#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/53/2225369.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225369_Fobs loop_ _publ_author_name 'Jiang, Qing-Min' 'Mao, Gui-Yun' 'Hao, Lu-Ye' 'Hao, Xin-Qi' 'Song, Mao-Ping' _publ_section_title ; 2-Iodo-4,6-dimethylpyrimidine ; _journal_coeditor_code SI2242 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o686 _journal_volume 66 _journal_year 2010 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.9298 _cell_length_b 7.0256 _cell_length_c 14.4993 _exptl_crystal_F_000 440.00 _reflns_d_resolution_high 0.8258 _[local]_cod_data_source_file si2242Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' B in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 301.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 25799.13 25584.40 506.08 o 4 0 0 2102.69 1865.80 39.23 o 6 0 0 980.21 1004.20 29.83 o 8 0 0 0.08 -3.71 4.85 o 2 1 0 7658.17 7935.50 110.96 o 4 1 0 5579.17 5541.28 78.63 o 6 1 0 2500.07 2400.99 44.70 o 8 1 0 598.18 616.00 15.87 o 0 2 0 91199.00 102509.66 3709.62 o 2 2 0 15500.25 15331.25 214.13 o 4 2 0 1610.73 1545.31 23.57 o 6 2 0 702.45 740.35 16.83 o 8 2 0 0.25 -0.39 3.51 o 2 3 0 2280.43 2306.38 55.63 o 4 3 0 2578.68 2518.34 37.32 o 6 3 0 1295.81 1265.27 25.72 o 8 3 0 312.78 319.84 15.90 o 0 4 0 20093.94 25965.66 880.77 o 2 4 0 4521.09 4372.87 62.65 o 4 4 0 616.90 612.13 12.65 o 6 4 0 278.41 285.02 14.07 o 8 4 0 0.78 8.20 10.76 o 2 5 0 458.79 456.10 10.24 o 4 5 0 587.09 554.69 16.06 o 6 5 0 357.35 366.36 16.71 o 0 6 0 3407.00 4177.81 115.95 o 2 6 0 729.02 730.80 16.83 o 4 6 0 101.24 112.66 6.16 o 6 6 0 67.24 81.33 8.52 o 2 7 0 63.92 65.66 6.29 o 4 7 0 66.94 73.58 9.19 o 0 8 0 430.05 469.24 28.97 o 2 8 0 60.11 64.08 10.92 o 1 0 1 7068.76 7609.72 145.84 o 2 0 1 2062.17 2099.00 33.13 o 3 0 1 1934.75 1949.75 28.42 o 4 0 1 4547.92 4449.18 63.43 o 5 0 1 202.43 186.37 4.86 o 6 0 1 2468.10 2394.10 44.53 o 7 0 1 333.71 323.61 9.91 o 8 0 1 678.83 673.68 16.84 o 9 0 1 10.97 10.04 4.02 o 0 1 1 26921.87 25532.16 438.39 o 1 1 1 2004.57 2178.87 24.17 o 2 1 1 17248.39 17235.50 170.72 o 3 1 1 2084.06 2278.57 23.37 o 4 1 1 5366.65 5276.28 53.01 o 5 1 1 391.82 395.23 5.56 o 6 1 1 791.37 803.34 11.81 o 7 1 1 2.71 6.29 2.85 o 8 1 1 5.17 14.16 2.83 o 9 1 1 0.18 -3.28 2.19 o 1 2 1 4147.46 4697.77 65.00 o 2 2 1 1401.66 1392.46 14.62 o 3 2 1 1248.51 1281.74 13.77 o 4 2 1 3146.75 3072.19 31.61 o 5 2 1 117.14 109.00 3.44 o 6 2 1 1750.43 1694.59 21.91 o 7 2 1 240.41 224.01 5.92 o 8 2 1 488.61 494.58 13.82 o 9 2 1 7.69 6.10 3.50 o 0 3 1 11716.38 11307.27 157.81 o 1 3 1 1012.62 1029.44 14.49 o 2 3 1 7801.64 7563.38 75.23 o 3 3 1 683.83 678.03 8.09 o 4 3 1 2580.87 2530.36 26.51 o 5 3 1 182.13 181.62 3.76 o 6 3 1 398.48 416.08 8.81 o 7 3 1 1.81 5.19 3.15 o 8 3 1 2.38 5.87 3.96 o 1 4 1 1102.76 1318.83 27.10 o 2 4 1 473.57 455.25 6.03 o 3 4 1 402.64 402.28 6.00 o 4 