#------------------------------------------------------------------------------ #$Date: 2010-05-06 17:22:57 +0300 (Thu, 06 May 2010) $ #$Revision: 1157 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2225581.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225581_Fobs loop_ _publ_author_name 'Wang, Chen-Yi' 'Li, Jing-Fen' 'Cao, Feng' _publ_section_title ; {6-[(2-Anilinoethyl)iminomethyl]-2-ethoxyphenolato}(thiocyanato-\kN)copper(II) ; _journal_coeditor_code HB5365 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m445 _journal_page_last m446 _journal_volume 66 _journal_year 2010 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.6786 _cell_length_b 10.4938 _cell_length_c 25.2618 _exptl_crystal_F_000 1672.00 _reflns_d_resolution_high 0.7971 _[local]_cod_data_source_file hb5365Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Pbcn in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 585.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 438.75 804.19 40.68 o 4 0 0 342932.16 312915.91 6593.14 o 6 0 0 36555.80 39063.02 633.43 o 8 0 0 249.02 281.34 45.00 o 10 0 0 7575.14 7640.84 202.27 o 12 0 0 4137.88 4642.68 165.73 o 14 0 0 3482.49 3241.81 234.69 o 1 1 0 79176.21 91571.22 4351.10 o 3 1 0 8682.43 8498.27 129.31 o 5 1 0 50151.79 50460.62 648.74 o 7 1 0 95.54 46.20 25.30 o 9 1 0 6669.34 6553.77 146.50 o 11 1 0 24.08 -28.92 28.29 o 13 1 0 556.66 570.99 54.12 o 15 1 0 16.02 -34.73 78.53 o 0 2 0 5317.70 6183.22 172.10 o 2 2 0 5942.68 5964.15 85.61 o 4 2 0 3591.28 3865.08 310.64 o 6 2 0 825.95 1025.92 109.05 o 8 2 0 1852.16 1731.59 70.62 o 10 2 0 3.41 24.56 35.85 o 12 2 0 359.36 349.29 56.58 o 14 2 0 78.46 -23.84 73.54 o 16 2 0 196.12 137.68 140.81 o 1 3 0 12626.48 14057.36 239.43 o 3 3 0 5748.83 6534.24 101.64 o 5 3 0 301.04 313.69 48.50 o 7 3 0 2192.18 2408.23 139.11 o 9 3 0 11.07 10.59 29.89 o 11 3 0 2584.01 2696.67 110.79 o 13 3 0 146.18 102.05 53.00 o 15 3 0 111.06 91.53 79.10 o 0 4 0 27261.84 24272.89 591.41 o 2 4 0 4912.49 4785.13 146.19 o 4 4 0 5341.37 5466.94 100.52 o 6 4 0 10.44 149.43 113.40 o 8 4 0 881.94 985.00 63.59 o 10 4 0 561.87 521.90 80.55 o 12 4 0 12.28 20.20 47.15 o 14 4 0 510.46 440.78 73.70 o 16 4 0 87.96 -49.72 90.40 o 1 5 0 13148.49 13386.65 268.83 o 3 5 0 5689.86 5938.57 99.97 o 5 5 0 17675.94 19072.18 259.26 o 7 5 0 199.79 274.33 60.97 o 9 5 0 6297.63 6380.74 171.02 o 11 5 0 291.43 263.84 69.83 o 13 5 0 687.05 698.97 93.21 o 15 5 