#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/55/2225578.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225578_Fobs loop_ _publ_author_name 'Gomes, Ligia R.' 'Santos, Lu\'is M. N. B. F.' 'Coutinho, Jo\~ao A. P.' 'Schr\"oder, Bernd' 'Low, John Nicolson' _publ_section_title ; N'-Benzoyl-N,N-diethylthiourea: a monoclinic polymorph ; _journal_coeditor_code HB5361 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o870 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.553 _cell_angle_gamma 90.000 _cell_length_a 20.1727 _cell_length_b 8.4717 _cell_length_c 14.8345 _exptl_crystal_F_000 1008.00 _reflns_d_resolution_high 0.7000 _[local]_cod_data_source_file hb5361Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ntt4 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 247.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 14295.87 9452.25 248.76 o 6 0 0 41199.87 42317.00 479.29 o 8 0 0 4567.67 4886.72 59.27 o 10 0 0 666.25 842.39 14.90 o 12 0 0 3030.72 3571.81 52.41 o 14 0 0 3074.32 3058.25 70.86 o 16 0 0 5521.41 5410.33 117.35 o 18 0 0 2866.53 2794.95 72.50 o 20 0 0 222.34 224.21 26.25 o 22 0 0 165.94 169.16 27.81 o 24 0 0 10.14 9.29 14.29 o 26 0 0 246.22 242.71 25.42 o 5 1 0 58466.08 58302.69 466.74 o 7 1 0 1336.61 1495.94 17.69 o 9 1 0 5.03 10.41 2.67 o 11 1 0 2747.95 2805.74 33.13 o 13 1 0 8396.79 8433.34 94.74 o 15 1 0 8512.99 8397.12 95.57 o 17 1 0 15.77 17.70 6.52 o 19 1 0 121.90 140.62 25.17 o 21 1 0 0.29 -7.85 7.85 o 23 1 0 33.80 28.63 13.08 o 25 1 0 34.92 47.59 14.80 o 27 1 0 125.49 121.84 22.24 o 0 2 0 44229.91 43521.68 655.05 o 2 2 0 18.34 12.66 2.28 o 4 2 0 6423.38 6490.51 47.92 o 6 2 0 51.51 68.27 2.83 o 8 2 0 1303.45 1389.05 16.52 o 10 2 0 15.64 15.56 3.97 o 12 2 0 9.68 36.33 5.66 o 14 2 0 3355.98 3267.85 49.23 o 16 2 0 3268.74 3149.78 49.16 o 18 2 0 327.42 372.35 14.72 o 20 2 0 252.90 270.98 13.36 o 22 2 0 105.30 117.02 17.05 o 24 2 0 67.47 83.52 20.91 o 26 2 0 31.06 29.00 19.21 o 1 3 0 17542.14 18130.50 134.46 o 3 3 0 1951.41 2134.23 21.02 o 5 3 0 61.92 65.62 3.88 o 7 3 0 776.67 797.47 12.22 o 9 3 0 154.13 170.74 7.16 o 11 3 0 1710.85 1611.23 22.86 o 13 3 0 0.38 -3.76 6.87 o 15 3 0 784.11 723.52 23.53 o 17 3 0 89.44 95.42 9.75 o 19 3 0 3.32 2.70 7.28 o 21 3 0 313.64 