#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:35:02 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181177 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/56/2225652.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225652_Fobs loop_ _publ_author_name 'Ahmad, Tanveer' 'Zia-ur-Rehman, Muhammad' 'Siddiqui, Hamid Latif' 'Mahmud, Shahid' 'Parvez, Masood' _publ_section_title ; 4-Nitro-N'-[(E)-3-pyridylmethylidene]benzohydrazide ; _journal_coeditor_code LH5020 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o976 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.609 _cell_angle_gamma 90.000 _cell_length_a 14.6158 _cell_length_b 8.1969 _cell_length_c 10.3645 _exptl_crystal_F_000 560.00 _reflns_d_resolution_high 0.8311 _cod_data_source_file lh5020Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' fnt27 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 77.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 713.54 682.73 11.17 o 3 0 0 5724.21 5234.44 83.98 o 4 0 0 2449.00 2389.66 29.72 o 5 0 0 149.30 150.80 2.44 o 6 0 0 1095.92 1118.16 20.14 o 7 0 0 4495.38 4509.19 63.68 o 8 0 0 598.64 675.63 10.56 o 9 0 0 108.73 108.13 2.64 o 10 0 0 138.84 139.05 2.21 o 11 0 0 168.11 155.73 1.90 o 12 0 0 181.63 180.53 2.04 o 13 0 0 13.00 12.11 0.55 o 14 0 0 0.02 0.48 0.27 o 15 0 0 63.02 61.26 1.31 o 16 0 0 19.03 18.33 1.00 o 17 0 0 5.51 2.77 0.64 o 1 1 0 1.57 -0.55 0.37 o 2 1 0 133.52 126.40 1.59 o 3 1 0 960.78 911.57 8.16 o 4 1 0 2187.23 2094.44 18.46 o 5 1 0 1176.14 1098.49 7.26 o 6 1 0 63.02 61.50 0.91 o 7 1 0 2580.22 2789.73 22.33 o 8 1 0 102.10 108.10 1.61 o 9 1 0 792.76 892.99 9.73 o 10 1 0 651.20 636.11 4.35 o 11 1 0 5.96 6.36 0.25 o 12 1 0 0.93 0.85 0.16 o 13 1 0 74.38 68.30 0.71 o 14 1 0 49.93 41.34 0.64 o 15 1 0 12.95 10.87 0.41 o 16 1 0 1.93 1.88 0.26 o 0 2 0 2271.22 2131.64 33.80 o 1 2 0 3572.35 3454.37 44.48 o 3 2 0 5940.17 5643.64 43.92 o 4 2 0 1946.66 1866.79 12.45 o 5 2 0 146.25 164.86 1.60 o 6 2 0 488.02 507.17 5.36 o 7 2 0 6.22 5.57 0.36 o 8 2 0 26.84 21.54 0.65 o 9 2 0 5.59 5.99 0.30 o 10 2 0 63.11 67.28 0.73 o 11 2 0 83.15 76.48 0.96 o 12 2 0 352.22 333.62 2.31 o 13 2 0 42.20 37.71 0.62 o 14 2 0 3.22 0.92 0.15 o 15 2 0 47.70 51.58 0.69 o 16 2 0 14.55 13.41 0.46 o 1 3 0 456.85 415.51 3.72 o 2 3 0 42.43 48.01 0.76 o 3 3 0 1240.12 1276.05 11.69 o 4 3 0 1030.77 1131.64 11.39 o 5 3 0 4164.75 4325.23 45.70 o 6 3 0 2.70 3.24 0.53 o 7 3 0 28.66 28.73 