#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/54/2225406.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225406_Fobs loop_ _publ_author_name 'Hu, Zhao-Jian' 'Guo, Xiu-Kai' 'Xu, Huan' 'He, Ming-Yang' 'Geng, Li' _publ_section_title ; 1-{4-[(1H-1,2,4-Triazol-1-yl)methyl]benzyl}-1H-1,2,4-triazol-4-ium perchlorate ; _journal_coeditor_code XU2715 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o537 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 124.500 _cell_angle_gamma 90.000 _cell_length_a 15.1400 _cell_length_b 11.3621 _cell_length_c 10.4080 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.8109 _[local]_cod_data_source_file xu2715Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 091209A in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 772.90 700.88 18.38 o 4 0 0 924.92 1012.70 17.90 o 6 0 0 7514.61 7174.59 175.43 o 8 0 0 483.37 559.94 12.43 o 10 0 0 548.01 586.29 13.73 o 12 0 0 172.14 158.11 6.62 o 14 0 0 72.37 48.03 7.94 o 1 1 0 988.29 815.11 6.74 o 3 1 0 7841.47 7622.10 98.05 o 5 1 0 3165.25 3053.72 42.30 o 7 1 0 1375.04 1336.92 20.42 o 9 1 0 598.11 628.66 9.85 o 11 1 0 42.69 32.69 2.52 o 13 1 0 116.68 126.19 7.37 o 15 1 0 4.56 0.00 3.39 o 0 2 0 1536.88 1378.92 22.90 o 2 2 0 964.71 910.47 9.99 o 4 2 0 2848.00 2982.85 49.06 o 6 2 0 273.52 258.95 6.52 o 8 2 0 546.64 443.06 10.33 o 10 2 0 1.55 1.28 2.06 o 12 2 0 47.74 61.55 3.43 o 14 2 0 42.83 72.64 6.64 o 1 3 0 20309.64 20763.06 276.02 o 3 3 0 6995.44 6839.15 91.11 o 5 3 0 6276.91 6562.49 88.93 o 7 3 0 81.72 32.19 2.86 o 9 3 0 56.00 60.07 3.71 o 11 3 0 0.15 0.00 1.60 o 13 3 0 112.52 86.66 6.94 o 15 3 0 7.33 28.78 5.16 o 0 4 0 59.20 40.52 3.76 o 2 4 0 2417.49 2199.94 71.44 o 4 4 0 359.62 379.34 5.32 o 6 4 0 1.79 2.27 1.22 o 8 4 0 165.56 227.43 5.86 o 10 4 0 8.24 15.94 2.21 o 12 4 0 39.51 33.50 3.21 o 14 4 0 0.49 0.00 3.21 o 1 5 0 208.21 230.55 3.73 o 3 5 0 5.50 17.91 1.10 o 5 5 0 500.21 532.30 8.18 o 7 5 0 40.88 26.84 2.17 o 9 5 0 4.90 16.98 2.16 o 11 5 0 7.09 6.24 1.95 o 13 5 0 63.30 48.95 8.98 o 0 6 0 244.56 195.25 7.52 o 2 6 0 2.63 5.22 0.81 o 4 6 0 597.06 667.16 9.78 o 6 6 0 225.16 274.50 6.31 o 8 6 0 610.25 639.13 12.03 o 10 6 0 89.76 66.81 3.82 o 12 6 0 0.09 2.84 2.34 o 1 7 0 