10.73 o 10 4 4 251.09 243.70 14.10 o 11 4 4 365.56 383.04 18.10 o 12 4 4 212.80 243.02 18.92 o 13 4 4 122.14 161.83 18.27 o 14 4 4 3.30 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14 2 6 52.00 6.59 18.73 o 15 2 6 59.32 9.80 44.19 o 1 3 6 482.13 464.55 16.39 o 2 3 6 64.75 96.67 9.21 o 3 3 6 40.90 29.07 7.54 o 4 3 6 2790.04 2683.41 63.40 o 5 3 6 174.10 165.36 7.84 o 6 3 6 5077.04 5061.08 57.98 o 7 3 6 2289.41 2369.88 35.16 o 8 3 6 7.57 -4.78 9.59 o 9 3 6 4576.54 4572.22 63.79 o 10 3 6 280.27 276.52 21.26 o 11 3 6 166.86 194.59 16.95 o 12 3 6 93.38 84.44 16.20 o 13 3 6 31.84 46.48 15.88 o 14 3 6 77.81 77.22 20.66 o 15 3 6 99.53 142.36 25.00 o 0 4 6 890.25 792.39 50.55 o 1 4 6 1214.70 1243.29 28.65 o 2 4 6 1028.08 1095.04 29.39 o 3 4 6 2193.49 2166.89 35.67 o 4 4 6 3931.91 3809.87 53.17 o 5 4 6 1331.44 1291.86 37.89 o 6 4 6 165.40 166.71 17.86 o 7 4 6 1460.60 1394.60 48.09 o 8 4 6 395.34 390.10 27.48 o 9 4 6 235.56 245.21 13.05 o 10 4 6 235.38 223.38 14.66 o 11 4 6 107.54 98.69 14.06 o 12 4 6 76.73 101.65 15.46 o 13 4 6 7.16 1.07 12.58 o 14 4 6 14.33 19.90 14.55 o 1 5 6 26.27 30.38 8.72 o 2 5 6 2.47 1.00 7.84 o 3 5 6 2434.59 2325.25 37.95 o 4 5 6 546.45 563.94 24.52 o 5 5 6 37.94 26.23 10.57 o 6 5 6 691.92 690.65 27.85 o 7 5 6 9.73 23.29 14.78 o 8 5 6 8.56 9.59 14.80 o 9 5 6 1179.18 1191.67 50.23 o 10 5 6 34.94 23.06 18.31 o 11 5 6 98.72 132.46 24.31 o 12 5 6 55.72 42.06 20.61 o 13 5 6 42.85 24.48 39.43 o 0 6 6 1008.97 923.11 38.14 o 1 6 6 444.01 417.97 18.84 o 2 6 6 378.18 415.81 18.98 o 3 6 6 238.02 241.97 20.25 o 4 6 6 180.15 177.38 18.81 o 5 6 6 19.59 2.38 8.35 o 6 6 6 120.80 118.22 21.42 o 7 6 6 315.00 376.49 29.51 o 8 6 6 13.26 12.73 18.29 o 9 6 6 114.86 107.32 25.10 o 10 6 6 82.29 79.24 23.81 o 11 6 6 16.55 33.73 21.08 o 12 6 6 66.79 35.05 23.65 o 1 7 6 42.80 62.68 11.74 o 2 7 6 89.99 59.46 13.17 o 3 7 6 140.10 140.23 18.03 o 4 7 6 373.22 386.65 26.47 o 5 7 6 2.50 -8.69 14.35 o 6 7 6 297.82 258.80 27.31 o 7 7 6 51.12 51.39 18.95 o 8 7 6 0.61 24.01 20.56 o 9 7 6 450.12 459.23 42.04 o 10 7 6 3.43 6.00 21.54 o 0 8 6 47.47 70.68 18.99 o 1 8 6 58.28 34.75 14.61 o 2 8 6 86.09 96.41 16.99 o 3 8 6 50.41 37.96 14.47 o 4 8 6 108.50 108.27 22.46 o 5 8 6 71.00 74.95 20.88 o 6 8 6 15.12 18.43 18.06 o 7 8 6 140.23 119.80 24.98 o 1 0 7 16005.45 15618.11 251.90 o 2 0 7 16654.06 18142.96 290.77 o 3 0 7 2888.57 2643.75 44.75 o 4 0 7 449.10 456.13 22.18 o 5 0 7 87.36 75.89 