326.62 17.05 o 23 3 0 192.13 143.79 18.17 o 25 3 0 25.72 -2.69 28.13 o 0 4 0 1134.51 1273.80 28.58 o 2 4 0 130.13 168.98 5.43 o 4 4 0 684.80 799.59 11.72 o 6 4 0 1984.18 2275.72 26.43 o 8 4 0 184.22 220.15 7.94 o 10 4 0 285.88 314.40 8.23 o 12 4 0 772.42 778.38 17.69 o 14 4 0 99.56 77.02 9.54 o 16 4 0 57.27 57.89 8.85 o 18 4 0 1017.20 1005.22 28.40 o 20 4 0 549.32 579.41 21.93 o 22 4 0 435.03 405.20 35.55 o 24 4 0 1.17 17.63 14.79 o 26 4 0 285.86 267.27 34.31 o 1 5 0 74.18 27.96 5.76 o 3 5 0 188.36 162.42 8.03 o 5 5 0 48.47 66.41 6.13 o 7 5 0 45.53 61.01 6.23 o 9 5 0 189.51 170.00 8.82 o 11 5 0 856.11 858.43 17.19 o 13 5 0 230.71 251.18 11.04 o 15 5 0 852.13 801.27 24.35 o 17 5 0 63.50 55.97 10.46 o 19 5 0 316.29 334.82 18.96 o 21 5 0 87.99 97.95 12.89 o 23 5 0 197.96 195.99 26.73 o 25 5 0 237.28 245.13 26.71 o 0 6 0 1049.94 1141.79 31.57 o 2 6 0 363.06 351.90 13.95 o 4 6 0 2645.63 2555.95 35.66 o 6 6 0 58.08 48.66 7.01 o 8 6 0 105.18 83.28 6.84 o 10 6 0 20.04 31.43 5.94 o 12 6 0 546.61 513.66 14.84 o 14 6 0 1571.28 1560.34 31.96 o 16 6 0 220.15 214.28 20.82 o 18 6 0 373.69 410.51 20.91 o 20 6 0 159.76 143.85 16.10 o 22 6 0 59.71 26.46 17.75 o 1 7 0 49.49 46.42 9.52 o 3 7 0 2531.20 2421.11 39.38 o 5 7 0 996.65 941.57 24.50 o 7 7 0 28.80 31.90 7.16 o 9 7 0 1309.02 1247.20 27.25 o 11 7 0 2543.91 2396.59 41.61 o 13 7 0 12.01 16.75 7.73 o 15 7 0 293.59 266.82 19.19 o 17 7 0 405.04 371.11 23.36 o 19 7 0 469.06 409.04 23.45 o 21 7 0 128.47 108.67 23.18 o 0 8 0 409.32 408.62 26.92 o 2 8 0 954.21 944.31 26.87 o 4 8 0 356.49 351.58 20.72 o 6 8 0 126.49 149.25 14.24 o 8 8 0 76.13 92.79 11.94 o 10 8 0 362.89 384.10 18.61 o 12 8 0 1254.02 1277.47 34.65 o 14 8 0 108.93 119.57 20.93 o 16 8 0 311.89 321.71 22.76 o 18 8 0 391.46 404.77 25.34 o 20 8 0 30.54 25.95 15.32 o 1 9 0 332.04 276.45 18.02 o 3 9 0 1017.53 959.94 32.99 o 5 9 0 181.97 201.57 23.28 o 7 9 0 27.27 26.93 12.25 o 9 9 0 2.99 -6.63 9.58 o 11 9 0 85.21 96.92 13.53 o 13 9 0 1139.73 1128.19 33.86 o 15 9 0 287.05 261.14 23.40 o 17 9 0 180.67 190.08 21.60 o 0 10 0 547.55 526.94 55.31 o 2 10 0 362.98 357.55 24.90 o 4 10 0 139.05 134.87 18.49 o 6 10 0 200.62 214.49 21.33 o 8 10 0 325.88 334.05 23.72 o 10 10 0 7.85 23.78 13.51 o 12 10 0 166.25 136.70 19.67 