929.98 806.09 9.86 o 3 7 0 80.67 86.94 3.04 o 5 7 0 0.02 0.00 0.85 o 7 7 0 45.35 59.76 3.34 o 9 7 0 63.86 44.47 3.50 o 11 7 0 20.76 12.65 4.79 o 13 7 0 62.51 54.73 6.34 o 0 8 0 1561.77 1416.27 25.99 o 2 8 0 122.89 91.32 2.45 o 4 8 0 16.74 11.88 1.56 o 6 8 0 84.34 112.26 3.67 o 8 8 0 42.00 51.34 3.54 o 10 8 0 74.17 88.01 4.51 o 12 8 0 83.80 73.28 5.31 o 1 9 0 429.32 361.16 7.65 o 3 9 0 595.14 568.71 9.40 o 5 9 0 166.73 204.21 7.84 o 7 9 0 79.09 86.16 4.30 o 9 9 0 127.37 149.39 9.40 o 11 9 0 3.30 7.75 2.71 o 0 10 0 418.59 460.26 11.60 o 2 10 0 1.78 1.54 1.51 o 4 10 0 0.20 0.79 1.40 o 6 10 0 232.05 211.68 12.09 o 8 10 0 32.54 35.92 3.86 o 10 10 0 5.37 4.47 4.59 o 1 11 0 397.55 374.67 7.46 o 3 11 0 4.44 7.65 3.42 o 5 11 0 244.88 229.45 6.69 o 7 11 0 4.08 6.31 2.53 o 9 11 0 1.90 0.00 2.24 o 0 12 0 285.30 258.13 12.11 o 2 12 0 12.20 14.45 2.61 o 4 12 0 169.63 163.72 5.88 o 6 12 0 77.61 73.19 4.34 o 1 13 0 89.40 97.27 5.46 o 3 13 0 37.47 37.48 4.10 o 5 13 0 31.86 37.11 4.10 o -15 1 1 83.00 45.47 5.46 o -13 1 1 66.62 78.59 4.34 o -11 1 1 1.74 0.92 1.69 o -9 1 1 625.27 579.80 9.23 o -7 1 1 1523.49 1582.68 23.54 o -5 1 1 2891.11 2783.40 49.32 o -3 1 1 28280.01 26903.41 361.30 o -1 1 1 483.00 629.71 8.28 o 1 1 1 15445.35 14814.32 131.79 o 3 1 1 303.16 316.36 4.57 o 5 1 1 976.55 865.30 21.72 o 7 1 1 2882.96 2855.13 38.89 o 9 1 1 0.72 0.99 1.23 o 11 1 1 7.63 8.56 3.25 o 13 1 1 6.35 29.12 4.73 o -16 2 1 32.34 12.98 5.85 o -14 2 1 99.03 125.86 4.71 o -12 2 1 302.83 325.88 7.05 o -10 2 1 321.85 348.46 8.03 o -8 2 1 629.40 637.24 15.30 o -6 2 1 63.64 99.81 3.18 o -4 2 1 1100.32 1036.68 61.82 o -2 2 1 8004.00 7978.64 273.79 o 0 2 1 2850.14 3210.70 25.77 o 2 2 1 44032.66 40481.32 393.12 o 4 2 1 195.15 311.40 5.09 o 6 2 1 256.41 245.01 5.52 o 8 2 1 287.33 250.56 7.02 o 10 2 1 126.29 133.23 4.02 o 12 2 1 111.65 80.40 10.65 o 14 2 1 87.49 63.49 6.64 o -15 3 1 4.31 2.43 3.39 o -13 3 1 46.99 52.09 3.28 o -11 3 1 374.09 336.09 8.11 o -9 3 1 51.57 43.19 3.21 o -7 3 1 2312.95 2467.44 42.16 o -5 3 1 57.31 40.39 3.02 o -3 3 1 1864.25 1803.01 24.80 o -1 3 1 143.43 132.59 2.45 o 1 3 1 16383.01 16192.36 165.87 o 3 3 1 581.63 557.74 22.75 o 5 3 1 689.38 777.66 10.92 o 7 3 1 20.98 52.25 3.04 o 9 3 1 333.03 