#------------------------------------------------------------------------------ #$Date: 2010-04-11 15:29:29 +0300 (Sun, 11 Apr 2010) $ #$Revision: 1088 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2225327.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225327_Fobs loop_ _publ_author_name 'Liu, Ping' 'Zhong, Wu' 'Chen, Pengfei' 'Yang, Xiaohong' 'Li, Song' _publ_section_title ; (1R*,2R*)-1-(7-Bromo-3-methoxynaphthalen-2-yl)-4-(dimethylamino)-2-(naphthalen-1-yl)-1-phenylbutan-2-ol ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o636 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.863 _cell_angle_gamma 90.000 _cell_length_a 12.7163 _cell_length_b 12.5051 _cell_length_c 17.7709 _exptl_crystal_F_000 1152.00 _reflns_d_resolution_high 0.7596 _[local]_cod_data_source_file nc2176Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' M100128E1 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 266.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2429.60 2618.37 81.90 o 4 0 0 18746.46 17473.68 276.90 o 6 0 0 319.69 209.30 19.81 o 8 0 0 102.58 198.55 57.50 o 10 0 0 4110.73 3966.61 131.62 o 12 0 0 1636.53 1619.89 99.37 o 14 0 0 1664.64 1726.72 85.46 o 1 1 0 21.89 22.89 5.48 o 2 1 0 3345.35 3372.86 61.58 o 3 1 0 710.85 688.71 15.95 o 4 1 0 6660.62 6364.01 49.21 o 5 1 0 10.86 30.34 5.12 o 6 1 0 682.32 593.08 16.72 o 7 1 0 947.04 961.07 30.34 o 8 1 0 85.92 66.27 7.91 o 9 1 0 542.71 535.56 24.00 o 10 1 0 578.18 498.60 39.84 o 11 1 0 3.61 15.16 14.57 o 12 1 0 853.67 919.83 49.66 o 13 1 0 242.28 211.25 63.86 o 14 1 0 80.89 80.29 32.49 o 15 1 0 7.12 14.44 18.22 o 0 2 0 14599.89 14278.25 399.01 o 1 2 0 9416.73 9467.65 70.69 o 2 2 0 15142.44 14583.46 157.56 o 3 2 0 10.35 11.99 3.96 o 4 2 0 4020.61 3755.48 131.23 o 5 2 0 3481.21 3465.22 84.60 o 6 2 0 3429.06 3455.60 70.60 o 7 2 0 890.61 1090.34 36.55 o 8 2 0 187.80 192.46 23.14 o 9 2 0 520.48 497.92 32.53 o 10 2 0 484.54 536.47 32.11 o 11 2 0 148.94 157.64 33.61 o 12 2 0 8.91 14.08 12.46 o 13 2 0 13.03 23.46 12.90 o 14 2 0 878.58 943.50 43.67 o 15 2 0 207.31 164.07 77.26 o 1 3 0 50.49 67.45 11.02 o 2 3 0 12554.03 12205.25 192.58 o 3 3 0 24437.95 24416.26 256.85 o 4 3 0 18.22 26.80 4.60 o 5 3 0 271.60 225.65 14.15 o 6 3 0 16.29 24.67 8.71 o 7 3 0 4468.97 4630.74 86.23 o 8 3 0 719.90 752.49 50.39 o 9 3 0 31.18 44.23 21.21 o 10 3 0 31.47 42.85 14.15 o 11 3 0 1117.34 1189.04 43.93 o 12 3 0 87.72 68.06 22.79 o 13 3 0 802.86 