o 14 10 0 18.27 24.68 20.54 o 1 11 0 706.31 700.49 40.11 o 3 11 0 9.93 14.87 16.69 o 5 11 0 23.57 16.48 16.11 o 7 11 0 20.45 34.98 15.60 o 9 11 0 0.07 -10.50 13.53 o 11 11 0 38.52 55.78 18.32 o 0 12 0 177.92 179.69 90.00 o 2 12 0 4.40 1.50 17.31 o -27 1 1 5.92 36.59 25.31 o -25 1 1 265.63 265.38 18.47 o -23 1 1 1368.60 1267.20 34.38 o -21 1 1 191.30 180.28 14.10 o -19 1 1 872.84 867.78 42.59 o -17 1 1 1218.46 1175.10 25.27 o -15 1 1 415.89 451.03 15.41 o -13 1 1 283.04 226.95 8.59 o -11 1 1 4764.79 5177.53 48.51 o -9 1 1 884.55 947.21 11.73 o -7 1 1 7877.55 8518.70 67.35 o -5 1 1 217.55 302.91 5.85 o -3 1 1 5118.01 5087.41 114.11 o 3 1 1 1777.48 1641.73 18.58 o 5 1 1 27296.98 27907.10 265.01 o 7 1 1 1954.10 2176.23 29.30 o 9 1 1 82.44 69.81 5.00 o 11 1 1 384.36 455.63 8.38 o 13 1 1 2122.82 2267.71 35.68 o 15 1 1 931.30 890.47 28.40 o 17 1 1 323.51 366.94 23.38 o 19 1 1 16.73 23.50 8.44 o 21 1 1 16.99 23.46 9.39 o 23 1 1 150.28 140.10 26.43 o 25 1 1 3.67 -12.40 12.40 o 27 1 1 24.54 11.86 15.48 o -26 2 1 178.94 180.98 26.68 o -24 2 1 16.19 5.86 11.14 o -22 2 1 38.15 9.22 7.94 o -20 2 1 52.11 53.24 8.78 o -18 2 1 50.51 39.77 9.34 o -16 2 1 842.20 910.11 26.46 o -14 2 1 748.57 751.98 17.66 o -12 2 1 2095.38 2090.32 31.40 o -10 2 1 11984.99 12314.41 145.23 o -8 2 1 9028.79 9505.34 82.38 o -6 2 1 9493.43 9904.08 73.76 o -4 2 1 2107.42 2011.31 16.95 o -2 2 1 194.11 224.65 5.44 o 0 2 1 24507.11 24285.25 162.99 o 2 2 1 100.87 95.77 3.06 o 4 2 1 6.63 12.60 2.30 o 6 2 1 3563.39 3575.06 32.62 o 8 2 1 1137.03 1107.71 15.12 o 10 2 1 0.12 -3.55 5.36 o 12 2 1 238.03 203.86 13.60 o 14 2 1 230.10 198.99 9.95 o 16 2 1 35.47 43.86 8.43 o 18 2 1 1399.26 1356.87 27.91 o 20 2 1 718.84 709.68 24.73 o 22 2 1 224.14 250.37 16.79 o 24 2 1 167.13 170.59 22.58 o 26 2 1 165.75 142.29 24.96 o -27 3 1 171.55 188.22 28.89 o -25 3 1 754.80 781.81 52.50 o -23 3 1 1315.53 1332.44 33.94 o -21 3 1 47.10 58.21 10.10 o -19 3 1 518.09 547.71 20.44 o -17 3 1 672.58 667.86 30.72 o -15 3 1 103.34 95.32 9.59 o -13 3 1 2682.91 2581.24 42.09 o -11 3 1 52.88 34.70 6.24 o -9 3 1 10064.09 10536.14 93.30 o -7 3 1 1826.89 2011.65 18.95 o -5 3 1 235.26 206.43 5.13 o -3 3 1 498.41 553.21 8.81 o -1 3 1 6422.35 6661.85 47.36 o 1 3 1 8906.42 9053.20 60.66 