#------------------------------------------------------------------------------ #$Date: 2010-05-06 17:22:57 +0300 (Thu, 06 May 2010) $ #$Revision: 1157 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2225677.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225677_Fobs loop_ _publ_author_name 'Liu, Hongsheng' 'Su, Lianjiang' 'Wang, Limin' 'Li, Weihong' _publ_section_title ; Poly[bis{3,3'-[(biphenyl-4,4'-diyl)dimethylene]diimidazol-1-ium} \g-octamolybdate(VI)] ; _journal_coeditor_code WM2312 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m443 _journal_page_last m444 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.145 _cell_angle_gamma 90.000 _cell_length_a 9.6460 _cell_length_b 17.3370 _cell_length_c 16.6620 _exptl_crystal_F_000 1760.00 _reflns_d_resolution_high 0.7490 _[local]_cod_data_source_file wm2312Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mm in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 596.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1638.34 1958.25 65.23 o 4 0 0 10130.91 10398.96 179.83 o 6 0 0 1102.78 1268.96 77.24 o 8 0 0 331.64 347.77 52.87 o 10 0 0 36.46 33.64 36.05 o 12 0 0 2196.41 2124.37 154.49 o 2 1 0 6226.96 5288.26 793.96 o 3 1 0 1783.90 1729.51 29.37 o 4 1 0 2285.78 2422.45 40.47 o 5 1 0 128939.85 129299.66 1364.09 o 6 1 0 3.20 14.66 6.99 o 7 1 0 6821.51 6989.55 284.60 o 8 1 0 1.29 20.33 43.94 o 9 1 0 467.82 426.79 51.84 o 10 1 0 5112.54 5170.48 158.62 o 11 1 0 90.14 104.60 34.41 o 12 1 0 1498.54 1500.59 91.63 o 1 2 0 30.83 32.18 4.11 o 2 2 0 112797.82 114986.16 1548.13 o 3 2 0 7481.96 7266.36 125.67 o 4 2 0 7841.67 7981.56 101.92 o 5 2 0 53466.15 54705.21 593.91 o 6 2 0 133.34 140.10 15.52 o 7 2 0 14197.31 13794.81 296.27 o 8 2 0 1495.14 1545.91 72.22 o 9 2 0 1682.32 1677.97 98.36 o 10 2 0 402.40 398.56 49.51 o 11 2 0 334.75 338.97 47.50 o 12 2 0 68.56 87.82 37.50 o 1 3 0 1312.39 1225.08 24.10 o 2 3 0 647.06 700.43 24.22 o 3 3 0 274.58 382.23 71.92 o 4 3 0 233.42 222.69 18.37 o 5 3 0 11438.53 11030.47 167.41 o 6 3 0 2345.44 2515.20 61.67 o 7 3 0 10137.14 9986.13 166.17 o 8 3 0 0.06 85.69 81.53 o 9 3 0 660.86 719.78 54.92 o 10 3 0 25228.71 24816.57 466.25 o 11 3 0 618.94 562.14 108.66 o 12 3 0 6084.18 5771.97 185.30 o 0 4 0 7637.81 7694.17 128.74 o 1 4 0 1409.90 1434.56 24.88 o 2 4 0 7523.01 7345.92 104.60 o 3 4 0 701.31 754.17 19.54 o 4 4 0 16.63 14.61 8.13 o 5 4 0 45619.86 44445.52 696.94 o 6 4 0 