#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:35:02 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181177 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/56/2225671.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225671_Fobs loop_ _publ_author_name 'Saraswathi, B. S.' 'Gowda, B. Thimme' 'Foro, Sabine' 'Fuess, Hartmut' _publ_section_title ; N-(2,4-Dimethylphenyl)succinimide ; _journal_coeditor_code VM2021 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o881 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.1461 _cell_length_b 11.1820 _cell_length_c 13.6760 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.8380 _cod_data_source_file vm2021Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ASE9 P212121' _shelx_refln_list_code 4 _shelx_f_calc_maximum 82.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 83.38 80.49 1.69 o 4 0 0 582.17 620.57 11.48 o 6 0 0 110.27 125.96 4.25 o 8 0 0 7.73 7.56 1.49 o 1 1 0 1407.40 1267.23 45.66 o 2 1 0 720.63 746.85 27.04 o 3 1 0 351.89 437.83 17.66 o 4 1 0 309.27 326.91 22.65 o 5 1 0 63.14 77.34 2.97 o 6 1 0 20.68 24.26 1.63 o 7 1 0 0.19 -1.97 2.37 o 8 1 0 13.29 9.42 1.49 o 0 2 0 9.80 10.42 0.64 o 1 2 0 57.81 48.25 1.30 o 2 2 0 10.10 10.67 1.15 o 3 2 0 1.71 0.45 0.78 o 4 2 0 24.88 39.11 5.20 o 5 2 0 30.47 38.22 2.36 o 6 2 0 8.38 10.00 2.53 o 7 2 0 6.24 8.18 1.59 o 8 2 0 54.88 53.33 1.86 o 1 3 0 2.96 4.74 0.49 o 2 3 0 1277.47 1148.38 181.89 o 3 3 0 16.60 31.40 3.19 o 4 3 0 0.15 1.15 1.05 o 5 3 0 7.48 4.44 1.64 o 6 3 0 19.41 23.13 1.68 o 7 3 0 0.11 1.35 2.26 o 8 3 0 28.13 24.31 3.00 o 0 4 0 1527.32 1371.99 58.05 o 1 4 0 555.32 554.38 18.06 o 2 4 0 452.74 395.34 51.73 o 3 4 0 204.31 175.75 36.64 o 4 4 0 65.32 73.14 2.63 o 5 4 0 38.90 47.81 1.97 o 6 4 0 4.11 3.21 1.64 o 7 4 0 33.00 32.22 1.68 o 8 4 0 31.20 26.74 2.19 o 1 5 0 34.22 36.90 0.83 o 2 5 0 144.87 153.27 20.19 o 3 5 0 58.73 62.10 7.87 o 4 5 0 626.45 658.25 67.30 o 5 5 0 56.32 59.64 6.35 o 6 5 0 5.86 1.29 3.85 o 7 5 0 0.07 1.07 1.13 o 0 6 0 12.94 14.26 1.05 o 1 6 0 70.60 79.34 2.71 o 2 6 0 20.59 21.63 1.80 o 3 6 0 2.41 0.80 1.55 o 4 6 0 112.27 132.07 10.02 o 5 6 0 0.84 -0.23 4.79 o 6 6 0 12.37 11.86 1.34 o 7 6 0 9.20 10.26 2.03 o 1 7 0 176.88 168.90 5.87 o 2 7 0 79.33 72.45 4.32 o 3 7 0 33.64 38.19 4.04 o 4 7 0 142.48 155.60 12.56 o 5 7 0 13.05 12.84 1.68 o 6 7 0 2.04 5.63 1.06 o 7 7 0 39.03 36.18 3.44 o 0 8 0 1143.25 1097.99 37.70 o 1 8 0 405.92 418.55 18.52 o 2 8 0 43.66 37.95 1.73 o 3 8 0 259.99 204.06 19.26 o 4 8 0 154.48 162.46 8.20 o 5 8 0 1.03 0.81 1.57 o 6 8 0 10.10 10.77 3.85 o 1 9 0 1.68 0.35 1.30 o 2 9 0 313.41 282.09 20.36 o 3 9 0 319.65 293.12 36.05 o 4 9 0 149.81 150.01 7.29 o 5 9 0 1.69 1.27 2.12 o 6 9 0 8.85 10.12 1.07 o 0 10 0 212.98 209.88 8.20 o 1 10 0 32.18 29.87 1.27 o 2 10 0 0.03 -1.41 1.64 o 3 10 0 6.47 7.40 1.39 o 4 10 0 0.57 3.65 4.56 o 5 10 0 0.91 0.64 1.93 o 1 11 0 17.29 18.54 1.48 o 2 11 0 22.06 19.42 1.29 o 3 