#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/53/2225322.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225322_Fobs loop_ _publ_author_name 'Keng, Thy Chun' 'Lo, Kong Mun' 'Ng, Seik Weng' _publ_section_title ; catena-Poly[[tris(4-fluorobenzyl)tin(IV)]{\m-[(N,N-diisopropylcarbamothioyl)sulfanyl]acetato-\k^2^O:O'}] ; _journal_coeditor_code LH2996 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m314 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.427 _cell_angle_gamma 90.000 _cell_length_a 11.2496 _cell_length_b 25.7598 _cell_length_c 11.4216 _exptl_crystal_F_000 1384.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file lh2996Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 367.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 36725.70 23921.11 407.88 o 2 0 0 14887.88 9782.39 115.92 o 3 0 0 70968.81 87884.79 1709.15 o 4 0 0 7782.57 5444.94 101.08 o 5 0 0 13956.89 13841.12 194.46 o 6 0 0 16771.49 18104.57 286.18 o 7 0 0 5506.56 5345.04 205.14 o 8 0 0 1053.34 1020.36 128.23 o 9 0 0 5499.41 5645.71 213.84 o 10 0 0 2323.35 2271.68 104.17 o 11 0 0 204.03 372.65 105.12 o 1 1 0 30885.29 34109.39 300.26 o 2 1 0 30229.00 35158.91 292.98 o 3 1 0 1808.20 2094.25 38.16 o 4 1 0 41466.07 44595.82 311.49 o 5 1 0 22075.89 23025.59 225.34 o 6 1 0 27.02 103.10 23.03 o 7 1 0 9623.49 10312.07 185.66 o 8 1 0 3066.60 3026.03 114.13 o 9 1 0 86.70 154.67 32.41 o 10 1 0 1882.79 1982.52 81.57 o 11 1 0 3726.55 3729.01 120.52 o 12 1 0 43.25 35.43 81.26 o 0 2 0 69341.27 51476.48 483.65 o 1 2 0 336.35 495.61 11.28 o 2 2 0 11655.56 18546.23 137.46 o 3 2 0 30270.61 27323.09 206.11 o 4 2 0 9574.27 13250.16 128.11 o 5 2 0 2235.99 2847.04 69.41 o 6 2 0 17942.25 18344.56 235.40 o 7 2 0 8746.23 10448.96 163.35 o 8 2 0 160.01 196.33 32.54 o 9 2 0 5569.93 5594.80 118.11 o 10 2 0 3605.36 3575.62 102.00 o 11 2 0 395.34 667.67 286.02 o 12 2 0 2348.43 2309.93 218.26 o 1 3 0 4585.26 5479.74 53.31 o 2 3 0 20247.89 20140.70 124.91 o 3 3 0 11337.84 12480.16 106.32 o 4 3 0 4792.06 5340.47 67.71 o 5 3 0 16340.13 17148.94 263.00 o 6 3 0 1388.48 1541.56 46.94 o 7 3 0 14264.61 15149.02 250.54 o 8 3 0 6894.05 6896.12 122.27 o 9 3 0 891.12 976.67 61.60 o 10 3 0 3119.29 3157.47 131.80 o 11 3 0 3805.63 3770.85 208.92 o 12 3 0 129.57 413.20 242.50 o 0 4 0 20405.42 24945.49 2049.15 o 1 4 0 23725.88 18736.82 146.84 o 2 4 0 669.56 1560.93 31.45 o 3 4 0 65030.17 74543.41 