#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:33:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181175 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/54/2225448.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225448_Fobs loop_ _publ_author_name 'Song, Yang' 'Parkin, Sean' 'Lehmler, Hans-Joachim' _publ_section_title ; 1-Bromo-2-chloro-4,5-dimethoxybenzene ; _journal_coeditor_code CI5050 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o813 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.926 _cell_angle_beta 75.932 _cell_angle_gamma 79.948 _cell_length_a 9.9264 _cell_length_b 9.9410 _cell_length_c 19.7219 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high .7698 _cod_data_source_file ci5050Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' k06356 - P1bar' _shelx_refln_list_code 4 _shelx_f_calc_maximum 285.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 94.18 100.95 3.40 o 2 0 0 3394.53 3245.87 54.22 o 3 0 0 35583.23 34337.26 556.28 o 4 0 0 1176.97 1216.41 39.07 o 5 0 0 5297.82 5319.32 81.37 o 6 0 0 3.87 3.98 8.59 o 7 0 0 2147.10 2132.18 65.31 o 8 0 0 2003.77 1983.30 91.98 o 9 0 0 335.79 253.05 35.20 o 10 0 0 2114.46 2245.73 120.26 o 11 0 0 16.41 -4.54 47.92 o 12 0 0 616.09 671.06 76.76 o -12 1 0 194.94 51.51 52.08 o -11 1 0 645.68 584.47 57.01 o -10 1 0 180.28 175.78 34.78 o -9 1 0 3366.18 3278.01 187.25 o -8 1 0 1011.29 937.34 74.85 o -7 1 0 2237.41 2115.11 65.93 o -6 1 0 30458.75 30509.57 462.62 o -5 1 0 558.04 603.65 23.93 o -4 1 0 11.90 17.60 8.30 o -3 1 0 33879.02 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5330.26 5228.63 81.58 o 7 2 0 862.61 805.12 25.09 o 8 2 0 1393.61 1338.78 62.18 o 9 2 0 483.87 416.08 79.66 o 10 2 0 518.79 540.83 55.65 o 11 2 0 1080.90 1203.03 90.81 o 12 2 0 .73 -1.84 81.85 o -11 3 0 2066.25 2227.90 168.83 o -10 3 0 520.25 518.66 68.00 o -9 3 0 316.69 355.44 37.16 o -8 3 0 12514.66 13023.77 328.82 o -7 3 0 335.92 338.08 19.47 o -6 3 0 .05 31.88 31.56 o -5 3 0 6766.16 6668.37 120.30 o -4 3 0 835.93 918.30 21.74 o -3 3 0 5178.37 5268.08 105.71 o -2 3 0 256.75 259.38 10.41 o -1 3 0 142.60 267.53 15.13 o 0 3 0 37907.02 36973.71 570.12 o 1 3 0 4111.05 4045.27 69.68 o 2 3 0 5109.86 5080.10 92.39 o 3 3 0 1512.11 1485.98 25.98 o 4 3 0 209.02 254.80 17.83 o 5 3 0 2079.53 2018.55 37.00 o 6 3 0 945.05 950.98 34.38 o 7 3 0 550.74 582.92 22.95 o 8 3 0 87.92 110.58 29.57 o 9 3 0 1128.70 1003.77 58.00 o 10 3 0 71.21 87.64 44.16 o 11 3 0 173.61 76.69 83.30 o 12 3 0 240.92 212.95 80.51 o -11 4 0 480.45 449.75 121.31 o -10 4 0 21.13 -57.74 73.91 o -9 4 0 762.81 677.39 61.71 o -8 4 0 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44.47 o 9 8 0 1131.71 1295.84 79.77 o 10 8 0 63.68 9.45 102.37 o -7 9 0 12.07 51.39 84.00 o -6 9 0 1932.88 1956.53 121.09 o -5 9 0 304.32 287.60 120.49 o -4 9 0 1581.95 1440.63 88.41 o -3 9 0 114.34 87.99 41.18 o -2 9 0 6372.54 6327.37 253.00 o -1 9 0 2701.22 2739.87 118.26 o 0 9 0 270.51 221.77 48.57 o 1 9 0 7134.32 7215.14 344.34 o 2 9 0 348.98 344.72 47.75 o 3 9 0 898.17 1006.63 67.58 o 4 9 0 1423.66 1431.42 59.41 o 5 9 0 33.50 85.24 52.91 o 6 9 0 2385.36 2645.27 101.82 o 7 9 0 526.99 450.37 62.30 o 8 9 0 144.29 231.94 56.29 o 9 9 0 1535.32 1400.95 158.85 o -6 10 0 76.29 32.62 128.59 o -5 10 0 2656.02 2561.34 212.24 o -4 10 0 249.05 232.74 95.62 o -3 10 0 926.01 766.90 75.30 o -2 10 0 2097.97 2148.70 180.56 o -1 10 0 3.34 -15.95 85.41 o 0 10 0 7533.70 7289.81 254.38 o 1 10 0 119.62 163.09 31.30 o 2 10 0 489.28 579.57 58.19 o 3 10 0 3070.59 3362.00 157.21 o 4 10 0 191.39 176.65 34.06 o 5 10 0 3291.50 3293.64 130.84 o 6 10 0 1189.20 1250.21 87.16 o 7 10 0 3.23 50.62 58.49 o 8 10 0 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