857.86 57.45 o 14 3 0 48.33 19.55 22.47 o 15 3 0 267.36 173.75 75.68 o 0 4 0 13.01 14.53 5.36 o 1 4 0 14149.95 14233.15 108.79 o 2 4 0 1524.99 1471.43 22.88 o 3 4 0 3941.70 3794.17 48.54 o 4 4 0 919.24 884.61 40.33 o 5 4 0 5036.25 4923.31 67.57 o 6 4 0 105.02 92.54 30.13 o 7 4 0 277.86 298.34 33.39 o 8 4 0 226.79 239.25 54.43 o 9 4 0 2968.40 3176.28 144.76 o 10 4 0 86.42 100.98 28.05 o 11 4 0 201.74 218.41 52.58 o 12 4 0 0.21 14.42 14.53 o 13 4 0 355.85 369.86 89.02 o 14 4 0 107.36 89.64 30.64 o 15 4 0 760.96 702.12 50.47 o 1 5 0 7282.82 6994.67 99.74 o 2 5 0 337.42 326.93 9.95 o 3 5 0 14665.13 15699.74 255.77 o 4 5 0 2361.94 2713.15 60.24 o 5 5 0 112.77 111.38 15.31 o 6 5 0 873.29 916.89 36.20 o 7 5 0 6248.32 6422.52 154.42 o 8 5 0 28.20 25.67 13.59 o 9 5 0 175.89 210.43 50.44 o 10 5 0 859.38 806.99 44.63 o 11 5 0 2099.28 2092.45 103.28 o 12 5 0 281.55 228.71 74.62 o 13 5 0 239.11 244.76 77.56 o 14 5 0 278.45 228.43 74.44 o 0 6 0 1103.00 1134.00 33.81 o 1 6 0 3151.21 3064.24 50.39 o 2 6 0 587.50 656.84 18.37 o 3 6 0 2489.26 2494.61 47.41 o 4 6 0 161.45 135.04 19.39 o 5 6 0 1724.60 1598.82 41.70 o 6 6 0 116.58 117.85 19.24 o 7 6 0 285.08 299.03 26.10 o 8 6 0 247.48 257.03 87.60 o 9 6 0 218.63 232.08 68.10 o 10 6 0 1072.35 1065.16 50.58 o 11 6 0 687.89 626.86 67.47 o 12 6 0 27.49 33.38 19.38 o 13 6 0 8.33 -2.91 17.77 o 14 6 0 208.07 162.97 76.28 o 1 7 0 3521.32 3525.60 52.29 o 2 7 0 4108.74 4204.65 156.34 o 3 7 0 912.55 798.18 32.93 o 4 7 0 68.48 58.31 15.23 o 5 7 0 756.06 786.14 31.84 o 6 7 0 1770.13 1763.48 51.90 o 7 7 0 2856.26 2820.91 61.22 o 8 7 0 1142.29 1148.21 49.31 o 9 7 0 497.19 477.53 54.12 o 10 7 0 106.56 131.27 49.04 o 11 7 0 161.79 185.30 66.35 o 12 7 0 314.79 361.31 56.11 o 13 7 0 328.44 234.66 117.35 o 14 7 0 0.54 8.57 15.32 o 0 8 0 10379.14 10972.62 195.37 o 1 8 0 2562.54 2608.47 59.04 o 2 8 0 1150.63 1246.49 38.22 o 3 8 0 136.13 144.87 38.86 o 4 8 0 6558.42 6556.66 127.02 o 5 8 0 3141.68 2993.54 89.92 o 6 8 0 337.44 344.65 20.30 o 7 8 0 123.89 143.90 51.63 o 8 8 0 651.84 578.29 47.45 o 9 8 0 167.57 188.15 46.97 o 10 8 0 994.25 997.22 46.74 o 11 8 0 158.41 133.44 65.51 o 12 8 0 0.51 13.48 16.29 o 13 8 0 45.05 25.08 27.32 o 1 9 0 373.91 384.67 22.73 o 2 9 0 3955.85 4109.43 79.92 o 3 9 0 10.96 11.18 13.10 o 4 9 0 4365.13 4367.81 113.92 o 5 9 0 2.37 -4.19 20.12 o 6 9 0 2252.13 2297.71 81.91 o 7 9 0 253.94 224.89 61.24 o 8 9 0 597.12 580.17 47.05 o 9 9 0 11.55 18.35 