1680.36 1702.45 50.04 o 7 4 0 15358.56 15603.70 237.01 o 8 4 0 3777.09 3934.45 121.25 o 9 4 0 1759.72 1756.36 102.30 o 10 4 0 3418.16 3296.36 123.92 o 11 4 0 697.10 656.79 61.42 o 12 4 0 2564.88 2372.86 156.20 o 1 5 0 119.58 102.64 7.40 o 2 5 0 5329.84 5604.06 85.94 o 3 5 0 4083.08 3861.20 64.94 o 4 5 0 6199.66 6559.16 133.75 o 5 5 0 3943.50 3747.08 94.05 o 6 5 0 112.05 137.12 19.39 o 7 5 0 8153.91 8270.83 147.43 o 8 5 0 3359.19 3320.88 109.97 o 9 5 0 2872.77 2578.48 136.29 o 10 5 0 18871.65 18957.68 379.60 o 11 5 0 2375.28 2171.24 103.92 o 12 5 0 5246.15 5048.94 171.98 o 0 6 0 12392.46 12014.29 198.85 o 1 6 0 2220.20 2281.89 38.26 o 2 6 0 53.04 64.19 8.07 o 3 6 0 29172.40 29151.26 376.47 o 4 6 0 525.60 472.14 17.48 o 5 6 0 17918.93 17115.91 246.47 o 6 6 0 1095.49 1086.04 48.68 o 7 6 0 1145.55 1149.94 52.63 o 8 6 0 6161.78 6081.37 159.68 o 9 6 0 31.23 43.60 30.90 o 10 6 0 3479.70 3547.92 128.52 o 11 6 0 302.86 266.53 44.73 o 1 7 0 396.48 449.21 15.41 o 2 7 0 38511.99 38547.20 489.83 o 3 7 0 18984.27 18138.66 246.34 o 4 7 0 1958.05 2025.12 44.86 o 5 7 0 17833.44 17246.81 306.11 o 6 7 0 526.13 550.92 35.76 o 7 7 0 2234.50 2181.68 78.34 o 8 7 0 7624.85 7675.78 151.11 o 9 7 0 2119.69 2176.22 94.11 o 10 7 0 8377.24 8480.18 218.20 o 11 7 0 1500.67 1402.02 84.15 o 0 8 0 28366.53 28384.36 447.79 o 1 8 0 2433.30 2413.78 43.49 o 2 8 0 5234.64 5177.64 88.60 o 3 8 0 44670.55 44047.62 561.85 o 4 8 0 83.24 109.39 16.70 o 5 8 0 11417.93 11279.23 220.16 o 6 8 0 168.29 174.43 24.11 o 7 8 0 4237.26 4066.47 115.27 o 8 8 0 2791.16 2789.16 81.60 o 9 8 0 223.02 214.65 37.49 o 10 8 0 434.53 537.75 101.79 o 11 8 0 10.19 3.84 25.70 o 1 9 0 2469.14 2302.12 44.02 o 2 9 0 61559.96 62150.37 780.52 o 3 9 0 14606.51 14570.36 209.47 o 4 9 0 605.17 602.34 72.61 o 5 9 0 6498.50 6410.59 179.89 o 6 9 0 971.05 871.34 48.79 o 7 9 0 632.58 612.21 48.75 o 8 9 0 3004.48 3014.34 107.97 o 9 9 0 66.38 120.01 29.86 o 10 9 0 381.95 339.48 47.44 o 11 9 0 5.64 22.84 27.91 o 0 10 0 11308.20 11673.88 260.23 o 1 10 0 88.37 80.70 11.84 o 2 10 0 10678.12 10491.75 138.11 o 3 10 0 16133.31 15769.14 227.22 o 4 10 0 6254.44 6210.77 141.38 o 5 10 0 251.73 241.80 27.32 o 6 10 0 4188.08 4078.89 115.68 o 7 10 0 4490.32 4410.91 180.58 o 8 10 0 653.08 720.36 52.66 o 9 10 0 600.67 505.60 51.81 o 10 10 0 932.97 1057.98 74.92 o 11 10 0 231.52 212.82 46.41 o 1 11 0 10479.44 10610.40 140.65 o 2 11 0 22302.44 22460.22 266.59 o 3 11 0 