4 1 1064.09 1010.67 13.18 o 5 4 1 27.26 26.76 2.35 o 6 4 1 631.30 621.90 14.21 o 7 4 1 94.10 88.35 6.39 o 8 4 1 184.53 190.00 9.07 o 0 5 1 2682.89 2554.05 37.89 o 1 5 1 263.40 261.49 6.47 o 2 5 1 1817.38 1723.36 20.73 o 3 5 1 128.01 128.20 3.93 o 4 5 1 632.57 636.16 10.74 o 5 5 1 47.19 49.29 3.24 o 6 5 1 106.40 119.31 6.19 o 7 5 1 0.58 -3.23 3.73 o 1 6 1 228.27 248.49 5.93 o 2 6 1 85.55 95.50 3.90 o 3 6 1 81.72 80.43 3.67 o 4 6 1 190.70 180.53 5.37 o 5 6 1 1.78 2.36 2.38 o 6 6 1 121.38 138.02 9.09 o 0 7 1 346.59 379.75 17.05 o 1 7 1 38.61 37.63 4.06 o 2 7 1 236.89 232.00 7.15 o 3 7 1 11.45 13.26 2.86 o 4 7 1 85.03 83.35 4.24 o 5 7 1 7.94 3.35 2.84 o 1 8 1 43.80 38.91 5.67 o 2 8 1 8.74 16.67 4.56 o 3 8 1 11.33 5.40 4.20 o 0 0 2 2978.41 3092.00 104.18 o 1 0 2 6398.00 6718.54 102.73 o 2 0 2 16241.13 16238.85 248.25 o 3 0 2 5048.10 5234.59 81.03 o 4 0 2 7501.85 7532.58 106.11 o 5 0 2 948.36 961.36 17.48 o 6 0 2 484.57 458.29 10.55 o 7 0 2 71.13 79.98 5.55 o 8 0 2 13.98 14.26 4.01 o 9 0 2 0.22 -1.18 3.63 o 1 1 2 111.13 116.61 2.22 o 2 1 2 1117.19 1110.74 11.69 o 3 1 2 673.99 675.27 7.69 o 4 1 2 3231.57 3181.89 32.55 o 5 1 2 877.33 855.54 11.25 o 6 1 2 1874.95 1781.64 21.60 o 7 1 2 585.24 595.16 10.45 o 8 1 2 504.20 499.30 9.76 o 9 1 2 87.91 92.61 5.35 o 0 2 2 2687.26 3271.50 78.15 o 1 2 2 4653.68 4632.98 50.73 o 2 2 2 9816.73 9775.85 96.64 o 3 2 2 3350.37 3393.17 34.45 o 4 2 2 4838.13 4919.43 49.70 o 5 2 2 664.20 659.73 9.28 o 6 2 2 338.31 345.62 6.35 o 7 2 2 51.98 57.69 4.40 o 8 2 2 11.59 17.39 3.38 o 9 2 2 0.16 1.82 3.05 o 1 3 2 99.89 101.59 2.14 o 2 3 2 643.64 604.78 7.17 o 3 3 2 379.24 374.26 5.32 o 4 3 2 1522.19 1469.00 16.14 o 5 3 2 427.46 409.57 7.23 o 6 3 2 908.35 888.45 13.92 o 7 3 2 302.66 297.64 9.38 o 8 3 2 258.27 256.23 8.95 o 0 4 2 1223.98 1306.58 37.87 o 1 4 2 1613.56 1528.45 16.40 o 2 4 2 3007.58 2867.22 31.11 o 3 4 2 1067.62 1041.36 13.30 o 4 4 2 1558.98 1547.25 18.98 o 5 4 2 233.00 229.40 5.36 o 6 4 2 114.43 137.86 5.22 o 7 4 2 20.24 24.68 5.36 o 8 4 2 6.38 11.42 4.38 o 1 5 2 27.72 28.13 2.36 o 2 5 2 166.56 157.37 3.99 o 3 5 2 101.75 103.48 3.33 o 4 5 2 403.78 375.92 7.11 o 5 5 2 106.22 110.73 4.68 o 6 5 2 227.75 227.69 7.38 o 7 5 2 84.82 93.36 6.61 o 0 6 2 193.94 234.29 8.05 o 1 6 2 283.64 277.10 6.31 o 2 6 2 544.48 499.20 8.50 o 3 6 2 181.89 175.51 5.13 o 4 6 2 297.21 293.23 6.89 o 5 6 2 43.43 42.06 3.65 o 6 6 2 19.21 24.16 3.81 o 1 7 2 3.88 2.28 3.01 o 2 7 2 20.88 22.12 3.43 o 3 7 2 14.41 9.94 3.06 o 4 7 2 62.38 56.94 4.09 o 5 7 2 13.90 12.88 3.14 o 0 8 2 7.82 23.81 6.76 o 1 8 2 28.49 29.65 4.99 o 2 8 2 57.97 61.96 6.02 o 3 8 2 17.51 17.95 4.17 o 1 0 3 762.26 865.66 48.54 o 2 0 3 917.03 923.40 17.49 o 3 0 3 1970.68 1939.64 31.30 o 4 0 3 1710.96 1649.79 27.43 o 5 0 3 1578.45 1507.47 25.87 o 6 0 3 1125.77 1107.98 20.38 o 7 0 3 800.14 780.05 17.90 o 8 0 3 266.84 269.93 11.30 o 9 0 3 227.20 