13.03 o 10 9 0 81.49 59.28 28.73 o 11 9 0 43.54 33.19 23.17 o 12 9 0 632.64 581.29 111.07 o 13 9 0 0.76 0.87 30.85 o 0 10 0 4951.49 5108.42 160.37 o 1 10 0 611.20 655.13 30.33 o 2 10 0 255.85 244.48 32.84 o 3 10 0 33.67 47.87 16.14 o 4 10 0 1413.05 1310.45 56.86 o 5 10 0 6.21 0.23 15.23 o 6 10 0 67.27 82.17 24.70 o 7 10 0 2.99 5.67 17.88 o 8 10 0 1074.31 1035.02 51.00 o 9 10 0 23.77 38.60 24.01 o 10 10 0 1819.67 1842.98 99.69 o 11 10 0 274.25 235.61 120.31 o 12 10 0 1.46 5.55 36.87 o 1 11 0 2635.06 2577.22 79.55 o 2 11 0 7344.51 7651.24 269.55 o 3 11 0 84.38 103.09 36.68 o 4 11 0 282.80 293.25 35.29 o 5 11 0 116.52 89.80 33.42 o 6 11 0 462.13 548.22 54.77 o 7 11 0 443.50 438.43 39.00 o 8 11 0 1332.35 1256.67 48.37 o 9 11 0 30.65 14.38 16.20 o 10 11 0 291.32 281.56 110.23 o 11 11 0 738.30 786.38 98.88 o 0 12 0 54.03 68.47 20.27 o 1 12 0 2039.32 2092.92 71.85 o 2 12 0 5.81 10.78 11.64 o 3 12 0 529.23 524.63 31.02 o 4 12 0 851.63 856.08 39.82 o 5 12 0 1028.56 1031.80 48.70 o 6 12 0 145.23 137.37 63.20 o 7 12 0 1.71 15.07 9.53 o 8 12 0 489.05 536.55 56.97 o 9 12 0 106.22 100.55 46.20 o 10 12 0 240.52 183.09 92.60 o 1 13 0 92.48 102.99 30.68 o 2 13 0 972.81 995.40 38.26 o 3 13 0 1295.90 1348.45 73.93 o 4 13 0 46.30 75.60 30.20 o 5 13 0 345.91 327.55 53.25 o 6 13 0 60.09 39.32 19.81 o 7 13 0 888.88 1047.87 70.52 o 8 13 0 635.39 767.57 89.03 o 9 13 0 9.72 -13.52 36.15 o 0 14 0 124.47 88.62 43.64 o 1 14 0 1923.40 2098.11 53.24 o 2 14 0 178.81 185.72 30.63 o 3 14 0 221.46 206.59 79.04 o 4 14 0 7.77 10.94 19.22 o 5 14 0 1733.18 1884.54 89.96 o 6 14 0 19.53 46.95 41.00 o 7 14 0 2.92 0.55 26.67 o 8 14 0 15.06 13.64 22.17 o 1 15 0 670.01 652.12 51.36 o 2 15 0 156.91 127.41 50.14 o 3 15 0 609.78 669.52 57.09 o 4 15 0 0.16 16.48 19.73 o 5 15 0 301.14 247.08 112.68 o 6 15 0 42.32 29.81 30.39 o 0 16 0 978.72 980.30 120.02 o 1 16 0 1290.81 1431.17 113.07 o 2 16 0 92.07 76.20 34.93 o 3 16 0 180.83 107.87 89.07 o -15 0 1 10.30 23.53 21.63 o -13 0 1 3539.75 3599.21 115.95 o -11 0 1 589.28 597.46 40.66 o -9 0 1 2875.93 2934.36 97.53 o -7 0 1 3931.73 3400.81 148.43 o -5 0 1 815.78 906.77 51.76 o -3 0 1 30211.52 28127.71 117.95 o 1 0 1 36051.77 32395.14 307.47 o 3 0 1 19392.65 17382.08 151.94 o 5 0 1 20330.54 22173.78 803.15 o 7 0 1 12369.42 13583.09 149.10 o 9 0 1 77.27 90.92 32.63 o 11 0 1 1645.29 1600.65 95.74 o 13 0 1 49.29 24.17 19.62 o 15 0 1 1153.15 1252.78 100.20 o -15 1 1 698.59 694.83 44.93 o -14 1 1 1.92 -1.25 16.58 o -13 1 1 291.32 337.38 71.22 o -12 1 1 107.77 114.51 33.89 o -11 1 1 1496.00 1589.37 65.02 o -10 1 1 571.08 486.66 29.65 o -9 1 1 3236.10 3247.48 59.35 o -8 1 1 9.99 11.03 3.25 o -7 1 1 422.27 375.65 18.57 o -6 1 1 1637.09 1785.85 32.23 o -5 1 1 3141.22 2841.38 57.20 o -4 1 1 199.32 193.71 8.60 o -3 1 1 32486.82 30426.47 359.46 o -2 1 1 12715.53 12036.50 42.48 o -1 1 1 782.74 837.11 11.03 o 0 1 1 311.39 297.44 7.43 o 1 1 1 3212.02 3067.20 43.42 o 2 1 1 17636.49 16185.68 169.70 o 3 1 1 2844.84 2845.23 25.44 o 4 1 1 23.67 33.40 5.53 o 5 1 1 5403.98 5151.98 51.81 o 6 1 1 5750.51 6546.47 79.08 o 7 1 1 689.29 718.49 23.62 o 8 1 1 1256.73 1283.27 36.46 o 9 1 1 4841.05 5072.47 176.10 o 10 1 1 37.76 51.01 15.09 o 11 1 1 522.23 535.98 36.67 o 12 1 1 5.76 16.09 10.70 o 13 1 1 40.51 46.36 19.74 o 14 1 1 349.28 287.90 50.82 o 15 1 1 68.62 50.04 19.06 o -15 2 1 97.87 72.15 41.67 o -14 2 1 2.03 -8.93 16.86 o -13 2 1 1194.35 1217.86 55.58 o -12 2 1 277.39 347.42 85.41 o -11 2 1 279.75 318.92 52.48 o -10 2 1 143.50 161.66 36.25 o -9 2 1 403.71 356.67 21.25 o -8 2 1 772.72 774.34 46.80 o -7 2 1 969.97 940.12 47.41 o -6 2 1 124.19 136.28 33.95 o -5 2 1 22.37 35.44 7.45 o -4 2 1 1653.90 1524.21 24.36 o -3 2 1 986.28 847.20 16.39 o -2 2 1 325.48 300.10 5.78 o -1 2 1 471.43 417.46 6.95 o 0 2 1 10854.38 10014.27 70.47 o 1 2 1 13569.42 12671.32 87.68 o 2 2 1 15110.60 14490.71 181.16 o 3 2 1 401.36 389.23 15.04 o 4 2 1 561.12 630.13 11.00 o 5 2 1 5080.15 5234.78 112.61 o 6 2 1 336.88 262.99 13.92 o 7 2 1 3035.95 3239.27 104.53 o 8 2 1 275.00 241.65 26.37 o 9 2 1 252.16 292.90 61.11 o 10 2 1 316.25 322.04 34.60 o 11 2 1 1652.91 1724.48 52.51 o 12 2 1 876.87 915.44 41.88 o 13 2 1 367.18 412.54 86.66 o 14 2 1 520.05 424.30 61.33 o 15 2 1 12.13 16.41 13.05 o -15 3 1 145.67 109.95 54.80 o -14 3 1 703.14 776.92 48.25 o -13 3 1 30.82 33.12 20.01 o -12 3 1 215.93 239.12 63.08 o -11 3 1 518.16 560.12 42.54 o -10 3 1 1014.10 959.15 33.92 o -9 3 1 2030.76 1989.08 78.58 o -8 3 1 9.19 8.03 11.35 o -7 3 1 29.56 66.30 20.67 o -6 3 1 4153.04 4225.40 149.77 o -5 3 1 4905.03 5001.96 82.26 o -4 3 1 359.58 295.61 9.86 o -3 3 1 1045.28 1025.32 18.06 o -2 3 1 16792.31 16291.50 125.54 o -1 3 1 122.34 127.71 4.99 o 0 3 1 21335.91 19816.22 297.03 o 1 3 1 20753.38 20185.07 192.25 o 2 3 1 81.72 94.26 9.43 o 3 3 1 150.97 119.52 9.90 o 4 3 1 10604.87 11213.24 229.93 o 5 3 1 6019.31 6181.49 112.40 o 6 3 