#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/54/2225417.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225417_Fobs loop_ _publ_author_name 'Saeed, Aamer' 'Khera, Rasheed Ahmad' 'Parvez, Masood' _publ_section_title ; 4,4,6-Trimethyl-1-(3-methylphenyl)-3,4-dihydropyrimidine-2(1H)-thione ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o635 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.5904 _cell_length_b 16.9189 _cell_length_c 30.5713 _exptl_crystal_F_000 2112.00 _reflns_d_resolution_high 0.8302 _[local]_cod_data_source_file zs2028Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound X' _shelx_refln_list_code 4 _shelx_f_calc_maximum 333.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 782.83 659.32 26.89 o 6 0 0 2329.01 2066.64 69.76 o 8 0 0 565.26 445.80 49.39 o 10 0 0 2872.15 3240.55 188.42 o 12 0 0 110.34 97.80 58.35 o 4 1 0 1700.72 1841.87 38.14 o 6 1 0 1203.82 1288.17 29.01 o 8 1 0 1507.08 1492.73 49.88 o 10 1 0 188.04 208.96 32.60 o 12 1 0 370.38 512.95 73.19 o 4 2 0 2245.31 2155.64 44.99 o 6 2 0 630.84 699.26 23.47 o 8 2 0 2680.43 2695.65 83.78 o 10 2 0 31.62 -6.52 38.96 o 12 2 0 9.60 0.00 16.30 o 2 3 0 2289.63 2402.25 47.43 o 4 3 0 4374.82 4616.89 87.86 o 6 3 0 238.24 263.40 18.42 o 8 3 0 209.95 255.58 29.67 o 10 3 0 9.15 -42.22 42.54 o 12 3 0 29.37 11.57 50.69 o 0 4 0 9709.36 10549.01 257.05 o 2 4 0 13.20 16.30 11.41 o 4 4 0 101.32 125.02 11.74 o 6 4 0 62.29 34.23 16.46 o 8 4 0 14.33 55.26 38.96 o 10 4 0 159.49 105.95 45.80 o 12 4 0 138.98 104.32 50.37 o 2 5 0 70.34 22.66 13.04 o 4 5 0 5118.67 5310.44 88.18 o 6 5 0 6263.59 6084.03 163.81 o 8 5 0 9254.60 9688.22 397.39 o 10 5 0 1083.77 1120.12 83.78 o 0 6 0 10504.70 10342.82 254.60 o 2 6 0 2.98 12.88 13.04 o 4 6 0 15198.58 15958.39 244.82 o 6 6 0 13360.06 13869.26 256.72 o 8 6 0 2702.07 2567.20 151.42 o 10 6 0 478.35 480.52 63.73 o 12 6 0 273.57 319.80 65.04 o 2 7 0 20924.47 21007.23 351.10 o 4 7 0 1273.04 1373.58 38.96 o 6 7 0 771.16 842.69 35.21 o 8 7 0 82.08 180.76 51.02 o 0 8 0 2566.50 2641.37 82.97 o 2 8 0 569.33 634.71 24.45 o 4 8 0 1810.74 1986.61 50.37 o 6 8 0 187.68 144.74 29.18 o 8 8 0 186.28 63.24 43.68 o 2 9 0 0.27 14.67 17.93 o 4 9 0 734.40 769.35 35.86 o 6 9 0 150.93 161.69 33.90 o 8 9 0 329.76 423.96 59.82 o 0 10 0 383.16 396.08 35.37 o 2 10 0 87.06 52.16 22.82 o 4 10 0 657.21 644.82 34.88 o 6 10 0 758.54 642.86 36.84 o 8 10 0 271.91 350.93 77.10 o 10 10 0 133.15 198.53 75.14 o 2 11 0 23574.97 23922.43 499.59 o 4 11 0 14845.57 14856.21 324.85 o 6 11 0 86.54 118.82 32.60 o 8 11 0 132.92 126.81 