#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/56/2225655.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225655_Fobs loop_ _publ_author_name 'Zhao, Dian-Ying' _publ_section_title ; Bis[\m-2,2'-dimethyl-1,1'-(oxydiethylene)bis(1H-benzimidazole)-\k^2^N^3^:N^3'^]bis[bis(4-methoxybenzoato-\k^2^O,O')cadmium(II)] ; _journal_coeditor_code LX2137 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m430 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 88.143 _cell_angle_beta 86.539 _cell_angle_gamma 74.863 _cell_length_a 9.0379 _cell_length_b 13.8130 _cell_length_c 13.9361 _exptl_crystal_F_000 768.00 _reflns_d_resolution_high 0.7282 _[local]_cod_data_source_file lx2137Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 244.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 599.21 593.58 35.03 o 3 0 0 1483.06 1479.48 54.86 o 4 0 0 69.95 75.07 30.32 o 5 0 0 1.60 -0.43 18.48 o 6 0 0 81.10 76.26 20.36 o 7 0 0 2792.22 2786.73 68.35 o 8 0 0 233.05 236.36 32.38 o 9 0 0 263.62 302.87 42.36 o 10 0 0 37.23 30.21 36.37 o 11 0 0 23.79 62.29 42.86 o -11 1 0 47.99 47.64 37.89 o -10 1 0 16.63 40.68 37.64 o -9 1 0 214.39 139.35 39.95 o -8 1 0 5.68 9.18 26.58 o -7 1 0 709.99 729.91 42.86 o -6 1 0 971.51 1013.15 37.50 o -5 1 0 2077.69 2221.17 54.52 o -4 1 0 8399.01 8529.80 92.21 o -3 1 0 7698.01 7751.97 77.96 o -2 1 0 15.15 18.50 19.09 o -1 1 0 703.18 663.87 26.82 o 2 1 0 2767.10 2752.36 57.44 o 3 1 0 5898.38 5787.07 97.34 o 4 1 0 5955.66 5963.58 114.96 o 5 1 0 2379.00 2452.22 83.89 o 6 1 0 575.90 604.13 39.46 o 7 1 0 22.97 7.57 21.68 o 8 1 0 332.22 296.98 27.76 o 9 1 0 34.97 55.40 34.61 o 10 1 0 5.51 -3.53 38.79 o 11 1 0 151.89 166.03 45.73 o 12 1 0 17.31 11.32 60.63 o -10 2 0 47.45 83.28 37.33 o -9 2 0 146.66 184.37 39.87 o -8 2 0 62.10 53.25 29.29 o -7 2 0 224.74 206.35 33.10 o -6 2 0 421.40 398.22 28.74 o -5 2 0 49.93 43.81 18.68 o -4 2 0 1635.21 1759.23 48.33 o -3 2 0 355.55 312.49 26.52 o -2 2 0 272.54 274.48 23.79 o -1 2 0 1665.34 1617.84 31.12 o 1 2 0 2520.25 2639.52 40.50 o 2 2 0 13107.82 12916.74 107.69 o 3 2 0 138.19 153.70 16.32 o 4 2 0 156.08 131.38 34.04 o 5 2 0 1597.41 1776.42 73.25 o 6 2 0 947.62 938.20 44.48 o 7 2 0 213.14 216.22 34.16 o 8 2 0 701.56 667.56 33.91 o 9 2 0 270.46 273.24 41.86 o 10 2 0 76.76 110.63 40.93 o 11 2 0 156.91 