0 31.71 2.31 82.69 o 0 6 0 19188.09 19954.65 541.34 o 2 6 0 1169.55 1188.00 52.36 o 4 6 0 13371.93 13220.31 202.20 o 6 6 0 3341.80 3245.70 95.75 o 8 6 0 7969.92 7974.00 185.32 o 10 6 0 448.24 462.03 64.87 o 12 6 0 1351.76 1329.82 97.85 o 14 6 0 135.31 174.55 69.96 o 1 7 0 18718.17 18527.62 377.25 o 3 7 0 16852.80 16583.40 350.45 o 5 7 0 1705.45 1760.31 85.36 o 7 7 0 1138.24 1363.59 137.01 o 9 7 0 232.78 236.40 58.41 o 11 7 0 179.83 253.19 64.85 o 13 7 0 1016.41 822.02 94.38 o 0 8 0 3804.44 4205.59 222.17 o 2 8 0 380.30 385.80 68.59 o 4 8 0 3846.58 3774.27 154.89 o 6 8 0 895.87 866.97 64.33 o 8 8 0 1607.19 1458.18 93.84 o 10 8 0 371.26 469.75 72.18 o 12 8 0 293.28 287.86 109.90 o 1 9 0 35.74 96.51 62.80 o 3 9 0 1.42 -37.98 55.61 o 5 9 0 609.04 705.63 84.45 o 7 9 0 0.38 -4.96 49.85 o 9 9 0 453.19 577.33 79.12 o 11 9 0 1.25 6.96 66.98 o 0 10 0 121.04 -12.52 97.00 o 2 10 0 199.15 184.45 62.65 o 4 10 0 135.35 72.16 72.92 o 6 10 0 153.73 145.41 61.56 o 8 10 0 935.75 1098.48 334.82 o 10 10 0 94.60 163.32 76.98 o 1 11 0 992.97 1267.31 123.91 o 3 11 0 1590.95 1521.85 101.29 o 5 11 0 164.65 86.69 54.26 o 7 11 0 194.63 235.52 63.66 o 9 11 0 139.05 176.01 76.94 o 0 12 0 2106.43 2315.58 231.56 o 2 12 0 124.12 36.49 85.17 o 4 12 0 1518.65 1664.08 100.72 o 6 12 0 570.74 745.55 108.85 o 1 13 0 516.58 453.73 168.97 o 1 1 1 4491.35 5144.44 152.21 o 2 1 1 48565.14 49353.88 476.14 o 3 1 1 0.10 -3.03 11.26 o 4 1 1 101710.98 103967.53 904.07 o 5 1 1 6280.54 6297.19 126.88 o 6 1 1 8839.01 8757.85 108.90 o 7 1 1 1361.61 1471.66 42.42 o 8 1 1 23453.11 23905.00 252.85 o 9 1 1 531.06 728.35 38.67 o 10 1 1 598.84 560.17 39.03 o 11 1 1 349.58 312.96 28.53 o 12 1 1 909.80 892.94 41.84 o 13 1 1 156.07 175.34 32.91 o 14 1 1 6.55 -58.31 49.87 o 15 1 1 38.56 -65.76 61.07 o 16 1 1 0.69 168.97 98.57 o 0 2 1 5174.23 6091.52 326.51 o 1 2 1 29324.30 32813.65 468.93 o 2 2 1 0.84 3.61 8.90 o 3 2 1 7032.82 7095.38 84.43 o 4 2 1 2000.26 2287.21 42.47 o 5 2 1 1890.54 1591.84 48.05 o 6 2 1 164.91 186.12 18.05 o 7 2 1 1826.77 1881.77 54.45 o 8 2 1 300.33 233.90 26.87 o 9 2 1 720.92 719.81 37.80 o 10 2 1 23.38 1.45 22.20 o 11 2 1 1656.42 1652.74 59.96 o 12 2 1 26.59 28.55 30.96 o 13 2 1 554.31 511.01 47.50 o 14 2 1 5.00 -15.74 37.89 o 15 2 1 1426.61 1620.78 116.19 o 16 2 1 1.21 70.12 91.65 o 1 3 1 1844.74 1860.89 136.02 o 2 3 1 20110.46 20350.94 325.13 o 3 3 1 2.91 6.37 13.45 o 4 3 1 7333.05 7511.62 88.46 o 5 3 1 