11 0 1.08 1.32 0.98 o 4 11 0 11.31 13.23 1.09 o 0 12 0 0.50 0.61 1.82 o 1 12 0 0.00 0.45 0.82 o 2 12 0 0.31 -0.59 1.06 o 3 12 0 7.76 8.40 0.78 o 1 13 0 6.33 8.37 0.71 o 1 0 1 2053.60 2055.57 151.51 o 2 0 1 37.46 43.28 2.80 o 3 0 1 297.69 337.25 6.41 o 4 0 1 27.53 23.83 1.82 o 5 0 1 43.31 42.46 2.50 o 6 0 1 0.66 -3.58 3.58 o 7 0 1 0.22 1.76 3.17 o 8 0 1 0.74 0.27 2.77 o 0 1 1 1470.44 1277.05 93.06 o 1 1 1 3422.39 3236.63 110.90 o 2 1 1 4207.20 4533.79 150.60 o 3 1 1 571.30 718.57 24.48 o 4 1 1 449.20 499.68 25.96 o 5 1 1 180.76 215.84 4.63 o 6 1 1 6.92 7.10 1.36 o 7 1 1 2.00 0.45 1.57 o 8 1 1 27.98 24.54 1.47 o 0 2 1 2369.95 2063.19 118.91 o 1 2 1 2073.18 1961.41 51.92 o 2 2 1 432.18 422.40 29.43 o 3 2 1 77.23 84.65 5.48 o 4 2 1 10.31 12.69 1.04 o 5 2 1 19.31 17.79 1.34 o 6 2 1 135.38 131.34 10.33 o 7 2 1 9.76 8.26 2.77 o 8 2 1 6.51 6.61 1.07 o 0 3 1 594.07 528.61 27.81 o 1 3 1 870.28 806.69 24.28 o 2 3 1 140.88 118.97 7.90 o 3 3 1 3.41 9.50 4.24 o 4 3 1 75.35 83.62 2.00 o 5 3 1 50.35 52.66 4.22 o 6 3 1 3.49 5.70 1.29 o 7 3 1 123.55 116.76 5.00 o 8 3 1 15.12 13.85 1.22 o 0 4 1 1249.74 1155.19 79.89 o 1 4 1 57.46 53.75 1.46 o 2 4 1 204.58 165.42 16.29 o 3 4 1 329.30 301.80 44.07 o 4 4 1 37.76 42.51 1.64 o 5 4 1 148.94 155.28 9.86 o 6 4 1 5.48 2.80 1.78 o 7 4 1 30.24 29.02 3.00 o 8 4 1 14.03 11.44 1.05 o 0 5 1 310.67 315.34 11.88 o 1 5 1 215.32 190.83 6.06 o 2 5 1 43.67 43.07 3.29 o 3 5 1 262.09 214.97 31.15 o 4 5 1 16.94 23.76 3.41 o 5 5 1 77.83 84.44 6.04 o 6 5 1 20.87 24.50 1.68 o 7 5 1 65.93 67.48 2.14 o 0 6 1 0.90 1.22 1.48 o 1 6 1 66.14 79.69 2.91 o 2 6 1 120.82 115.07 8.53 o 3 6 1 52.31 44.18 3.67 o 4 6 1 374.17 395.95 44.92 o 5 6 1 42.15 48.26 2.21 o 6 6 1 2.99 3.89 1.75 o 7 6 1 30.51 26.95 1.82 o 0 7 1 312.48 323.17 16.50 o 1 7 1 438.87 453.68 18.02 o 2 7 1 23.43 23.54 1.02 o 3 7 1 12.43 11.63 1.52 o 4 7 1 26.36 24.83 3.75 o 5 7 1 44.38 43.90 4.22 o 6 7 1 25.67 29.34 1.66 o 7 7 1 5.55 2.97 1.27 o 0 8 1 194.44 184.86 14.51 o 1 8 1 38.94 40.92 2.32 o 2 8 1 108.32 93.10 5.58 o 3 8 1 100.62 93.98 8.01 o 4 8 1 57.81 59.24 4.46 o 5 8 1 42.83 42.46 2.67 o 6 8 1 52.12 49.50 3.71 o 0 9 1 123.89 123.29 10.60 o 1 9 1 49.30 50.00 2.08 o 2 9 1 254.47 236.05 16.16 o 3 9 1 11.29 11.43 0.99 o 4 9 1 68.72 60.05 4.46 o 5 9 1 7.06 9.73 1.62 o 6 9 1 42.77 43.39 4.46 o 0 10 1 58.73 62.60 4.69 o 1 10 1 167.88 166.28 3.47 o 2 10 1 2.08 1.40 1.34 o 3 10 1 4.40 5.93 1.41 o 4 10 1 16.99 20.42 1.42 o 5 10 1 7.51 6.87 1.07 o 0 11 1 0.30 3.68 1.59 o 1 11 1 0.68 1.60 1.24 o 2 11 1 26.37 26.72 1.10 o 3 11 1 12.30 11.65 0.96 o 4 11 1 31.23 30.37 1.96 o 0 12 1 0.15 0.00 1.91 o 1 12 1 3.42 1.96 0.96 o 2 12 1 10.31 10.48 0.85 o 3 12 1 9.69 9.32 0.76 o 0 13 1 33.00 38.32 1.40 o 1 13 1 0.59 -0.17 0.82 o 0 0 2 4054.17 3547.98 16.40 o 1 0 2 1591.00 1435.70 91.33 o 2 0 2 2528.61 2595.37 213.72 o 3 0 2 19.87 27.73 3.48 o 4 0 2 473.01 520.93 10.80 o 5 0 2 3.32 4.93 1.76 o 6 0 2 69.57 69.53 3.24 o 7 0 