415.43 473.56 25.05 o 4 11 0 8334.15 8444.51 179.66 o 5 11 0 185.59 208.86 27.00 o 6 11 0 509.32 546.28 61.97 o 7 11 0 7931.43 8118.96 191.67 o 8 11 0 2486.56 2526.23 97.48 o 9 11 0 2649.69 2465.32 84.90 o 10 11 0 42.40 56.99 31.56 o 0 12 0 0.35 -7.29 7.82 o 1 12 0 440.34 441.27 20.94 o 2 12 0 7731.91 7898.25 115.59 o 3 12 0 577.80 597.09 29.44 o 4 12 0 2941.86 2913.69 180.92 o 5 12 0 26.52 38.29 26.78 o 6 12 0 0.20 26.90 18.43 o 7 12 0 2218.36 2195.35 88.65 o 8 12 0 3126.79 3182.05 112.92 o 9 12 0 3959.40 3694.35 196.89 o 10 12 0 2588.95 2686.83 119.54 o 1 13 0 1587.57 1640.18 48.61 o 2 13 0 47.72 102.02 19.18 o 3 13 0 5394.43 5219.98 104.09 o 4 13 0 6496.78 6577.41 156.21 o 5 13 0 759.19 684.74 45.30 o 6 13 0 1806.35 1855.56 78.99 o 7 13 0 5450.12 5290.64 149.54 o 8 13 0 9268.67 9110.76 381.93 o 9 13 0 4230.81 4046.11 136.63 o 10 13 0 16.14 36.20 30.67 o 0 14 0 2245.93 2286.82 75.65 o 1 14 0 11.21 11.78 11.00 o 2 14 0 65.91 90.00 24.87 o 3 14 0 8081.33 7948.16 177.80 o 4 14 0 20.77 8.48 12.97 o 5 14 0 5.05 8.51 11.64 o 6 14 0 2955.94 3035.16 122.39 o 7 14 0 80.80 85.65 28.26 o 8 14 0 3359.92 3198.46 118.00 o 9 14 0 3951.80 3907.01 136.81 o 1 15 0 9960.66 10012.16 146.66 o 2 15 0 2665.40 2627.26 61.32 o 3 15 0 7968.18 7789.37 179.24 o 4 15 0 222.44 249.48 31.42 o 5 15 0 1171.29 1063.03 79.99 o 6 15 0 1509.55 1406.80 72.56 o 7 15 0 884.25 925.96 63.18 o 8 15 0 5601.83 5499.77 264.86 o 9 15 0 928.43 1002.30 71.98 o 0 16 0 5340.04 5357.66 136.67 o 1 16 0 2316.14 2401.21 59.50 o 2 16 0 1504.79 1483.27 46.38 o 3 16 0 3019.49 3010.50 99.40 o 4 16 0 1938.68 1863.39 78.28 o 5 16 0 0.46 -11.34 14.70 o 6 16 0 4040.71 4249.64 158.09 o 7 16 0 283.86 262.20 48.41 o 8 16 0 2367.93 2224.10 122.56 o 1 17 0 6710.52 6962.81 127.50 o 2 17 0 467.29 454.12 28.74 o 3 17 0 3870.27 3804.83 118.67 o 4 17 0 2619.78 2538.96 80.68 o 5 17 0 2086.38 2222.93 92.63 o 6 17 0 1638.86 1602.57 79.92 o 7 17 0 37.93 20.94 26.37 o 8 17 0 140.97 114.32 47.72 o 0 18 0 4817.45 5054.09 158.26 o 1 18 0 7092.32 7371.58 126.91 o 2 18 0 645.54 655.33 39.03 o 3 18 0 140.87 143.28 26.43 o 4 18 0 2004.06 1946.77 84.30 o 5 18 0 16.69 22.19 20.80 o 6 18 0 1010.07 927.05 64.00 o 7 18 0 7.68 1.37 22.66 o 1 19 0 1555.29 1608.84 63.13 o 2 19 0 0.03 12.04 16.26 o 3 19 0 609.18 569.76 49.00 o 4 19 0 6005.70 5955.37 222.98 o 5 19 0 716.03 666.93 57.16 o 6 19 0 1002.47 967.43 84.11 o 7 19 0 70.85 55.96 29.52 o 0 20 0 1402.84 