138.43 42.85 o 12 2 0 10.33 -4.41 59.04 o -10 3 0 23.92 31.67 36.32 o -9 3 0 0.42 8.08 34.23 o -8 3 0 462.87 475.73 69.37 o -7 3 0 279.76 283.87 36.17 o -6 3 0 322.48 340.33 28.81 o -5 3 0 306.21 313.54 26.83 o -4 3 0 480.72 417.56 31.65 o -3 3 0 7004.49 7119.94 133.77 o -2 3 0 3321.83 3279.11 58.61 o -1 3 0 1121.72 1140.81 24.64 o 0 3 0 4901.81 4987.18 36.12 o 1 3 0 34068.53 31358.98 481.67 o 2 3 0 5751.39 5539.93 48.76 o 3 3 0 118.67 85.00 17.46 o 4 3 0 10891.43 11321.45 85.67 o 5 3 0 3756.49 3855.10 56.45 o 6 3 0 17.16 9.46 15.00 o 7 3 0 61.43 48.00 17.69 o 8 3 0 55.08 51.86 15.12 o 9 3 0 14.62 12.88 18.10 o 10 3 0 31.73 20.97 58.36 o 11 3 0 64.45 77.28 61.39 o 12 3 0 7.75 -25.15 67.70 o -10 4 0 154.36 188.06 70.28 o -9 4 0 520.02 462.65 46.84 o -8 4 0 375.90 403.70 68.08 o -7 4 0 4.90 3.21 29.93 o -6 4 0 30.77 31.44 30.95 o -5 4 0 0.22 -0.59 20.34 o -4 4 0 704.68 697.04 39.98 o -3 4 0 5870.01 5805.23 122.33 o -2 4 0 3158.70 3141.05 48.36 o -1 4 0 218.52 181.04 12.72 o 0 4 0 6859.60 7093.14 60.33 o 1 4 0 3779.54 3697.79 41.47 o 2 4 0 1806.43 1840.46 36.93 o 3 4 0 1459.43 1483.91 31.59 o 4 4 0 163.23 187.85 19.15 o 5 4 0 2408.28 2367.77 46.65 o 6 4 0 622.62 606.47 25.40 o 7 4 0 53.55 42.13 18.44 o 8 4 0 61.80 69.06 19.95 o 9 4 0 478.84 444.95 29.46 o 10 4 0 51.38 54.02 61.85 o 11 4 0 0.12 28.34 67.70 o -10 5 0 12.58 41.56 59.88 o -9 5 0 35.62 23.25 56.15 o -8 5 0 299.45 353.40 69.98 o -7 5 0 671.63 611.21 74.77 o -6 5 0 776.63 709.89 55.92 o -5 5 0 462.67 526.00 41.18 o -4 5 0 447.42 416.66 23.67 o -3 5 0 204.43 232.70 19.44 o -2 5 0 9.87 10.06 13.34 o -1 5 0 11.23 6.02 10.69 o 0 5 0 247.74 281.46 17.65 o 1 5 0 2319.07 2112.42 43.50 o 2 5 0 2117.33 2071.33 77.31 o 3 5 0 954.02 919.71 31.04 o 4 5 0 259.41 194.37 15.90 o 5 5 0 647.70 591.55 29.29 o 6 5 0 49.94 47.12 17.90 o 7 5 0 1.46 -4.81 19.06 o 8 5 0 456.50 416.53 28.21 o 9 5 0 344.95 333.09 25.86 o 10 5 0 131.74 124.08 69.07 o 11 5 0 75.51 111.92 72.11 o -9 6 0 81.27 111.24 55.85 o -8 6 0 75.56 56.00 56.38 o -7 6 0 99.58 82.29 49.31 o -6 6 0 239.31 212.78 26.27 o -5 6 0 10.27 11.98 15.88 o -4 6 0 1612.06 1652.16 39.45 o -3 6 0 3287.64 3341.35 49.20 o -2 6 0 4147.98 4055.58 82.02 o -1 6 0 2071.22 2121.24 32.13 o 0 6 0 4912.90 4758.15 58.02 o 1 6 0 1661.25 1685.57 34.63 o 2 6 0 57.26 60.63 19.31 o 3 