2 0.33 2.09 2.84 o 8 0 2 0.64 -2.43 2.43 o 0 1 2 1504.28 1276.18 25.79 o 1 1 2 6819.02 6115.08 186.77 o 2 1 2 2481.86 2517.93 90.96 o 3 1 2 387.04 451.25 17.42 o 4 1 2 7.65 7.29 1.45 o 5 1 2 108.72 125.27 2.78 o 6 1 2 14.34 14.69 1.62 o 7 1 2 18.82 18.32 1.59 o 8 1 2 11.51 11.90 1.19 o 0 2 2 4.76 10.05 3.24 o 1 2 2 4092.84 3566.34 87.87 o 2 2 2 4.28 5.77 1.25 o 3 2 2 318.07 323.84 15.90 o 4 2 2 185.76 216.92 16.17 o 5 2 2 74.26 75.22 4.42 o 6 2 2 29.04 29.09 1.81 o 7 2 2 26.45 25.54 3.41 o 8 2 2 33.27 28.90 2.84 o 0 3 2 1253.65 1103.23 63.79 o 1 3 2 638.90 610.55 16.37 o 2 3 2 557.82 584.28 26.84 o 3 3 2 78.29 75.44 2.26 o 4 3 2 52.45 50.54 5.84 o 5 3 2 4.10 7.26 1.20 o 6 3 2 2.55 0.55 2.74 o 7 3 2 1.20 2.41 2.33 o 8 3 2 23.94 21.86 1.38 o 0 4 2 14.66 12.87 0.86 o 1 4 2 428.03 412.60 10.90 o 2 4 2 1488.02 1422.67 58.94 o 3 4 2 431.28 448.51 25.71 o 4 4 2 149.36 159.14 17.82 o 5 4 2 21.93 21.24 1.54 o 6 4 2 22.00 22.87 1.68 o 7 4 2 55.76 55.09 7.26 o 8 4 2 14.34 14.76 3.04 o 0 5 2 80.95 84.80 4.56 o 1 5 2 605.19 610.97 15.92 o 2 5 2 461.54 445.45 19.43 o 3 5 2 258.67 226.29 89.30 o 4 5 2 93.31 79.04 8.74 o 5 5 2 21.00 21.63 1.82 o 6 5 2 75.38 84.76 4.89 o 7 5 2 0.32 0.63 1.45 o 0 6 2 55.47 62.35 2.57 o 1 6 2 145.84 131.88 2.44 o 2 6 2 51.58 52.83 1.51 o 3 6 2 172.72 142.55 40.67 o 4 6 2 168.90 183.50 16.57 o 5 6 2 17.57 21.60 2.80 o 6 6 2 1.96 -0.08 2.55 o 7 6 2 5.08 3.12 1.11 o 0 7 2 164.03 163.65 12.18 o 1 7 2 203.26 219.14 8.84 o 2 7 2 33.81 31.00 3.35 o 3 7 2 6.11 6.28 0.99 o 4 7 2 108.28 99.46 8.13 o 5 7 2 124.81 123.63 8.03 o 6 7 2 36.87 39.72 1.70 o 7 7 2 22.27 20.11 1.22 o 0 8 2 37.28 44.96 3.48 o 1 8 2 163.97 158.74 5.44 o 2 8 2 1.49 -0.51 1.32 o 3 8 2 202.15 176.25 17.52 o 4 8 2 79.18 83.32 5.77 o 5 8 2 39.11 39.74 1.83 o 6 8 2 7.67 7.73 1.18 o 0 9 2 0.24 -0.88 2.63 o 1 9 2 107.70 107.55 3.07 o 2 9 2 72.68 67.31 3.38 o 3 9 2 99.07 88.79 9.36 o 4 9 2 22.44 25.59 1.63 o 5 9 2 2.69 3.55 2.67 o 6 9 2 12.20 10.82 2.46 o 0 10 2 99.86 112.28 8.67 o 1 10 2 143.62 142.39 3.47 o 2 10 2 112.49 110.12 3.61 o 3 10 2 28.79 28.50 1.76 o 4 10 2 7.14 7.88 1.18 o 5 10 2 4.72 5.13 1.02 o 0 11 2 60.08 65.68 2.33 o 1 11 2 47.79 46.28 1.75 o 2 11 2 72.37 78.86 5.02 o 3 11 2 11.20 9.80 2.69 o 4 11 2 0.45 -1.85 1.85 o 0 12 2 0.22 -1.86 1.86 o 1 12 2 7.65 8.90 0.95 o 2 12 2 4.11 3.62 1.12 o 3 12 2 3.53 3.09 0.88 o 0 13 2 56.00 61.14 1.76 o 1 13 2 12.06 13.40 0.75 o 1 0 3 27.18 22.65 0.84 o 2 0 3 4824.65 4820.98 308.66 o 3 0 3 1228.68 1477.88 15.93 o 4 0 3 32.30 42.66 1.96 o 5 0 3 5.16 3.92 1.82 o 6 0 3 2.53 0.74 3.24 o 7 0 3 0.39 -3.44 3.44 o 8 0 3 0.72 1.15 1.35 o 0 1 3 410.44 337.68 3.60 o 1 1 3 1832.48 1686.34 39.24 o 2 1 3 790.54 766.48 29.59 o 3 1 3 301.21 282.32 10.19 o 4 1 3 13.42 13.48 2.36 o 5 1 3 17.28 24.35 3.51 o 6 1 3 41.20 43.77 2.05 o 7 1 3 25.77 25.90 1.72 o 8 1 3 8.27 8.56 1.32 o 0 2 3 539.44 476.92 25.11 o 1 2 3 1340.91 1283.53 44.30 o 2 2 3 1061.60 1119.18 32.19 