1.92 o 8 3 0 21.99 21.44 0.64 o 9 3 0 58.66 62.08 0.90 o 10 3 0 24.21 25.46 0.53 o 11 3 0 34.78 30.46 0.53 o 12 3 0 236.37 266.27 2.66 o 13 3 0 158.44 150.36 1.60 o 14 3 0 41.93 46.50 0.77 o 15 3 0 80.49 92.35 1.02 o 16 3 0 0.07 0.21 0.20 o 0 4 0 830.69 871.53 12.20 o 1 4 0 8.74 8.72 0.57 o 2 4 0 392.94 438.33 5.54 o 3 4 0 12.57 11.95 0.85 o 4 4 0 414.54 422.87 8.11 o 5 4 0 1688.30 1796.53 24.49 o 6 4 0 1233.18 1263.88 17.86 o 7 4 0 92.02 100.39 1.72 o 8 4 0 31.99 31.96 0.53 o 9 4 0 126.64 121.92 1.16 o 10 4 0 13.62 12.88 0.42 o 11 4 0 28.07 19.84 0.51 o 12 4 0 175.86 138.09 1.44 o 13 4 0 5.68 5.81 0.28 o 14 4 0 224.69 235.31 2.24 o 15 4 0 3.28 2.96 0.26 o 1 5 0 591.13 619.54 7.71 o 2 5 0 1101.75 1118.76 15.89 o 3 5 0 96.19 80.32 3.19 o 4 5 0 24.78 21.44 0.76 o 5 5 0 149.37 144.26 3.31 o 6 5 0 57.85 58.56 0.89 o 7 5 0 995.58 971.07 6.11 o 8 5 0 2.23 2.80 0.24 o 9 5 0 49.03 46.36 0.73 o 10 5 0 6.48 8.26 0.50 o 11 5 0 0.29 2.05 0.48 o 12 5 0 138.69 128.92 1.37 o 13 5 0 14.85 15.70 0.77 o 14 5 0 151.21 154.39 1.80 o 0 6 0 531.09 555.38 11.28 o 1 6 0 298.08 305.02 3.56 o 2 6 0 102.03 108.91 1.64 o 3 6 0 4.44 4.32 0.35 o 4 6 0 29.73 29.56 0.61 o 5 6 0 86.62 92.61 1.15 o 6 6 0 64.28 68.26 0.98 o 7 6 0 97.29 101.31 1.27 o 8 6 0 1203.26 1137.55 8.09 o 9 6 0 90.36 82.26 1.15 o 10 6 0 112.44 98.71 1.33 o 11 6 0 1.99 3.32 0.33 o 12 6 0 4.12 5.30 0.39 o 13 6 0 54.18 61.65 3.41 o 1 7 0 144.45 149.06 1.69 o 2 7 0 314.80 316.94 2.78 o 3 7 0 68.23 70.77 1.04 o 4 7 0 15.87 15.13 0.51 o 5 7 0 322.92 335.58 2.76 o 6 7 0 36.33 40.49 0.74 o 7 7 0 81.55 80.11 2.06 o 8 7 0 0.47 0.48 0.23 o 9 7 0 3.55 5.94 0.39 o 10 7 0 15.67 14.38 0.54 o 11 7 0 80.24 71.19 0.99 o 12 7 0 77.34 79.11 2.24 o 0 8 0 41.43 42.65 1.22 o 1 8 0 18.56 17.07 0.58 o 2 8 0 0.89 1.51 0.25 o 3 8 0 12.41 13.68 0.49 o 4 8 0 0.07 -0.12 0.23 o 5 8 0 28.73 25.70 0.63 o 6 8 0 181.47 176.53 1.88 o 7 8 0 22.15 24.95 0.58 o 8 8 0 46.54 51.38 0.88 o 9 8 0 5.22 6.05 0.33 o 10 8 0 12.59 12.81 0.64 o 1 9 0 13.53 12.23 0.50 o 2 9 0 68.08 67.42 1.09 o 3 9 0 16.40 19.91 0.48 o 4 9 0 104.72 106.84 1.24 o 5 9 0 333.94 328.06 2.96 o 6 9 0 52.48 56.25 0.85 o 7 9 0 34.00 35.22 0.75 o -17 1 1 62.53 61.04 1.92 o -16 1 1 0.21 0.52 0.23 o -15 1 1 15.11 14.59 0.36 o -14 1 1 6.16 10.59 0.34 o -13 1 1 27.99 29.85 0.50 o -12 1 1 108.76 102.61 0.81 o -11 1 1 703.38 687.03 4.99 o -10 1 1 462.30 472.49 3.97 o -9 1 1 1695.65 1733.10 15.93 o -8 1 1 0.04 0.76 