58.19 o 0 12 0 20249.85 20230.38 700.56 o 2 12 0 7772.74 7910.57 222.65 o 4 12 0 2953.18 3001.43 106.11 o 6 12 0 827.75 794.12 50.04 o 2 13 0 3934.79 3895.79 136.10 o 4 13 0 3785.24 3931.16 131.70 o 6 13 0 327.87 344.90 70.41 o 8 13 0 181.33 256.88 55.58 o 0 14 0 959.82 1061.44 86.88 o 2 14 0 10.41 -46.70 31.13 o 4 14 0 66.09 52.16 29.18 o 6 14 0 133.07 173.27 63.73 o 2 15 0 47.19 83.29 37.65 o 4 15 0 13.07 53.95 34.39 o 6 15 0 255.36 337.40 45.97 o 0 16 0 13119.69 14021.82 545.06 o 2 16 0 6012.85 6287.29 198.53 o 4 16 0 1966.34 1887.18 140.34 o 6 16 0 503.47 511.16 58.35 o 2 17 0 3126.83 3108.68 193.64 o 4 17 0 906.21 929.08 105.79 o 6 17 0 3537.20 3931.16 187.28 o 0 18 0 686.13 844.98 93.89 o 4 19 0 0.69 19.72 66.99 o 2 20 0 55.75 -66.50 71.72 o 1 1 1 2.19 3.16 8.07 o 2 1 1 22473.74 21398.92 318.99 o 3 1 1 3213.37 3543.78 47.60 o 4 1 1 35.77 39.04 7.45 o 5 1 1 2.30 28.16 7.12 o 6 1 1 140.62 143.40 12.14 o 7 1 1 43.46 75.91 9.22 o 8 1 1 3.43 15.07 11.85 o 9 1 1 84.74 48.06 13.77 o 10 1 1 334.19 362.51 26.23 o 11 1 1 87.75 59.62 29.29 o 12 1 1 26.26 31.57 37.55 o 3 2 1 27927.12 25625.79 281.60 o 4 2 1 4725.62 4525.39 63.27 o 5 2 1 2116.04 1881.89 29.68 o 6 2 1 262.71 308.61 15.57 o 7 2 1 54.33 73.73 8.54 o 8 2 1 27.24 45.94 12.79 o 9 2 1 627.26 616.74 41.56 o 10 2 1 219.21 225.78 46.21 o 11 2 1 55.80 59.66 31.11 o 12 2 1 93.70 154.68 52.16 o 1 3 1 3300.09 3183.38 48.29 o 2 3 1 1921.49 2011.97 28.18 o 3 3 1 12047.93 11926.81 130.98 o 4 3 1 3126.42 3223.30 43.70 o 5 3 1 7212.18 7069.24 97.62 o 6 3 1 1953.61 1961.09 36.61 o 7 3 1 3232.20 3366.65 62.40 o 8 3 1 875.80 842.69 36.39 o 9 3 1 1418.90 1474.40 54.22 o 10 3 1 140.22 190.17 31.49 o 11 3 1 72.15 66.50 42.22 o 12 3 1 165.51 186.27 37.33 o 0 4 1 2136.60 2486.03 48.25 o 1 4 1 10953.33 11413.04 224.28 o 2 4 1 3685.09 3628.39 48.12 o 3 4 1 762.32 732.82 15.44 o 4 4 1 4906.97 4853.17 59.64 o 5 4 1 1.36 14.51 11.33 o 6 4 1 2171.52 2002.47 40.72 o 7 4 1 2.66 -8.83 27.71 o 8 4 1 0.13 31.73 32.52 o 9 4 1 357.77 293.92 36.76 o 10 4 1 264.90 373.92 50.04 o 11 4 1 66.69 26.99 39.77 o 12 4 1 11.28 -41.56 37.22 o 1 5 1 863.23 857.90 16.71 o 2 5 1 1182.98 1190.22 19.71 o 3 5 1 45.79 86.48 9.81 o 4 5 1 185.85 170.99 16.30 o 5 5 1 1300.64 1473.00 44.91 o 6 5 1 140.52 200.15 17.60 o 7 5 1 2316.66 2214.36 72.54 o 8 5 1 462.23 489.04 37.79 o 9 5 1 279.02 175.11 22.07 o 10 5 1 391.22 324.20 52.32 o 11 5 1 102.88 111.00 47.60 o 12 5 1 44.04 60.15 56.89 o 0 6 1 210.10 180.76 16.30 o 1 6 1 14.55 -4.10 10.37 o 2 6 1 78.15 63.52 10.68 o 3 6 1 40.39 59.11 10.37 o 4 6 1 