#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:33:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181175 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/54/2225443.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225443_Fobs loop_ _publ_author_name 'Benzerka, Saida' 'Bouraiou, Abdelmalek' 'Bouacida, Sofiane' 'Roisnel, Thierry' 'Belfaitah, Ali' _publ_section_title ; 2-Bromoethyl 2-chloro-6-methylquinoline-3-carboxylate ; _journal_coeditor_code BQ2201 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1006 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.167 _cell_angle_gamma 90.000 _cell_length_a 6.1740 _cell_length_b 29.0515 _cell_length_c 7.2875 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.7706 _cod_data_source_file bq2201Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' import in P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 211.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7045.03 7723.67 215.43 o 4 0 0 2971.10 3110.42 136.81 o 6 0 0 24.47 43.03 24.53 o 1 1 0 7867.99 8577.92 178.47 o 2 1 0 26178.13 27403.51 582.23 o 3 1 0 1030.78 1177.97 39.16 o 4 1 0 132.19 94.72 11.13 o 5 1 0 146.10 188.73 23.30 o 6 1 0 117.93 155.04 18.59 o 7 1 0 204.33 202.41 23.56 o 1 2 0 1229.69 1220.44 29.16 o 2 2 0 52.21 51.79 5.32 o 3 2 0 69.99 71.21 7.44 o 4 2 0 1709.47 1611.77 53.75 o 5 2 0 763.42 719.68 32.36 o 6 2 0 819.25 866.65 38.97 o 7 2 0 168.33 169.52 23.14 o 1 3 0 95.78 93.94 3.07 o 2 3 0 498.51 393.55 12.79 o 3 3 0 472.68 322.75 11.94 o 4 3 0 2213.39 2322.90 74.27 o 5 3 0 674.36 667.61 30.03 o 6 3 0 189.80 203.34 20.01 o 7 3 0 477.74 506.12 33.04 o 0 4 0 155.63 108.39 9.23 o 1 4 0 25258.42 25596.34 533.14 o 2 4 0 2985.83 3370.32 73.39 o 3 4 0 65.45 124.09 11.78 o 4 4 0 822.94 892.05 27.72 o 5 4 0 1469.66 1351.53 49.37 o 6 4 0 1888.60 1864.25 66.65 o 7 4 0 306.63 299.40 26.57 o 1 5 0 8186.88 8713.46 200.54 o 2 5 0 39.95 66.46 3.10 o 3 5 0 5559.87 5810.59 147.88 o 4 5 0 1639.51 1702.95 47.67 o 5 5 0 10.27 18.30 11.58 o 6 5 0 3.92 -13.80 13.80 o 7 5 0 16.13 26.71 19.06 o 0 6 0 221.66 283.12 8.93 o 1 6 0 21437.30 22253.69 463.05 o 2 6 0 492.42 498.02 17.95 o 3 6 0 4646.22 4902.87 125.22 o 4 6 0 0.49 -5.56 5.56 o 5 6 0 1221.04 1258.40 51.76 o 6 6 0 189.94 183.62 20.13 o 7 6 0 8.66 27.62 18.95 o 1 7 0 11371.33 11805.05 246.19 o 2 7 0 26.47 15.28 2.95 o 3 7 0 5610.99 5518.99 