186.58 185.82 42.16 o 6 3 1 15199.81 15190.13 320.93 o 7 3 1 34.84 86.44 20.29 o 8 3 1 4827.19 4767.35 85.43 o 9 3 1 45.11 57.03 23.03 o 10 3 1 3451.50 3392.63 106.35 o 11 3 1 81.10 114.09 33.58 o 12 3 1 1218.07 1309.66 59.77 o 13 3 1 64.75 32.75 35.92 o 14 3 1 395.85 395.53 49.37 o 15 3 1 1.49 -43.43 54.42 o 16 3 1 127.43 168.82 90.85 o 0 4 1 110.36 16.02 75.10 o 1 4 1 17660.50 17380.20 275.14 o 2 4 1 72.79 41.62 21.95 o 3 4 1 47849.64 48270.58 412.16 o 4 4 1 333.54 542.15 66.27 o 5 4 1 1712.24 1813.84 99.43 o 6 4 1 522.64 528.40 46.82 o 7 4 1 20534.88 20825.29 231.06 o 8 4 1 16.72 14.39 21.14 o 9 4 1 56.13 37.07 25.37 o 10 4 1 54.21 -2.30 27.87 o 11 4 1 2570.64 2669.39 76.52 o 12 4 1 1.67 -37.08 32.97 o 13 4 1 162.54 141.34 39.67 o 14 4 1 8.87 56.15 41.61 o 15 4 1 35.09 1.38 57.07 o 16 4 1 5.70 -29.16 69.53 o 1 5 1 871.16 1584.52 59.88 o 2 5 1 25929.39 24621.81 248.38 o 3 5 1 0.47 -20.47 13.65 o 4 5 1 300.30 355.05 30.76 o 5 5 1 323.84 560.86 34.52 o 6 5 1 1128.50 1211.74 45.79 o 7 5 1 127.96 160.53 26.74 o 8 5 1 256.93 273.74 32.07 o 9 5 1 44.96 117.78 34.35 o 10 5 1 4.68 15.93 30.12 o 11 5 1 2.86 -22.77 33.05 o 12 5 1 1291.33 1351.68 65.16 o 13 5 1 0.00 13.33 39.11 o 14 5 1 201.56 190.10 44.82 o 15 5 1 2.60 20.25 51.46 o 0 6 1 42.28 250.43 48.68 o 1 6 1 1314.62 1504.43 48.95 o 2 6 1 52.89 30.13 20.46 o 3 6 1 686.51 646.11 26.45 o 4 6 1 17.35 68.26 23.90 o 5 6 1 262.68 290.18 25.98 o 6 6 1 69.59 60.64 24.39 o 7 6 1 890.41 1070.93 126.99 o 8 6 1 56.85 100.05 33.64 o 9 6 1 542.22 663.76 54.52 o 10 6 1 3.33 67.01 33.68 o 11 6 1 267.94 297.99 44.84 o 12 6 1 2.81 37.19 40.46 o 13 6 1 621.67 610.48 73.98 o 14 6 1 0.92 -34.98 43.89 o 15 6 1 12.38 -9.26 56.25 o 1 7 1 1.81 86.68 29.95 o 2 7 1 461.29 458.24 36.19 o 3 7 1 167.97 229.70 47.34 o 4 7 1 134.61 88.69 27.85 o 5 7 1 58.70 33.77 22.69 o 6 7 1 208.17 209.61 34.59 o 7 7 1 16.21 -14.87 30.09 o 8 7 1 122.87 116.95 35.07 o 9 7 1 0.32 5.46 33.32 o 10 7 1 79.71 36.98 37.65 o 11 7 1 0.00 -12.98 37.81 o 12 7 1 144.35 151.73 45.91 o 13 7 1 2.50 40.84 42.96 o 14 7 1 54.17 38.58 49.82 o 0 8 1 530.25 613.89 66.51 o 1 8 1 7.98 -14.01 22.77 o 2 8 1 0.28 5.83 35.93 o 3 8 1 3678.08 3344.51 100.10 o 4 8 1 79.43 71.14 41.79 o 5 8 1 153.65 144.65 31.76 o 6 8 1 3.06 2.81 28.58 o 7 8 1 4607.65 4820.94 97.91 o 8 8 1 71.18 88.38 37.08 o 9 8 1 190.36 192.72 42.40 o 10 8 1 15.85 -17.36 39.31 o 11 8 1 1011.82 1164.21 69.37 o 12 8 1 14.14 -59.78 