o 3 3 1 7.02 21.53 2.72 o 5 3 1 5755.19 5734.57 45.64 o 7 3 1 905.69 955.26 14.02 o 9 3 1 1186.48 1155.40 15.85 o 11 3 1 13.25 17.58 4.11 o 13 3 1 1345.65 1375.94 25.04 o 15 3 1 2033.69 2082.26 40.40 o 17 3 1 381.81 352.02 14.52 o 19 3 1 765.02 807.01 22.47 o 21 3 1 176.71 210.44 19.77 o 23 3 1 669.02 647.16 42.00 o 25 3 1 42.42 25.24 27.50 o -26 4 1 83.77 76.17 23.81 o -24 4 1 1086.80 1157.71 44.39 o -22 4 1 303.00 317.31 27.06 o -20 4 1 107.54 96.65 16.89 o -18 4 1 447.30 476.90 27.38 o -16 4 1 632.28 602.86 19.84 o -14 4 1 5127.70 5081.37 73.42 o -12 4 1 1182.98 1093.16 18.01 o -10 4 1 10.16 1.70 4.06 o -8 4 1 3796.01 3868.58 35.46 o -6 4 1 190.11 160.38 5.91 o -4 4 1 92.89 93.45 5.86 o -2 4 1 1443.64 1267.06 17.15 o 0 4 1 1.39 12.72 3.34 o 2 4 1 1168.77 1118.75 14.70 o 4 4 1 14884.98 15488.47 121.80 o 6 4 1 9673.41 10196.11 82.46 o 8 4 1 53.57 44.13 4.19 o 10 4 1 121.11 166.27 7.07 o 12 4 1 609.42 612.37 14.77 o 14 4 1 1456.87 1482.54 23.45 o 16 4 1 709.66 667.50 21.84 o 18 4 1 667.76 681.66 22.37 o 20 4 1 365.51 389.10 17.15 o 22 4 1 487.03 531.61 31.29 o 24 4 1 21.72 -0.61 19.59 o -25 5 1 5.06 40.87 18.13 o -23 5 1 17.04 28.38 17.59 o -21 5 1 87.60 113.13 15.52 o -19 5 1 442.95 403.33 21.90 o -17 5 1 308.01 331.62 17.17 o -15 5 1 684.34 672.20 22.41 o -13 5 1 1808.58 1803.68 24.97 o -11 5 1 1864.21 1742.84 27.56 o -9 5 1 4822.62 4943.52 48.10 o -7 5 1 92.04 96.30 6.53 o -5 5 1 14.98 11.17 4.32 o -3 5 1 378.60 378.54 14.81 o -1 5 1 3684.12 3633.55 41.29 o 1 5 1 8893.58 9152.17 86.46 o 3 5 1 3753.34 3605.39 40.32 o 5 5 1 317.56 268.53 9.93 o 7 5 1 718.30 668.52 13.58 o 9 5 1 98.44 93.21 6.58 o 11 5 1 139.20 143.83 7.77 o 13 5 1 342.44 359.61 12.84 o 15 5 1 43.14 60.12 10.89 o 17 5 1 2688.86 2515.24 52.45 o 19 5 1 2465.92 2514.44 68.38 o 21 5 1 1209.60 1176.99 47.03 o 23 5 1 81.55 90.73 20.18 o -24 6 1 936.84 954.41 46.33 o -22 6 1 45.33 52.27 13.53 o -20 6 1 62.30 51.09 12.36 o -18 6 1 127.69 130.75 14.15 o -16 6 1 401.36 406.66 20.25 o -14 6 1 453.62 436.23 13.70 o -12 6 1 1430.40 1351.07 27.21 o -10 6 1 598.84 565.58 13.56 o -8 6 1 1374.94 1316.46 35.49 o -6 6 1 382.50 358.27 14.13 o -4 6 1 324.67 318.84 12.26 o -2 6 1 343.85 276.56 12.87 o 0 6 1 842.65 859.99 20.91 o 2 6 1 2199.59 2222.41 35.43 