#------------------------------------------------------------------------------ #$Date: 2010-05-06 17:22:57 +0300 (Thu, 06 May 2010) $ #$Revision: 1157 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2225629.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225629_Fobs loop_ _publ_author_name 'Khan, Islam Ullah' Ejaz '\,Sahin, Onur' 'B\"uy\"ukg\"ung\"or, Orhan' _publ_section_title ; Diazidobis(propane-1,3-diamine)copper(II) ; _journal_coeditor_code OM2325 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m434 _journal_page_last m435 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 93.296 _cell_angle_beta 98.306 _cell_angle_gamma 119.453 _cell_length_a 6.6869 _cell_length_b 6.7743 _cell_length_c 8.2445 _exptl_crystal_F_000 155.00 _reflns_d_resolution_high 0.7573 _[local]_cod_data_source_file om2325Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 58R in P1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 45.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 341.52 335.91 3.77 o 3 0 0 820.21 855.42 11.23 o 4 0 0 548.61 585.77 7.77 o 5 0 0 193.81 199.88 3.16 o 6 0 0 10.52 11.64 0.61 o 7 0 0 95.08 93.88 2.48 o -7 1 0 17.83 18.23 0.64 o -6 1 0 7.89 8.41 0.42 o -5 1 0 79.75 84.55 2.20 o -4 1 0 163.67 169.54 3.52 o -3 1 0 2.24 1.43 0.12 o -2 1 0 10.49 15.64 0.24 o 1 1 0 11.12 11.77 0.25 o 2 1 0 523.56 531.81 6.46 o 3 1 0 1095.12 1109.12 15.14 o 4 1 0 305.33 311.09 4.99 o 5 1 0 49.29 49.23 1.04 o 6 1 0 103.51 104.42 2.70 o -8 2 0 64.16 66.44 1.87 o -7 2 0 16.74 17.45 0.68 o -6 2 0 165.12 156.64 2.55 o -5 2 0 34.54 34.88 0.60 o -4 2 0 413.81 402.65 4.48 o -3 2 0 142.43 135.88 1.54 o -2 2 0 3.83 3.66 0.18 o -1 2 0 551.99 570.83 8.00 o 0 2 0 376.16 422.75 4.18 o 1 2 0 333.61 347.36 4.28 o 2 2 0 64.68 63.27 1.02 o 3 2 0 196.59 206.31 3.28 o 4 2 0 8.67 8.76 0.46 o 5 2 0 1.74 2.00 0.48 o 6 2 0 56.95 54.01 2.46 o -8 3 0 63.80 63.99 1.45 o -7 3 0 110.74 108.99 2.25 o -6 3 0 122.82 125.32 2.07 o -5 3 0 533.48 526.38 8.86 o -4 3 0 732.94 743.00 8.19 o -3 3 0 327.04 321.25 3.56 o -2 3 0 455.44 436.09 4.84 o -1 3 0 1108.64 1151.21 17.49 o 0 3 0 835.15 831.90 9.36 o 1 3 0 81.02 76.80 1.09 o 2 3 0 186.24 196.08 2.56 o 3 3 0 62.98 62.87 1.44 o 4 3 0 3.96 3.68 0.45 o 5 3 0 16.69 16.51 1.39 o -8 4 0 23.36 23.03 0.83 o -7 4 0 50.68 