228.75 9.44 o 0 1 3 7928.74 7824.71 119.40 o 1 1 3 23220.88 25433.26 629.29 o 2 1 3 7118.09 7215.82 71.51 o 3 1 3 6753.81 6837.20 68.06 o 4 1 3 2133.39 2129.49 22.27 o 5 1 3 1135.94 1096.47 13.93 o 6 1 3 90.36 93.39 3.27 o 7 1 3 113.59 110.80 4.21 o 8 1 3 2.12 0.63 2.77 o 9 1 3 0.91 2.36 3.11 o 1 2 3 291.18 327.31 8.62 o 2 2 3 721.78 729.68 9.15 o 3 2 3 1190.17 1131.67 12.92 o 4 2 3 1177.18 1139.77 12.72 o 5 2 3 1129.38 1099.30 14.05 o 6 2 3 789.92 778.11 11.71 o 7 2 3 577.77 549.43 11.71 o 8 2 3 191.21 197.81 7.02 o 9 2 3 165.81 169.19 7.04 o 0 3 3 3655.37 3459.48 54.57 o 1 3 3 8016.24 8488.22 216.69 o 2 3 3 3070.50 2988.00 33.69 o 3 3 3 3226.04 3236.35 34.81 o 4 3 3 969.69 953.46 12.35 o 5 3 3 574.40 571.32 9.80 o 6 3 3 44.93 53.35 3.25 o 7 3 3 55.52 61.26 4.31 o 8 3 3 1.57 2.28 2.81 o 1 4 3 47.57 57.24 2.59 o 2 4 3 265.63 257.75 4.78 o 3 4 3 337.36 302.86 5.46 o 4 4 3 412.19 396.86 6.67 o 5 4 3 409.25 404.22 7.98 o 6 4 3 282.01 283.07 6.74 o 7 4 3 221.59 206.57 8.93 o 8 4 3 71.00 75.98 7.62 o 0 5 3 865.64 809.17 19.05 o 1 5 3 1710.11 1787.29 54.30 o 2 5 3 707.14 669.06 10.14 o 3 5 3 809.96 788.47 11.04 o 4 5 3 232.79 236.00 5.16 o 5 5 3 152.70 167.76 5.64 o 6 5 3 10.47 14.62 3.34 o 7 5 3 14.12 14.63 4.28 o 1 6 3 4.48 5.57 2.49 o 2 6 3 46.01 48.68 4.01 o 3 6 3 47.32 44.49 2.92 o 4 6 3 79.19 88.55 4.06 o 5 6 3 75.83 75.32 4.76 o 6 6 3 54.50 60.20 4.72 o 0 7 3 113.69 116.58 7.59 o 1 7 3 218.66 236.25 14.12 o 2 7 3 92.18 94.27 4.99 o 3 7 3 114.07 105.33 6.34 o 4 7 3 31.59 37.62 4.51 o 5 7 3 22.00 20.07 4.28 o 1 8 3 0.04 7.94 6.40 o 2 8 3 4.32 4.73 3.69 o 0 0 4 4820.90 4945.24 111.21 o 1 0 4 19560.32 19492.89 272.84 o 2 0 4 4347.69 4339.39 67.32 o 3 0 4 8433.48 8288.11 143.51 o 4 0 4 236.43 213.15 6.91 o 5 0 4 1920.76 1852.05 31.23 o 6 0 4 56.57 48.18 4.08 o 7 0 4 142.81 156.79 7.65 o 8 0 4 1.46 -1.48 3.26 o 9 0 4 0.00 19.14 6.38 o 1 1 4 406.18 410.97 5.17 o 2 1 4 1362.86 1426.83 21.18 o 3 1 4 2399.14 2380.39 25.67 o 4 1 4 560.60 541.43 7.68 o 5 1 4 2345.67 2255.70 26.42 o 6 1 4 173.34 171.13 4.31 o 7 1 4 811.77 773.87 11.31 o 8 1 4 65.10 69.53 4.56 o 9 1 4 227.91 246.57 8.15 o 0 2 4 2699.52 2730.53 87.07 o 1 2 4 12961.79 12986.03 140.45 o 2 2 4 2859.62 2840.67 31.92 o 3 2 4 5935.85 5759.13 60.25 o 4 2 4 193.64 188.15 3.62 o 5 2 4 1359.34 1336.10 18.94 o 6 2 4 43.27 42.67 2.97 o 7 2 4 99.63 115.52 4.52 o 8 2 4 1.23 0.85 2.70 o 9 2 4 0.00 9.59 6.76 o 1 3 4 171.98 181.80 3.59 o 2 3 4 439.24 423.32 7.97 o 3 3 4 1144.75 1133.98 14.15 o 4 3 4 276.82 269.26 5.03 o 5 3 4 1186.75 1150.31 16.90 o 6 3 4 92.40 100.14 4.40 o 7 3 4 413.59 392.54 9.06 o 8 3 4 34.72 30.63 3.84 o 0 4 4 713.72 715.03 22.14 o 1 4 4 4149.21 4013.12 44.94 o 2 4 4 914.77 896.45 11.68 o 3 4 4 2057.36 1973.84 23.47 o 4 4 4 83.38 93.46 3.17 o 5 4 4 488.18 480.01 9.06 o 6 4 4 20.94 20.53 2.77 o 7 4 4 34.79 39.26 4.18 o 8 4 4 0.65 1.65 3.75 o 1 5 4 