o 3 2 3 205.60 258.70 16.61 o 4 2 3 406.44 429.52 19.81 o 5 2 3 33.75 33.59 1.89 o 6 2 3 59.53 63.26 2.60 o 7 2 3 84.29 88.72 7.53 o 8 2 3 8.79 7.37 1.05 o 0 3 3 3286.65 2946.24 182.53 o 1 3 3 1032.55 975.85 27.98 o 2 3 3 999.70 1064.11 37.46 o 3 3 3 202.39 225.46 22.01 o 4 3 3 55.75 47.86 4.08 o 5 3 3 16.90 16.81 1.38 o 6 3 3 213.09 217.56 12.22 o 7 3 3 8.64 9.08 3.21 o 8 3 3 17.30 17.12 1.16 o 0 4 3 58.03 51.85 1.24 o 1 4 3 104.77 114.91 4.16 o 2 4 3 525.83 517.98 17.99 o 3 4 3 326.02 375.62 25.01 o 4 4 3 129.89 170.35 17.38 o 5 4 3 48.42 42.89 2.97 o 6 4 3 53.93 56.81 2.10 o 7 4 3 1.17 0.61 1.82 o 0 5 3 815.90 809.15 62.44 o 1 5 3 400.08 410.07 15.04 o 2 5 3 418.89 412.30 14.37 o 3 5 3 56.89 71.66 8.47 o 4 5 3 6.61 9.70 1.22 o 5 5 3 124.88 139.99 6.55 o 6 5 3 129.32 126.51 14.85 o 7 5 3 29.55 29.45 2.40 o 0 6 3 387.27 419.99 25.04 o 1 6 3 25.23 19.97 0.95 o 2 6 3 38.93 36.96 2.07 o 3 6 3 92.69 107.98 7.49 o 4 6 3 55.96 52.09 5.50 o 5 6 3 68.07 74.59 4.46 o 6 6 3 43.22 41.48 1.91 o 7 6 3 10.53 9.43 1.21 o 0 7 3 5.64 5.33 1.10 o 1 7 3 112.06 101.90 3.07 o 2 7 3 8.63 8.78 0.89 o 3 7 3 18.99 19.86 1.38 o 4 7 3 8.20 8.23 1.62 o 5 7 3 16.29 15.84 1.82 o 6 7 3 2.60 3.75 1.51 o 7 7 3 20.06 17.43 1.15 o 0 8 3 0.91 -0.15 2.70 o 1 8 3 46.03 48.32 2.02 o 2 8 3 27.42 25.90 1.18 o 3 8 3 31.70 30.74 1.99 o 4 8 3 52.63 57.26 7.43 o 5 8 3 31.87 29.75 1.78 o 6 8 3 9.46 9.66 1.22 o 0 9 3 181.87 188.74 10.77 o 1 9 3 136.48 137.39 6.72 o 2 9 3 18.27 18.49 1.48 o 3 9 3 18.37 19.58 2.23 o 4 9 3 29.62 33.21 3.65 o 5 9 3 17.25 14.09 1.49 o 6 9 3 7.99 6.62 1.08 o 0 10 3 13.90 12.06 1.62 o 1 10 3 118.89 118.29 2.48 o 2 10 3 66.68 63.28 3.15 o 3 10 3 292.82 285.19 20.99 o 4 10 3 6.47 7.34 1.24 o 5 10 3 0.87 -0.17 1.60 o 0 11 3 0.02 0.51 2.11 o 1 11 3 38.94 42.19 1.34 o 2 11 3 50.59 49.69 1.67 o 3 11 3 36.99 37.78 1.66 o 4 11 3 14.65 17.42 1.24 o 0 12 3 30.16 27.37 1.47 o 1 12 3 6.06 5.60 0.89 o 2 12 3 37.92 43.89 2.08 o 3 12 3 16.42 14.29 1.16 o 0 13 3 4.83 4.56 0.91 o 1 13 3 2.08 1.81 0.74 o 0 0 4 37.85 31.05 1.28 o 1 0 4 2005.71 1972.39 61.60 o 2 0 4 264.83 293.04 9.28 o 3 0 4 6.34 3.44 1.22 o 4 0 4 118.27 125.22 3.85 o 5 0 4 17.56 22.07 2.23 o 6 0 4 37.75 41.45 2.57 o 7 0 4 0.52 1.01 3.31 o 8 0 4 19.93 16.47 1.69 o 0 1 4 798.34 720.30 16.64 o 1 1 4 852.11 763.98 18.99 o 2 1 4 820.75 860.51 23.00 o 3 1 4 542.84 601.99 42.97 o 4 1 4 342.00 360.87 6.94 o 5 1 4 131.28 160.26 4.46 o 6 1 4 101.22 101.13 2.58 o 7 1 4 28.96 26.71 1.62 o 8 1 4 0.79 0.38 1.55 o 0 2 4 173.48 160.79 3.08 o 1 2 4 192.98 201.56 5.30 o 2 2 4 784.31 753.14 15.37 o 3 2 4 128.94 144.75 12.39 o 4 2 4 270.77 305.98 5.99 o 5 2 4 104.13 118.30 2.77 o 6 2 4 5.89 5.37 1.58 o 7 2 4 24.03 25.16 1.62 o 8 2 4 5.34 4.59 2.26 o 0 3 4 67.20 48.03 4.56 o 1 3 4 176.12 187.92 7.42 o 2 3 4 152.00 179.54 6.43 o 3 3 4 187.54 205.21 21.37 o 4 3 4 33.76 32.86 2.19 o 5 3 4 19.59 18.98 2.06 o 6 3 4 78.53 85.03 7.73 o 7 3 4 73.75 68.43 4.12 o 