1508.33 1501.56 25.36 o 5 6 1 37.53 32.73 10.59 o 6 6 1 123.52 162.12 13.82 o 7 6 1 300.53 286.48 31.28 o 8 6 1 120.36 83.77 34.47 o 9 6 1 2.56 14.88 29.42 o 10 6 1 217.34 283.96 41.60 o 11 6 1 173.03 108.45 38.43 o 12 6 1 3.54 -49.70 37.26 o 1 7 1 3830.34 3829.21 51.13 o 2 7 1 684.09 696.17 18.09 o 3 7 1 9808.02 10184.34 140.42 o 4 7 1 4.88 2.74 11.02 o 5 7 1 16.58 -12.69 9.68 o 6 7 1 387.15 414.02 23.22 o 7 7 1 990.61 940.97 39.28 o 8 7 1 1655.93 1496.36 184.68 o 11 7 1 5.09 38.36 49.88 o 0 8 1 7751.19 7903.40 143.60 o 1 8 1 2548.35 2540.87 42.79 o 2 8 1 29.44 46.82 21.11 o 3 8 1 978.44 925.41 22.59 o 4 8 1 8444.17 8891.07 118.48 o 5 8 1 2010.93 2178.47 52.73 o 6 8 1 469.30 440.68 21.99 o 7 8 1 1.63 25.22 16.82 o 8 8 1 205.50 158.85 32.56 o 10 8 1 340.91 393.71 49.08 o 11 8 1 217.91 243.81 44.90 o 1 9 1 2.56 2.48 11.39 o 2 9 1 789.95 764.77 20.51 o 3 9 1 57.22 36.47 12.62 o 4 9 1 794.87 803.50 25.87 o 5 9 1 37.02 38.96 16.19 o 6 9 1 131.84 218.17 26.81 o 7 9 1 17.27 -5.72 17.23 o 8 9 1 140.19 188.26 49.39 o 11 9 1 33.38 27.58 43.68 o 0 10 1 1050.79 948.97 34.88 o 1 10 1 576.85 582.18 19.94 o 2 10 1 212.64 194.33 35.21 o 3 10 1 146.71 184.95 17.81 o 4 10 1 1643.77 1521.07 37.86 o 5 10 1 1960.81 2027.06 58.19 o 6 10 1 145.28 187.91 25.39 o 7 10 1 630.27 628.56 32.07 o 8 10 1 279.20 293.74 42.52 o 11 10 1 21.57 52.16 68.30 o 1 11 1 46.07 60.48 16.49 o 2 11 1 4764.63 4803.80 86.79 o 3 11 1 34.65 -0.24 17.90 o 4 11 1 2407.80 2490.79 52.65 o 5 11 1 47.31 112.82 62.84 o 6 11 1 338.51 273.03 37.08 o 7 11 1 717.00 637.69 49.39 o 8 11 1 297.39 288.83 63.08 o 0 12 1 2762.01 2579.59 94.38 o 1 12 1 315.23 279.82 40.34 o 2 12 1 2554.41 2774.29 70.64 o 3 12 1 2088.35 2145.30 89.73 o 4 12 1 133.44 157.46 23.34 o 5 12 1 338.00 374.10 32.03 o 6 12 1 2.85 -15.50 42.46 o 7 12 1 154.67 131.45 64.47 o 8 12 1 561.70 444.17 73.19 o 1 13 1 989.72 1072.64 88.51 o 2 13 1 131.81 121.91 25.67 o 3 13 1 925.72 984.95 40.27 o 4 13 1 102.35 155.77 33.15 o 5 13 1 1018.90 1027.42 43.01 o 6 13 1 1005.78 947.58 52.35 o 7 13 1 449.00 441.64 90.30 o 8 13 1 1.10 60.15 53.79 o 9 13 1 16.63 -4.89 50.69 o 0 14 1 3204.68 3176.49 113.77 o 1 14 1 5377.56 5313.52 116.52 o 2 14 1 2996.64 3028.30 76.89 o 3 14 1 1662.56 1593.59 55.79 o 4 14 1 297.93 300.02 51.43 o 5 14 1 1203.22 1146.50 180.03 o 6 14 1 11.40 1.49 39.15 o 7 14 1 0.15 -8.15 39.28 o 1 15 1 459.82 480.05 90.46 o 2 15 1 13.19 43.12 54.69 o 3 15 1 360.89 334.46 31.62 o 4 15 1 86.31 156.64 66.67 o 5 15 1 38.01 55.74 47.43 o 6 15 1 27.48 7.60 31.52 o 0 16 1 2849.49 3117.65 121.76 o 1 16 1 