49.71 1.01 o -6 4 0 40.80 41.26 1.32 o -5 4 0 578.89 582.63 8.69 o -4 4 0 33.16 30.76 0.55 o -3 4 0 178.79 175.65 1.90 o -2 4 0 1113.49 1176.88 21.99 o -1 4 0 709.84 723.01 8.16 o 0 4 0 350.92 364.49 4.55 o 1 4 0 34.21 35.78 0.72 o 2 4 0 472.60 456.46 8.02 o 3 4 0 74.99 74.58 2.12 o 4 4 0 34.34 35.35 1.69 o -8 5 0 8.69 9.31 0.59 o -7 5 0 6.16 5.55 0.31 o -6 5 0 86.47 88.11 1.50 o -5 5 0 8.87 9.90 0.29 o -4 5 0 9.09 9.15 0.31 o -3 5 0 96.25 99.51 1.80 o -2 5 0 260.36 264.68 3.67 o -1 5 0 25.68 27.23 0.71 o 0 5 0 2.39 2.42 0.25 o 1 5 0 207.16 202.46 4.63 o 2 5 0 90.31 86.36 2.39 o 3 5 0 18.36 18.37 1.14 o -8 6 0 30.56 29.73 0.74 o -7 6 0 34.26 38.56 1.03 o -6 6 0 127.92 135.25 2.22 o -5 6 0 11.74 12.70 0.46 o -4 6 0 124.38 126.84 1.70 o -3 6 0 64.18 65.80 1.10 o -2 6 0 33.53 33.82 0.73 o -1 6 0 2.66 3.04 0.35 o 0 6 0 11.19 10.73 0.80 o 1 6 0 86.36 85.06 2.88 o 2 6 0 0.74 0.17 0.63 o -8 7 0 28.32 27.48 0.76 o -7 7 0 55.22 55.34 1.10 o -6 7 0 60.54 60.31 1.18 o -5 7 0 112.22 111.99 1.95 o -4 7 0 38.18 38.23 1.26 o -3 7 0 117.81 124.71 2.17 o -2 7 0 61.62 60.70 1.51 o -1 7 0 35.00 34.92 1.36 o 0 7 0 68.18 66.79 2.10 o 1 7 0 8.09 8.54 0.95 o -7 8 0 19.33 17.35 0.74 o -6 8 0 11.80 9.58 0.58 o -5 8 0 19.81 18.88 0.80 o -4 8 0 8.81 8.95 0.62 o -3 8 0 76.94 79.57 3.29 o -2 8 0 16.89 16.97 1.60 o -1 8 0 12.93 12.54 1.03 o 1 -8 1 17.21 19.17 1.38 o 2 -8 1 54.42 57.02 1.87 o 3 -8 1 56.28 56.50 2.63 o 4 -8 1 20.83 18.86 1.08 o 5 -8 1 24.04 23.59 1.11 o 6 -8 1 68.29 70.90 1.64 o 7 -8 1 26.04 25.42 0.90 o -1 -7 1 4.07 5.29 0.84 o 0 -7 1 3.89 5.18 1.03 o 1 -7 1 5.07 5.09 0.69 o 2 -7 1 53.49 53.85 1.39 o 3 -7 1 69.84 67.80 1.34 o 4 -7 1 2.23 2.55 0.40 o 5 -7 1 162.57 176.33 2.91 o 6 -7 1 44.99 48.82 1.17 o 7 -7 1 24.24 26.15 0.75 o 8 -7 1 24.08 24.17 1.28 o -2 -6 1 43.82 41.02 1.60 o -1 -6 1 3.30 3.62 0.67 o 0 -6 1 0.85 0.38 0.51 o 1 -6 1 42.31 40.79 1.24 o 2 -6 1 77.63 76.17 1.42 o 3 -6 1 11.16 10.90 0.41 o 4 -6 1 21.58 23.13 0.56 o 5 -6 1 43.77 46.57 0.97 o 6 -6 1 15.17 16.59 0.54 o 7 -6 1 8.56 9.63 0.47 o 8 -6 1 31.65 30.81 0.82 o -3 -5 1 107.67 101.60 2.78 o -2 -5 1 35.50 37.79 1.40 o -1 -5 1 163.21 163.35 3.82 o 0 -5 1 62.79 65.28 1.02 o 1 -5 1 458.91 475.71 5.92 o 2 -5 1 234.63 239.10 3.33 o 3 -5 1 25.61 25.78 0.45 o 4 -5 1 189.70 193.91 