8 3 4 3.73 1.05 1.55 o 0 4 4 767.49 782.33 49.48 o 1 4 4 1188.82 1223.03 35.07 o 2 4 4 1067.66 1082.71 31.32 o 3 4 4 39.99 41.53 2.60 o 4 4 4 59.32 71.18 5.97 o 5 4 4 181.55 186.05 8.57 o 6 4 4 38.45 39.78 1.92 o 7 4 4 89.70 80.82 2.33 o 0 5 4 0.44 5.23 1.15 o 1 5 4 501.96 475.77 21.08 o 2 5 4 128.70 118.87 2.51 o 3 5 4 247.14 274.94 16.88 o 4 5 4 10.04 14.20 1.38 o 5 5 4 88.48 93.87 13.26 o 6 5 4 6.80 6.43 1.34 o 7 5 4 29.00 26.43 3.27 o 0 6 4 36.91 41.76 1.48 o 1 6 4 14.67 18.46 1.41 o 2 6 4 17.61 21.56 1.27 o 3 6 4 57.40 62.97 7.19 o 4 6 4 73.26 69.30 8.84 o 5 6 4 65.38 68.73 6.14 o 6 6 4 29.18 31.94 1.71 o 7 6 4 18.69 18.59 1.55 o 0 7 4 9.02 3.43 1.96 o 1 7 4 18.90 21.36 1.27 o 2 7 4 42.16 43.73 1.92 o 3 7 4 40.33 44.87 2.60 o 4 7 4 87.97 88.48 11.31 o 5 7 4 16.53 17.58 1.39 o 6 7 4 0.12 0.73 1.41 o 0 8 4 47.00 45.08 1.86 o 1 8 4 113.94 106.71 2.61 o 2 8 4 57.26 62.38 2.42 o 3 8 4 114.13 115.52 4.96 o 4 8 4 38.89 35.56 1.81 o 5 8 4 35.28 35.95 1.71 o 6 8 4 2.82 0.47 1.72 o 0 9 4 8.19 7.93 1.29 o 1 9 4 26.22 23.09 1.69 o 2 9 4 203.23 199.72 10.07 o 3 9 4 108.84 97.10 2.60 o 4 9 4 6.68 7.09 2.03 o 5 9 4 4.25 2.62 1.45 o 0 10 4 83.87 84.59 3.98 o 1 10 4 19.30 19.53 1.30 o 2 10 4 36.06 33.82 2.84 o 3 10 4 15.87 12.08 1.52 o 4 10 4 2.25 -0.98 1.96 o 5 10 4 6.46 6.73 1.02 o 0 11 4 2.26 1.21 1.48 o 1 11 4 12.37 9.39 1.97 o 2 11 4 98.99 92.80 4.88 o 3 11 4 9.23 11.37 1.99 o 4 11 4 19.38 19.94 1.19 o 0 12 4 59.40 59.63 2.94 o 1 12 4 13.06 14.60 0.92 o 2 12 4 0.38 0.31 0.83 o 3 12 4 2.77 4.31 0.81 o 1 0 5 3.03 0.52 1.38 o 2 0 5 252.11 276.32 15.42 o 3 0 5 2.95 5.13 1.15 o 4 0 5 770.66 913.88 15.93 o 5 0 5 143.34 147.36 4.66 o 6 0 5 86.37 95.65 3.71 o 7 0 5 3.38 5.40 1.62 o 8 0 5 2.03 -0.20 2.23 o 0 1 5 1198.37 1091.86 19.00 o 1 1 5 147.77 146.96 2.04 o 2 1 5 575.03 563.56 11.95 o 3 1 5 408.05 447.84 6.92 o 4 1 5 183.72 230.94 5.06 o 5 1 5 94.17 98.52 6.55 o 6 1 5 52.73 55.76 2.10 o 7 1 5 3.83 2.65 1.20 o 8 1 5 16.05 12.74 1.11 o 0 2 5 87.70 92.04 2.36 o 1 2 5 430.17 401.23 13.03 o 2 2 5 708.69 711.15 28.87 o 3 2 5 356.31 400.16 13.33 o 4 2 5 0.20 1.33 1.05 o 5 2 5 34.80 34.66 1.72 o 6 2 5 10.48 9.13 1.41 o 7 2 5 72.95 74.96 2.15 o 8 2 5 12.88 9.71 1.02 o 0 3 5 59.08 70.02 3.31 o 1 3 5 605.98 603.31 18.40 o 2 3 5 876.33 910.28 28.78 o 3 3 5 68.23 75.06 2.80 o 4 3 5 14.73 17.89 1.33 o 5 3 5 51.56 53.23 3.58 o 6 3 5 205.55 195.54 7.46 o 7 3 5 0.11 1.45 2.05 o 0 4 5 9.78 11.94 1.76 o 1 4 5 484.37 470.54 21.66 o 2 4 5 99.60 101.38 2.14 o 3 4 5 346.05 381.31 39.46 o 4 4 5 7.80 9.49 1.34 o 5 4 5 114.56 108.74 4.52 o 6 4 5 84.40 88.98 6.55 o 7 4 5 9.41 7.34 1.21 o 0 5 5 1107.70 1035.09 38.48 o 1 5 5 759.95 705.78 24.88 o 2 5 5 59.06 55.20 1.19 o 3 5 5 175.96 182.77 22.48 o 4 5 5 90.60 106.94 7.22 o 5 5 5 138.63 142.63 7.56 o 6 5 5 84.01 77.58 2.39 o 7 5 5 1.16 1.56 2.19 o 0 6 5 3.17 2.32 1.18 o 1 6 5 192.16 190.42 6.83 o 2 6 5 28.62 31.92 1.24 o 3 6 5 77.67 83.93 5.23 o 4 6 5 14.23 