o 4 6 1 833.28 835.35 17.57 o 6 6 1 1203.07 1274.08 21.45 o 8 6 1 1579.45 1574.38 22.09 o 10 6 1 105.58 77.52 8.22 o 12 6 1 101.54 131.89 15.56 o 14 6 1 1325.67 1318.32 30.63 o 16 6 1 1658.07 1659.48 39.44 o 18 6 1 383.32 368.62 21.70 o 20 6 1 52.12 32.92 23.12 o 22 6 1 377.77 443.56 34.43 o -21 7 1 13.70 4.96 11.97 o -19 7 1 3.23 -11.13 11.13 o -17 7 1 67.43 56.31 13.08 o -15 7 1 387.10 415.90 22.21 o -13 7 1 954.69 940.20 24.02 o -11 7 1 2.13 1.86 6.75 o -9 7 1 221.43 217.82 12.94 o -7 7 1 719.29 696.46 18.46 o -5 7 1 86.51 82.09 9.85 o -3 7 1 39.00 26.41 8.20 o -1 7 1 642.25 562.87 18.80 o 1 7 1 0.33 -3.47 7.96 o 3 7 1 3188.81 3132.43 50.29 o 5 7 1 1266.78 1300.11 27.13 o 7 7 1 464.63 460.29 19.02 o 9 7 1 1106.46 1175.44 25.76 o 11 7 1 18.77 14.69 7.56 o 13 7 1 29.43 29.79 10.29 o 15 7 1 16.80 17.23 11.51 o 17 7 1 240.72 252.92 19.74 o 19 7 1 128.59 92.75 23.55 o 21 7 1 826.37 858.67 46.73 o -20 8 1 5.25 -5.15 13.29 o -18 8 1 116.61 80.69 16.14 o -16 8 1 214.10 225.49 20.37 o -14 8 1 14.71 6.65 9.34 o -12 8 1 10.55 -5.29 8.35 o -10 8 1 89.12 100.44 12.08 o -8 8 1 3383.04 3286.36 51.41 o -6 8 1 1249.29 1182.55 27.58 o -4 8 1 61.83 67.23 10.22 o -2 8 1 382.07 421.01 23.68 o 0 8 1 60.52 88.96 11.52 o 2 8 1 173.37 147.66 13.72 o 4 8 1 138.63 152.07 18.91 o 6 8 1 2229.79 2162.96 47.72 o 8 8 1 484.39 441.63 20.58 o 10 8 1 446.11 471.93 19.91 o 12 8 1 179.66 162.57 13.04 o 14 8 1 15.25 -6.09 11.30 o 16 8 1 269.64 271.35 26.96 o 18 8 1 71.39 73.85 19.31 o 20 8 1 38.86 23.68 19.35 o -17 9 1 3.12 12.11 14.24 o -15 9 1 355.63 362.99 25.44 o -13 9 1 12.82 21.20 11.75 o -11 9 1 132.28 117.69 14.26 o -9 9 1 1010.14 1010.58 30.47 o -7 9 1 171.62 176.24 18.12 o -5 9 1 1069.08 1127.30 32.98 o -3 9 1 25.38 15.30 10.04 o -1 9 1 571.65 625.85 26.14 o 1 9 1 128.12 115.15 13.99 o 3 9 1 502.97 520.65 26.29 o 5 9 1 159.37 182.97 18.50 o 7 9 1 685.35 689.57 29.62 o 9 9 1 4.24 -0.12 10.47 o 11 9 1 576.76 574.59 25.52 o 13 9 1 235.70 193.01 27.50 o 15 9 1 85.00 71.94 21.43 o 17 9 1 3.95 7.29 20.48 o -14 10 1 54.79 40.16 30.72 o -12 10 1 55.57 56.45 14.84 o -10 10 1 593.03 594.34 27.29 o -8 10 1 134.83 135.03 26.00 o -6 10 1 484.30 509.76 25.54 o -4 10 1 13.09 15.97 12.89 o -2 10 1 111.07 109.25 16.86 o 0 10 1 239.92 256.61 