140.89 o 4 7 0 3.89 -0.04 6.05 o 5 7 0 844.54 889.25 36.73 o 6 7 0 35.12 15.64 14.75 o 7 7 0 636.54 722.57 38.59 o 0 8 0 1395.66 1412.59 37.75 o 1 8 0 4863.42 5501.72 119.93 o 2 8 0 148.70 180.63 6.18 o 3 8 0 2089.58 2021.69 54.49 o 4 8 0 614.98 601.35 21.10 o 5 8 0 5096.91 5228.74 136.72 o 6 8 0 1385.91 1313.43 51.95 o 7 8 0 241.04 267.72 26.22 o 1 9 0 498.30 438.47 11.08 o 2 9 0 39.52 25.84 3.13 o 3 9 0 3673.33 3359.15 77.62 o 4 9 0 1417.69 1416.98 41.08 o 5 9 0 609.71 604.13 23.03 o 6 9 0 283.56 290.15 23.55 o 7 9 0 362.74 406.19 42.06 o 0 10 0 3321.90 3403.48 84.86 o 1 10 0 312.06 356.99 10.43 o 2 10 0 23.25 22.18 7.16 o 3 10 0 590.13 699.38 18.95 o 4 10 0 577.74 556.35 25.12 o 5 10 0 805.92 810.14 31.82 o 6 10 0 2318.20 2239.30 79.87 o 7 10 0 45.06 39.22 23.34 o 1 11 0 1432.10 1728.72 35.21 o 2 11 0 2813.53 2693.51 58.36 o 3 11 0 1611.37 1545.54 37.54 o 4 11 0 264.77 251.53 13.03 o 5 11 0 107.23 103.64 10.98 o 6 11 0 237.13 266.18 22.56 o 7 11 0 314.08 305.96 32.52 o 0 12 0 13088.16 13261.70 361.15 o 1 12 0 1875.79 2094.56 42.33 o 2 12 0 1082.54 1159.55 26.83 o 3 12 0 1737.03 1691.92 41.20 o 4 12 0 3341.37 3451.86 91.81 o 5 12 0 60.36 85.68 10.92 o 6 12 0 224.59 235.79 26.72 o 7 12 0 4.18 -7.52 37.33 o 1 13 0 845.50 1088.27 25.00 o 2 13 0 14256.58 14418.94 291.39 o 3 13 0 996.09 1072.00 27.59 o 4 13 0 1326.54 1240.00 37.41 o 5 13 0 3.17 2.97 9.25 o 6 13 0 481.79 531.98 35.77 o 7 13 0 158.83 164.89 28.65 o 0 14 0 13111.02 13476.21 367.83 o 1 14 0 104.51 117.46 8.55 o 2 14 0 434.73 525.15 18.84 o 3 14 0 100.25 110.44 6.82 o 4 14 0 7902.50 7851.67 200.79 o 5 14 0 1761.82 1674.05 49.64 o 6 14 0 44.84 83.02 15.07 o 7 14 0 160.28 200.31 29.81 o 1 15 0 24.03 38.37 4.35 o 2 15 0 3903.39 3618.62 78.03 o 3 15 0 2198.06 2111.75 50.90 o 4 15 0 44.97 33.69 8.58 o 5 15 0 30.14 33.60 11.64 o 6 15 0 807.81 781.85 49.88 o 7 15 0 936.80 892.26 52.73 o 0 16 0 1940.67 2154.12 62.22 o 1 16 0 2660.28 2656.86 64.25 o 2 16 0 2576.10 2957.69 61.97 o 3 16 0 8.88 7.70 5.05 o 4 16 0 191.10 195.45 16.68 o 5 16 0 830.73 817.66 38.43 o 6 16 0 174.49 165.63 17.96 o 7 16 0 67.12 38.92 29.60 o 1 17 0 630.90 629.07 16.92 o 2 17 0 328.58 360.53 11.19 o 3 17 0 2695.45 2686.31 59.37 o 4 17 0 4321.59 4173.78 97.55 o 5 17 0 228.62 245.88 17.79 o 6 17 0 23.53 9.20 14.47 o 7 17 0 18.04 14.18 28.41 o 0 18 0 343.01 306.56 13.66 o 1 18 0 5780.52 5678.10 123.99 o 