0.17 o -7 1 1 4563.58 4720.01 43.60 o -6 1 1 616.96 621.19 4.65 o -5 1 1 118.37 117.73 1.10 o -4 1 1 339.21 333.39 2.87 o -3 1 1 2747.39 2689.08 24.43 o -2 1 1 187.58 212.39 2.35 o -1 1 1 111.50 81.66 1.39 o 0 1 1 1815.66 1660.78 17.47 o 1 1 1 2184.82 2066.63 21.75 o 2 1 1 8.26 6.78 0.32 o 3 1 1 308.31 346.05 3.28 o 4 1 1 841.80 766.71 5.86 o 5 1 1 1173.77 1165.85 8.81 o 6 1 1 4.26 5.35 0.31 o 7 1 1 1085.76 1240.20 12.55 o 8 1 1 453.90 462.07 5.21 o 9 1 1 0.92 1.39 0.53 o 10 1 1 11.85 15.35 0.42 o 11 1 1 0.19 0.57 0.23 o 12 1 1 75.75 77.92 0.84 o 13 1 1 492.44 479.15 3.55 o 14 1 1 399.69 379.25 3.19 o 15 1 1 0.02 0.05 0.18 o 16 1 1 33.01 30.11 0.62 o -17 2 1 57.96 66.27 1.21 o -16 2 1 33.19 36.19 0.70 o -15 2 1 7.55 7.88 0.32 o -14 2 1 423.15 371.73 2.69 o -13 2 1 1.59 2.58 0.22 o -12 2 1 2.81 3.52 0.25 o -11 2 1 4.41 4.86 0.24 o -10 2 1 127.46 124.98 1.18 o -9 2 1 140.29 142.85 1.78 o -8 2 1 10.63 19.05 0.72 o -7 2 1 68.73 82.89 1.32 o -6 2 1 590.27 605.96 6.29 o -5 2 1 1145.88 1180.28 9.61 o -4 2 1 426.81 467.10 3.90 o -3 2 1 1823.37 1706.04 14.71 o -1 2 1 63.70 62.56 0.92 o 0 2 1 611.89 602.30 5.79 o 1 2 1 164.31 124.28 1.53 o 2 2 1 2703.13 2613.05 20.46 o 3 2 1 2651.22 2514.06 21.07 o 4 2 1 3611.39 3621.72 27.99 o 5 2 1 2819.97 2882.62 22.30 o 6 2 1 1031.60 1116.46 10.37 o 7 2 1 75.70 65.90 1.47 o 8 2 1 126.64 133.94 3.39 o 9 2 1 155.79 150.93 1.61 o 10 2 1 25.10 29.10 0.57 o 11 2 1 32.93 31.43 0.54 o 12 2 1 760.32 776.53 4.87 o 13 2 1 24.20 28.91 0.60 o 14 2 1 554.23 527.76 3.66 o 15 2 1 63.32 59.27 0.88 o 16 2 1 4.20 5.02 0.25 o -16 3 1 14.81 15.42 0.38 o -15 3 1 327.35 321.22 2.40 o -14 3 1 3.39 5.73 0.34 o -13 3 1 467.75 459.46 3.63 o -12 3 1 398.17 371.25 2.86 o -11 3 1 83.62 82.71 1.19 o -10 3 1 159.76 154.32 1.45 o -9 3 1 129.30 129.30 1.35 o -8 3 1 330.51 329.96 5.11 o -7 3 1 289.06 282.11 4.53 o -6 3 1 0.97 0.64 0.43 o -5 3 1 590.03 694.46 10.10 o -4 3 1 601.49 595.92 8.74 o -3 3 1 6.49 4.50 0.36 o -2 3 1 784.53 731.66 7.47 o -1 3 1 218.53 225.26 2.33 o 0 3 1 71.02 53.22 0.79 o 1 3 1 601.22 584.07 5.67 o 2 3 1 1729.10 1624.86 13.75 o 3 3 1 10.72 9.07 0.33 o 4 3 1 0.47 1.94 0.28 o 5 3 1 767.91 842.07 9.89 o 6 3 1 54.00 70.80 1.44 o 7 3 1 85.80 76.43 2.07 o 8 3 1 33.57 26.12 0.65 o 9 3 1 405.86 379.96 2.75 o 10 3 1 112.88 109.04 1.02 o 11 3 1 65.51 70.51 0.88 o 12 3 1 536.37 495.35 4.21 o 13 3 1 153.62 142.28 1.51 o 14 3 1 52.23 50.91 0.73 o 15 3 1 21.31 22.89 0.69 o 