16.34 1.53 o 5 6 5 5.41 4.61 1.41 o 6 6 5 20.91 23.05 3.00 o 7 6 5 5.96 4.65 0.87 o 0 7 5 42.42 38.81 2.53 o 1 7 5 20.29 17.88 1.01 o 2 7 5 14.77 16.37 1.10 o 3 7 5 23.73 25.38 3.54 o 4 7 5 8.83 8.96 1.34 o 5 7 5 132.49 131.53 4.66 o 6 7 5 1.51 1.09 2.63 o 0 8 5 114.14 105.53 7.22 o 1 8 5 28.93 30.74 2.38 o 2 8 5 61.12 60.85 3.64 o 3 8 5 4.95 -1.23 2.23 o 4 8 5 12.44 13.45 1.96 o 5 8 5 15.20 14.48 1.99 o 6 8 5 4.14 2.00 2.36 o 0 9 5 9.97 12.02 1.34 o 1 9 5 16.60 19.76 1.40 o 2 9 5 393.64 364.89 14.05 o 3 9 5 54.88 64.58 5.40 o 4 9 5 18.85 18.51 4.46 o 5 9 5 2.89 2.95 3.78 o 0 10 5 55.73 64.90 5.74 o 1 10 5 47.04 45.76 1.32 o 2 10 5 9.37 7.04 0.97 o 3 10 5 42.14 43.25 1.87 o 4 10 5 14.58 11.71 1.23 o 5 10 5 12.28 9.50 0.95 o 0 11 5 10.49 14.46 1.25 o 1 11 5 17.37 17.22 0.98 o 2 11 5 43.63 38.69 2.30 o 3 11 5 4.78 5.37 1.00 o 4 11 5 8.81 12.10 1.35 o 0 12 5 22.71 22.98 2.19 o 1 12 5 24.31 23.65 1.29 o 2 12 5 20.52 20.06 1.16 o 0 0 6 2.40 1.42 1.96 o 1 0 6 0.00 7.04 3.58 o 2 0 6 207.87 231.95 11.95 o 3 0 6 190.20 210.21 6.28 o 4 0 6 638.79 640.48 14.11 o 5 0 6 520.55 536.93 14.38 o 6 0 6 140.86 149.59 4.39 o 7 0 6 1.20 -0.88 2.97 o 0 1 6 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7 43.36 38.07 1.11 o 2 5 7 55.21 54.61 2.00 o 3 5 7 119.48 122.53 6.11 o 4 5 7 11.86 9.67 2.23 o 5 5 7 34.91 34.36 1.99 o 6 5 7 7.14 6.36 1.24 o 7 5 7 9.08 8.57 0.95 o 0 6 7 50.03 53.85 2.80 o 1 6 7 142.20 141.68 4.75 o 2 6 7 149.68 136.79 4.48 o 3 6 7 217.34 218.51 5.60 o 4 6 7 145.52 151.69 8.54 o 5 6 7 19.56 23.01 1.54 o 6 6 7 2.46 2.50 1.31 o 0 7 7 192.61 183.34 15.86 o 1 7 7 135.72 121.40 3.34 o 2 7 7 47.46 49.06 1.47 o 3 7 7 5.88 8.68 1.29 o 4 7 7 41.07 38.40 3.04 o 5 7 7 43.81 44.79 1.72 o 6 7 7 9.39 10.29 1.28 o 0 8 7 53.37 54.18 4.12 o 1 8 7 358.20 349.16 10.89 o 2 8 7 9.68 12.56 1.64 o 3 8 7 47.59 47.46 2.05 o 4 8 7 5.42 4.05 1.15 o 5 8 7 10.80 11.29 1.96 o 0 9 7 77.97 79.28 4.32 o 1 9 7 8.00 8.91 1.63 o 2 9 7 34.00 29.17 2.23 o 3 9 7 13.33 13.44 1.38 o 4 9 7 31.01 33.06 2.90 o 5 9 7 19.93 16.28 2.53 o 0 10 7 12.89 12.50 1.43 o 1 10 7 1.19 1.58 1.03 o 2 10 7 3.86 4.79 0.89 o 3 10 7 13.18 10.14 5.33 o 4 10 7 27.32 27.80 4.15 o 0 11 7 6.79 9.94 4.29 o 1 11 7 1.14 -1.03 1.08 o 2 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8.67 o 5 4 8 45.90 46.83 2.05 o 6 4 8 0.83 0.41 3.00 o 0 5 8 226.83 224.44 4.89 o 1 5 8 145.64 135.37 3.09 o 2 5 8 8.88 10.11 0.92 o 3 5 8 170.27 160.70 3.53 o 4 5 8 9.04 11.71 1.34 o 5 5 8 1.67 1.52 2.20 o 6 5 8 3.10 1.28 1.28 o 0 6 8 47.80 42.91 1.91 o 1 6 8 49.64 51.76 2.09 o 2 6 8 190.91 179.52 6.15 o 3 6 8 28.88 23.03 2.40 o 4 6 8 1.82 1.49 2.16 o 5 6 8 0.31 2.03 1.10 o 6 6 8 3.38 2.66 1.35 o 0 7 8 159.02 160.81 3.50 o 1 7 8 33.36 31.49 2.10 o 2 7 8 137.62 136.96 3.44 o 3 7 8 168.96 160.67 6.24 o 4 7 8 56.38 49.19 1.91 o 5 7 8 2.28 0.90 1.20 o 0 8 8 66.34 68.25 6.04 o 1 8 8 3.89 3.39 1.05 o 2 8 8 32.48 35.44 1.65 o 3 8 8 16.55 10.31 1.43 o 4 