6 0 859.34 875.97 28.66 o 4 6 0 130.18 97.61 18.85 o 5 6 0 4103.82 4166.65 73.17 o 6 6 0 597.55 642.36 28.47 o 7 6 0 2663.61 2635.79 58.56 o 8 6 0 1549.30 1419.33 44.17 o 9 6 0 317.50 261.70 43.12 o 10 6 0 0.26 -1.29 59.04 o 11 6 0 0.60 -9.12 71.04 o -9 7 0 128.31 106.15 63.45 o -8 7 0 120.57 116.03 62.15 o -7 7 0 574.14 617.52 73.78 o -6 7 0 668.63 646.77 35.43 o -5 7 0 1297.47 1319.62 48.29 o -4 7 0 1202.66 1199.30 35.51 o -3 7 0 30.07 43.86 15.49 o -2 7 0 370.82 328.62 22.11 o -1 7 0 33.23 55.51 13.27 o 0 7 0 266.59 250.17 18.42 o 1 7 0 1457.88 1372.75 33.92 o 2 7 0 7288.16 7508.77 76.29 o 3 7 0 3843.17 3744.45 56.73 o 4 7 0 1204.34 1290.08 35.35 o 5 7 0 273.21 262.30 19.45 o 6 7 0 246.30 227.08 23.95 o 7 7 0 16.34 12.58 22.32 o 8 7 0 271.48 252.93 26.81 o 9 7 0 276.04 267.33 23.71 o 10 7 0 226.29 188.74 75.76 o 11 7 0 100.18 115.80 65.95 o -8 8 0 15.42 4.26 64.51 o -7 8 0 45.08 41.11 57.06 o -6 8 0 104.96 83.73 57.44 o -5 8 0 58.90 46.24 16.94 o -4 8 0 1272.37 1257.15 39.99 o -3 8 0 655.79 698.11 31.95 o -2 8 0 1192.14 1191.25 31.26 o -1 8 0 569.77 542.15 21.94 o 0 8 0 1193.70 1061.88 30.13 o 1 8 0 543.76 613.73 27.60 o 2 8 0 11.61 21.04 24.84 o 3 8 0 1.65 3.21 24.93 o 4 8 0 91.16 82.99 22.15 o 5 8 0 1403.93 1435.23 55.99 o 6 8 0 1016.88 968.01 44.00 o 7 8 0 781.87 829.20 41.75 o 8 8 0 113.42 123.23 25.51 o 9 8 0 24.63 21.43 53.42 o 10 8 0 20.76 27.51 57.67 o 11 8 0 3.74 38.98 80.16 o -8 9 0 85.81 90.80 64.89 o -7 9 0 167.01 178.64 60.48 o -6 9 0 271.63 275.29 59.04 o -5 9 0 45.26 12.01 53.11 o -4 9 0 47.98 39.11 16.58 o -3 9 0 103.65 92.02 17.92 o -2 9 0 212.05 216.97 21.53 o -1 9 0 892.58 934.05 27.96 o 0 9 0 850.06 835.70 27.46 o 1 9 0 1702.03 1738.00 38.00 o 2 9 0 1711.92 1700.34 47.99 o 3 9 0 976.69 951.54 44.74 o 4 9 0 1204.36 1253.65 50.45 o 5 9 0 864.76 868.13 44.77 o 6 9 0 16.23 12.36 19.62 o 7 9 0 617.98 568.80 39.07 o 8 9 0 363.07 397.11 34.17 o 9 9 0 175.12 178.49 62.46 o 10 9 0 186.81 231.07 74.62 o -7 10 0 6.94 12.39 60.41 o -6 10 0 239.88 171.27 57.44 o -5 10 0 187.25 180.08 59.88 o -4 10 0 396.32 368.34 33.13 o -3 10 0 332.14 335.09 24.27 o -2 10 0 1503.92 1472.56 41.00 o -1 10 0 607.17 592.75 25.87 o 0 10 0 102.33 99.48 18.42 o 1 10 0 256.22 277.46 23.04 o 2 10 0 196.20 228.44 28.30 o 3 10 0 278.45 266.70 28.90 o 4 10 0 682.28 