406.04 8.76 o 11 3 1 35.90 24.74 4.13 o 13 3 1 12.60 3.50 3.39 o -14 4 1 0.63 0.00 2.25 o -12 4 1 296.81 302.60 7.98 o -10 4 1 17.74 9.76 2.02 o -8 4 1 432.21 390.74 9.40 o -6 4 1 305.45 308.69 6.32 o -4 4 1 1079.79 1052.35 17.12 o -2 4 1 16.58 14.63 7.29 o 0 4 1 22.34 24.17 1.25 o 2 4 1 1141.75 1155.13 16.87 o 4 4 1 1.75 5.07 1.22 o 6 4 1 2873.69 2824.57 35.01 o 8 4 1 14.47 5.99 1.81 o 10 4 1 168.64 134.17 4.95 o 12 4 1 149.94 176.12 9.00 o -15 5 1 1.79 6.43 6.06 o -13 5 1 5.38 8.08 2.33 o -11 5 1 615.25 632.41 14.36 o -9 5 1 106.46 82.80 3.58 o -7 5 1 91.03 123.40 3.92 o -5 5 1 205.55 271.63 5.75 o -3 5 1 2020.52 2002.33 21.63 o -1 5 1 85.70 49.72 1.34 o 1 5 1 3044.15 3087.72 35.91 o 3 5 1 1941.42 1986.55 24.36 o 5 5 1 1134.94 1110.10 15.13 o 7 5 1 300.39 384.38 8.10 o 9 5 1 3.80 7.92 1.91 o 11 5 1 14.28 19.28 5.64 o 13 5 1 66.56 39.55 5.46 o -14 6 1 9.44 8.51 2.85 o -12 6 1 29.87 25.45 2.89 o -10 6 1 38.13 35.57 3.03 o -8 6 1 256.89 289.76 6.86 o -6 6 1 201.23 214.04 5.38 o -4 6 1 7.56 9.89 1.25 o -2 6 1 0.81 3.04 1.84 o 0 6 1 33.69 15.73 1.19 o 2 6 1 480.15 516.89 7.90 o 4 6 1 1013.37 1099.78 13.27 o 6 6 1 0.92 10.40 1.52 o 8 6 1 11.15 3.68 1.95 o 10 6 1 8.31 12.80 2.26 o 12 6 1 1.40 2.43 3.39 o -13 7 1 51.93 47.44 6.68 o -11 7 1 28.40 28.23 3.03 o -9 7 1 180.83 209.30 6.51 o -7 7 1 348.39 437.31 9.01 o -5 7 1 103.66 113.02 5.44 o -3 7 1 48.91 22.21 2.08 o -1 7 1 416.75 300.74 5.97 o 1 7 1 594.94 539.03 8.33 o 3 7 1 0.33 6.14 1.12 o 5 7 1 994.28 1047.68 15.61 o 7 7 1 0.20 3.61 2.53 o 9 7 1 33.76 25.05 2.67 o 11 7 1 2.60 1.98 3.39 o -12 8 1 25.33 20.65 3.32 o -10 8 1 17.94 27.53 3.48 o -8 8 1 3.13 0.86 1.56 o -6 8 1 32.00 44.76 2.62 o -4 8 1 837.46 849.07 12.41 o 0 8 1 9.00 1.37 0.65 o 2 8 1 1299.53 1348.47 17.27 o 4 8 1 10.82 18.13 1.65 o 6 8 1 24.03 50.13 2.74 o 8 8 1 140.94 153.83 5.34 o 10 8 1 13.02 9.61 2.33 o -11 9 1 24.43 12.68 2.90 o -9 9 1 70.78 52.81 4.24 o -7 9 1 231.74 251.11 9.40 o -5 9 1 311.13 306.76 6.36 o -3 9 1 758.85 731.87 14.59 o -1 9 1 10.67 6.10 1.06 o 1 9 1 116.47 137.13 3.96 o 3 9 1 375.64 368.88 7.06 o 5 9 1 179.41 151.56 4.50 o 7 9 1 33.61 39.74 3.21 o 9 9 1 27.76 23.04 2.87 o -10 10 1 6.70 5.39 2.92 o -8 10 1 45.63 55.64 4.39 o -6 10 1 