2 18 0 167.95 170.83 8.65 o 3 18 0 375.36 361.28 13.63 o 4 18 0 15.26 7.01 6.95 o 5 18 0 1529.61 1539.42 53.26 o 6 18 0 736.93 842.76 37.08 o 1 19 0 3373.74 3291.16 80.97 o 2 19 0 75.74 57.75 6.63 o 3 19 0 2512.35 2531.64 60.89 o 4 19 0 22.00 25.36 7.24 o 5 19 0 755.98 788.99 33.46 o 6 19 0 47.90 57.25 17.33 o 0 20 0 508.21 527.59 19.91 o 1 20 0 3174.74 3360.41 72.13 o 2 20 0 724.32 760.45 21.79 o 3 20 0 1987.56 1821.59 47.05 o 4 20 0 11.29 16.66 7.93 o 5 20 0 770.95 854.92 38.92 o 6 20 0 354.83 311.29 25.65 o 1 21 0 2754.40 2653.98 58.02 o 2 21 0 86.57 94.00 7.68 o 3 21 0 4412.43 4003.32 97.13 o 4 21 0 618.07 671.94 29.77 o 5 21 0 152.18 150.66 17.94 o 6 21 0 40.61 32.55 17.68 o 0 22 0 1382.66 1355.46 55.11 o 1 22 0 1102.51 1165.80 28.48 o 2 22 0 903.28 876.64 24.39 o 3 22 0 28.09 18.55 7.87 o 4 22 0 940.55 866.48 36.70 o 5 22 0 943.93 1008.61 44.39 o 6 22 0 478.67 443.70 44.47 o 1 23 0 405.92 426.89 14.20 o 2 23 0 1056.99 947.50 29.38 o 3 23 0 120.29 123.08 11.05 o 4 23 0 1066.07 1018.87 42.52 o 5 23 0 456.43 460.45 27.90 o 6 23 0 287.60 398.86 28.73 o 0 24 0 168.36 205.38 13.80 o 1 24 0 1230.29 1236.40 30.48 o 2 24 0 169.09 195.26 11.66 o 3 24 0 22.69 32.26 10.80 o 4 24 0 819.25 845.09 37.92 o 5 24 0 100.99 114.30 22.81 o 6 24 0 326.64 350.33 32.08 o 1 25 0 349.30 342.67 14.94 o 2 25 0 2808.68 2588.08 74.22 o 3 25 0 1.97 -1.36 11.48 o 4 25 0 42.54 34.94 14.22 o 5 25 0 185.56 164.96 23.64 o 0 26 0 6744.84 6963.25 243.89 o 1 26 0 86.21 75.22 11.33 o 2 26 0 100.58 117.21 11.71 o 3 26 0 0.71 -0.40 9.31 o 4 26 0 1811.36 1841.32 68.69 o 5 26 0 349.22 293.10 24.61 o 1 27 0 5.20 1.31 8.77 o 2 27 0 4115.66 3916.86 129.31 o 3 27 0 627.97 619.93 24.65 o 4 27 0 47.30 71.09 22.10 o 5 27 0 199.81 273.37 37.21 o 0 28 0 1370.67 1379.72 63.43 o 1 28 0 219.16 225.98 19.48 o 2 28 0 15.33 41.87 10.21 o 3 28 0 64.42 54.43 19.38 o 4 28 0 454.10 481.87 34.70 o 5 28 0 1045.26 990.35 46.36 o 1 29 0 327.86 310.15 16.99 o 2 29 0 461.73 516.94 22.21 o 3 29 0 651.90 633.43 25.68 o 4 29 0 381.64 386.34 26.34 o 5 29 0 46.37 46.48 37.40 o 0 30 0 12.29 33.04 25.29 o 1 30 0 741.34 751.07 29.21 o 2 30 0 190.68 164.65 13.90 o 3 30 0 188.18 184.69 15.11 o 4 30 0 71.05 62.72 25.00 o 1 31 0 1472.03 1460.94 47.53 o 2 31 0 122.69 110.82 13.39 o 3 31 0 681.40 622.93 26.32 o 4 31 0 11.80 -11.20 16.12 o 0 32 0 199.91 201.73 24.63 o 1 32 0 1460.78 1539.84 49.85 