788.05 37.48 o 5 10 0 604.20 533.14 40.01 o 6 10 0 928.47 897.63 46.20 o 7 10 0 310.41 309.41 73.55 o 8 10 0 0.34 -5.89 26.42 o 9 10 0 3.98 0.38 59.19 o 10 10 0 25.17 50.00 74.16 o -7 11 0 186.56 223.77 67.40 o -6 11 0 155.21 153.26 61.93 o -5 11 0 17.63 21.73 48.71 o -4 11 0 29.24 -8.97 56.00 o -3 11 0 134.56 105.73 18.14 o -2 11 0 340.30 378.38 25.42 o -1 11 0 300.93 306.93 22.45 o 0 11 0 1323.41 1322.36 39.68 o 1 11 0 1035.43 1068.78 49.03 o 2 11 0 417.27 399.28 31.79 o 3 11 0 112.88 126.36 26.72 o 4 11 0 1.27 -8.00 25.54 o 5 11 0 22.19 32.25 24.60 o 6 11 0 124.90 135.80 25.73 o 7 11 0 211.03 226.79 26.85 o 8 11 0 12.23 -3.19 67.25 o 9 11 0 254.39 210.40 78.95 o 10 11 0 83.20 82.67 77.12 o -6 12 0 171.60 185.93 69.60 o -5 12 0 163.42 230.38 70.13 o -4 12 0 326.75 355.60 70.44 o -3 12 0 365.74 384.71 69.37 o -2 12 0 465.36 421.49 59.15 o -1 12 0 4.12 0.78 16.66 o 0 12 0 64.06 81.65 20.66 o 1 12 0 55.00 71.60 28.98 o 2 12 0 124.54 149.98 34.95 o 3 12 0 949.16 973.49 55.23 o 4 12 0 943.25 867.58 54.09 o 5 12 0 659.19 684.34 39.07 o 6 12 0 152.42 148.89 26.28 o 7 12 0 56.68 65.26 34.03 o 8 12 0 8.41 7.46 30.48 o 9 12 0 9.02 12.84 73.63 o -5 13 0 41.01 -2.81 65.57 o -4 13 0 20.93 30.55 59.50 o -3 13 0 88.81 107.59 50.61 o -2 13 0 428.46 372.32 67.70 o -1 13 0 929.28 942.16 102.16 o 0 13 0 597.99 603.84 42.05 o 1 13 0 280.27 350.03 38.07 o 2 13 0 391.66 466.27 44.64 o 3 13 0 382.67 360.45 43.13 o 4 13 0 38.36 56.31 36.76 o 5 13 0 156.22 134.48 38.05 o 6 13 0 162.42 178.68 40.16 o 7 13 0 35.95 34.87 34.46 o 8 13 0 92.05 121.73 68.69 o 9 13 0 137.17 149.69 65.04 o -4 14 0 45.60 63.98 60.48 o -3 14 0 48.11 44.75 62.38 o -2 14 0 254.35 285.09 63.45 o -1 14 0 4.70 17.48 76.14 o 0 14 0 12.81 -0.67 28.41 o 1 14 0 325.57 283.02 37.97 o 2 14 0 217.02 222.63 39.50 o 3 14 0 368.28 410.45 46.72 o 4 14 0 247.96 304.03 44.74 o 5 14 0 292.41 356.58 48.06 o 6 14 0 72.27 97.78 39.69 o 7 14 0 27.13 22.51 37.67 o 8 14 0 9.41 4.79 68.99 o -3 15 0 33.66 3.57 61.24 o -2 15 0 30.90 88.98 56.84 o 0 15 0 139.47 144.44 74.84 o 1 15 0 354.91 361.95 40.34 o 2 15 0 170.03 190.49 39.43 o 3 15 0 11.57 22.00 37.61 o 4 15 0 21.63 16.03 37.29 o 5 15 0 10.14 23.80 37.10 o 6 15 0 49.44 67.85 41.00 o 7 15 0 71.02 77.94 39.29 o 8 15 0 69.60 89.74 56.68 o -1 16 0 7.53 73.70 61.55 o 0 16 0 35.10 