#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/53/2225389.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225389_Fobs loop_ _publ_author_name 'Chantrapromma, Suchada' 'Fun, Hoong-Kun' 'Padaki, Mahesh' 'Suwunwong, Thitipone' 'Isloor, Arun M.' _publ_section_title ; 6-(4-Bromophenyl)-2-ethoxy-4-(2,4,5-trimethoxyphenyl)nicotinonitrile ; _journal_coeditor_code TK2622 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o641 _journal_page_last o642 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 92.201 _cell_angle_beta 91.968 _cell_angle_gamma 99.586 _cell_length_a 7.9631 _cell_length_b 11.0499 _cell_length_c 23.9690 _exptl_crystal_F_000 960.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file tk2622Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tcm27bm in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 341.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 182.98 121.38 13.67 o 2 0 0 10062.79 10740.84 296.84 o 3 0 0 1072.72 1108.53 63.97 o 4 0 0 1945.50 2022.23 96.65 o 5 0 0 6358.03 5643.62 203.98 o 6 0 0 163.45 133.32 49.54 o 7 0 0 56.86 71.33 54.75 o 8 0 0 55.57 46.96 45.24 o 9 0 0 267.01 435.42 67.64 o 10 0 0 401.03 299.19 69.48 o -9 1 0 29.17 83.54 70.99 o -8 1 0 1149.22 1277.05 121.34 o -7 1 0 303.62 214.87 61.41 o -5 1 0 495.01 34.31 14.47 o -4 1 0 3346.76 2382.17 99.62 o -3 1 0 5069.53 4996.96 157.57 o -2 1 0 23.27 60.32 7.40 o -1 1 0 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