16 3 1 213.60 244.36 4.27 o -15 4 1 91.88 91.78 1.45 o -14 4 1 211.36 231.38 1.97 o -13 4 1 22.72 24.45 0.57 o -12 4 1 60.18 46.77 0.84 o -11 4 1 41.00 35.09 0.63 o -10 4 1 61.59 54.67 0.73 o -9 4 1 26.71 21.21 0.65 o -8 4 1 80.23 65.95 1.02 o -7 4 1 24.71 21.63 0.79 o -6 4 1 1644.23 1702.30 19.00 o -5 4 1 2618.27 2550.30 27.61 o -4 4 1 900.97 900.46 12.89 o -3 4 1 209.59 242.88 4.30 o -2 4 1 11.56 17.85 0.91 o -1 4 1 969.47 935.04 10.83 o 0 4 1 0.68 0.85 0.21 o 1 4 1 18.53 14.26 0.62 o 2 4 1 4.25 4.90 0.49 o 3 4 1 244.84 267.03 4.67 o 4 4 1 0.04 0.17 0.36 o 5 4 1 248.49 262.03 6.62 o 6 4 1 849.17 820.89 14.82 o 7 4 1 1.90 2.86 0.28 o 8 4 1 214.22 210.18 1.63 o 9 4 1 0.41 0.66 0.19 o 10 4 1 1.96 1.28 0.24 o 11 4 1 0.71 2.24 0.24 o 12 4 1 180.14 146.03 1.70 o 13 4 1 23.00 24.14 0.74 o 14 4 1 194.80 183.62 1.81 o 15 4 1 24.08 28.99 0.62 o -15 5 1 24.61 24.69 0.96 o -14 5 1 69.41 68.52 1.51 o -13 5 1 9.17 10.87 0.58 o -12 5 1 9.20 5.99 0.41 o -11 5 1 122.09 109.24 1.01 o -10 5 1 102.47 92.18 0.93 o -9 5 1 104.54 101.09 0.98 o -8 5 1 44.57 43.92 0.75 o -7 5 1 96.39 86.71 0.85 o -6 5 1 77.19 74.39 1.09 o -5 5 1 344.33 344.40 4.32 o -4 5 1 16.07 23.90 1.64 o -3 5 1 37.81 39.19 1.07 o -2 5 1 66.78 59.49 1.50 o -1 5 1 149.36 146.46 2.46 o 0 5 1 755.63 779.94 11.85 o 1 5 1 9.73 8.55 0.62 o 2 5 1 332.02 323.46 4.59 o 3 5 1 835.20 815.54 15.25 o 4 5 1 0.67 0.96 0.32 o 5 5 1 2.15 3.57 0.33 o 6 5 1 236.09 219.13 1.82 o 7 5 1 106.64 116.03 1.21 o 8 5 1 29.92 29.09 0.58 o 9 5 1 52.22 49.63 1.06 o 10 5 1 48.73 44.28 0.76 o 11 5 1 6.90 7.84 0.40 o 12 5 1 0.16 0.28 0.32 o 13 5 1 18.83 19.97 0.51 o 14 5 1 113.90 126.99 1.72 o -13 6 1 0.99 2.66 0.34 o -12 6 1 5.28 9.52 0.40 o -11 6 1 41.08 41.10 0.80 o -10 6 1 4.76 5.39 0.36 o -9 6 1 0.54 0.86 0.22 o -8 6 1 68.36 68.03 1.00 o -7 6 1 2435.95 2252.63 14.37 o -6 6 1 67.59 69.68 1.01 o -5 6 1 28.16 30.47 0.79 o -4 6 1 69.92 62.75 1.05 o -3 6 1 81.95 73.76 1.10 o -2 6 1 18.36 20.36 0.72 o -1 6 1 72.04 69.31 1.48 o 0 6 1 117.10 113.62 1.80 o 1 6 1 86.78 95.98 1.55 o 2 6 1 165.52 169.23 1.86 o 3 6 1 67.33 54.19 0.95 o 4 6 1 89.00 81.93 1.23 o 5 6 1 71.87 73.46 0.99 o 6 6 1 0.98 1.89 0.16 o 7 6 1 216.78 227.40 1.84 o 8 6 1 72.04 68.53 1.00 o 9 6 1 83.43 69.75 1.11 o 10 6 1 36.05 28.36 0.67 o 11 6 1 0.24 0.66 0.24 o 12 6 1 39.50 44.47 0.89 o 13 6 1 74.18 72.57 1.28 o -11 7 1 127.64 127.14 1.47 o -10 7 1 8.98 9.11 0.43 o -9 7 1 302.26 286.75 2.68 o -8 7 