o 2 32 0 8.52 20.34 11.33 o 3 32 0 1143.42 1156.36 40.05 o 4 32 0 67.23 71.93 19.13 o 1 33 0 1819.72 1800.28 57.23 o 2 33 0 244.89 282.40 27.57 o 3 33 0 1726.52 1696.64 54.13 o 0 34 0 149.65 136.33 22.96 o 1 34 0 1373.20 1455.26 48.62 o 2 34 0 388.59 415.68 21.84 o 3 34 0 19.93 21.56 13.20 o 1 35 0 332.22 398.48 22.76 o 2 35 0 371.04 409.98 23.54 o 0 36 0 2278.40 2500.56 108.90 o 1 36 0 156.76 222.65 19.04 o 2 36 0 5.88 22.52 13.76 o 1 37 0 805.08 839.09 34.93 o -7 0 1 915.72 992.29 85.12 o -5 0 1 2675.71 2678.58 123.39 o -3 0 1 2779.11 2753.58 168.79 o -1 0 1 10160.22 10654.33 436.18 o 1 0 1 12894.01 13690.45 395.45 o 3 0 1 197.65 254.79 12.53 o 5 0 1 1258.23 1386.56 204.63 o 7 0 1 488.54 527.20 80.81 o -7 1 1 523.41 549.26 33.78 o -6 1 1 3.15 7.04 13.65 o -5 1 1 2491.07 2535.27 82.70 o -4 1 1 317.82 373.96 17.17 o -3 1 1 6508.47 6891.67 286.86 o -2 1 1 1419.17 1641.17 50.42 o -1 1 1 825.27 851.97 24.73 o 0 1 1 128.27 129.56 5.57 o 1 1 1 4985.24 5026.98 103.70 o 2 1 1 327.96 426.97 12.04 o 3 1 1 9579.19 9753.40 219.96 o 4 1 1 1839.88 1820.31 44.21 o 5 1 1 61.72 80.49 13.91 o 6 1 1 56.48 31.72 15.11 o 7 1 1 24.77 61.09 19.82 o -7 2 1 135.82 148.43 22.41 o -6 2 1 166.23 186.20 20.09 o -5 2 1 2153.24 2200.38 61.40 o -4 2 1 218.36 238.86 13.13 o -3 2 1 4553.09 4790.62 201.91 o -2 2 1 281.75 353.11 13.74 o -1 2 1 971.82 1063.80 39.43 o 0 2 1 1759.72 1581.54 33.44 o 1 2 1 11590.32 11929.94 244.21 o 2 2 1 10956.70 12050.85 277.92 o 3 2 1 46.68 40.27 5.04 o 4 2 1 477.64 459.22 17.05 o 5 2 1 1547.42 1631.69 57.69 o 6 2 1 940.96 966.74 42.34 o 7 2 1 422.87 438.42 33.30 o -7 3 1 668.84 715.67 51.51 o -6 3 1 133.93 131.24 23.38 o -5 3 1 49.05 53.61 9.50 o -4 3 1 474.84 397.91 18.33 o -3 3 1 612.32 580.31 55.53 o -2 3 1 128.65 175.44 9.53 o -1 3 1 3349.30 3587.74 92.66 o 0 3 1 13.43 20.63 2.29 o 1 3 1 28.74 15.39 1.92 o 2 3 1 3470.31 3634.56 85.56 o 3 3 1 3646.51 3333.45 86.88 o 4 3 1 7217.07 7315.62 186.71 o 5 3 1 1203.38 1132.20 43.85 o 6 3 1 2.50 4.06 14.13 o 7 3 1 524.88 576.94 34.96 o -7 4 1 41.81 36.35 22.98 o -6 4 1 437.19 430.69 28.16 o -5 4 1 338.96 338.22 15.61 o -4 4 1 1784.95 1716.96 52.92 o -3 4 1 71.45 62.26 14.84 o -2 4 1 11.99 15.58 4.83 o -1 4 1 214.47 248.39 12.92 o 0 4 1 2726.76 2838.46 57.34 o 1 4 1 9711.14 10072.41 185.35 o 2 4 1 9124.27 9412.09 217.67 o 3 4 1 2391.93 2526.16 66.95 o 4 4 1 390.77 402.01 15.90 