43.63 51.03 3.03 o 2 5 4 77.38 73.45 3.60 o 3 5 4 277.59 280.53 5.61 o 4 5 4 68.56 71.92 3.08 o 5 5 4 307.43 298.08 7.64 o 6 5 4 25.27 30.00 3.38 o 7 5 4 108.49 108.57 6.71 o 0 6 4 108.94 115.32 8.71 o 1 6 4 714.83 688.81 12.42 o 2 6 4 176.46 177.06 5.27 o 3 6 4 380.93 366.32 8.32 o 4 6 4 18.12 20.69 3.09 o 5 6 4 92.82 103.37 5.51 o 6 6 4 7.54 2.42 3.30 o 1 7 4 6.15 7.69 2.79 o 2 7 4 7.79 29.82 14.11 o 3 7 4 37.00 42.32 4.10 o 4 7 4 9.83 5.21 3.45 o 5 7 4 44.18 40.88 5.37 o 0 8 4 8.63 17.21 6.28 o 1 8 4 70.01 67.65 5.42 o 2 8 4 23.43 26.24 3.99 o 1 0 5 4.26 8.50 2.00 o 2 0 5 350.53 355.86 8.78 o 3 0 5 5165.22 5398.26 83.93 o 4 0 5 76.21 79.06 4.11 o 5 0 5 5097.02 4836.57 76.57 o 6 0 5 5.37 3.94 2.37 o 7 0 5 778.75 765.29 16.02 o 8 0 5 3.01 8.60 3.38 o 9 0 5 176.01 190.44 13.07 o 0 1 5 691.00 672.79 10.80 o 1 1 5 20012.81 20000.48 197.38 o 2 1 5 177.16 170.21 2.75 o 3 1 5 7714.93 7767.15 77.25 o 4 1 5 11.50 15.01 2.06 o 5 1 5 1513.35 1469.88 19.21 o 6 1 5 23.87 27.49 2.19 o 7 1 5 111.56 124.99 4.91 o 8 1 5 15.17 15.58 3.16 o 9 1 5 2.06 4.50 3.23 o 1 2 5 0.96 14.89 3.17 o 2 2 5 178.07 171.04 4.54 o 3 2 5 3481.32 3610.07 36.76 o 4 2 5 50.47 52.63 2.71 o 5 2 5 3578.24 3392.84 43.64 o 6 2 5 4.19 4.31 2.89 o 7 2 5 539.20 530.38 10.90 o 8 2 5 2.29 7.21 3.28 o 0 3 5 154.11 150.38 5.20 o 1 3 5 8732.35 8492.59 92.75 o 2 3 5 53.99 53.53 2.58 o 3 3 5 3599.05 3613.12 50.16 o 4 3 5 3.51 1.43 1.63 o 5 3 5 725.92 727.72 12.02 o 6 3 5 11.96 14.67 2.56 o 7 3 5 59.23 69.82 4.05 o 8 3 5 8.96 7.66 3.15 o 1 4 5 0.99 7.67 2.27 o 2 4 5 44.03 42.48 2.42 o 3 4 5 1202.21 1165.32 14.94 o 4 4 5 15.11 14.71 2.19 o 5 4 5 1329.27 1272.61 18.80 o 6 4 5 1.76 -0.06 2.32 o 7 4 5 179.81 187.97 6.07 o 8 4 5 1.06 7.75 3.90 o 0 5 5 23.25 24.21 3.58 o 1 5 5 2036.91 1946.41 26.44 o 2 5 5 10.94 9.40 2.27 o 3 5 5 910.47 908.63 12.52 o 4 5 5 0.33 -1.04 1.97 o 5 5 5 174.83 199.43 5.94 o 6 5 5 2.98 2.94 2.71 o 7 5 5 17.00 29.38 4.17 o 1 6 5 0.48 13.71 6.56 o 2 6 5 7.67 8.15 2.49 o 3 6 5 240.75 240.91 6.31 o 4 6 5 2.08 -1.27 2.63 o 5 6 5 289.17 284.70 8.53 o 6 6 5 0.34 -1.11 3.09 o 0 7 5 2.15 2.63 3.50 o 1 7 5 263.58 261.73 6.88 o 2 7 5 1.67 2.34 2.64 o 3 7 5 131.25 144.15 6.24 o 4 7 5 0.00 -2.79 3.11 o 1 8 5 1.41 3.91 3.86 o 0 0 6 1100.14 1211.19 25.96 o 1 0 6 13511.61 13357.85 186.34 o 2 0 6 4300.75 5537.55 206.62 o 3 0 6 6442.65 6410.46 99.45 o 4 0 6 456.60 498.61 10.44 o 5 0 6 1473.23 1429.70 30.17 o 6 0 6 44.41 41.67 4.07 o 7 0 6 74.54 87.51 7.46 o 8 0 6 25.65 25.24 6.29 o 9 0 6 5.06 13.99 6.58 o 1 1 6 180.45 166.52 2.84 o 2 1 6 536.24 599.37 17.48 o 3 1 6 2260.41 2193.22 22.93 o 4 1 6 202.32 213.49 4.30 o 5 1 6 2633.39 2644.87 30.75 o 6 1 6 14.89 14.43 2.37 o 7 1 6 868.12 871.75 14.25 o 8 1 6 19.04 7.55 3.30 o 0 2 6 559.25 593.97 10.00 o 1 2 6 9330.42 9137.96 94.62 o 2 2 6 2690.72 3170.58 77.43 o 3 2 6 4350.02 4228.45 47.33 o 4 2 6 331.11 352.79 