23.89 -2.43 60.88 o 2 16 1 1923.70 1910.24 86.07 o 3 16 1 1.09 13.29 47.31 o 4 16 1 1730.07 1766.40 91.60 o 5 16 1 49.34 58.84 48.90 o 6 16 1 211.20 169.02 49.78 o 7 16 1 217.50 156.10 44.92 o 1 17 1 159.66 83.29 78.08 o 2 17 1 755.53 789.56 63.57 o 3 17 1 20.87 34.23 55.26 o 4 17 1 159.38 210.58 50.44 o 5 17 1 94.12 87.69 40.91 o 6 17 1 5.35 50.53 50.53 o 0 18 1 167.42 242.87 84.27 o 1 18 1 206.92 197.39 60.15 o 2 18 1 17.23 34.30 43.19 o 3 18 1 293.17 207.23 72.86 o 4 18 1 379.37 297.14 77.91 o 1 19 1 148.70 40.75 43.85 o 2 19 1 7.98 -27.55 44.01 o 3 19 1 2.71 -23.72 40.22 o 4 19 1 49.41 81.68 40.14 o 0 20 1 5.31 50.53 66.50 o 1 20 1 26.18 17.93 60.31 o 2 20 1 111.53 87.69 74.82 o 2 0 2 845.75 796.40 31.95 o 3 0 2 3380.52 3144.70 126.81 o 4 0 2 322.04 276.61 17.44 o 5 0 2 10847.33 10682.18 183.53 o 6 0 2 89.53 84.76 11.08 o 7 0 2 0.19 -1.63 13.20 o 8 0 2 33.74 11.57 13.20 o 9 0 2 1064.06 1101.37 40.26 o 10 0 2 11.06 -12.88 25.75 o 11 0 2 476.36 520.29 42.38 o 12 0 2 68.73 120.62 54.93 o 3 1 2 36096.63 34758.20 433.11 o 4 1 2 1812.29 1929.87 46.13 o 5 1 2 3166.09 3314.04 60.24 o 6 1 2 157.61 142.56 8.49 o 7 1 2 716.43 629.84 15.00 o 8 1 2 275.87 252.02 14.47 o 9 1 2 3.27 21.19 19.56 o 10 1 2 282.99 216.00 25.67 o 11 1 2 100.76 136.69 27.72 o 12 1 2 28.00 56.52 35.26 o 2 2 2 11595.75 11025.24 142.36 o 3 2 2 3166.64 3037.60 71.23 o 4 2 2 599.61 503.77 29.99 o 5 2 2 108.04 113.56 9.91 o 6 2 2 339.28 219.35 15.16 o 7 2 2 34.57 20.14 8.63 o 8 2 2 203.19 165.39 14.28 o 9 2 2 6.27 9.02 17.69 o 10 2 2 118.00 56.49 51.34 o 11 2 2 8.53 -44.35 29.57 o 12 2 2 1.25 -58.68 39.12 o 1 3 2 1046.99 1004.71 18.90 o 2 3 2 111248.24 104292.05 3285.53 o 3 3 2 737.53 614.96 13.36 o 4 3 2 13284.93 12197.08 132.37 o 5 3 2 13.93 27.13 12.22 o 6 3 2 205.22 301.18 12.76 o 7 3 2 69.95 44.79 24.53 o 8 3 2 3784.12 3793.18 90.15 o 9 3 2 240.41 273.61 19.75 o 10 3 2 1056.24 999.34 84.27 o 11 3 2 286.96 186.14 53.95 o 12 3 2 8.80 -8.13 31.30 o 0 4 2 14195.11 13547.83 225.59 o 1 4 2 3568.59 3510.21 47.37 o 2 4 2 1962.99 1868.08 40.18 o 3 4 2 33.01 34.72 8.07 o 4 4 2 8732.49 8921.24 102.46 o 5 4 2 1329.16 1385.68 23.81 o 6 4 2 2270.87 2244.72 40.62 o 7 4 2 0.48 -3.34 13.95 o 8 4 2 768.72 642.86 57.37 o 9 4 2 430.97 421.27 29.01 o 10 4 2 268.44 278.04 43.93 o 11 4 2 620.88 627.02 60.31 o 12 4 2 79.06 63.90 34.21 o 1 5 2 2829.39 2744.07 38.90 o 2 5 2 2787.35 2900.62 39.94 o 3 5 2 17009.70 16897.21 210.10 o 4 5 2 1171.64 1275.27 30.24 o 5 5 2 229.02 210.95 11.17 o 6 5 2 331.57 322.24 15.84 o 7 5 2 3679.23 3889.80 96.67 o 8 5 2 2.65 66.81 