39.85 o 13 8 1 148.32 99.86 49.44 o 1 9 1 23.30 -42.42 31.38 o 2 9 1 8885.44 8517.24 152.36 o 3 9 1 1.70 11.08 35.28 o 4 9 1 11.98 -3.40 41.21 o 5 9 1 116.80 98.72 34.92 o 6 9 1 1567.32 1702.02 73.94 o 7 9 1 1.63 24.13 34.14 o 8 9 1 419.04 473.82 56.81 o 9 9 1 38.19 75.78 43.55 o 10 9 1 150.72 208.17 46.53 o 11 9 1 0.79 -14.46 42.16 o 12 9 1 855.80 1013.38 68.95 o 0 10 1 19.81 63.48 69.67 o 1 10 1 1750.88 1723.13 89.10 o 2 10 1 11.03 14.81 38.99 o 3 10 1 3125.17 3147.50 97.14 o 4 10 1 3.36 30.29 40.95 o 5 10 1 743.80 671.99 49.84 o 6 10 1 38.53 15.42 35.21 o 7 10 1 2320.39 2400.30 80.96 o 8 10 1 0.07 14.03 47.04 o 9 10 1 76.60 39.06 52.57 o 10 10 1 1.84 -6.60 48.22 o 11 10 1 756.76 740.10 69.75 o 1 11 1 0.92 -68.96 51.91 o 2 11 1 2923.19 2756.79 115.84 o 3 11 1 25.25 74.41 42.12 o 4 11 1 582.12 562.70 57.45 o 5 11 1 22.98 56.85 39.25 o 6 11 1 1833.91 1900.10 90.11 o 7 11 1 4.25 -18.39 41.10 o 8 11 1 290.76 373.55 64.37 o 9 11 1 0.01 3.04 54.18 o 0 12 1 10.56 9.51 85.17 o 1 12 1 1664.64 1573.81 100.81 o 2 12 1 0.77 -41.87 54.59 o 3 12 1 336.71 314.16 72.11 o 4 12 1 1.75 83.34 42.46 o 5 12 1 440.66 471.47 51.89 o 6 12 1 0.18 -29.98 39.79 o 7 12 1 16.95 95.68 78.34 o 1 13 1 2.42 50.07 134.55 o 0 0 2 149726.59 141985.58 3132.29 o 1 0 2 890.34 1032.62 43.81 o 2 0 2 1442.59 1254.24 90.75 o 3 0 2 71307.73 73639.76 1616.21 o 4 0 2 63525.25 60165.25 966.54 o 5 0 2 849.59 709.24 34.85 o 6 0 2 677.36 588.10 36.33 o 7 0 2 5883.02 5940.03 106.28 o 8 0 2 2163.38 2063.26 62.91 o 9 0 2 5455.26 5352.65 95.78 o 10 0 2 4290.77 3905.03 83.99 o 11 0 2 287.84 255.30 32.64 o 12 0 2 109.51 86.34 46.22 o 13 0 2 17.41 -33.99 43.74 o 14 0 2 1726.67 1798.13 103.37 o 15 0 2 377.52 384.89 137.68 o 16 0 2 33.42 -65.71 125.17 o 17 0 2 58.59 309.79 140.81 o 1 1 2 15281.61 15001.50 165.19 o 2 1 2 2215.44 2003.69 80.00 o 3 1 2 6901.50 6570.05 97.82 o 4 1 2 2308.06 2515.95 59.47 o 5 1 2 22834.97 21023.23 248.28 o 6 1 2 0.97 10.73 14.00 o 7 1 2 4138.26 4174.32 64.09 o 8 1 2 236.00 285.19 43.88 o 9 1 2 8182.66 7282.91 93.14 o 10 1 2 14.71 19.77 19.61 o 11 1 2 661.36 604.07 35.90 o 12 1 2 511.72 424.34 33.64 o 13 1 2 987.43 1002.23 56.31 o 14 1 2 83.65 61.66 37.64 o 15 1 2 0.24 -48.50 79.66 o 16 1 2 86.75 -24.91 82.95 o 17 1 2 82.62 89.28 101.71 o 0 2 2 961.47 1503.42 59.40 o 1 2 2 9740.47 11485.75 140.43 o 2 2 2 1313.39 1415.89 28.75 o 3 2 2 768.74 731.96 21.20 o 4 2 2 4078.25 4376.02 319.98 o 5 2 2 6310.19 