1 783.03 774.06 35.14 o 7 3 1 17.50 23.08 11.86 o 8 3 1 1930.06 1900.26 67.21 o 9 3 1 1165.66 1184.95 60.04 o 10 3 1 758.69 835.09 37.75 o 11 3 1 429.04 406.05 42.38 o 12 3 1 485.99 494.87 42.70 o 13 3 1 622.81 597.66 45.13 o 14 3 1 391.15 340.83 97.55 o 15 3 1 4.88 14.71 17.07 o -15 4 1 143.06 109.08 64.45 o -14 4 1 15.38 31.38 17.20 o -13 4 1 8.72 12.16 13.69 o -12 4 1 1966.67 2079.08 99.42 o -11 4 1 361.55 396.77 70.69 o -10 4 1 20.40 37.47 19.20 o -9 4 1 314.35 314.17 66.19 o -8 4 1 5708.33 5857.64 300.16 o -7 4 1 309.78 318.34 25.04 o -6 4 1 577.93 540.55 28.53 o -5 4 1 477.21 542.84 17.54 o -4 4 1 2457.54 2295.20 33.84 o -3 4 1 6178.02 6814.81 84.02 o -2 4 1 13203.68 12964.83 119.14 o -1 4 1 522.56 515.60 11.43 o 0 4 1 703.07 712.68 13.83 o 1 4 1 3350.85 3387.59 22.60 o 2 4 1 11829.04 11490.53 128.99 o 3 4 1 1718.45 1990.83 22.12 o 4 4 1 466.27 508.15 19.66 o 5 4 1 212.73 205.01 16.87 o 6 4 1 5083.17 5203.98 85.87 o 7 4 1 46.96 72.08 21.43 o 8 4 1 2662.28 2705.17 89.46 o 9 4 1 1366.96 1347.05 55.70 o 10 4 1 302.19 324.85 41.08 o 11 4 1 2.20 19.97 12.60 o 12 4 1 1352.52 1366.19 61.92 o 13 4 1 428.67 370.68 53.74 o 14 4 1 14.67 19.28 13.22 o -15 5 1 186.10 142.54 61.99 o -14 5 1 1822.19 1968.56 81.62 o -13 5 1 1.29 20.18 13.73 o -12 5 1 121.36 120.43 36.30 o -11 5 1 3.41 10.23 17.39 o -10 5 1 1298.43 1366.03 73.31 o -9 5 1 1544.30 1513.04 59.74 o -8 5 1 173.00 169.74 50.92 o -7 5 1 47.75 39.90 14.10 o -6 5 1 4743.15 4756.34 138.67 o -5 5 1 0.49 7.03 4.71 o -4 5 1 7960.24 7788.95 112.56 o -3 5 1 6933.45 7425.59 87.06 o -2 5 1 10254.37 10869.78 151.07 o -1 5 1 213.78 193.56 7.66 o 0 5 1 11188.65 10788.83 197.69 o 1 5 1 554.22 537.97 11.18 o 2 5 1 4459.05 4667.31 82.05 o 3 5 1 4430.65 5029.34 68.64 o 4 5 1 17353.69 18310.89 399.57 o 5 5 1 48.52 79.87 19.53 o 6 5 1 4186.98 4221.57 88.40 o 7 5 1 245.84 309.81 58.70 o 8 5 1 13675.03 13539.45 519.02 o 9 5 1 43.21 54.39 19.62 o 10 5 1 40.59 31.68 13.11 o 11 5 1 88.47 67.56 27.92 o 12 5 1 180.63 165.97 56.04 o 13 5 1 9.04 8.85 14.55 o 14 5 1 101.00 110.10 43.06 o -14 6 1 240.41 151.98 69.39 o -13 6 1 67.49 73.96 28.09 o -12 6 1 438.89 461.11 110.55 o -11 6 1 19.02 42.40 21.97 o -10 6 1 349.53 309.85 46.35 o -9 6 1 787.79 751.82 43.11 o -8 6 1 96.79 101.58 28.30 o -7 6 1 10.25 16.78 8.83 o -6 6 1 716.02 745.42 34.37 o -5 6 1 218.90 266.94 15.62 o -4 6 1 296.42 225.71 16.14 o -3 6 1 1494.05 1398.93 40.57 o -2 6 1 19804.72 20869.61 386.84 