2.47 o 5 -5 1 44.24 42.80 0.86 o 6 -5 1 131.49 122.77 2.25 o 7 -5 1 6.12 5.60 0.31 o 8 -5 1 15.54 15.14 0.70 o -4 -4 1 9.04 8.64 0.82 o -3 -4 1 46.72 48.44 1.58 o -2 -4 1 164.14 164.66 2.70 o -1 -4 1 99.02 94.14 1.91 o 0 -4 1 369.79 361.60 4.18 o 1 -4 1 719.17 733.63 8.28 o 2 -4 1 335.49 335.61 3.82 o 3 -4 1 177.78 178.87 2.09 o 4 -4 1 528.19 511.08 8.86 o 5 -4 1 613.19 610.81 8.13 o 6 -4 1 76.41 76.70 1.40 o 7 -4 1 47.43 48.31 1.05 o 8 -4 1 58.43 59.03 1.42 o -5 -3 1 0.61 0.80 0.80 o -4 -3 1 17.52 19.48 0.79 o -3 -3 1 91.64 94.94 1.64 o -2 -3 1 112.31 110.72 1.69 o -1 -3 1 112.29 140.58 1.72 o 0 -3 1 906.47 902.30 10.14 o 1 -3 1 99.50 90.59 0.98 o 2 -3 1 19.54 14.39 0.24 o 3 -3 1 414.76 401.42 4.51 o 4 -3 1 476.87 487.38 5.46 o 5 -3 1 283.26 277.15 3.81 o 6 -3 1 0.82 0.85 0.25 o 7 -3 1 175.85 179.43 2.96 o 8 -3 1 83.14 76.58 3.63 o -6 -2 1 20.44 21.50 1.09 o -5 -2 1 71.90 72.24 2.59 o -4 -2 1 306.73 309.89 4.31 o -3 -2 1 272.61 274.26 3.79 o -2 -2 1 2.72 4.23 0.18 o -1 -2 1 432.31 468.49 5.31 o 0 -2 1 664.96 704.31 8.27 o 1 -2 1 70.20 76.85 0.77 o 2 -2 1 17.46 25.51 0.37 o 3 -2 1 325.61 321.05 3.37 o 4 -2 1 157.82 156.26 2.23 o 5 -2 1 3.33 3.68 0.21 o 6 -2 1 81.73 78.16 1.44 o 7 -2 1 63.32 60.31 1.25 o 8 -2 1 13.90 12.20 0.84 o -7 -1 1 7.64 7.31 0.76 o -6 -1 1 130.30 127.63 3.13 o -5 -1 1 136.02 140.45 2.34 o -4 -1 1 328.81 346.43 4.70 o -3 -1 1 364.20 363.72 4.88 o -2 -1 1 338.70 352.91 3.98 o 2 -1 1 383.86 407.11 4.02 o 3 -1 1 871.07 880.87 14.22 o 4 -1 1 380.81 400.57 4.89 o 5 -1 1 49.75 50.52 0.81 o 6 -1 1 161.92 157.85 2.64 o 7 -1 1 9.91 9.71 0.60 o -7 0 1 42.92 43.44 1.40 o -6 0 1 11.47 10.90 0.73 o -5 0 1 38.48 44.40 0.90 o -4 0 1 116.17 118.28 1.68 o -3 0 1 298.34 298.70 3.61 o -2 0 1 751.90 798.86 22.77 o 0 0 1 2061.73 0.02 0.01 o 1 0 1 21.06 19.41 0.29 o 3 0 1 1195.91 1287.59 21.69 o 4 0 1 318.27 330.19 5.81 o 5 0 1 161.01 165.49 2.70 o 6 0 1 58.00 57.17 1.69 o 7 0 1 95.55 92.31 2.51 o -8 1 1 26.84 28.02 1.09 o -7 1 1 50.90 53.60 1.27 o -6 1 1 0.63 0.57 0.26 o -5 1 1 252.99 256.24 3.46 o -4 1 1 281.73 268.07 3.24 o -3 1 1 34.09 28.27 0.54 o -1 1 1 13.27 12.63 0.20 o 0 1 1 157.54 192.71 2.34 o 1 1 1 163.53 184.33 2.12 o 2 1 1 975.04 1032.51 12.45 o 3 1 1 261.27 261.41 4.04 o 4 1 1 4.46 4.81 0.33 o 5 1 1 49.26 52.79 1.28 o 