490.52 o 4 4 0 13824.56 13130.48 119.32 o 5 4 0 349.36 285.10 23.89 o 6 4 0 20253.46 21891.66 242.33 o 7 4 0 9254.46 9146.80 118.59 o 8 4 0 10.81 114.75 26.04 o 9 4 0 824.87 973.43 58.52 o 10 4 0 1967.20 2219.04 180.92 o 11 4 0 767.84 813.76 231.28 o 12 4 0 2261.35 2286.95 182.33 o 13 4 0 852.81 824.70 169.13 o 1 5 0 13714.51 13654.67 137.24 o 2 5 0 7201.41 7078.89 75.13 o 3 5 0 2573.38 2452.25 36.63 o 4 5 0 3118.88 2880.07 46.28 o 5 5 0 6288.13 6562.12 82.53 o 6 5 0 578.84 625.70 32.97 o 7 5 0 4727.21 4783.04 82.33 o 8 5 0 7523.89 7633.93 112.44 o 9 5 0 87.86 34.87 36.10 o 10 5 0 1273.14 1464.51 155.61 o 11 5 0 1618.27 1682.15 404.14 o 12 5 0 230.01 256.82 164.65 o 13 5 0 84.89 634.34 198.05 o 0 6 0 13073.54 12039.30 141.21 o 1 6 0 2956.80 4156.92 73.81 o 2 6 0 719.15 556.18 25.00 o 3 6 0 5814.98 5111.26 88.40 o 4 6 0 795.55 905.39 26.30 o 5 6 0 2718.19 2651.96 48.87 o 6 6 0 4439.08 4322.11 70.18 o 7 6 0 666.72 740.05 39.39 o 8 6 0 1230.49 1323.43 50.56 o 9 6 0 167.37 134.76 65.65 o 10 6 0 2251.64 2330.55 168.40 o 11 6 0 0.20 20.99 68.79 o 12 6 0 346.94 503.40 184.46 o 13 6 0 350.82 743.82 370.09 o 1 7 0 29401.12 31542.96 240.80 o 2 7 0 2181.38 2729.05 46.85 o 3 7 0 78.80 37.88 11.76 o 4 7 0 10745.42 11680.49 120.60 o 5 7 0 2699.67 2338.73 44.64 o 6 7 0 1419.59 1532.58 41.43 o 7 7 0 97.33 109.38 20.34 o 8 7 0 535.92 430.45 46.78 o 9 7 0 76.56 93.35 62.50 o 10 7 0 1241.05 1280.78 243.97 o 11 7 0 541.00 539.11 115.87 o 12 7 0 117.77 178.53 91.80 o 13 7 0 35.84 507.03 323.58 o 0 8 0 7433.37 8032.89 116.97 o 1 8 0 11546.23 11146.32 103.16 o 2 8 0 477.37 599.40 24.11 o 3 8 0 1301.20 1259.42 34.41 o 4 8 0 2949.10 3093.71 55.77 o 5 8 0 197.17 201.29 21.82 o 6 8 0 1297.30 1261.95 40.75 o 7 8 0 888.52 870.64 37.05 o 8 8 0 253.76 315.93 57.02 o 9 8 0 37.50 40.56 58.70 o 10 8 0 1305.32 1603.87 170.75 o 11 8 0 31.83 -14.15 100.92 o 12 8 0 158.37 92.69 79.48 o 1 9 0 1789.44 2184.03 40.86 o 2 9 0 3.77 32.59 23.72 o 3 9 0 458.89 667.45 29.41 o 4 9 0 53.02 -14.73 13.38 o 5 9 0 90.69 98.84 18.76 o 6 9 0 814.97 682.50 28.64 o 7 9 0 56.38 -15.15 32.71 o 8 9 0 138.18 147.36 49.59 o 9 9 0 856.90 728.21 130.83 o 10 9 0 144.77 202.27 164.95 o 11 9 0 407.45 479.55 115.18 o 12 9 0 34.27 133.37 90.29 o 0 10 0 4283.64 4659.24 92.92 o 1 10 0 1838.08 1777.62 39.52 o 2 10 0 54.86 32.04 14.23 o 3 10 0 3.25 4.42 21.27 o 4 10 0 607.14 607.99 29.60 o 5 10 0 25.43 17.85 17.92 o 6 