9.42 o 6 0 7 1906.81 1923.20 33.68 o 7 0 7 317.23 338.94 12.07 o 8 0 7 2651.60 2529.45 52.79 o 9 0 7 18.11 3.82 7.46 o 10 0 7 1089.81 1056.07 35.17 o 11 0 7 6.96 12.51 11.80 o 12 0 7 182.94 189.16 24.04 o 13 0 7 177.09 164.40 47.59 o 14 0 7 11.51 2.55 18.73 o 15 0 7 89.24 48.47 27.88 o 16 0 7 5.43 38.84 24.48 o 0 1 7 857.34 932.55 18.10 o 1 1 7 116.62 131.71 8.85 o 2 1 7 20.73 15.08 3.40 o 3 1 7 24643.92 25605.75 206.85 o 4 1 7 247.50 296.07 14.24 o 5 1 7 9269.60 9374.10 91.38 o 6 1 7 2812.01 2803.91 47.59 o 7 1 7 2413.65 2498.11 34.84 o 8 1 7 813.62 862.44 17.25 o 9 1 7 317.53 297.30 15.68 o 10 1 7 100.98 84.74 18.45 o 11 1 7 84.81 99.84 20.33 o 12 1 7 140.28 185.66 24.50 o 13 1 7 382.60 457.51 34.12 o 14 1 7 201.72 236.61 50.31 o 15 1 7 284.30 263.75 79.55 o 16 1 7 36.24 76.97 25.47 o 1 2 7 1791.25 1583.32 24.52 o 2 2 7 3268.42 3634.40 40.08 o 3 2 7 4047.94 4069.80 44.69 o 4 2 7 4532.97 4434.73 48.71 o 5 2 7 31.67 20.95 8.63 o 6 2 7 1355.10 1300.83 26.93 o 7 2 7 820.61 804.91 21.58 o 8 2 7 95.60 93.87 7.93 o 9 2 7 57.70 42.22 8.74 o 10 2 7 1972.15 1920.04 49.07 o 11 2 7 114.05 99.12 16.84 o 12 2 7 3.70 0.16 13.33 o 13 2 7 93.62 126.14 37.39 o 14 2 7 111.02 108.86 24.04 o 15 2 7 32.62 18.94 20.66 o 0 3 7 413.71 462.06 33.32 o 1 3 7 500.45 512.05 18.90 o 2 3 7 199.51 177.24 12.44 o 3 3 7 3721.11 3828.80 60.13 o 4 3 7 2727.77 3002.67 40.38 o 5 3 7 4301.63 4286.06 52.88 o 6 3 7 927.46 901.87 19.64 o 7 3 7 974.90 997.58 21.65 o 8 3 7 59.64 58.44 11.45 o 9 3 7 6.27 -8.13 8.13 o 10 3 7 1.00 5.53 7.59 o 11 3 7 54.21 81.78 15.75 o 12 3 7 188.81 175.01 26.83 o 13 3 7 86.97 74.20 17.23 o 14 3 7 63.65 62.08 20.66 o 15 3 7 139.03 212.55 28.35 o 1 4 7 1240.12 1067.47 26.93 o 2 4 7 100.92 100.18 10.01 o 3 4 7 2102.64 2119.70 39.71 o 4 4 7 888.58 857.88 33.45 o 5 4 7 158.66 147.76 15.59 o 6 4 7 478.28 505.98 40.47 o 7 4 7 242.63 219.55 19.32 o 8 4 7 503.03 492.44 22.52 o 9 4 7 11.44 11.51 7.47 o 10 4 7 536.89 564.90 28.61 o 11 4 7 29.95 12.56 10.08 o 12 4 7 28.29 26.30 14.21 o 13 4 7 41.22 55.67 14.95 o 14 4 7 39.25 43.14 15.85 o 0 5 7 485.08 490.65 27.46 o 1 5 7 102.57 105.53 13.00 o 2 5 7 68.80 52.25 16.40 o 3 5 7 3572.94 3517.13 59.20 o 4 5 7 15.98 2.75 10.25 o 5 5 7 1943.92 1982.92 55.04 o 6 5 7 1026.69 1057.32 37.49 o 7 5 7 584.31 519.02 69.77 o 8 5 7 401.24 481.58 34.54 o 9 5 7 113.22 127.52 29.09 o 10 5 7 9.13 -0.28 16.77 o 11 5 7 27.64 17.58 17.65 o 12 5 7 46.06 54.26 22.20 o 