o -1 6 1 3131.44 3268.84 44.40 o 0 6 1 475.07 451.26 14.33 o 1 6 1 2412.70 2498.49 59.29 o 2 6 1 2633.82 2520.27 53.22 o 3 6 1 241.88 222.28 14.24 o 4 6 1 3155.05 3638.06 55.54 o 5 6 1 655.61 691.69 29.52 o 6 6 1 3744.77 3693.53 96.60 o 7 6 1 178.27 163.88 7.98 o 8 6 1 783.19 780.23 63.75 o 9 6 1 284.26 259.02 67.45 o 10 6 1 854.86 757.33 48.36 o 11 6 1 616.36 554.50 52.81 o 12 6 1 721.37 688.58 57.97 o 13 6 1 101.77 74.84 32.54 o 14 6 1 191.41 135.91 48.62 o -14 7 1 1058.87 1105.01 73.89 o -13 7 1 236.72 174.11 84.82 o -12 7 1 3.93 10.51 22.03 o -11 7 1 187.58 200.02 68.65 o -10 7 1 1213.39 1178.07 66.70 o -9 7 1 656.36 632.27 35.34 o -8 7 1 114.17 113.87 36.66 o -7 7 1 297.62 251.01 23.01 o -6 7 1 1437.91 1472.98 45.10 o -5 7 1 2026.22 2138.36 68.86 o -4 7 1 2861.64 3052.99 104.16 o -3 7 1 14.46 18.66 11.60 o -2 7 1 508.66 473.40 16.41 o -1 7 1 398.40 343.23 14.07 o 0 7 1 4977.33 5026.54 64.69 o 1 7 1 1098.46 997.90 37.17 o 2 7 1 1314.46 1456.49 33.79 o 3 7 1 1085.57 1069.28 40.94 o 4 7 1 1960.82 1908.63 63.11 o 5 7 1 147.36 119.09 31.61 o 6 7 1 429.35 441.29 59.55 o 7 7 1 1168.32 1115.33 37.48 o 8 7 1 1196.36 1172.44 52.43 o 9 7 1 485.38 487.49 44.26 o 10 7 1 1855.58 1716.96 96.58 o 11 7 1 194.63 135.81 62.15 o 12 7 1 138.48 146.92 58.58 o 13 7 1 268.86 252.61 54.41 o -13 8 1 638.52 653.03 52.61 o -12 8 1 516.75 496.54 41.20 o -11 8 1 374.39 366.52 113.75 o -10 8 1 252.93 208.14 62.55 o -9 8 1 1100.62 961.14 76.15 o -8 8 1 224.01 198.14 73.72 o -7 8 1 4938.14 4819.19 152.76 o -6 8 1 24.30 22.77 8.23 o -5 8 1 123.41 127.11 16.89 o -4 8 1 819.51 758.89 40.40 o -3 8 1 3455.53 3507.66 79.30 o -2 8 1 1412.21 1462.65 43.66 o -1 8 1 6173.44 6370.19 134.70 o 0 8 1 1118.82 1120.95 29.33 o 1 8 1 2365.45 2406.97 57.44 o 2 8 1 3776.04 3905.77 81.75 o 3 8 1 5579.66 5640.31 245.98 o 4 8 1 470.45 483.11 25.04 o 5 8 1 1107.56 1017.44 43.00 o 6 8 1 102.84 103.60 26.28 o 7 8 1 1327.76 1440.85 64.45 o 8 8 1 22.71 11.45 16.88 o 9 8 1 9.57 9.17 17.68 o 10 8 1 139.03 96.27 43.00 o 11 8 1 2152.87 2224.51 99.31 o 12 8 1 26.20 19.12 27.84 o 13 8 1 4.22 11.06 20.68 o -13 9 1 558.21 505.67 45.10 o -12 9 1 106.49 94.52 36.32 o -11 9 1 689.88 708.34 50.09 o -10 9 1 618.20 533.96 63.84 o -9 9 1 342.57 351.18 92.13 o -8 9 1 38.08 41.52 16.80 o -7 9 1 1624.30 1682.20 77.59 o -6 9 1 389.01 384.64 36.50 o -5 9 1 3523.01 3546.47 91.27 o -4 9 1 7.78 17.27 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