10 0 69.23 69.97 18.79 o 7 10 0 45.65 19.20 36.59 o 8 10 0 443.42 479.42 68.48 o 9 10 0 17.82 6.50 60.48 o 10 10 0 0.94 69.76 71.85 o 11 10 0 0.11 28.94 67.96 o 12 10 0 10.30 147.28 262.99 o 13 10 0 18.22 954.06 195.03 o 1 11 0 1030.54 1057.80 79.14 o 2 11 0 3730.99 3420.47 68.23 o 3 11 0 191.77 248.48 39.87 o 4 11 0 29.99 -5.30 13.78 o 5 11 0 904.39 903.64 51.05 o 6 11 0 820.82 746.41 35.70 o 7 11 0 799.65 912.75 85.54 o 8 11 0 559.96 636.45 77.85 o 9 11 0 9.01 -16.80 56.59 o 10 11 0 263.49 470.80 136.23 o 11 11 0 16.46 -48.59 87.76 o 12 11 0 3.70 202.40 296.88 o 13 11 0 74.81 778.67 448.72 o 0 12 0 1842.90 2111.20 67.81 o 1 12 0 137.91 85.62 14.53 o 2 12 0 685.68 616.86 36.33 o 3 12 0 4.88 -14.12 24.63 o 4 12 0 292.63 284.74 45.53 o 5 12 0 200.88 156.04 21.52 o 6 12 0 628.87 614.55 67.60 o 7 12 0 45.85 14.83 37.75 o 8 12 0 238.71 230.54 58.44 o 9 12 0 302.17 380.71 99.65 o 10 12 0 967.37 886.51 164.11 o 11 12 0 2.66 31.46 104.18 o 12 12 0 108.24 279.70 296.36 o 1 13 0 1944.11 1944.26 53.16 o 2 13 0 4287.50 4320.63 87.06 o 3 13 0 3.39 1.26 27.46 o 4 13 0 375.73 392.95 54.60 o 5 13 0 640.10 625.94 67.61 o 6 13 0 24.53 12.82 32.45 o 7 13 0 291.52 254.40 57.15 o 8 13 0 1644.11 1467.70 104.83 o 9 13 0 105.37 54.23 65.84 o 10 13 0 72.06 103.09 81.91 o 11 13 0 184.81 191.91 146.71 o 12 13 0 85.62 336.12 197.05 o 0 14 0 5506.53 5740.24 181.33 o 1 14 0 75.77 79.69 20.94 o 2 14 0 3128.97 3127.57 75.58 o 3 14 0 4635.11 4580.13 84.86 o 4 14 0 413.01 378.47 53.17 o 5 14 0 1477.63 1336.26 84.91 o 6 14 0 18.04 3.52 34.54 o 7 14 0 511.98 619.24 76.68 o 8 14 0 264.72 265.82 97.38 o 9 14 0 4.86 2.75 86.56 o 10 14 0 265.36 228.51 126.23 o 11 14 0 12.34 -0.66 71.32 o 12 14 0 135.62 479.87 354.53 o 1 15 0 6387.55 6195.64 101.38 o 2 15 0 8312.95 8441.13 132.59 o 3 15 0 33.05 19.23 19.21 o 4 15 0 2619.90 2575.95 108.12 o 5 15 0 117.91 139.96 44.05 o 6 15 0 12.02 14.52 36.90 o 7 15 0 3485.11 3306.66 136.40 o 8 15 0 1983.88 1837.72 197.72 o 9 15 0 115.28 139.29 118.13 o 10 15 0 71.91 100.84 84.98 o 11 15 0 350.77 364.51 125.91 o 12 15 0 97.05 375.81 429.23 o 0 16 0 2758.96 2601.59 86.31 o 1 16 0 599.74 517.10 40.93 o 2 16 0 1832.94 1835.10 66.50 o 3 16 0 4310.04 3788.39 98.01 o 4 16 0 1922.23 1875.97 103.30 o 5 16 0 622.22 623.30 71.30 o 6 16 0 1068.64 1022.46 93.31 o 7 16 0 2731.49 2854.55 135.52 o 8 16 0 0.82 32.77 93.17 o 9 16 0 487.33 520.27 112.97 o 10 16 0 280.01 