24.97 o 9 5 2 108.88 93.07 53.79 o 10 5 2 330.64 358.19 40.22 o 11 5 2 269.90 329.35 43.94 o 12 5 2 57.72 152.24 46.29 o 0 6 2 168.74 174.24 15.97 o 1 6 2 34.83 58.97 10.49 o 2 6 2 55.25 65.39 9.81 o 3 6 2 5.04 17.55 9.86 o 4 6 2 18.63 14.25 8.61 o 5 6 2 1191.87 1207.03 21.84 o 6 6 2 142.81 141.99 13.20 o 7 6 2 113.16 145.11 31.62 o 8 6 2 9.83 21.52 33.50 o 9 6 2 1895.29 1887.44 85.74 o 10 6 2 36.38 64.07 33.63 o 11 6 2 481.42 699.26 79.05 o 12 6 2 0.09 46.79 37.98 o 1 7 2 6194.84 6441.81 84.68 o 2 7 2 221.38 234.45 16.06 o 3 7 2 4747.29 4584.14 61.83 o 4 7 2 0.11 -8.39 10.97 o 5 7 2 93.74 98.61 11.35 o 6 7 2 7.20 4.92 19.40 o 7 7 2 2856.94 2932.40 82.98 o 8 7 2 499.78 491.55 40.91 o 9 7 2 189.29 101.06 50.37 o 10 7 2 63.96 105.95 59.00 o 11 7 2 270.93 328.47 54.20 o 0 8 2 16221.70 15917.64 275.14 o 1 8 2 2.11 5.87 15.40 o 2 8 2 2982.41 2774.67 43.52 o 3 8 2 142.56 170.53 26.89 o 4 8 2 1287.41 1268.26 25.36 o 5 8 2 37.80 50.41 17.77 o 6 8 2 906.70 824.84 28.98 o 7 8 2 435.16 402.44 63.41 o 8 8 2 158.05 94.55 33.16 o 10 8 2 539.25 601.23 54.46 o 1 9 2 68.80 104.67 34.96 o 2 9 2 8083.28 8041.54 110.01 o 3 9 2 231.25 245.80 15.64 o 4 9 2 2485.20 2394.72 48.84 o 5 9 2 422.78 436.26 37.16 o 6 9 2 604.31 542.50 25.69 o 7 9 2 243.00 209.51 43.85 o 8 9 2 240.37 248.38 28.65 o 11 9 2 47.15 61.94 65.52 o 0 10 2 2074.93 2030.13 50.86 o 1 10 2 970.81 842.18 23.97 o 2 10 2 224.22 245.44 57.78 o 3 10 2 994.97 1025.48 30.16 o 4 10 2 2832.65 2898.15 71.64 o 5 10 2 2678.15 2539.42 57.68 o 6 10 2 597.33 568.46 24.54 o 7 10 2 964.80 912.81 53.71 o 8 10 2 337.50 334.75 43.49 o 11 10 2 34.96 37.31 48.12 o 1 11 2 1303.40 1299.19 36.34 o 2 11 2 247.49 264.59 21.31 o 3 11 2 1176.07 1098.68 34.06 o 4 11 2 6.74 12.19 22.66 o 5 11 2 888.96 821.07 45.07 o 6 11 2 1.76 48.90 29.18 o 7 11 2 36.61 42.94 35.85 o 8 11 2 7.17 -8.15 52.32 o 0 12 2 2080.39 1954.34 78.56 o 1 12 2 3982.83 4111.38 91.33 o 2 12 2 1490.29 1499.42 50.04 o 3 12 2 902.82 917.43 54.60 o 4 12 2 823.22 899.90 46.48 o 5 12 2 3007.43 2958.75 76.04 o 6 12 2 0.10 -48.17 40.75 o 7 12 2 629.25 561.69 82.31 o 8 12 2 13.27 40.75 60.31 o 1 13 2 1138.88 1139.40 43.31 o 2 13 2 1.35 -32.66 21.77 o 3 13 2 2581.75 2633.20 67.37 o 4 13 2 18.79 37.21 27.64 o 5 13 2 495.07 512.14 34.86 o 6 13 2 711.38 652.92 92.66 o 7 13 2 127.49 216.56 52.81 o 8 13 2 120.84 114.42 57.05 o 9 13 2 2.21 -50.53 73.51 o 0 14 2 3511.11 3628.48 126.49 o 1 14 2 13.22 51.65 32.52 o 2 14 2 1195.33 1195.83 45.41 o 3 14 2 11.60 -31.23 32.44 o 4 14 2 2418.49 2525.49 70.24 o 5 14 2 52.66 69.62 32.67 o 6 14 2 