178.29 199.78 11.45 o -4 10 1 374.88 369.64 8.46 o -2 10 1 186.22 161.71 5.13 o 0 10 1 767.84 709.06 11.18 o 2 10 1 424.46 407.16 7.79 o 4 10 1 9.08 12.73 1.97 o 6 10 1 271.02 266.88 6.81 o 8 10 1 5.35 3.66 2.20 o -9 11 1 102.91 96.84 5.94 o -7 11 1 7.34 9.92 3.55 o -5 11 1 4.54 9.60 2.36 o -3 11 1 492.31 500.53 10.47 o -1 11 1 3.00 3.10 1.73 o 1 11 1 179.82 190.47 5.96 o 3 11 1 282.02 294.86 6.68 o 5 11 1 3.65 6.20 1.98 o 7 11 1 29.40 33.14 3.79 o -8 12 1 78.87 83.61 5.56 o -6 12 1 1.57 1.62 1.98 o -4 12 1 51.01 61.11 4.04 o -2 12 1 279.19 250.53 7.08 o 0 12 1 145.19 140.45 5.39 o 2 12 1 130.01 99.72 5.16 o 4 12 1 20.16 15.71 2.91 o 6 12 1 20.80 26.76 3.13 o -5 13 1 103.65 97.38 5.21 o -3 13 1 136.45 136.01 6.48 o -1 13 1 0.25 0.00 1.60 o 1 13 1 358.08 342.71 22.35 o 3 13 1 4.22 4.01 2.20 o -16 0 2 126.78 186.53 8.56 o -14 0 2 383.80 372.40 11.42 o -12 0 2 350.05 342.22 10.11 o -10 0 2 3650.90 3701.71 63.38 o -8 0 2 551.91 552.26 12.07 o -6 0 2 76.93 90.62 3.51 o -4 0 2 3668.61 3954.23 96.49 o -2 0 2 704.23 928.10 23.81 o 0 0 2 31929.76 27880.88 470.27 o 2 0 2 4930.72 5173.51 81.97 o 4 0 2 2018.23 1948.92 32.71 o 8 0 2 18.89 40.16 3.22 o 10 0 2 30.92 68.08 8.35 o 12 0 2 14.90 0.00 4.18 o -15 1 2 65.86 55.65 3.68 o -13 1 2 29.95 26.93 3.01 o -11 1 2 42.59 39.81 2.54 o -9 1 2 6.05 5.80 1.49 o -7 1 2 1170.47 1191.43 18.19 o -5 1 2 1242.47 1192.09 22.15 o -3 1 2 9368.57 9312.16 124.67 o -1 1 2 3938.96 4064.40 37.33 o 1 1 2 7416.48 7503.71 68.07 o 3 1 2 540.99 483.88 5.25 o 5 1 2 144.97 116.57 2.55 o 7 1 2 271.10 238.41 5.20 o 9 1 2 145.16 151.23 16.08 o 11 1 2 19.13 10.40 3.21 o 13 1 2 54.19 67.79 9.61 o -16 2 2 2.39 8.08 2.32 o -14 2 2 16.80 11.29 2.13 o -12 2 2 79.66 92.86 3.78 o -10 2 2 57.48 81.03 3.72 o -8 2 2 1442.76 1503.35 22.73 o -6 2 2 3.43 5.59 1.03 o -4 2 2 1320.06 1268.14 22.99 o -2 2 2 18682.01 17467.50 267.14 o 0 2 2 11019.39 10394.40 120.92 o 2 2 2 1022.55 979.56 9.56 o 4 2 2 412.18 379.96 6.05 o 6 2 2 5.51 0.98 1.33 o 8 2 2 711.82 649.49 9.92 o 10 2 2 75.37 98.08 6.60 o 12 2 2 44.39 22.38 4.27 o -15 3 2 88.62 67.81 3.96 o -13 3 2 24.85 20.98 2.81 o -11 3 2 7.53 9.84 2.10 o -9 3 2 1433.70 1442.97 22.38 o -7 3 2 715.56 833.35 13.42 o -5 3 2 761.63 773.85 14.17 