6537.71 104.62 o 6 2 2 1193.56 1126.71 35.34 o 7 2 2 187.64 223.94 25.08 o 8 2 2 6218.05 6055.14 83.95 o 9 2 2 3.61 23.12 21.60 o 10 2 2 535.71 490.89 36.19 o 11 2 2 1.15 49.89 32.65 o 12 2 2 1897.03 1998.34 74.94 o 13 2 2 588.42 514.36 44.06 o 14 2 2 41.70 13.97 36.68 o 15 2 2 0.03 70.94 63.04 o 16 2 2 161.55 139.89 97.28 o 1 3 2 7368.67 6831.92 80.39 o 2 3 2 2036.62 2071.52 101.46 o 3 3 2 7010.44 7237.87 107.86 o 4 3 2 729.88 998.96 37.18 o 5 3 2 7.97 30.83 26.55 o 6 3 2 87.68 57.62 22.65 o 7 3 2 262.61 236.82 24.69 o 8 3 2 58.84 70.94 28.22 o 9 3 2 0.16 -10.20 20.91 o 10 3 2 217.44 247.44 31.52 o 11 3 2 1622.14 1424.37 58.21 o 12 3 2 3.43 -3.89 28.68 o 13 3 2 174.94 143.38 39.36 o 14 3 2 10.49 -19.43 42.86 o 15 3 2 123.29 167.01 59.98 o 16 3 2 0.01 38.98 87.21 o 0 4 2 22915.19 25335.57 347.78 o 1 4 2 32.13 -41.33 27.55 o 2 4 2 1552.41 1677.91 38.09 o 3 4 2 1026.11 1171.38 85.84 o 4 4 2 6797.36 6734.08 81.23 o 5 4 2 426.46 549.85 33.71 o 6 4 2 1608.00 1708.22 115.64 o 7 4 2 1014.01 1214.61 94.46 o 8 4 2 2.87 4.99 20.88 o 9 4 2 238.71 202.96 31.07 o 10 4 2 125.54 155.59 33.07 o 11 4 2 0.20 28.87 31.11 o 12 4 2 2.40 -28.49 31.71 o 13 4 2 0.06 -11.60 33.16 o 14 4 2 314.05 333.24 54.21 o 15 4 2 13.83 -25.11 54.49 o 16 4 2 136.46 160.90 78.01 o 1 5 2 20695.81 20309.97 231.78 o 2 5 2 393.31 369.68 40.52 o 3 5 2 4758.40 4926.36 77.83 o 4 5 2 0.20 32.37 15.56 o 5 5 2 20473.45 19712.10 188.08 o 6 5 2 365.25 496.38 68.17 o 7 5 2 80.29 67.40 25.01 o 8 5 2 71.76 69.63 28.69 o 9 5 2 5855.25 5775.03 119.36 o 10 5 2 1.10 27.33 30.49 o 11 5 2 31.13 52.31 41.05 o 12 5 2 122.72 149.42 37.30 o 13 5 2 654.92 622.61 50.28 o 14 5 2 5.70 -16.03 47.54 o 15 5 2 2.05 31.39 56.47 o 0 6 2 19695.30 18727.77 288.44 o 1 6 2 1515.75 1507.84 44.29 o 2 6 2 2801.56 2501.11 86.76 o 3 6 2 285.18 292.30 29.18 o 4 6 2 16398.76 15450.01 185.58 o 5 6 2 8.63 71.26 20.67 o 6 6 2 4376.65 4258.53 79.43 o 7 6 2 24.63 62.90 44.13 o 8 6 2 6628.45 6608.60 117.12 o 9 6 2 222.02 223.99 39.38 o 10 6 2 686.74 639.48 48.29 o 11 6 2 11.57 45.01 37.44 o 12 6 2 1105.35 1156.62 72.98 o 13 6 2 70.94 44.67 40.62 o 14 6 2 74.64 53.78 51.49 o 15 6 2 5.03 -7.11 59.79 o 1 7 2 13361.22 12259.28 154.52 o 2 7 2 45.52 0.88 20.75 o 3 7 2 11288.35 10673.81 243.47 o 4 7 2 329.13 430.32 36.31 o 5 7 2 2003.38 1931.55 57.15 o 6 7 2 1.22 14.60 22.98 o 7 7 2 662.60 713.99 47.77 o 8 7 2 42.32 79.31 34.21 o 9 7 2 405.35 481.69 46.61 o 10 7 2 3.42 