312.17 127.10 o 11 16 0 31.73 222.32 218.19 o 12 16 0 439.60 1805.49 241.49 o 1 17 0 1349.91 1329.69 57.43 o 2 17 0 7932.29 7661.31 132.52 o 3 17 0 978.04 1060.88 81.89 o 4 17 0 838.69 815.85 78.66 o 5 17 0 8947.06 8374.21 203.88 o 6 17 0 3193.25 2982.54 152.75 o 7 17 0 1668.06 1564.06 102.79 o 8 17 0 2084.65 2010.49 167.91 o 9 17 0 128.19 204.37 109.54 o 10 17 0 712.18 809.47 248.65 o 11 17 0 1147.97 1372.31 401.85 o 0 18 0 5406.09 5118.40 128.67 o 1 18 0 1315.35 1210.10 57.99 o 2 18 0 54.07 47.95 24.44 o 3 18 0 3528.89 3422.34 123.12 o 4 18 0 2474.90 2429.41 111.90 o 5 18 0 368.20 382.47 62.49 o 6 18 0 2373.10 2140.07 114.47 o 7 18 0 1968.89 1836.31 111.77 o 8 18 0 88.20 157.95 76.58 o 9 18 0 2746.41 2572.14 194.93 o 10 18 0 1342.49 1689.65 536.23 o 11 18 0 11.72 372.50 232.01 o 1 19 0 4166.51 3880.81 96.31 o 2 19 0 4669.17 4292.16 101.25 o 3 19 0 303.30 297.70 54.50 o 4 19 0 7635.71 7569.38 192.93 o 5 19 0 6953.19 6960.94 212.70 o 6 19 0 262.85 295.10 62.54 o 7 19 0 2357.48 2188.95 222.66 o 8 19 0 2462.07 2193.51 175.32 o 9 19 0 65.67 146.33 90.50 o 10 19 0 823.94 985.27 308.74 o 11 19 0 1103.36 1366.85 524.48 o 0 20 0 16457.96 15594.92 360.52 o 1 20 0 4791.58 4708.51 108.95 o 2 20 0 1301.53 1307.52 94.60 o 3 20 0 6508.44 6226.36 171.89 o 4 20 0 580.57 644.00 76.76 o 5 20 0 1929.78 1851.94 111.14 o 6 20 0 1985.57 1883.49 112.00 o 7 20 0 803.74 870.76 133.71 o 8 20 0 451.04 464.75 111.90 o 9 20 0 1241.03 1218.86 464.82 o 10 20 0 523.91 1333.75 283.43 o 1 21 0 9095.81 9098.50 230.36 o 2 21 0 6500.00 6695.06 229.31 o 3 21 0 16.87 113.75 46.36 o 4 21 0 8615.02 7935.72 205.24 o 5 21 0 1413.58 1503.20 111.00 o 6 21 0 6.68 95.10 66.61 o 7 21 0 2357.78 2252.15 180.70 o 8 21 0 1957.87 1941.60 186.78 o 9 21 0 31.06 123.45 87.02 o 10 21 0 394.57 1138.97 239.39 o 0 22 0 3127.52 3154.66 168.65 o 1 22 0 177.92 278.50 73.67 o 2 22 0 4055.67 4130.10 187.81 o 3 22 0 8663.59 8216.69 263.43 o 4 22 0 305.03 459.98 98.70 o 5 22 0 139.90 152.12 77.54 o 6 22 0 3765.67 3474.09 208.92 o 7 22 0 1372.14 1349.51 168.02 o 8 22 0 281.04 352.10 102.26 o 9 22 0 995.06 997.08 190.27 o 10 22 0 327.87 1291.14 257.33 o 1 23 0 2740.74 2661.65 157.23 o 2 23 0 4087.18 4176.79 229.95 o 3 23 0 186.30 283.43 80.23 o 4 23 0 996.04 782.54 121.15 o 5 23 0 1600.07 1613.10 171.08 o 6 23 0 73.83 193.35 78.70 o 7 23 0 1435.80 1254.95 161.05 o 8 23 0 2769.42 2610.95 200.90 o 9 23 0 144.37 380.37 