6.93 o 5 2 6 1026.80 1006.41 15.26 o 6 2 6 36.44 34.07 2.92 o 7 2 6 55.01 61.72 3.84 o 8 2 6 18.58 14.26 3.43 o 1 3 6 113.95 124.18 3.23 o 2 3 6 177.08 190.36 6.99 o 3 3 6 1129.26 1105.24 14.10 o 4 3 6 97.32 105.86 3.87 o 5 3 6 1310.02 1331.59 19.41 o 6 3 6 7.59 5.55 2.36 o 7 3 6 444.58 461.73 9.56 o 8 3 6 10.11 4.48 3.14 o 0 4 6 114.29 109.38 6.19 o 1 4 6 3173.70 2982.30 38.53 o 2 4 6 858.11 968.94 31.08 o 3 4 6 1451.56 1400.33 17.58 o 4 4 6 134.28 132.59 4.58 o 5 4 6 360.00 361.01 7.83 o 6 4 6 21.95 19.83 3.01 o 7 4 6 22.21 21.42 3.19 o 1 5 6 29.36 37.53 2.90 o 2 5 6 27.34 32.58 2.88 o 3 5 6 289.21 277.40 6.13 o 4 5 6 27.78 23.19 2.81 o 5 5 6 345.74 353.90 7.96 o 6 5 6 1.79 -1.66 2.49 o 7 5 6 120.10 124.20 5.83 o 0 6 6 6.72 2.48 3.29 o 1 6 6 576.17 549.28 10.17 o 2 6 6 183.51 183.53 6.66 o 3 6 6 257.64 259.88 6.61 o 4 6 6 33.25 27.71 3.57 o 5 6 6 68.03 60.78 5.10 o 1 7 6 3.55 4.78 2.64 o 2 7 6 1.58 -1.49 2.48 o 3 7 6 40.89 41.93 4.18 o 4 7 6 5.62 5.11 4.19 o 1 0 7 1576.42 1857.22 65.33 o 2 0 7 305.20 309.34 6.28 o 3 0 7 863.29 916.78 66.32 o 4 0 7 226.52 235.48 6.61 o 5 0 7 537.14 542.49 11.86 o 6 0 7 220.01 216.68 7.09 o 7 0 7 815.38 833.16 27.15 o 8 0 7 118.24 123.96 8.58 o 0 1 7 2840.88 2879.62 41.74 o 1 1 7 7299.61 7314.75 100.43 o 2 1 7 2819.74 2878.58 29.61 o 3 1 7 3108.17 3057.17 32.95 o 4 1 7 1054.64 1068.23 13.68 o 5 1 7 695.82 659.44 11.05 o 6 1 7 125.56 121.09 4.46 o 7 1 7 18.40 18.14 2.94 o 8 1 7 22.36 24.79 3.19 o 1 2 7 1025.18 1123.34 19.83 o 2 2 7 199.97 199.45 4.06 o 3 2 7 592.84 566.48 9.60 o 4 2 7 165.22 159.30 4.70 o 5 2 7 368.21 387.52 7.89 o 6 2 7 160.21 161.64 5.26 o 7 2 7 601.51 584.64 11.06 o 8 2 7 86.12 80.14 4.86 o 0 3 7 1366.91 1418.74 27.64 o 1 3 7 3457.56 3328.79 37.75 o 2 3 7 1395.86 1373.52 16.95 o 3 3 7 1521.85 1482.24 18.25 o 4 3 7 550.50 529.56 9.48 o 5 3 7 370.07 372.83 7.86 o 6 3 7 61.81 55.40 3.66 o 7 3 7 9.29 13.50 3.02 o 8 3 7 11.06 7.34 3.25 o 1 4 7 357.69 387.83 8.82 o 2 4 7 63.65 67.34 2.85 o 3 4 7 195.61 203.70 9.15 o 4 4 7 58.58 62.29 3.73 o 5 4 7 112.85 122.05 4.73 o 6 4 7 60.92 60.80 3.86 o 7 4 7 246.71 253.57 7.17 o 0 5 7 330.01 314.02 10.27 o 1 5 7 864.86 858.16 14.01 o 2 5 7 350.76 329.31 7.21 o 3 5 7 369.49 366.26 7.74 o 4 5 7 150.29 141.68 5.01 o 5 5 7 108.69 109.60 4.68 o 6 5 7 14.89 14.50 3.54 o 1 6 7 87.52 93.92 4.28 o 2 6 7 10.91 10.29 2.59 o 3 6 7 30.33 42.61 3.35 o 4 6 7 10.25 7.25 3.22 o 5 6 7 12.97 18.03 3.99 o 0 7 7 42.27 36.39 4.97 o 1 7 7 122.19 130.69 5.28 o 2 7 7 50.34 48.05 3.71 o 3 7 7 44.88 48.94 4.52 o 0 0 8 6459.31 6769.73 135.46 o 1 0 8 4901.49 4891.64 69.86 o 2 0 8 2588.05 2529.77 37.25 o 3 0 8 1798.92 1795.40 30.13 o 4 0 8 1486.70 1535.96 75.93 o 5 0 8 133.07 129.91 5.62 o 6 0 8 652.05 638.83 19.17 o 7 0 8 0.18 3.32 4.39 o 8 0 8 18.02 25.08 5.61 o 1 1 8 428.33 416.32 5.66 o 2 1 8 394.09 419.62 8.17 o 3 1 8 997.51 996.77 12.80 o 4 