31.09 o 2 10 1 120.02 129.71 17.75 o 4 10 1 22.18 -11.58 11.58 o 6 10 1 398.80 424.28 30.13 o 8 10 1 216.82 245.76 21.33 o 10 10 1 365.36 379.01 24.40 o 12 10 1 9.73 14.31 19.78 o 14 10 1 19.68 11.28 19.53 o -11 11 1 468.75 509.37 34.28 o -9 11 1 349.49 450.58 34.37 o -7 11 1 10.88 6.20 15.69 o -5 11 1 235.59 241.13 26.17 o -3 11 1 14.02 39.30 17.87 o -1 11 1 6.97 -4.43 15.06 o 1 11 1 164.87 169.82 24.89 o 3 11 1 849.79 969.88 45.95 o 5 11 1 160.37 144.57 22.94 o 7 11 1 233.00 240.57 23.15 o 9 11 1 129.98 114.39 23.69 o 11 11 1 13.51 17.22 20.58 o -2 12 1 157.78 214.12 29.09 o 0 12 1 157.23 210.68 28.97 o 2 12 1 9.90 -3.26 19.61 o -28 0 2 856.80 803.36 90.32 o -26 0 2 1365.20 1333.74 114.07 o -24 0 2 16.71 12.12 15.24 o -22 0 2 26.10 45.63 25.94 o -20 0 2 12.53 20.15 12.38 o -18 0 2 2710.42 2674.60 53.59 o -16 0 2 9163.16 9375.39 149.66 o -14 0 2 2620.17 2682.12 89.60 o -12 0 2 10403.83 10394.79 121.47 o -10 0 2 53702.81 56584.43 633.68 o -8 0 2 21970.34 22631.41 232.22 o -6 0 2 61018.32 60028.93 617.54 o -4 0 2 11300.71 11365.98 129.62 o 4 0 2 1553.63 1518.07 22.82 o 6 0 2 24653.72 25889.44 378.18 o 8 0 2 3073.17 2783.20 50.09 o 10 0 2 3833.44 3535.62 61.68 o 12 0 2 0.96 -5.50 12.40 o 14 0 2 1790.43 1764.84 53.87 o 16 0 2 2306.69 2262.09 61.51 o 18 0 2 1875.94 1829.79 55.13 o 20 0 2 2387.29 2231.34 81.57 o 22 0 2 284.52 255.22 23.18 o 24 0 2 287.04 300.33 35.00 o 26 0 2 4.21 10.00 32.50 o -27 1 2 273.74 352.08 23.58 o -25 1 2 433.25 469.58 23.16 o -23 1 2 1802.53 1727.74 44.11 o -21 1 2 1793.24 1762.14 34.17 o -19 1 2 25.52 25.46 7.54 o -17 1 2 293.62 278.15 16.75 o -15 1 2 2166.23 2278.43 30.17 o -13 1 2 7893.90 7949.68 82.79 o -11 1 2 2246.13 2763.56 30.83 o -9 1 2 1109.13 1107.20 12.25 o -7 1 2 787.06 849.19 9.91 o -5 1 2 27379.71 28277.98 226.04 o -3 1 2 28601.37 27365.95 302.00 o 3 1 2 5548.57 5657.61 60.94 o 5 1 2 31359.72 31283.01 250.45 o 7 1 2 7.71 36.31 4.44 o 9 1 2 294.36 204.83 10.18 o 11 1 2 957.97 951.34 15.66 o 13 1 2 1203.04 1169.79 20.14 o 15 1 2 373.70 390.31 11.36 o 17 1 2 2171.99 2142.86 42.17 o 19 1 2 161.87 185.04 18.49 o 21 1 2 1066.12 1135.88 30.66 o 23 1 2 168.07 155.39 13.99 o 25 1 2 296.17 242.88 24.13 o -26 2 2 670.11 683.96 30.53 o -24 2 2 160.66 152.58 16.51 o -22 2 2 