108.95 o 10 23 0 738.29 1488.08 230.67 o 0 24 0 3515.55 3871.48 433.91 o 1 24 0 1099.82 1106.30 120.09 o 2 24 0 20.55 123.32 66.11 o 3 24 0 1625.17 1499.65 136.68 o 4 24 0 854.38 968.43 136.87 o 5 24 0 127.09 209.57 81.77 o 6 24 0 2467.16 2298.10 183.00 o 7 24 0 1322.76 1244.59 164.20 o 8 24 0 28.97 157.64 82.35 o 9 24 0 901.53 828.30 182.04 o 1 25 0 1714.53 1888.55 143.72 o 2 25 0 1156.48 1056.54 126.59 o 3 25 0 45.02 82.75 71.90 o 4 25 0 2462.32 2366.68 190.37 o 5 25 0 1654.89 1569.23 184.52 o 6 25 0 86.74 200.60 170.24 o 7 25 0 506.65 513.31 116.55 o 8 25 0 683.18 679.20 132.61 o 9 25 0 29.56 457.34 253.53 o 0 26 0 3786.31 3945.73 455.64 o 1 26 0 941.08 1049.07 125.60 o 2 26 0 51.97 14.40 78.38 o 3 26 0 1990.83 1901.11 161.38 o 4 26 0 521.16 607.29 112.75 o 5 26 0 768.53 766.38 135.45 o 6 26 0 672.12 646.99 171.56 o 7 26 0 129.63 176.39 93.97 o 8 26 0 201.17 341.22 209.19 o 1 27 0 617.11 570.59 196.64 o 2 27 0 783.57 959.87 129.96 o 3 27 0 12.33 115.58 75.87 o 4 27 0 1049.79 1115.22 146.02 o 5 27 0 609.90 676.64 119.05 o 6 27 0 141.50 299.23 98.03 o 7 27 0 190.82 245.25 95.09 o 8 27 0 130.59 314.89 209.00 o 0 28 0 261.91 270.63 240.76 o 1 28 0 186.33 300.26 176.08 o 2 28 0 1.22 69.48 72.93 o 3 28 0 436.07 390.11 130.77 o 4 28 0 105.13 141.64 106.81 o 5 28 0 0.09 15.11 128.52 o 6 28 0 220.81 280.23 135.72 o 7 28 0 301.32 381.40 113.40 o 1 29 0 10.29 44.47 148.99 o 2 29 0 168.79 128.23 161.56 o 3 29 0 26.25 19.72 139.48 o 4 29 0 55.14 101.15 78.63 o 5 29 0 38.72 77.21 143.49 o 6 29 0 73.23 150.41 165.06 o 7 29 0 88.35 236.48 139.18 o 0 30 0 7.89 188.32 240.04 o 1 30 0 3.30 149.27 164.41 o 2 30 0 24.08 127.48 160.55 o 3 30 0 1.41 22.08 144.49 o 4 30 0 50.71 -50.00 114.67 o 5 30 0 16.83 91.35 153.84 o 6 30 0 2.30 125.18 277.90 o 1 31 0 40.87 119.46 165.81 o 2 31 0 0.14 85.97 160.87 o 3 31 0 8.70 113.56 167.55 o 4 31 0 7.52 47.36 84.80 o 5 31 0 35.03 -52.05 87.67 o 0 32 0 69.32 108.04 233.41 o 1 32 0 7.77 105.38 156.58 o 2 32 0 0.49 150.20 154.15 o 3 32 0 2.78 227.60 192.95 o 4 32 0 84.86 238.73 367.80 o 1 33 0 33.22 225.46 168.75 o 2 33 0 55.57 285.10 173.91 o -12 1 1 143.30 139.15 96.00 o -11 1 1 181.85 140.75 36.22 o -10 1 1 246.71 254.97 34.82 o -9 1 1 265.32 150.58 27.96 o -8 1 1 0.01 4.81 21.29 o -7 1 1 2108.16 2613.21 69.21 o -6 1 1 5.06 -8.89 15.32 o -5 1 1 590.86 490.43 31.42 o -4 1 1 2745.90 4039.63 78.00 o -3 1 1 4264.46 2267.99 49.10 o -2 1 1 1412.24 317.90 22.28 o -1 1 1 2201.49 202.71 13.26 o 0 1 1 2342.74 226.99 9.97 o 1 1 1 13593.51 8613.31 69.78 o 2 1 1 3272.84 6437.38 66.70 o 3 1 1 1698.58 1238.75 32.18 o 4 1 1 103.01 396.81 24.97 o 5 1 1 431.87 325.84 25.99 o 6 1 1 20.58 37.84 17.26 o 7 1 1 480.82 551.14 39.98 o 8 1 1 721.78 625.07 45.65 o 9 1 1 58.55 93.94 32.54 o 10 1 1 17.32 12.48 43.69 o 11 1 1 18.83 -24.30 70.18 o -12 2 1 90.49 -52.85 48.79 o -11 2 1 10.60 2.15 33.33 o -10 2 1 1.63 -17.33 21.94 o -9 2 1 721.53 647.36 52.92 o -8 2 1 7693.26 8182.71 150.81 o -7 2 1 285.65 339.38 34.34 o -6 2 1 3689.65 3849.84 79.31 o -5 2 1 5133.86 5777.76 90.37 o -4 2 1 233.73 246.54 21.75 o -3 2 1 29277.07 33066.77 472.50 o -2 2 1 2569.19 2970.21 61.58 o -1 2 1 164.51 184.70 17.22 o 0 2 1 9445.11 9713.14 170.16 o 1 2 1 18667.89 19928.24 119.34 o 2 2 1 240.33 379.19 19.42 o 3 2 1 1.56 4.32 10.07 o 4 2 1 3598.68 3223.05 58.04 o 5 2 1 1187.26 1320.33 42.37 o 6 2 1 531.40 587.81 37.57 o 7 2 1 44.79 35.06 20.37 o 8 2 1 3.21 -4.70 19.66 o 9 2 1 91.47 75.51 33.07 o 10 2 1 77.76 95.38 46.20 o 11 2 1 420.65 434.92 123.03 o 12 2 1 10.87 60.90 89.26 o -13 3 1 138.89 57.03 89.56 o -12 3 1 523.20 558.54 139.62 o -11 3 1 54.80 95.50 47.55 o -10 3 1 1424.11 1354.79 69.46 o -9 3 1 1083.43 1211.27 61.43 o -8 3 1 803.14 840.68 53.55 o -7 3 1 2674.97 2563.60 69.64 o -6 3 1 736.53 999.60 44.01 o -5 3 1 5067.26 6132.44 91.74 o -4 3 1 13954.01 13091.24 136.98 o -3 3 1 27935.57 37041.96 395.71 o -2 3 1 784.37 175.28 31.54 o -1 3 1 28908.21 23023.19 206.63 o 0 3 1 3169.09 6819.62 91.02 o 1 3 1 0.66 444.03 27.81 o 2 3 1 17021.06 14815.23 157.32 o 3 3 1 374.06 555.64 24.44 o 4 3 1 2827.87 3635.54 61.27 o 5 3 1 4297.59 3813.80 68.50 o 6 3 1 1425.35 1433.90 47.97 o 7 3 1 27.59 29.25 19.81 o 8 3 1 35.57 -7.17 23.43 o 9 3 1 476.30 504.64 54.15 o 10 3 1 0.21 50.15 61.02 o 11 3 1 248.41 253.04 150.57 o 12 3 1 290.21 409.48 124.70 o -13 4 1 2.13 845.32 182.54 o -12 4 1 1006.01 993.31 154.71 o -11 4 1 749.92 855.80 175.76 o -10 4 1 0.16 -13.61 26.49 o -9 4 1 1252.72 1341.68 78.37 o -8 4 1 1356.41 1396.92 58.85 o -7 4 1 216.49 223.61 29.56 o -6 4 1 2972.67 3050.04 68.65 o -5 4 1 975.49 1057.16 39.29 o -4 4 1 106.03 44.65 13.67 o -3 4 1 24875.49 26186.60 394.92 o -2 4 1 512.52 562.71 28.05 o -1 4 1 10042.91 10121.98 110.50 o 0 4 1 6199.69 6846.55 74.29 o 1 4 1 199.24 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