2170.88 2126.69 67.12 o 7 14 2 42.90 37.27 82.88 o 1 15 2 180.19 115.43 36.72 o 2 15 2 877.94 966.41 43.94 o 3 15 2 82.83 84.95 45.58 o 4 15 2 792.21 876.33 98.04 o 5 15 2 0.19 -52.04 34.69 o 6 15 2 10.44 39.31 52.97 o 0 16 2 233.29 212.39 73.02 o 1 16 2 598.29 631.77 37.33 o 2 16 2 186.06 191.59 31.01 o 3 16 2 51.94 56.30 58.03 o 4 16 2 839.43 844.64 67.70 o 5 16 2 442.32 445.02 53.88 o 6 16 2 431.19 473.51 86.06 o 7 16 2 235.32 171.15 47.60 o 1 17 2 1157.63 968.00 72.45 o 2 17 2 156.65 213.15 47.60 o 3 17 2 869.46 919.30 66.18 o 4 17 2 11.00 -71.15 47.43 o 5 17 2 479.97 380.27 91.28 o 6 17 2 43.13 27.55 44.01 o 0 18 2 185.02 111.00 63.73 o 1 18 2 1373.13 1323.22 87.25 o 2 18 2 23.08 -47.06 38.03 o 3 18 2 214.28 270.25 55.91 o 4 18 2 3.67 0.18 43.22 o 5 18 2 1612.73 1759.55 159.25 o 1 19 2 1.03 -53.95 42.71 o 2 19 2 19.33 55.26 40.75 o 3 19 2 123.36 153.54 72.04 o 0 20 2 406.87 480.52 83.13 o 1 20 2 23.73 -50.53 46.62 o 2 20 2 38.22 34.23 69.93 o 2 1 3 210.85 317.90 10.38 o 3 1 3 18076.05 16522.27 248.66 o 4 1 3 844.61 813.61 19.35 o 5 1 3 713.15 669.05 15.00 o 6 1 3 0.91 5.70 6.92 o 7 1 3 1059.76 1022.96 22.75 o 8 1 3 61.42 31.70 9.34 o 9 1 3 87.02 67.94 16.54 o 10 1 3 27.36 47.74 24.45 o 11 1 3 176.04 157.62 37.82 o 12 1 3 0.05 -10.64 36.51 o 0 2 3 140.18 -12.22 8.15 o 2 2 3 46.75 59.97 12.96 o 3 2 3 1684.03 1594.37 22.76 o 4 2 3 447.19 471.85 15.00 o 5 2 3 3888.40 3852.15 61.19 o 6 2 3 12.79 19.16 9.86 o 7 2 3 17.86 10.19 10.55 o 8 2 3 384.91 349.19 15.23 o 9 2 3 538.68 402.70 38.06 o 10 2 3 123.89 116.43 25.39 o 11 2 3 126.13 173.27 36.19 o 12 2 3 6.53 18.52 60.31 o 1 3 3 3204.29 3228.24 45.06 o 2 3 3 1020.11 1084.01 16.94 o 3 3 3 489.66 462.04 14.67 o 4 3 3 401.09 465.90 16.46 o 5 3 3 1767.74 1809.79 44.82 o 6 3 3 1294.64 1333.11 25.10 o 7 3 3 252.16 255.01 13.86 o 8 3 3 1527.43 1427.02 47.19 o 9 3 3 199.45 157.34 21.84 o 10 3 3 23.21 -29.60 24.32 o 11 3 3 79.71 -9.10 57.05 o 12 3 3 50.56 60.44 35.76 o 0 4 3 24132.27 24411.91 403.74 o 1 4 3 18525.41 17471.89 203.77 o 2 4 3 10.98 -5.53 7.47 o 3 4 3 9748.44 9540.14 113.39 o 4 4 3 763.87 804.43 17.20 o 5 4 3 17310.04 17275.44 197.92 o 6 4 3 669.16 654.18 19.02 o 7 4 3 39.97 14.62 31.62 o 8 4 3 91.38 115.93 59.74 o 9 4 3 439.60 475.68 84.11 o 10 4 3 135.86 93.53 69.52 o 11 4 3 272.39 312.25 48.74 o 12 4 3 20.80 67.78 32.98 o 1 5 3 3017.57 3030.27 40.86 o 2 5 3 47.10 33.44 9.01 o 3 5 3 3615.57 3563.32 65.04 o 4 5 3 5692.88 6058.16 73.19 o 5 5 3 88.61 107.44 9.70 o 6 5 3 1115.45 1147.94 24.92 o 7 5 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