o -3 3 2 493.59 210.99 36.55 o -1 3 2 11914.88 11721.76 102.21 o 1 3 2 616.51 578.52 9.15 o 3 3 2 184.24 194.67 6.76 o 5 3 2 349.72 293.07 9.77 o 7 3 2 2.97 1.14 1.33 o 9 3 2 24.90 12.87 3.39 o 11 3 2 3.03 0.00 2.66 o 13 3 2 2.93 0.00 3.39 o -16 4 2 24.48 16.80 2.81 o -14 4 2 53.16 61.68 4.24 o -12 4 2 18.78 11.88 2.27 o -10 4 2 237.01 279.34 7.76 o -8 4 2 12.06 13.37 1.90 o -6 4 2 955.09 949.26 17.40 o -4 4 2 362.29 422.75 6.10 o -2 4 2 229.17 207.78 7.53 o 0 4 2 347.55 196.31 6.68 o 2 4 2 8.01 4.35 0.76 o 4 4 2 2118.35 2211.06 27.56 o 6 4 2 19.48 15.21 1.57 o 8 4 2 0.88 0.43 1.97 o 10 4 2 13.97 11.29 3.51 o 12 4 2 19.48 28.80 5.16 o -15 5 2 13.20 16.46 3.54 o -13 5 2 12.72 8.87 2.27 o -11 5 2 5.53 2.13 1.84 o -9 5 2 262.48 258.73 7.20 o -7 5 2 405.05 453.49 8.55 o -5 5 2 709.80 785.97 43.94 o -3 5 2 370.62 384.04 5.99 o -1 5 2 8.85 10.74 1.05 o 1 5 2 442.05 533.05 18.23 o 3 5 2 4641.95 4578.61 48.27 o 5 5 2 291.19 362.68 6.50 o 7 5 2 209.22 164.89 4.51 o 9 5 2 36.02 49.44 10.65 o 11 5 2 28.33 37.08 5.29 o -14 6 2 128.61 111.88 6.39 o -12 6 2 30.27 32.89 3.12 o -10 6 2 2.78 13.58 2.12 o -8 6 2 136.60 196.48 5.30 o -6 6 2 430.30 438.31 8.27 o -4 6 2 18.24 40.53 2.10 o -2 6 2 4097.20 4001.04 47.07 o 0 6 2 450.44 407.76 7.90 o 2 6 2 684.89 749.96 9.43 o 4 6 2 945.33 1113.64 13.60 o 6 6 2 1.84 13.05 1.70 o 8 6 2 145.91 153.26 6.49 o 10 6 2 51.62 46.37 7.10 o 12 6 2 0.22 0.00 3.54 o -13 7 2 0.66 2.09 4.39 o -11 7 2 73.23 82.90 7.10 o -9 7 2 0.70 1.45 1.55 o -7 7 2 17.47 25.87 2.31 o -5 7 2 1.00 0.04 0.78 o -3 7 2 267.83 209.29 3.99 o -1 7 2 130.81 97.88 2.79 o 1 7 2 245.21 253.34 4.28 o 3 7 2 1031.33 1122.35 13.68 o 5 7 2 36.35 29.30 1.98 o 7 7 2 2.92 0.00 1.47 o 9 7 2 6.82 4.40 4.18 o 11 7 2 9.61 17.59 4.80 o -14 8 2 0.51 0.84 2.57 o -12 8 2 10.29 17.30 3.22 o -10 8 2 247.89 257.42 14.41 o -8 8 2 93.80 57.62 5.85 o -6 8 2 152.14 163.28 5.90 o -4 8 2 6.57 2.63 1.01 o -2 8 2 743.81 765.60 11.13 o 0 8 2 389.56 349.42 5.54 o 2 8 2 174.40 205.69 4.41 o 4 8 2 190.21 256.94 5.42 o 6 8 2 69.05 57.57 3.09 o 8 8 2 47.39 43.98 5.35 o 10 8 2 2.03 5.43 3.68 o -13 9 2 0.90 0.00 2.30 o -11 9 2 19.83 13.44 2.95 o -9 9 2 208.75 264.37 8.80 o -7 9 2 1028.56 1074.17 21.98 o -5 9 2 140.79 145.07 