8 8 27.03 26.18 3.88 o 5 8 8 9.70 7.13 1.05 o 0 9 8 7.04 7.10 1.42 o 1 9 8 5.40 4.80 1.13 o 2 9 8 8.84 9.29 0.86 o 3 9 8 15.94 16.24 1.33 o 4 9 8 56.78 54.75 4.25 o 0 10 8 21.55 19.92 1.69 o 1 10 8 6.11 6.84 0.84 o 2 10 8 0.62 1.26 1.73 o 3 10 8 5.23 5.69 1.10 o 0 11 8 0.15 2.36 1.62 o 1 11 8 1.99 1.03 1.15 o 2 11 8 8.96 11.16 0.81 o 1 0 9 70.84 80.43 1.97 o 2 0 9 0.06 -1.22 2.09 o 3 0 9 19.91 22.28 1.96 o 4 0 9 100.19 95.32 3.65 o 5 0 9 108.17 101.19 3.65 o 6 0 9 109.47 104.43 3.58 o 7 0 9 5.11 4.46 1.28 o 0 1 9 26.85 17.07 2.09 o 1 1 9 22.87 20.71 0.95 o 2 1 9 60.25 64.14 2.36 o 3 1 9 24.24 25.64 1.62 o 4 1 9 144.53 148.99 3.33 o 5 1 9 11.68 10.46 1.39 o 6 1 9 8.36 6.53 1.24 o 7 1 9 15.34 14.18 1.00 o 0 2 9 433.32 452.11 8.11 o 1 2 9 11.18 12.61 0.87 o 2 2 9 37.01 34.92 1.18 o 3 2 9 123.77 116.60 5.06 o 4 2 9 12.71 16.08 1.58 o 5 2 9 53.29 53.67 2.05 o 6 2 9 8.24 8.03 1.19 o 0 3 9 35.14 25.97 1.43 o 1 3 9 41.60 43.64 1.95 o 2 3 9 52.10 53.61 1.75 o 3 3 9 368.54 367.32 8.94 o 4 3 9 34.00 34.44 2.23 o 5 3 9 2.24 -1.25 2.48 o 6 3 9 8.06 7.60 1.15 o 0 4 9 21.10 25.80 1.72 o 1 4 9 103.93 113.67 2.81 o 2 4 9 3.24 3.80 1.26 o 3 4 9 10.78 9.70 1.82 o 4 4 9 39.72 51.09 2.97 o 5 4 9 27.76 24.21 1.67 o 6 4 9 1.32 1.08 1.86 o 0 5 9 28.51 33.00 2.73 o 1 5 9 186.78 189.92 6.00 o 2 5 9 107.04 109.98 2.87 o 3 5 9 54.15 61.67 3.31 o 4 5 9 94.49 86.06 2.42 o 5 5 9 5.19 5.44 1.10 o 6 5 9 11.33 10.36 1.05 o 0 6 9 270.16 255.03 14.92 o 1 6 9 93.72 93.82 4.04 o 2 6 9 8.53 8.22 1.54 o 3 6 9 54.90 58.81 2.10 o 4 6 9 6.20 4.96 1.19 o 5 6 9 25.51 27.87 2.73 o 0 7 9 32.94 33.04 1.86 o 1 7 9 1.07 0.78 1.38 o 2 7 9 56.46 55.83 3.04 o 3 7 9 14.74 14.38 1.48 o 4 7 9 10.27 10.34 1.29 o 5 7 9 18.48 17.73 1.18 o 0 8 9 7.27 4.13 2.57 o 1 8 9 101.23 98.94 2.57 o 2 8 9 2.17 2.93 1.56 o 3 8 9 1.05 2.46 1.25 o 4 8 9 9.84 7.11 1.13 o 0 9 9 1.46 -1.97 1.97 o 1 9 9 46.89 47.82 1.56 o 2 9 9 11.19 11.72 0.98 o 3 9 9 19.82 19.07 2.23 o 4 9 9 10.05 10.56 2.09 o 0 10 9 7.79 8.27 1.15 o 1 10 9 1.00 1.49 0.97 o 2 10 9 28.67 29.06 1.18 o 3 10 9 8.76 11.61 0.92 o 0 11 9 0.23 -0.84 1.43 o 1 11 9 2.24 0.90 0.83 o 0 0 10 47.86 53.19 2.77 o 1 0 10 16.58 16.00 1.42 o 2 0 10 3.88 1.97 1.43 o 3 0 10 67.82 73.99 3.24 o 4 0 10 22.67 17.89 2.23 o 5 0 10 2.60 0.34 3.11 o 6 0 10 4.73 3.31 1.55 o 0 1 10 0.00 -0.69 1.83 o 1 1 10 133.15 132.15 1.94 o 2 1 10 16.62 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6.61 1.36 o 3 3 11 22.98 21.63 2.23 o 4 3 11 57.49 51.30 1.93 o 5 3 11 1.00 1.07 1.81 o 6 3 11 4.12 3.71 1.22 o 0 4 11 0.49 -0.23 1.33 o 1 4 11 35.65 36.04 2.48 o 2 4 11 71.43 62.49 1.60 o 3 4 11 77.22 76.00 5.77 o 4 4 11 8.92 7.43 1.15 o 5 4 11 9.58 7.49 1.11 o 0 5 11 80.84 91.35 2.67 o 1 5 11 97.64 101.65 2.14 o 2 5 11 23.98 24.72 1.45 o 3 5 11 16.44 14.91 1.48 o 4 5 11 6.48 5.72 1.13 o 5 5 11 3.03 1.85 1.13 o 0 6 11 25.17 27.23 1.81 o 1 6 11 21.64 21.03 1.10 o 2 6 11 11.25 13.88 1.15 o 3 6 11 12.94 14.60 1.34 o 4 