1 126.76 108.21 1.40 o -7 7 1 504.70 507.16 4.32 o -6 7 1 1.49 0.91 0.23 o -5 7 1 95.45 91.74 1.22 o -4 7 1 3.44 2.35 0.24 o -3 7 1 123.25 118.79 1.40 o -2 7 1 260.24 233.42 2.53 o -1 7 1 1.17 1.96 0.30 o 0 7 1 141.36 132.08 3.85 o 1 7 1 0.32 0.69 0.28 o 2 7 1 62.90 68.13 1.30 o 3 7 1 4.66 8.91 0.56 o 4 7 1 140.05 129.59 1.51 o 5 7 1 71.85 67.76 0.98 o 6 7 1 0.28 0.43 0.25 o 7 7 1 0.18 0.43 0.23 o 8 7 1 5.60 6.18 0.43 o 9 7 1 10.01 6.85 0.39 o 10 7 1 108.31 120.01 1.39 o 11 7 1 17.21 15.91 0.48 o -10 8 1 104.04 83.55 1.36 o -9 8 1 42.45 38.04 0.71 o -8 8 1 44.95 45.94 0.78 o -7 8 1 74.32 76.53 1.10 o -6 8 1 243.37 225.34 2.25 o -5 8 1 162.35 151.98 1.71 o -4 8 1 8.12 10.65 0.47 o -3 8 1 8.16 7.70 0.43 o -2 8 1 53.68 58.55 0.98 o -1 8 1 55.20 64.84 1.12 o 0 8 1 0.90 0.36 0.25 o 1 8 1 63.23 54.77 0.95 o 2 8 1 4.53 6.57 0.36 o 3 8 1 5.92 6.99 0.40 o 4 8 1 291.28 315.96 3.62 o 5 8 1 332.02 356.00 3.16 o 6 8 1 738.14 778.99 6.06 o 7 8 1 1.91 0.60 0.23 o 8 8 1 41.49 41.56 0.73 o 9 8 1 10.84 13.23 0.46 o -7 9 1 34.75 39.06 0.91 o -6 9 1 75.17 72.84 1.03 o -5 9 1 71.94 73.78 1.39 o -4 9 1 0.83 3.29 0.35 o -3 9 1 13.16 13.43 0.58 o -2 9 1 32.02 24.63 0.61 o -1 9 1 35.41 32.18 0.68 o 0 9 1 3.60 5.61 0.36 o 1 9 1 22.85 21.48 0.56 o 2 9 1 0.49 1.31 0.23 o 3 9 1 24.59 21.30 0.53 o 4 9 1 13.35 11.24 0.42 o 5 9 1 22.16 22.95 0.78 o 6 9 1 1.95 3.01 0.46 o -16 0 2 806.45 787.21 9.81 o -15 0 2 8.75 10.76 0.57 o -14 0 2 170.95 171.62 2.06 o -13 0 2 4.21 5.10 0.42 o -12 0 2 488.57 489.56 4.39 o -11 0 2 71.40 67.49 1.35 o -10 0 2 450.58 523.29 7.92 o -9 0 2 67.39 63.47 1.52 o -8 0 2 20.42 13.67 0.80 o -7 0 2 40.66 47.40 2.77 o -6 0 2 126.63 99.29 2.22 o -5 0 2 142.22 132.32 1.81 o -4 0 2 4138.24 3887.74 48.73 o -3 0 2 345.49 281.70 3.15 o -2 0 2 1036.26 1065.37 13.83 o -1 0 2 2431.17 2472.54 38.20 o 2 0 2 549.63 629.97 8.06 o 3 0 2 135.77 178.42 2.54 o 4 0 2 119.63 149.78 2.06 o 5 0 2 91.23 98.09 1.51 o 6 0 2 274.32 280.37 4.59 o 7 0 2 13.23 8.20 0.75 o 8 0 2 24.07 22.65 1.12 o 9 0 2 82.16 73.18 1.62 o 10 0 2 3047.62 2973.35 32.22 o 11 0 2 24.08 35.42 0.84 o 12 0 2 2040.34 1949.13 14.03 o 13 0 2 103.30 104.08 1.61 o 14 0 2 109.30 115.40 1.63 o 15 0 2 209.65 212.26 3.47 o 16 0 2 12.77 11.29 0.46 o -17 1 2 25.54 20.92 0.75 o -16 1 2 34.39 32.42 0.64 o -15 1 2 5.52 7.70 0.34 o -14 1 2 8.85 6.77 0.29 o -13 1 2 50.11 55.07 0.81 o -12 1 2 7.07 6.88 0.29 o -11 1 2 0.29 0.14 0.20 o -10 1 2 70.75 77.56 0.95 