1 8 572.81 594.37 12.50 o 5 1 8 493.94 474.84 8.95 o 6 1 8 566.57 555.58 10.31 o 7 1 8 282.29 302.05 7.50 o 8 1 8 181.20 182.87 7.50 o 0 2 8 4432.80 4561.85 65.46 o 1 2 8 3257.35 3195.18 34.40 o 2 2 8 1776.96 1738.08 20.81 o 3 2 8 1254.15 1220.06 17.39 o 4 2 8 1026.20 998.19 35.08 o 5 2 8 96.69 88.54 4.00 o 6 2 8 478.04 460.52 9.29 o 7 2 8 0.09 2.07 2.54 o 8 2 8 13.23 16.32 3.24 o 1 3 8 187.25 185.00 4.16 o 2 3 8 201.26 195.58 5.48 o 3 3 8 467.54 455.08 7.84 o 4 3 8 278.92 269.49 6.37 o 5 3 8 247.65 240.42 6.26 o 6 3 8 290.63 283.58 7.15 o 7 3 8 151.79 169.89 5.98 o 0 4 8 1589.14 1495.05 29.88 o 1 4 8 1080.06 1055.25 15.83 o 2 4 8 597.64 565.63 9.93 o 3 4 8 441.07 423.96 7.74 o 4 4 8 349.13 355.84 12.61 o 5 4 8 37.24 40.27 3.34 o 6 4 8 195.40 185.52 6.05 o 7 4 8 0.01 -0.56 2.76 o 1 5 8 43.80 41.99 3.19 o 2 5 8 59.41 79.35 10.62 o 3 5 8 111.43 111.97 4.89 o 4 5 8 67.43 68.44 4.57 o 5 5 8 61.92 61.96 3.93 o 6 5 8 80.04 85.09 4.65 o 0 6 8 329.49 288.27 10.21 o 1 6 8 197.83 205.32 6.15 o 2 6 8 95.99 93.97 4.38 o 3 6 8 84.37 89.66 4.77 o 4 6 8 60.66 66.54 4.82 o 5 6 8 7.64 7.22 3.31 o 1 7 8 5.93 6.29 2.79 o 2 7 8 10.89 16.95 3.10 o 3 7 8 14.18 14.10 3.37 o 1 0 9 60.18 61.68 3.29 o 2 0 9 396.43 389.32 7.95 o 3 0 9 483.48 575.15 28.22 o 4 0 9 1106.20 1120.14 20.63 o 5 0 9 417.40 412.14 11.76 o 6 0 9 706.91 750.92 21.70 o 7 0 9 85.69 91.75 7.96 o 8 0 9 199.67 252.36 20.46 o 0 1 9 5119.78 5065.85 72.47 o 1 1 9 582.50 554.53 7.21 o 2 1 9 3682.29 3621.15 37.24 o 3 1 9 427.03 400.50 18.16 o 4 1 9 1543.35 1486.98 21.05 o 5 1 9 21.27 15.11 2.50 o 6 1 9 337.11 330.60 7.67 o 7 1 9 4.11 2.86 2.86 o 8 1 9 6.08 10.89 3.75 o 1 2 9 41.69 38.68 2.18 o 2 2 9 300.14 303.19 5.57 o 3 2 9 350.44 393.89 16.61 o 4 2 9 786.67 793.27 12.84 o 5 2 9 304.29 310.24 7.11 o 6 2 9 502.82 520.71 10.16 o 7 2 9 60.20 71.07 4.25 o 0 3 9 2557.26 2525.71 47.19 o 1 3 9 306.85 306.09 6.61 o 2 3 9 1821.45 1752.97 21.40 o 3 3 9 221.83 230.58 11.11 o 4 3 9 762.01 710.77 12.06 o 5 3 9 9.31 11.84 2.55 o 6 3 9 178.27 166.93 5.75 o 7 3 9 2.31 1.54 2.71 o 1 4 9 13.75 10.59 2.43 o 2 4 9 120.93 129.77 4.57 o 3 4 9 136.07 157.63 5.94 o 4 4 9 287.82 297.74 7.14 o 5 4 9 120.36 119.76 4.90 o 6 4 9 184.14 187.82 6.78 o 0 5 9 645.87 617.57 15.75 o 1 5 9 79.49 87.45 4.11 o 2 5 9 461.80 431.99 10.09 o 3 5 9 61.33 75.41 4.81 o 4 5 9 194.67 179.86 6.77 o 5 5 9 1.68 1.47 3.09 o 6 5 9 52.11 49.00 4.73 o 1 6 9 2.22 1.24 2.45 o 2 6 9 26.58 24.36 3.18 o 3 6 9 30.64 36.79 4.13 o 4 6 9 56.59 59.74 4.85 o 0 7 9 88.53 82.96 8.06 o 1 7 9 10.78 9.77 3.03 o 2 7 9 62.79 60.12 4.23 o 0 0 10 7877.90 7468.82 150.03 o 1 0 10 22.51 40.64 7.24 o 2 0 10 3774.79 3709.25 54.19 o 3 0 10 11.74 25.31 8.43 o 4 0 10 935.00 957.13 20.86 o 5 0 10 3.91 6.19 4.20 o 6 0 10 146.07 134.40 9.06 o 7 0 10 23.26 37.01 6.18 o 1 1 10 28.03 26.63 1.82 o 2 1 10 444.89 501.09 13.37 o 3 1 10 117.76 115.94 4.12 o 