71.88 85.69 11.82 o -20 2 2 3.74 0.12 7.87 o -18 2 2 449.18 405.46 15.44 o -16 2 2 1965.34 2041.94 40.81 o -14 2 2 3302.57 3272.79 48.38 o -12 2 2 858.15 822.87 14.47 o -10 2 2 1696.50 1716.95 25.18 o -8 2 2 4726.75 4836.60 42.45 o -6 2 2 4544.57 4549.95 38.50 o -4 2 2 2417.99 2340.64 26.59 o -2 2 2 101.01 104.85 3.94 o 0 2 2 3646.49 3619.44 29.11 o 2 2 2 3070.30 3087.90 24.52 o 4 2 2 3523.53 3526.73 31.46 o 6 2 2 5864.67 5857.46 51.44 o 8 2 2 59.12 46.56 6.94 o 10 2 2 670.07 613.50 18.14 o 12 2 2 212.73 181.13 11.88 o 14 2 2 1027.49 990.95 25.34 o 16 2 2 1352.05 1256.18 33.42 o 18 2 2 128.31 152.09 18.37 o 20 2 2 1216.48 1269.64 30.77 o 22 2 2 1322.29 1260.58 46.10 o 24 2 2 7.07 18.13 14.81 o 26 2 2 5.28 15.00 20.63 o -27 3 2 35.52 64.45 21.62 o -25 3 2 372.09 399.62 25.58 o -23 3 2 178.15 148.41 13.83 o -21 3 2 481.68 441.49 20.17 o -19 3 2 17.16 10.35 7.58 o -17 3 2 269.26 244.93 13.11 o -15 3 2 470.36 404.99 22.19 o -13 3 2 75.56 66.23 5.54 o -11 3 2 1972.70 1955.98 28.89 o -9 3 2 7386.37 7576.95 77.96 o -7 3 2 1.06 0.28 2.34 o -5 3 2 3284.83 3609.32 30.32 o -3 3 2 649.62 676.48 9.80 o -1 3 2 1995.76 2088.75 20.10 o 1 3 2 4725.54 4702.57 36.60 o 3 3 2 39.35 22.08 2.75 o 5 3 2 659.98 773.37 11.48 o 7 3 2 2656.17 2709.53 29.14 o 9 3 2 5450.05 5499.51 52.82 o 11 3 2 40.25 42.61 5.27 o 13 3 2 58.35 58.89 7.52 o 15 3 2 437.17 470.83 19.57 o 17 3 2 2389.84 2210.32 50.23 o 19 3 2 249.96 213.56 22.37 o 21 3 2 5.64 -7.88 30.31 o 23 3 2 13.31 -15.43 15.43 o 25 3 2 498.11 461.05 49.69 o -26 4 2 9.99 29.69 36.25 o -24 4 2 189.26 211.64 16.83 o -22 4 2 201.24 211.78 18.13 o -20 4 2 31.22 23.62 9.28 o -18 4 2 113.92 120.99 12.54 o -16 4 2 30.05 45.84 10.04 o -14 4 2 387.21 355.21 15.87 o -12 4 2 278.57 323.56 11.18 o -10 4 2 125.90 178.13 6.44 o -8 4 2 34.11 53.39 5.37 o -6 4 2 4741.38 5234.77 49.47 o -4 4 2 563.72 666.58 13.25 o -2 4 2 76.57 87.33 5.28 o 0 4 2 4270.29 4803.45 41.65 o 2 4 2 1692.65 1966.98 23.41 o 4 4 2 8.41 1.11 3.10 o 6 4 2 1558.73 1646.85 19.91 o 8 4 2 0.49 2.29 3.45 o 10 4 2 179.36 214.68 10.67 o 12 4 2 1431.47 1459.37 21.50 o 14 4 2 77.43 78.51 6.42 o 16 4 2 2508.85 2391.62 47.06 o 18 4 2 6.72 24.91 12.76 o 20 4 2 407.64 405.47 27.61 o 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