6 11 6.91 6.61 0.99 o 0 7 11 47.31 48.92 5.00 o 1 7 11 30.14 28.36 1.18 o 2 7 11 1.57 0.46 1.34 o 3 7 11 6.71 7.55 1.15 o 4 7 11 6.10 6.20 0.92 o 0 8 11 6.43 5.75 1.22 o 1 8 11 1.22 1.86 0.90 o 2 8 11 9.31 8.18 1.18 o 3 8 11 8.71 8.50 1.05 o 0 9 11 3.87 2.03 1.25 o 1 9 11 10.78 13.55 0.85 o 2 9 11 0.59 1.12 0.84 o 0 0 12 5.27 6.68 1.89 o 1 0 12 2.40 -1.75 2.25 o 2 0 12 11.26 13.49 1.34 o 3 0 12 4.15 3.98 1.82 o 4 0 12 2.67 1.96 2.90 o 5 0 12 2.76 0.27 2.50 o 0 1 12 0.03 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2.38 1.22 o 2 8 12 9.53 12.95 1.20 o 0 9 12 0.01 -0.85 1.31 o 1 0 13 17.13 16.35 1.99 o 2 0 13 8.57 10.30 1.86 o 3 0 13 0.03 0.34 1.62 o 4 0 13 1.65 -0.27 1.35 o 5 0 13 13.27 17.08 1.49 o 0 1 13 2.13 5.96 2.23 o 1 1 13 38.53 35.62 2.51 o 2 1 13 18.14 20.98 1.11 o 3 1 13 11.00 13.06 1.38 o 4 1 13 7.50 6.58 1.15 o 5 1 13 6.04 6.24 0.97 o 0 2 13 22.74 23.55 1.68 o 1 2 13 6.77 8.84 0.95 o 2 2 13 102.22 98.46 1.80 o 3 2 13 3.36 -0.26 2.31 o 4 2 13 0.64 1.06 1.08 o 0 3 13 64.22 60.60 2.16 o 1 3 13 12.40 13.22 1.15 o 2 3 13 33.72 31.22 1.20 o 3 3 13 4.98 5.84 1.05 o 4 3 13 13.20 12.49 1.07 o 0 4 13 9.18 9.02 1.72 o 1 4 13 39.56 40.20 1.37 o 2 4 13 1.27 0.86 1.01 o 3 4 13 9.62 10.57 1.15 o 4 4 13 1.58 3.14 0.91 o 0 5 13 17.90 17.32 1.47 o 1 5 13 67.16 63.57 1.42 o 2 5 13 7.19 8.57 0.94 o 3 5 13 21.17 19.16 1.89 o 4 5 13 1.39 -0.14 1.40 o 0 6 13 12.49 13.01 1.19 o 1 6 13 25.43 25.72 1.07 o 2 6 13 17.20 16.63 0.92 o 3 6 13 13.59 14.15 1.10 o 0 7 13 0.22 -1.05 1.05 o 1 7 13 16.20 15.51 0.95 o 2 7 13 4.64 5.50 0.66 o 0 8 13 0.00 -0.92 1.36 o 0 0 14 38.87 41.58 2.36 o 1 0 14 49.77 42.46 1.91 o 2 0 14 84.50 80.17 4.52 o 3 0 14 61.57 73.65 2.90 o 4 0 14 0.06 0.61 2.23 o 0 1 14 8.77 9.96 1.43 o 1 1 14 21.80 19.92 1.41 o 2 1 14 23.64 23.93 1.10 o 3 1 14 5.43 5.39 1.10 o 4 1 14 11.98 13.14 1.18 o 0 2 14 39.33 37.54 4.62 o 1 2 14 61.99 62.91 2.21 o 2 2 14 54.40 53.19 1.39 o 3 2 14 2.01 3.72 1.52 o 4 2 14 1.07 1.82 1.00 o 0 3 14 6.32 7.17 1.20 o 1 3 14 17.21 15.90 0.93 o 2 3 14 2.40 2.89 1.21 o 3 3 14 6.85 5.67 1.18 o 0 4 14 47.62 47.22 1.86 o 1 4 14 13.84 14.36 1.00 o 2 4 14 4.20 4.60 1.22 o 3 4 14 3.44 5.23 0.86 o 0 5 14 1.03 1.76 1.33 o 1 5 14 7.45 7.02 0.95 o 2 5 14 11.97 11.44 0.78 o 0 6 14 0.90 0.98 1.53 o 1 6 14 1.63 1.98 0.78 o 2 6 14 18.08 17.87 0.77 o 1 0 15 3.97 4.62 1.04 o 2 0 15 19.93 23.63 3.68 o 3 0 15 1.85 1.55 2.30 o 0 1 15 0.07 0.59 2.09 o 1 1 15 41.83 42.84 1.43 o 2 1 15 8.41 10.61 0.83 o 3 1 15 39.66 39.91 1.48 o 0 2 15 8.48 8.44 1.21 o 1 2 15 7.39 7.55 0.78 o 2 2 15 5.12 5.91 1.20 o 3 2 15 8.66 9.67 1.08 o 0 3 15 38.39 37.34 1.58 o 1 3 15 4.26 4.98 0.80 o 2 3 15 16.18 16.44 0.93 o 0 4 15 3.38 3.17 0.91 o 1 4 15 5.82 6.21 1.35 o 2 4 15 0.45 -0.92 1.01 o 0 5 15 14.96 14.55 1.38 o 1 5 15 9.86 10.61 0.71 o 0 0 16 4.27 4.19 1.22 o 1 0 16 0.02 1.03 1.01 o 0 1 16 1.75 -0.33 1.86 o 1 1 16 2.48 2.69 0.75 o 0 2 16 36.75 37.34 1.43 o 1 2 16 5.58 5.96 0.91 o