58.83 38.29 o 11 7 2 148.04 126.91 39.72 o 12 7 2 0.00 18.23 39.66 o 13 7 2 741.41 830.48 66.25 o 14 7 2 6.22 2.44 55.75 o 0 8 2 3798.55 3660.03 218.06 o 1 8 2 68.89 37.44 25.09 o 2 8 2 756.84 759.10 49.94 o 3 8 2 2.71 44.42 32.11 o 4 8 2 3652.30 3421.74 83.09 o 5 8 2 121.37 101.10 29.56 o 6 8 2 1690.68 1930.08 67.12 o 7 8 2 13.98 98.34 39.68 o 8 8 2 1630.02 1778.56 72.40 o 9 8 2 29.35 61.79 36.29 o 10 8 2 387.70 411.73 46.90 o 11 8 2 18.87 48.72 41.19 o 12 8 2 246.69 336.87 51.61 o 13 8 2 24.10 -69.98 48.55 o 1 9 2 58.17 56.45 35.76 o 2 9 2 30.96 149.85 40.23 o 3 9 2 121.74 116.72 39.47 o 4 9 2 768.32 726.30 52.66 o 5 9 2 926.31 948.21 60.22 o 6 9 2 23.66 21.81 30.32 o 7 9 2 26.01 -22.22 32.54 o 8 9 2 146.55 134.78 45.71 o 9 9 2 551.91 596.48 56.77 o 10 9 2 2.18 5.48 39.96 o 11 9 2 4.02 -56.64 41.90 o 12 9 2 5.28 12.89 45.84 o 0 10 2 103.10 -59.68 60.82 o 1 10 2 139.29 101.96 50.33 o 2 10 2 109.78 30.15 39.80 o 3 10 2 86.26 194.72 44.66 o 4 10 2 104.39 68.64 38.50 o 5 10 2 2.40 5.88 34.61 o 6 10 2 73.82 83.97 38.01 o 7 10 2 2.65 114.65 41.35 o 8 10 2 721.95 733.57 68.52 o 9 10 2 89.09 52.87 48.75 o 10 10 2 77.45 14.61 50.28 o 11 10 2 0.62 80.29 53.81 o 1 11 2 1078.96 1209.27 84.38 o 2 11 2 30.21 121.63 55.88 o 3 11 2 1662.36 1520.98 81.15 o 4 11 2 42.41 27.40 41.49 o 5 11 2 112.33 112.46 42.38 o 6 11 2 19.49 -27.40 39.41 o 7 11 2 207.29 268.43 49.38 o 8 11 2 41.04 70.45 55.82 o 9 11 2 68.18 81.76 55.93 o 0 12 2 2179.94 2139.46 160.41 o 1 12 2 0.32 96.71 63.07 o 2 12 2 130.66 181.47 65.31 o 3 12 2 11.63 88.98 63.05 o 4 12 2 1515.64 1390.10 69.45 o 5 12 2 0.94 46.26 39.90 o 6 12 2 594.61 612.63 59.16 o 1 13 2 424.81 159.59 137.68 o 2 13 2 21.34 103.26 143.94 o 1 1 3 64.33 38.79 8.35 o 2 1 3 248.21 207.40 44.52 o 3 1 3 60.62 60.73 10.27 o 4 1 3 5114.83 5070.68 86.91 o 5 1 3 2234.87 2557.35 78.43 o 6 1 3 6039.57 5438.41 65.64 o 7 1 3 2.02 2.57 13.24 o 8 1 3 2744.65 2699.60 49.73 o 9 1 3 696.84 828.05 42.27 o 10 1 3 3574.05 3579.29 64.56 o 11 1 3 4.58 37.09 21.99 o 12 1 3 91.73 99.88 29.07 o 13 1 3 226.03 209.37 40.75 o 14 1 3 113.80 25.18 44.87 o 15 1 3 0.07 -11.47 62.06 o 16 1 3 10.23 33.89 91.80 o 17 1 3 81.26 203.79 105.93 o 0 2 3 220.06 179.26 14.98 o 1 2 3 22792.35 23814.73 293.20 o 2 2 3 188.20 301.82 21.60 o 3 2 3 4027.27 4016.09 92.77 o 4 2 3 924.16 1223.39 51.09 o 5 2 3 5879.91 5988.05 78.22 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31 2.43 3.18 60.46 o