13 5 7 122.13 80.23 44.87 o 1 6 7 1256.37 1245.06 31.95 o 2 6 7 165.17 119.69 15.39 o 3 6 7 654.44 692.42 29.61 o 4 6 7 282.44 292.86 22.09 o 5 6 7 11.65 9.89 11.68 o 6 6 7 232.63 250.29 28.50 o 7 6 7 78.31 120.75 23.23 o 8 6 7 127.76 122.63 23.99 o 9 6 7 2.80 0.80 17.95 o 10 6 7 226.37 210.21 29.58 o 11 6 7 2.85 -9.07 22.54 o 12 6 7 43.28 17.00 26.92 o 0 7 7 195.69 174.77 31.40 o 1 7 7 10.64 6.84 10.41 o 2 7 7 45.26 42.40 14.48 o 3 7 7 810.58 840.10 34.84 o 4 7 7 68.83 61.04 15.60 o 5 7 7 525.31 515.82 33.88 o 6 7 7 129.90 134.95 21.96 o 7 7 7 86.35 58.82 22.21 o 8 7 7 14.45 -8.87 18.39 o 9 7 7 8.32 -3.99 20.08 o 10 7 7 0.08 -20.61 20.61 o 1 8 7 88.18 62.60 15.36 o 2 8 7 4.74 -7.94 12.82 o 3 8 7 241.38 257.28 22.47 o 4 8 7 102.46 63.60 20.11 o 5 8 7 17.79 15.56 17.47 o 6 8 7 44.58 51.27 24.31 o 7 8 7 49.78 80.99 26.52 o 0 0 8 866.36 716.87 23.83 o 1 0 8 1639.07 1899.79 30.09 o 2 0 8 1864.42 2029.89 37.46 o 3 0 8 406.14 317.97 12.37 o 4 0 8 10546.33 11423.60 131.04 o 5 0 8 8614.33 8317.69 100.69 o 6 0 8 2492.98 2423.40 40.14 o 7 0 8 1444.00 1492.78 34.51 o 8 0 8 3.43 1.06 15.95 o 9 0 8 867.76 916.01 32.14 o 10 0 8 773.36 868.94 79.55 o 11 0 8 60.13 31.34 14.73 o 12 0 8 347.50 409.57 31.69 o 13 0 8 1.63 11.88 18.19 o 14 0 8 36.75 23.80 19.23 o 15 0 8 131.50 100.08 48.95 o 16 0 8 32.33 41.99 23.98 o 1 1 8 375.81 463.62 10.36 o 2 1 8 19.58 17.91 4.15 o 3 1 8 7963.57 8187.97 73.65 o 4 1 8 12.30 5.20 5.88 o 5 1 8 286.58 278.11 10.16 o 6 1 8 1587.71 1524.23 23.00 o 7 1 8 1317.61 1325.18 21.06 o 8 1 8 218.86 216.54 10.47 o 9 1 8 1300.41 1266.21 29.31 o 10 1 8 639.75 600.03 25.19 o 11 1 8 374.43 380.87 24.70 o 12 1 8 79.72 91.01 17.24 o 13 1 8 186.07 208.15 27.39 o 14 1 8 90.58 84.25 22.58 o 15 1 8 1.90 -22.64 29.24 o 16 1 8 3.33 31.69 26.52 o 0 2 8 11.49 41.82 12.26 o 1 2 8 2685.72 2846.51 32.99 o 2 2 8 3452.46 3758.44 42.20 o 3 2 8 8897.47 8723.13 85.49 o 4 2 8 45.89 66.47 5.92 o 5 2 8 4431.41 4015.78 41.65 o 6 2 8 5737.75 5697.35 61.49 o 7 2 8 1399.76 1313.22 31.06 o 8 2 8 1803.76 1754.79 26.77 o 9 2 8 6.37 2.95 8.11 o 10 2 8 1010.23 1030.79 50.97 o 11 2 8 13.75 7.78 11.80 o 12 2 8 343.97 328.86 50.27 o 13 2 8 85.20 67.54 18.33 o 14 2 8 98.85 86.80 23.54 o 15 2 8 150.34 169.99 28.85 o 1 3 8 2368.47 2385.48 44.20 o 2 3 8 1179.64 1211.77 45.78 o 3 3 8 1282.69 1360.76 31.41 o 4 3 8 510.38 461.20 13.61 o 5 3 8 875.16 906.31 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