4 1 10 1009.19 1021.63 15.69 o 5 1 10 90.56 93.15 4.17 o 6 1 10 516.17 532.15 11.19 o 7 1 10 8.79 11.01 3.68 o 0 2 10 5520.01 5170.54 91.93 o 1 2 10 14.48 13.22 1.91 o 2 2 10 2655.77 2562.46 30.09 o 3 2 10 7.29 5.68 2.14 o 4 2 10 665.10 653.49 11.37 o 5 2 10 3.07 4.70 2.46 o 6 2 10 105.56 102.02 4.66 o 7 2 10 16.64 20.72 3.21 o 1 3 10 16.92 16.84 2.49 o 2 3 10 216.63 235.84 6.49 o 3 3 10 63.81 64.28 3.71 o 4 3 10 508.65 502.80 9.66 o 5 3 10 46.08 50.28 3.65 o 6 3 10 269.60 270.65 7.20 o 7 3 10 4.00 0.42 2.69 o 0 4 10 1996.20 1917.14 37.83 o 1 4 10 4.33 3.41 2.31 o 2 4 10 949.89 907.95 14.52 o 3 4 10 2.57 5.11 2.87 o 4 4 10 240.75 253.06 7.88 o 5 4 10 1.36 3.08 2.57 o 6 4 10 40.17 36.46 3.66 o 1 5 10 5.95 5.80 2.55 o 2 5 10 54.44 64.07 3.89 o 3 5 10 19.76 13.88 3.47 o 4 5 10 135.81 144.26 6.50 o 5 5 10 13.03 14.33 3.64 o 0 6 10 407.16 412.84 13.10 o 1 6 10 0.55 -3.67 2.45 o 2 6 10 181.39 189.77 6.65 o 3 6 10 0.64 -0.46 2.96 o 4 6 10 45.09 46.00 4.62 o 1 0 11 208.76 213.10 9.85 o 2 0 11 406.00 404.25 9.71 o 4 0 11 824.23 867.38 23.53 o 5 0 11 0.56 -2.92 3.96 o 6 0 11 435.10 454.02 16.49 o 7 0 11 15.57 16.42 5.78 o 0 1 11 4827.23 4611.59 73.13 o 1 1 11 199.42 206.88 4.45 o 2 1 11 2584.32 2562.68 33.80 o 3 1 11 151.78 138.85 6.78 o 4 1 11 582.45 559.36 10.26 o 5 1 11 59.73 49.26 5.12 o 6 1 11 64.16 59.86 5.11 o 7 1 11 17.50 13.04 3.83 o 1 2 11 154.52 153.67 4.50 o 2 2 11 275.07 281.39 6.46 o 3 2 11 31.94 25.19 3.84 o 4 2 11 587.46 598.35 10.89 o 5 2 11 0.59 -1.40 2.40 o 6 2 11 316.93 334.89 8.13 o 7 2 11 11.77 7.34 3.34 o 0 3 11 2401.80 2316.38 44.39 o 1 3 11 99.34 97.20 4.18 o 2 3 11 1295.45 1257.45 19.99 o 3 3 11 74.13 80.54 11.55 o 4 3 11 300.31 279.20 6.99 o 5 3 11 31.01 26.17 3.24 o 6 3 11 33.25 31.16 3.51 o 1 4 11 69.76 66.69 3.79 o 2 4 11 88.31 93.77 4.60 o 3 4 11 13.83 23.03 8.39 o 4 4 11 216.36 218.17 7.58 o 5 4 11 0.55 0.50 3.45 o 0 5 11 640.41 590.44 15.81 o 1 5 11 27.23 19.02 3.13 o 2 5 11 340.99 351.98 8.82 o 3 5 11 18.42 30.90 5.70 o 4 5 11 81.13 89.46 5.56 o 1 6 11 22.09 16.27 3.18 o 2 6 11 13.65 22.72 3.95 o 3 6 11 3.78 7.69 3.40 o 0 0 12 477.93 479.39 13.96 o 1 0 12 395.77 415.77 9.96 o 2 0 12 1395.79 1370.03 24.63 o 3 0 12 546.33 524.26 16.31 o 4 0 12 664.57 630.58 57.23 o 5 0 12 180.33 162.22 9.76 o 6 0 12 23.39 22.19 5.98 o 7 0 12 24.08 18.24 6.36 o 1 1 12 32.44 38.27 2.50 o 2 1 12 141.31 162.76 5.00 o 3 1 12 62.92 73.62 3.76 o 4 1 12 336.99 403.71 13.14 o 5 1 12 56.10 66.20 5.04 o 6 1 12 229.59 229.22 8.31 o 0 2 12 322.78 321.76 10.00 o 1 2 12 283.59 276.08 6.55 o 2 2 12 1010.08 996.87 16.45 o 3 2 12 389.68 366.20 7.94 o 4 2 12 485.47 494.04 17.83 o 5 2 12 128.60 118.46 5.06 o 6 2 12 15.64 15.97 3.52 o 1 3 12 19.95 19.07 2.73 o 2 3 12 70.08 85.30 4.82 o 3 3 12 36.06 44.26 4.04 o 4 3 12 180.36 219.57 8.78 o 5 3 12 28.19 31.82 3.50 o 6 3 12 118.87 117.64 5.37 o 0 4 12 91.40 104.83 6.60 o 