4.88 o -3 9 2 315.34 286.82 6.78 o -1 9 2 1303.64 1247.72 15.14 o 1 9 2 64.79 62.24 2.51 o 3 9 2 844.16 911.67 12.10 o 5 9 2 232.37 267.95 6.17 o 7 9 2 5.58 4.40 1.98 o 9 9 2 8.92 5.63 3.68 o -12 10 2 30.20 27.69 5.43 o -10 10 2 5.64 0.00 2.09 o -8 10 2 0.39 0.00 2.15 o -6 10 2 61.84 57.19 3.64 o -4 10 2 104.68 111.18 4.51 o -2 10 2 201.38 219.18 6.04 o 0 10 2 16.89 14.38 2.24 o 2 10 2 273.11 257.25 6.01 o 4 10 2 35.22 34.21 2.77 o 6 10 2 15.73 19.13 2.77 o 8 10 2 46.61 53.72 4.19 o -9 11 2 8.12 4.15 2.71 o -7 11 2 28.01 16.44 3.09 o -5 11 2 230.01 209.91 6.49 o -3 11 2 9.98 9.04 2.43 o -1 11 2 741.96 721.70 13.64 o 1 11 2 35.76 32.81 3.02 o 3 11 2 11.95 13.50 2.27 o 5 11 2 7.11 8.70 2.10 o 7 11 2 3.02 7.77 2.78 o -8 12 2 121.23 112.71 6.32 o -6 12 2 62.55 61.37 4.29 o -4 12 2 80.57 72.00 4.15 o -2 12 2 273.23 271.21 7.60 o 0 12 2 3.53 6.35 2.01 o 2 12 2 93.47 92.01 4.76 o 4 12 2 138.61 124.88 6.12 o -5 13 2 0.97 2.22 2.10 o -3 13 2 5.82 2.49 1.89 o -1 13 2 11.85 9.20 2.44 o 1 13 2 37.46 31.60 3.68 o 3 13 2 0.48 1.06 2.92 o -17 1 3 66.82 35.37 3.29 o -15 1 3 315.74 320.73 7.63 o -13 1 3 646.71 661.65 11.34 o -11 1 3 8.12 13.28 2.38 o -9 1 3 1.43 6.97 1.52 o -7 1 3 2342.92 2275.29 62.58 o -5 1 3 235.67 251.32 4.97 o -3 1 3 6240.04 6310.31 122.49 o -1 1 3 6012.18 5984.25 55.32 o 1 1 3 29.53 38.86 1.07 o 3 1 3 37.33 61.29 2.86 o 7 1 3 0.03 2.64 3.97 o 9 1 3 10.87 3.87 2.79 o 11 1 3 0.56 2.61 3.09 o -16 2 3 0.92 2.06 2.01 o -14 2 3 144.31 138.38 5.49 o -12 2 3 327.17 331.29 8.29 o -10 2 3 7.01 7.70 2.03 o -8 2 3 1522.64 1592.72 31.49 o -6 2 3 71.44 102.12 2.98 o -4 2 3 293.22 274.19 5.59 o -2 2 3 507.30 480.89 7.13 o 0 2 3 306.66 348.92 5.30 o 2 2 3 975.28 911.00 9.19 o 4 2 3 626.50 618.65 9.53 o 6 2 3 0.11 0.00 0.76 o 8 2 3 0.98 0.00 2.36 o 10 2 3 52.70 93.19 11.70 o 12 2 3 0.44 6.42 3.68 o -17 3 3 9.60 7.71 2.53 o -15 3 3 3.49 5.47 1.99 o -13 3 3 42.38 42.71 5.00 o -11 3 3 154.51 134.93 4.69 o -9 3 3 276.15 255.39 6.12 o -7 3 3 167.06 154.71 5.85 o -5 3 3 2.95 1.71 0.66 o -3 3 3 1535.12 1571.77 25.81 o -1 3 3 1058.93 1092.36 15.74 o 1 3 3 259.38 256.40 4.17 o 3 3 3 2850.53 2990.87 36.34 o 5 3 3 25.66 42.03 3.70 o 7 3 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