o 5 4 1 1968.67 1907.95 65.55 o 6 4 1 2909.02 2886.88 96.45 o 7 4 1 217.12 296.97 26.95 o -7 5 1 114.18 123.98 21.37 o -6 5 1 3350.95 3206.23 104.97 o -5 5 1 963.00 939.89 30.72 o -4 5 1 285.26 317.45 20.39 o -3 5 1 205.05 209.28 16.72 o -2 5 1 9295.44 9247.31 256.77 o -1 5 1 3914.69 4315.69 98.94 o 0 5 1 621.65 592.11 16.10 o 1 5 1 248.49 258.24 6.56 o 2 5 1 4972.48 4800.61 112.15 o 3 5 1 1620.22 1601.74 44.00 o 4 5 1 1946.66 1961.23 64.36 o 5 5 1 356.66 373.68 25.04 o 6 5 1 340.71 306.80 24.84 o 7 5 1 182.54 229.95 25.01 o -7 6 1 284.41 247.81 25.73 o -6 6 1 10.08 14.75 9.09 o -5 6 1 796.19 848.87 28.57 o -4 6 1 10020.47 10150.84 284.48 o -3 6 1 0.67 2.10 3.35 o -2 6 1 1402.48 1515.04 44.52 o -1 6 1 284.40 341.62 15.17 o 0 6 1 22665.77 22062.12 502.47 o 1 6 1 296.52 332.80 7.90 o 2 6 1 2549.89 2616.11 56.55 o 3 6 1 13.64 49.36 5.96 o 4 6 1 284.78 302.82 17.53 o 5 6 1 201.27 148.77 15.69 o 6 6 1 51.70 33.69 15.89 o 7 6 1 35.50 41.35 23.38 o -7 7 1 2.15 -14.20 17.77 o -6 7 1 335.05 380.32 19.08 o -5 7 1 1060.25 1124.42 35.52 o -4 7 1 21.93 41.59 7.83 o -3 7 1 540.79 667.45 26.26 o -2 7 1 22415.86 22849.12 596.57 o -1 7 1 188.16 229.56 14.33 o 0 7 1 1652.81 1601.06 34.62 o 1 7 1 543.52 499.88 10.01 o 2 7 1 5537.84 5543.89 117.27 o 3 7 1 1296.87 1380.39 38.89 o 4 7 1 32.67 28.58 9.79 o 5 7 1 595.80 614.79 29.25 o 6 7 1 9.90 2.82 14.92 o 7 7 1 1.95 16.92 23.85 o -7 8 1 78.70 81.88 20.81 o -6 8 1 51.84 65.14 14.34 o -5 8 1 7.52 12.32 8.15 o -4 8 1 6664.89 6848.63 194.43 o -3 8 1 329.60 382.81 17.66 o -2 8 1 1171.83 1245.78 34.99 o -1 8 1 1011.34 1058.89 31.21 o 0 8 1 18848.46 18635.43 378.51 o 1 8 1 5039.04 5196.10 99.97 o 2 8 1 1677.04 1595.20 38.05 o 3 8 1 2365.60 2297.47 61.57 o 4 8 1 2404.65 2364.78 75.91 o 5 8 1 184.90 197.47 23.84 o 6 8 1 516.37 526.94 29.97 o 7 8 1 2.02 19.04 22.73 o -7 9 1 446.52 465.43 31.92 o -6 9 1 423.45 472.91 35.24 o -5 9 1 246.95 257.15 14.55 o -4 9 1 548.71 596.41 25.10 o -3 9 1 235.91 185.65 11.93 o -2 9 1 11249.62 12405.92 323.18 o -1 9 1 2412.22 2372.78 53.97 o 0 9 1 1121.81 1046.92 23.69 o 1 9 1 1483.14 1582.81 33.98 o 2 9 1 6331.42 6743.65 170.57 o 3 9 1 3986.74 3783.17 98.51 o 4 9 1 5195.59 5234.44 157.73 o 5 9 1 124.44 111.98 15.30 o 6 9 1 22.04 1.72 18.87 o 7 9 1 936.54 969.83 55.31 o -7 10 1 22.30 6.78 19.03 o -6 10 1 612.05 607.41 29.25 o -5 10 1 2862.66 2921.75 80.22 o -4 10 1 164.03 