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Information card for entry 2225541
Preview
| Coordinates | 2225541.cif |
|---|---|
| Structure factors | 2225541.hkl |
| Original IUCr paper | HTML |
| Chemical name | Di-μ-chlorido-bis{[μ-1,8-bis(diisopropylphosphanyl)-9,10-dihydro- 9,10-ethanoanthracene-κ^2^<i>P</i>:<i>P</i>']-μ-chlorido-μ-methylidene- dipalladium(II)} tetrahydrofuran pentasolvate |
|---|---|
| Formula | C78 H124 Cl4 O5 P4 Pd4 |
| Calculated formula | C78 H124 Cl4 O5 P4 Pd4 |
| Title of publication | Di-μ-chlorido-bis{[μ-1,8-bis(diisopropylphosphanyl)-9,10-dihydro-9,10-ethanoanthracene-κ^2^<i>P</i>:<i>P</i>']-μ-chlorido-μ-methylidene-dipalladium(II)} tetrahydrofuran pentasolvate |
| Authors of publication | Schnetz, Thomas; Rominger, Frank; Hofmann, Peter |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2010 |
| Journal volume | 66 |
| Journal issue | 4 |
| Pages of publication | m453 - m454 |
| a | 12.5799 ± 0.0001 Å |
| b | 17.283 ± 0.0003 Å |
| c | 19.7558 ± 0.0002 Å |
| α | 79.877 ± 0.001° |
| β | 74.703 ± 0.001° |
| γ | 80.717 ± 0.001° |
| Cell volume | 4048.61 ± 0.09 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0999 |
| Residual factor for significantly intense reflections | 0.0466 |
| Weighted residual factors for significantly intense reflections | 0.0879 |
| Weighted residual factors for all reflections included in the refinement | 0.1055 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.012 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181176 (current) | 2016-04-03 | hkl/2/22/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22/55. |
2225541.cif 2225541.hkl |
| 176789 | 2016-02-20 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22. |
2225541.cif 2225541.hkl |
| 120072 | 2014-07-11 | Adding DOIs to range 2 structures. | 2225541.cif 2225541.hkl |
| 88064 | 2013-08-29 | Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet. | 2225541.cif 2225541.hkl |
| 26848 | 2011-09-28 | cif/2/, hkl/2/, html/ Reorganising CIFs of the range 2* into the "prefix-directory" tree. |
2225541.cif 2225541.hkl |
| 1157 | 2010-05-06 | hkl/ Adding Fobs data for the recent IUCr deposition. |
2225541.cif 2225541.hkl |
| 1144 | 2010-05-03 | cif/2/ Adding CIFs from Acta-Cryst-E-2010_04/ deposition. |
2225541.cif |
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