o -9 1 2 1543.74 1575.39 16.21 o -8 1 2 692.00 705.78 6.74 o -7 1 2 2233.79 2319.26 20.37 o -6 1 2 215.57 189.71 2.11 o -5 1 2 1293.41 1253.27 8.87 o -4 1 2 39.54 40.99 0.53 o -3 1 2 4872.97 4506.48 30.18 o -2 1 2 3489.75 3293.90 32.59 o -1 1 2 6018.92 5618.78 53.16 o 0 1 2 0.97 3.35 0.27 o 1 1 2 2822.92 2528.93 30.32 o 2 1 2 313.62 310.09 3.61 o 3 1 2 3997.77 3785.15 45.86 o 4 1 2 215.34 223.59 1.96 o 5 1 2 79.49 65.70 0.85 o 6 1 2 124.87 142.48 1.99 o 7 1 2 245.93 240.39 3.39 o 8 1 2 0.58 2.55 0.29 o 9 1 2 28.88 32.26 0.64 o 10 1 2 226.89 221.43 1.78 o 11 1 2 79.75 73.77 0.87 o 12 1 2 1.58 1.25 0.20 o 13 1 2 76.00 80.57 1.07 o 14 1 2 26.09 27.82 0.65 o 15 1 2 13.70 13.74 0.48 o 16 1 2 19.74 21.30 0.48 o -17 2 2 2.01 2.03 0.30 o -16 2 2 1.15 0.97 0.18 o -15 2 2 28.09 27.01 0.50 o -14 2 2 165.58 148.88 1.49 o -13 2 2 109.15 110.87 1.29 o -12 2 2 8.06 10.24 0.32 o -11 2 2 13.06 12.55 0.37 o -10 2 2 80.04 89.06 0.94 o -9 2 2 145.85 120.71 1.41 o -8 2 2 143.87 142.95 1.82 o -7 2 2 73.84 88.05 1.51 o -6 2 2 125.54 140.16 1.97 o -5 2 2 996.24 937.46 8.37 o -4 2 2 355.81 395.39 3.98 o -3 2 2 103.39 108.71 1.15 o -1 2 2 0.08 2.26 0.26 o 0 2 2 727.39 705.80 6.08 o 1 2 2 113.10 127.97 1.31 o 2 2 2 450.28 438.08 3.60 o 3 2 2 466.05 490.14 5.08 o 4 2 2 552.54 544.41 4.36 o 5 2 2 203.99 210.93 2.66 o 6 2 2 4.63 7.05 0.53 o 7 2 2 37.41 35.00 1.15 o 8 2 2 170.35 169.47 3.31 o 9 2 2 543.55 527.10 3.61 o 10 2 2 151.24 152.88 1.36 o 11 2 2 42.94 41.86 0.63 o 12 2 2 358.06 332.51 3.36 o 13 2 2 66.06 61.36 0.89 o 14 2 2 412.25 432.08 4.18 o 15 2 2 204.51 216.00 1.90 o 16 2 2 4.37 5.76 0.43 o -16 3 2 0.44 0.58 0.13 o -15 3 2 6.41 8.78 0.36 o -14 3 2 255.27 241.32 2.15 o -13 3 2 2.15 3.80 0.31 o -12 3 2 15.06 16.59 0.58 o -11 3 2 48.64 46.41 0.62 o -10 3 2 4.38 5.60 0.35 o -9 3 2 186.91 186.77 1.75 o -8 3 2 13.39 11.65 0.48 o -7 3 2 1.49 2.25 0.31 o -6 3 2 212.56 239.64 3.43 o -5 3 2 1067.59 1088.77 12.55 o -4 3 2 251.93 256.60 3.48 o -3 3 2 41.53 44.39 0.92 o -2 3 2 157.99 196.30 1.86 o -1 3 2 673.28 632.04 4.99 o 0 3 2 418.47 439.40 3.35 o 1 3 2 189.53 189.38 1.69 o 2 3 2 3.30 -0.18 0.47 o 3 3 2 90.96 106.34 1.37 o 4 3 2 4.54 5.57 0.44 o 5 3 2 2576.78 2794.42 30.90 o 6 3 2 7.25 9.39 1.71 o 7 3 2 503.59 508.72 7.38 o 8 3 2 597.92 570.23 5.68 o 9 3 2 63.46 56.59 0.71 o 10 3 2 2.63 2.31 0.27 o 11 3 2 43.74 42.88 0.66 o 12 3 2 0.25 2.48 0.22 o 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