161.88 11.60 o -3 10 1 5850.88 5977.15 169.39 o -2 10 1 914.36 1141.48 32.92 o -1 10 1 342.07 353.61 8.97 o 0 10 1 2538.27 2698.11 57.49 o 1 10 1 9918.72 10242.56 206.64 o 2 10 1 6656.96 7233.56 160.48 o 3 10 1 1479.70 1606.36 44.60 o 4 10 1 427.14 410.21 20.93 o 5 10 1 2219.78 2214.37 90.46 o 6 10 1 1160.07 1180.90 57.40 o 7 10 1 136.92 131.05 27.59 o -7 11 1 141.34 170.72 27.74 o -6 11 1 1.92 4.57 10.51 o -5 11 1 73.28 113.37 11.50 o -4 11 1 57.58 61.17 9.26 o -3 11 1 5605.38 5659.42 151.33 o -2 11 1 896.05 1148.26 28.92 o -1 11 1 8874.15 8551.66 177.88 o 0 11 1 895.88 959.75 22.25 o 1 11 1 1460.88 1767.91 45.55 o 2 11 1 198.49 280.41 10.53 o 3 11 1 1560.88 1540.68 43.30 o 4 11 1 924.54 946.05 25.52 o 5 11 1 236.10 245.84 21.38 o 6 11 1 2.75 26.50 19.92 o 7 11 1 185.81 193.30 30.28 o -7 12 1 225.08 227.74 33.37 o -6 12 1 168.70 173.76 14.76 o -5 12 1 1311.78 1308.87 40.70 o -4 12 1 228.09 233.17 22.80 o -3 12 1 6232.07 6153.55 163.55 o -2 12 1 1224.32 1526.41 40.48 o -1 12 1 4943.57 5680.16 121.56 o 0 12 1 2.31 13.88 4.35 o 1 12 1 8979.80 8782.27 210.63 o 2 12 1 1177.13 1294.02 37.20 o 3 12 1 24.14 15.61 5.98 o 4 12 1 231.18 225.95 11.73 o 5 12 1 263.20 278.71 20.28 o 6 12 1 722.46 836.45 56.39 o 7 12 1 344.12 327.86 54.87 o -7 13 1 325.31 319.31 32.92 o -6 13 1 17.65 11.47 11.32 o -5 13 1 1551.16 1588.10 47.67 o -4 13 1 161.32 174.29 12.34 o -3 13 1 2927.34 2851.60 79.09 o -2 13 1 593.35 677.91 16.50 o -1 13 1 16684.81 17496.74 380.45 o 0 13 1 1245.83 1327.04 36.51 o 1 13 1 12759.03 14402.77 327.80 o 2 13 1 270.00 301.73 13.26 o 3 13 1 3139.81 3085.05 87.74 o 4 13 1 88.14 97.96 6.90 o 5 13 1 263.89 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63.36 o -1 4 9 239.46 274.46 29.53 o 0 4 9 8.88 5.49 20.77 o 1 4 9 230.77 222.93 32.90 o -3 5 9 163.91 252.38 120.94 o -2 5 9 125.03 123.25 59.83 o -1 5 9 210.85 226.98 48.77 o 0 5 9 236.87 259.98 30.41 o -3 6 9 31.50 97.18 59.56 o -2 6 9 271.16 377.01 78.33 o -1 6 9 21.06 5.07 21.81 o 0 6 9 34.27 43.16 22.49 o -3 7 9 27.55 61.23 30.77 o -2 7 9 237.66 243.69 37.60 o -1 7 9 15.62 15.38 21.17 o 0 7 9 239.99 216.22 71.11 o -2 8 9 174.32 228.43 37.77 o -1 8 9 74.43 99.78 23.70 o 0 8 9 2.90 13.19 21.14 o -2 9 9 3.71 -1.55 28.83 o -1 9 9 238.95 318.95 26.70 o 0 9 9 308.25 387.32 61.22 o -2 10 9 672.32 803.77 62.55 o -1 10 9 490.71 550.85 33.71 o -1 11 9 587.68 559.55 34.29 o