6 1 1 81.04 80.96 2.75 o -8 2 1 56.71 59.59 1.37 o -7 2 1 26.09 26.34 0.68 o -6 2 1 313.59 318.39 4.88 o -5 2 1 351.28 355.63 6.19 o -4 2 1 377.55 380.19 6.37 o -3 2 1 111.68 99.54 2.19 o 0 2 1 63.29 81.31 1.11 o 1 2 1 667.54 711.22 9.50 o 2 2 1 215.29 222.05 3.12 o 3 2 1 32.21 29.93 0.73 o 4 2 1 6.00 5.90 0.47 o 5 2 1 49.77 48.89 1.89 o 6 2 1 54.93 45.50 2.28 o -8 3 1 35.34 33.39 0.88 o -7 3 1 63.20 61.28 1.14 o -6 3 1 290.06 294.64 3.99 o -5 3 1 69.79 71.99 1.97 o -4 3 1 288.27 279.44 4.72 o -3 3 1 1000.95 1058.91 17.57 o -1 3 1 733.67 751.69 7.86 o 0 3 1 163.94 157.28 1.89 o 1 3 1 805.87 808.43 9.88 o 2 3 1 145.86 140.99 1.92 o 3 3 1 98.59 97.23 2.03 o 4 3 1 71.43 74.86 3.27 o 5 3 1 58.62 56.75 2.66 o -8 4 1 23.83 22.93 0.79 o -7 4 1 44.43 45.89 0.90 o -6 4 1 1.27 1.49 0.17 o -5 4 1 168.90 165.01 2.86 o -4 4 1 77.77 74.40 0.92 o -3 4 1 377.72 384.01 4.31 o -2 4 1 167.19 174.52 2.04 o -1 4 1 32.00 28.63 0.46 o 0 4 1 409.54 417.99 5.21 o 1 4 1 106.16 103.26 1.61 o 2 4 1 237.03 226.23 5.09 o 3 4 1 25.48 26.17 1.43 o 4 4 1 41.76 43.96 1.62 o -8 5 1 15.60 16.15 0.79 o -7 5 1 26.97 26.71 0.57 o -6 5 1 66.98 67.86 1.06 o -5 5 1 174.96 176.36 2.44 o -4 5 1 19.11 19.15 0.43 o -3 5 1 83.46 87.15 1.11 o -2 5 1 53.37 54.28 1.12 o -1 5 1 26.32 24.76 0.66 o 0 5 1 96.11 97.90 2.05 o 1 5 1 53.14 54.10 1.68 o 2 5 1 16.96 14.84 0.97 o 3 5 1 0.27 0.33 0.62 o -8 6 1 22.33 22.80 0.71 o -7 6 1 66.68 68.08 1.21 o -6 6 1 206.51 202.17 3.17 o -5 6 1 13.75 13.43 0.45 o -4 6 1 180.42 183.86 2.61 o -3 6 1 122.61 127.78 1.91 o -2 6 1 100.34 100.28 1.77 o -1 6 1 83.78 79.54 1.78 o 0 6 1 35.05 35.21 1.31 o 1 6 1 54.77 51.58 2.70 o 2 6 1 2.77 1.30 0.78 o -8 7 1 21.97 22.17 0.62 o -7 7 1 32.00 30.17 0.73 o -6 7 1 29.47 26.80 0.69 o -5 7 1 24.40 24.19 0.67 o -4 7 1 113.92 119.10 2.08 o -3 7 1 67.18 71.76 1.41 o -2 7 1 41.60 41.23 1.20 o -1 7 1 42.16 44.38 2.33 o 0 7 1 45.21 45.66 1.68 o -7 8 1 10.31 9.89 0.58 o -6 8 1 3.62 4.03 0.45 o -5 8 1 42.43 45.25 1.29 o -4 8 1 4.24 4.00 0.51 o -3 8 1 22.00 18.98 1.57 o -2 8 1 3.39 2.46 1.02 o -1 8 1 14.28 17.04 1.76 o 1 -8 2 14.87 17.36 1.14 o 2 -8 2 34.57 36.60 1.45 o 3 -8 2 6.43 6.21 1.13 o 4 -8 2 57.86 61.66 1.98 o 5 -8 2 23.35 25.93 1.22 o 6 -8 2 42.63 45.53 1.27 o -1 -7 2 0.16 -0.38 0.64 o 0 -7 2 0.89 0.12 0.60 o 1 -7 2 33.62 30.82 1.69 o 2 -7 2 28.21 27.46 1.14 o 3 -7 2 13.24 14.03 0.58 o 4 -7 2 3.89 4.60 0.39 o 5 -7 2 69.07 73.05 1.64 o 6 -7 2 14.11 14.48 0.69 o 7 -7 2 13.83 16.02 0.75 o -2 -6 2 45.48 45.82 1.71 o -1 -6 2 0.41 0.33 0.55 o 0 -6 2 143.59 141.06 3.44 o 1 -6 2 140.74 139.84 2.38 o 2 -6 2 21.19 21.91 0.65 o 3 -6 2 17.55 18.08 0.47 o 4 -6 2 42.38 43.23 0.83 o 5 -6 2 168.27 172.11 2.83 o 6 -6 2 0.41 0.41 0.28 o 7 -6 2 13.48 13.73 0.60 o 8 -6 2 29.23 27.96 0.96 o -3 -5 2 55.44 54.15 3.18 o -2 -5 2 12.80 14.05 0.93 o -1 -5 2 174.01 174.27 4.05 o 0 -5 2 248.16 254.19 3.56 o 1 -5 2 174.84 181.37 2.20 o 2 -5 2 46.30 47.35 0.85 o 3 -5 2 184.07 186.12 2.40 o 4 -5 2 572.14 599.95 7.31 o 5 -5 2 38.59 37.31 0.81 o 6 -5 2 41.78 42.29 0.94 o 7 -5 2 56.04 58.46 1.10 o 8 -5 2 48.07 46.07 2.75 o -4 -4 2 14.92 13.64 1.28 o -3 -4 2 44.86 44.41 1.21 o -2 -4 2 5.38 4.65 0.34 o -1 -4 2 223.26 209.73 2.74 o 0 -4 2 44.24 39.78 0.62 o 1 -4 2 180.34 171.24 2.05 o 2 -4 2 300.35 282.15 3.27 o 3 -4 2 444.67 451.43 5.10 o 4 -4 2 335.86 333.94 6.31 o 5 -4 2 15.26 18.10 0.39 o 6 -4 2 175.08 178.23 2.93 o 7 -4 2 105.10 104.39 1.92 o 8 -4 2 43.25 43.03 1.51 o -5 -3 2 32.48 33.43 1.30 o -4 -3 2 82.39 81.48 1.78 o -3 -3 2 36.53 36.43 0.76 o -2 -3 2 112.29 107.50 1.86 o -1 -3 2 5.65 5.54 0.22 o 0 -3 2 540.88 558.63 6.33 o 1 -3 2 115.15 111.68 1.19 o 2 -3 2 209.26 207.15 2.54 o 3 -3 2 178.01 171.80 2.48 o 4 -3 2 31.90 31.53 0.52 o 5 -3 2 152.42 152.69 2.02 o 6 -3 2 33.26 33.86 0.83 o 7 -3 2 102.06 99.78 1.85 o 8 -3 2 14.22 11.98 0.86 o -6 -2 2 21.64 21.92 1.93 o -5 -2 2 100.18 103.27 2.75 o -4 -2 2 162.22 162.19 2.37 o -3 -2 2 142.77 146.71 2.12 o -2 -2 2 395.37 431.13 4.90 o -1 -2 2 680.87 742.10 7.35 o 1 -2 2 2.83 3.13 0.10 o 2 -2 2 253.27 231.30 2.23 o 3 -2 2 865.03 899.32 12.90 o 4 -2 2 161.24 162.72 2.48 o 5 -2 2 63.05 62.25 0.96 o 6 -2 2 48.16 47.70 1.04 o 7 -2 2 62.44 60.54 1.84 o -7 -1 2 5.27 5.46 1.00 o -6 -1 2 37.64 39.95 1.31 o -5 -1 2 38.69 40.98 1.12 o -4 -1 2 145.65 148.55 2.13 o -3 -1 2 218.36 227.85 2.84 o -2 -1 2 399.50 422.23 5.11 o 0 -1 2 76.82 98.85 1.02 o 1 -1 2 880.27 895.15 18.65 o 3 -1 2 1067.67 1107.75 17.83 o 4 -1 2 125.30 128.23 1.71 o 5 -1 2 51.23 54.47 0.97 o 6 -1 2 280.10 271.14 4.97 o 7 -1 2 13.29 13.16 0.74 o -7 0 2 7.24 7.24 0.60 o -6 0 2 58.99 60.83 1.36 o -5 0 2 52.61 50.62 1.12 o -4 0 2 148.82 143.72 2.26 o -3 0 2 265.21 273.44 3.64 o -2 0 2 276.93 283.08 3.73 o -1 0 2 120.18 106.15 1.07 o 0 0 2 1.65 2.23 0.10 o 2 0 2 817.15 816.46 9.18 o 3 0 2 44.33 40.75 0.66 o 4 0 2 65.86 66.87 1.11 o 5 0 2 219.86 226.41 3.24 o 6 0 2 118.28 119.97 2.50 o 7 0 2 10.65 9.62 0.84 o -8 1 2 19.33 19.68 1.51 o -7 1 2 110.47 111.15 2.64 o -6 1 2 29.72 31.69 0.80 o -5 1 2 312.08 314.54 4.73 o -4 1 2 231.94 231.60 3.47 o -3 1 2 201.68 222.21 4.52 o -1 1 2 64.24 61.24 0.64 o 1 1 2 19.60 15.01 0.29 o 2 1 2 275.91 275.15 3.80 o 3 1 2 46.90 45.75 0.83 o 4 1 2 114.78 113.64 2.09 o 5 1 2 168.65 168.29 3.26 o 6 1 2 3.69 3.43 0.65 o -8 2 2 50.31 51.56 1.50 o -7 2 2 51.66 53.55 1.05 o -6 2 2 80.44 86.76 1.64 o -5 2 2 365.34 376.11 7.64 o -3 2 2 332.64 356.24 10.53 o -1 2 2 834.94 874.55 11.29 o 0 2 2 236.08 215.03 2.33 o 1 2 2 243.13 234.03 2.98 o 2 2 2 389.29 392.65 5.39 o 3 2 2 122.85 121.32 2.09 o 4 2 2 92.36 94.95 2.03 o 5 2 2 39.13 37.66 2.00 o -8 3 2 22.65 24.48 0.78 o -7 3 2 4.47 5.29 0.29 o -6 3 2 259.23 255.87 5.46 o -5 3 2 53.17 49.23 1.98 o -4 3 2 319.07 326.14 5.47 o -3 3 2 474.81 490.98 6.46 o -2 3 2 341.93 337.07 3.77 o -1 3 2 369.85 357.28 4.05 o 0 3 2 78.92 71.42 1.01 o 1 3 2 1002.27 1024.46 12.48 o 2 3 2 69.01 67.53 1.16 o 3 3 2 63.70 67.31 1.57 o 4 3 2 62.54 62.92 1.93 o 5 3 2 25.63 25.17 1.79 o -8 4 2 13.98 14.29 0.65 o -7 4 2 51.34 52.73 2.38 o -6 4 2 106.44 103.35 3.66 o -5 4 2 92.36 91.93 1.67 o -4 4 2 151.79 148.51 1.86 o -3 4 2 131.40 129.17 1.65 o -2 4 2 43.82 41.44 0.59 o -1 4 2 141.55 136.82 2.23 o 0 4 2 350.75 368.25 4.62 o 1 4 2 107.19 108.02 1.89 o 2 4 2 13.80 14.90 1.04 o 3 4 2 42.77 40.48 1.50 o 4 4 2 51.48 54.51 2.26 o -8 5 2 22.96 22.94 0.70 o -7 5 2 91.61 89.74 3.90 o -6 5 2 40.70 39.54 0.66 o -5 5 2 212.08 214.55 3.03 o -4 5 2 35.60 38.91 0.52 o -3 5 2 167.11 178.93 2.11 o -2 5 2 163.46 169.06 2.20 o -1 5 2 99.74 101.09 1.78 o 0 5 2 120.39 119.30 2.42 o 1 5 2 0.47 0.04 0.50 o 2 5 2 65.37 64.60 2.01 o 3 5 2 25.67 25.95 1.35 o -8 6 2 14.73 15.38 0.50 o -7 6 2 52.58 50.78 1.52 o -6 6 2 82.50 81.70 1.39 o -5 6 2 38.06 38.94 0.80 o -4 6 2 103.63 106.11 1.81 o -3 6 2 140.51 141.28 2.09 o -2 6 2 90.25 89.87 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