1 4 12 102.14 98.16 4.51 o 2 4 12 388.73 388.55 9.96 o 3 4 12 145.57 136.43 6.22 o 4 4 12 193.54 213.24 7.60 o 5 4 12 47.55 41.79 4.53 o 1 5 12 7.52 6.29 2.73 o 2 5 12 16.95 14.48 3.61 o 3 5 12 11.86 9.38 4.30 o 4 5 12 53.09 61.41 5.01 o 0 6 12 7.75 6.58 4.21 o 1 6 12 18.61 13.80 3.27 o 1 0 13 51.46 56.29 3.98 o 2 0 13 230.29 251.06 10.65 o 3 0 13 29.06 34.93 5.47 o 4 0 13 234.13 260.85 11.95 o 5 0 13 168.12 182.71 10.42 o 6 0 13 137.61 146.12 10.14 o 0 1 13 450.44 435.30 12.00 o 1 1 13 659.62 610.75 9.99 o 2 1 13 490.87 477.06 9.79 o 3 1 13 489.14 450.64 9.09 o 4 1 13 173.39 162.86 6.10 o 5 1 13 135.09 127.71 6.49 o 6 1 13 2.29 16.08 6.70 o 1 2 13 42.35 42.47 3.24 o 2 2 13 169.67 183.67 6.50 o 3 2 13 19.68 22.74 3.12 o 4 2 13 168.30 170.26 5.76 o 5 2 13 124.68 127.99 5.83 o 6 2 13 98.60 118.98 7.65 o 0 3 13 224.52 220.95 8.82 o 1 3 13 332.78 314.76 7.53 o 2 3 13 250.44 254.14 7.86 o 3 3 13 259.50 239.96 7.74 o 4 3 13 90.00 87.60 5.34 o 5 3 13 69.08 59.75 4.61 o 1 4 13 24.78 23.23 3.38 o 2 4 13 68.63 81.61 5.16 o 3 4 13 6.04 6.57 3.28 o 4 4 13 63.55 67.83 4.99 o 0 5 13 55.03 61.41 5.86 o 1 5 13 85.95 80.07 4.87 o 2 5 13 67.72 80.29 5.43 o 3 5 13 76.47 67.17 6.72 o 0 0 14 557.41 538.80 15.89 o 1 0 14 1133.68 1140.58 24.31 o 2 0 14 106.98 102.37 7.53 o 3 0 14 408.47 408.23 14.91 o 4 0 14 2.65 0.76 5.22 o 5 0 14 106.13 99.51 8.50 o 1 1 14 9.50 16.07 2.86 o 2 1 14 69.58 71.87 5.11 o 3 1 14 107.42 124.76 5.42 o 4 1 14 65.95 75.54 6.12 o 5 1 14 135.14 156.83 7.12 o 0 2 14 418.67 411.69 12.39 o 1 2 14 810.01 788.16 15.50 o 2 2 14 75.22 84.03 5.00 o 3 2 14 294.89 275.85 9.09 o 4 2 14 1.50 9.76 3.63 o 5 2 14 77.33 71.60 4.90 o 1 3 14 3.83 6.02 3.10 o 2 3 14 38.96 42.99 4.31 o 3 3 14 52.53 64.90 4.89 o 4 3 14 32.49 44.40 4.48 o 0 4 14 182.11 198.99 10.19 o 1 4 14 302.28 291.76 8.93 o 2 4 14 26.08 33.79 4.20 o 3 4 14 111.74 109.06 6.02 o 1 5 14 0.55 -1.67 3.19 o 1 0 15 53.55 71.38 9.91 o 2 0 15 12.29 6.52 4.53 o 3 0 15 157.95 182.96 10.22 o 4 0 15 15.81 11.15 5.09 o 0 1 15 44.27 41.63 4.84 o 1 1 15 627.80 590.13 12.61 o 2 1 15 7.75 5.51 3.07 o 3 1 15 256.38 233.59 8.63 o 4 1 15 3.78 -0.74 3.23 o 1 2 15 40.59 43.00 4.06 o 2 2 15 8.37 8.70 3.23 o 3 2 15 116.46 119.70 6.17 o 4 2 15 11.13 12.74 4.01 o 0 3 15 23.26 22.77 4.69 o 1 3 15 331.48 333.04 9.46 o 2 3 15 4.24 4.34 3.28 o 3 3 15 131.43 132.21 6.44 o 1 4 15 18.28 19.20 3.89 o 2 4 15 2.75 1.09 3.25 o 0 0 16 21.39 12.36 8.52 o 1 0 16 410.68 414.18 17.88 o 2 0 16 27.05 26.16 6.63 o 3 0 16 184.97 177.29 13.09 o 1 1 16 14.82 17.41 3.85 o 2 1 16 0.17 2.93 3.85 o 3 1 16 101.82 111.71 6.55 o 0 2 16 16.14 5.79 4.89 o 1 2 16 297.72 304.20 8.93 o 2 2 16 20.07 15.71 3.56 o 3 2 16 132.58 130.82 7.36 o 1 3 16 7.93 7.57 3.48 o 2 3 16 0.18 1.74 3.15 o 1 0 17 14.15 17.79 9.59 o 2 0 17 6.62 9.48 5.81 o 0 1 17 66.72 68.39 11.72 o 1 1 17 146.52 162.01 11.32 o 2 1 17 73.95 68.42 6.37 o