82.90 69.22 o 1 16 0 181.78 158.43 84.57 o 2 16 0 126.02 149.54 38.90 o 3 16 0 286.00 253.32 44.07 o 4 16 0 75.24 82.29 39.65 o 5 16 0 165.82 161.58 45.03 o 6 16 0 110.54 107.82 43.71 o 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336.99 31.89 o -4 -12 1 44.25 39.04 24.59 o -3 -12 1 31.61 42.35 34.30 o -2 -12 1 419.24 416.08 32.83 o -1 -12 1 606.88 607.16 34.33 o 0 -12 1 738.11 726.19 34.42 o 1 -12 1 168.02 182.49 25.38 o 2 -12 1 682.28 643.72 37.81 o 3 -12 1 81.08 55.39 47.87 o 4 -12 1 2.50 6.99 59.42 o 5 -12 1 45.61 -24.62 61.17 o 6 -12 1 12.45 49.31 67.32 o -10 -11 1 0.30 11.25 62.38 o -9 -11 1 6.24 -10.71 67.32 o -8 -11 1 96.77 115.76 28.07 o -7 -11 1 11.31 16.56 50.76 o -6 -11 1 94.75 116.15 28.50 o -5 -11 1 691.22 705.53 37.15 o -4 -11 1 543.80 551.42 35.30 o -3 -11 1 476.18 452.70 33.53 o -2 -11 1 0.56 0.62 21.11 o -1 -11 1 31.18 30.33 22.63 o 0 -11 1 39.18 36.84 20.51 o 1 -11 1 722.06 713.42 31.98 o 2 -11 1 1066.64 987.61 43.59 o 3 -11 1 55.97 51.29 20.09 o 4 -11 1 170.45 256.14 66.56 o 5 -11 1 135.34 168.23 53.95 o 6 -11 1 38.53 17.70 50.99 o -10 -10 1 75.07 71.73 61.01 o -9 -10 1 272.06 320.96 79.78 o -8 -10 1 98.51 91.96 24.15 o -7 -10 1 89.25 83.99 28.44 o -6 -10 1 41.07 24.42 23.93 o -5 -10 1 236.37 173.27 31.63 o -4 -10 1 190.19 190.75 33.01 o -3 -10 1 418.80 465.66 32.20 o -2 -10 1 1957.81 1871.18 43.61 o -1 -10 1 773.90 807.35 31.75 o 0 -10 1 1291.16 1278.25 35.25 o 1 -10 1 524.24 538.65 28.09 o 2 -10 1 546.21 531.00 33.83 o 3 -10 1 0.06 12.00 18.69 o 4 -10 1 0.03 1.27 18.05 o 5 -10 1 1.29 6.61 57.75 o 6 -10 1 74.64 38.45 59.57 o 7 -10 1 42.39 48.10 61.32 o -10 -9 1 1.74 6.53 69.83 o -9 -9 1 72.25 59.95 68.84 o -8 -9 1 150.11 171.07 23.72 o -7 -9 1 3.61 0.61 22.06 o -6 -9 1 1113.09 1111.94 36.45 o -5 -9 1 1817.83 1791.45 56.25 o -4 -9 1 1040.92 1008.73 46.58 o -3 -9 1 89.34 89.35 24.38 o -2 -9 1 24.17 15.21 22.42 o -1 -9 1 5.72 14.12 18.33 o 0 -9 1 128.49 157.84 19.59 o 1 -9 1 236.56 233.12 19.89 o 2 -9 1 1087.46 1085.12 42.22 o 3 -9 1 2551.60 2547.09 60.24 o 4 -9 1 149.98 142.48 22.97 o 5 -9 1 45.04 46.87 18.83 o 6 -9 1 38.67 68.69 58.36 o 7 -9 1 19.79 2.74 62.00 o 8 -9 1 1.30 -10.94 59.12 o -11 -8 1 107.68 96.96 67.09 o -10 -8 1 111.96 105.09 71.35 o -9 -8 1 290.70 311.00 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