1436.19 62.20 o 1 20 0 5264.58 5490.95 110.27 o 2 20 0 68.44 130.73 29.52 o 3 20 0 395.43 407.43 45.85 o 4 20 0 1073.90 1153.43 69.45 o 5 20 0 164.77 202.55 46.00 o 6 20 0 1071.78 1235.21 96.13 o 1 21 0 547.50 528.84 51.02 o 2 21 0 6.28 -9.45 16.71 o 3 21 0 37.41 36.41 21.89 o 4 21 0 2233.08 2480.03 138.01 o 5 21 0 69.34 76.21 33.99 o 0 22 0 6.78 5.03 19.45 o 1 22 0 51.71 63.69 21.48 o 2 22 0 511.09 554.44 70.38 o 3 22 0 0.74 -18.88 23.34 o 1 23 0 735.99 873.47 77.93 o -11 0 1 269.26 169.25 54.24 o -9 0 1 2990.01 2894.06 147.96 o -7 0 1 3128.94 3164.58 135.95 o -5 0 1 355753.06 340364.91 5046.00 o -3 0 1 88338.58 85866.40 1280.10 o 1 0 1 4002.52 3606.76 88.92 o 3 0 1 5707.99 5725.49 107.29 o 5 0 1 7999.19 8395.27 159.29 o 7 0 1 3369.61 3166.99 144.87 o 9 0 1 51.04 20.60 30.55 o 11 0 1 2112.69 2006.27 144.19 o -12 1 1 168.49 188.96 42.97 o -11 1 1 1.01 -3.78 20.14 o -10 1 1 15404.10 15689.66 324.08 o -9 1 1 1167.91 1156.57 65.12 o -8 1 1 959.65 1031.55 55.95 o -7 1 1 2712.18 2730.52 88.48 o -6 1 1 9313.28 9785.77 152.47 o -5 1 1 6545.51 6694.48 90.98 o -4 1 1 23133.92 24152.40 269.74 o -3 1 1 5385.60 5195.50 92.22 o -2 1 1 37.65 60.30 7.90 o -1 1 1 93.37 91.69 5.08 o 0 1 1 214284.84 157976.23 41433.27 o 1 1 1 169.08 196.74 8.98 o 2 1 1 67184.57 70163.66 1163.17 o 3 1 1 108.56 115.50 7.63 o 4 1 1 120.39 129.35 9.17 o 5 1 1 12224.47 12182.76 153.16 o 6 1 1 46.44 47.27 12.24 o 7 1 1 11095.63 11206.39 234.50 o 8 1 1 6.85 30.45 20.22 o 9 1 1 251.71 248.28 38.30 o 10 1 1 8988.73 8893.98 227.34 o 11 1 1 176.07 151.38 39.32 o 12 1 1 11794.41 11638.58 542.42 o -12 2 1 2891.98 2782.55 120.97 o -11 2 1 0.47 5.60 21.47 o -10 2 1 15509.01 15689.52 343.48 o -9 2 1 2256.64 2415.83 156.38 o -8 2 1 116.03 92.03 22.03 o -7 2 1 6545.38 6571.63 154.02 o -6 2 1 889.30 942.27 42.59 o -5 2 1 137087.47 135619.80 1642.98 o -3 2 1 35110.59 33735.18 725.06 o -2 2 1 16457.47 17441.14 273.64 o -1 2 1 6822.74 6651.14 150.54 o 0 2 1 17455.73 18728.27 429.47 o 1 2 1 52.53 66.87 14.06 o 2 2 1 122855.83 125378.78 1533.08 o 3 2 1 12670.11 12705.81 172.36 o 4 2 1 500.55 446.43 21.69 o 5 2 1 3.75 20.11 8.23 o 6 2 1 985.57 1051.72 37.72 o 7 2 1 447.64 501.43 76.56 o 8 2 1 1250.50 1228.40 66.25 o 9 2 1 224.55 259.18 49.95 o 10 2 1 7048.47 7365.59 407.33 o 11 2 1 259.49 270.24 46.95 o 12 2 1 2095.91 2113.32 112.99 o -12 3 1 2732.16 2696.25 119.66 o -11 3 1 238.57 225.11 55.44 o -10 3 1 2821.31 2752.07 109.95 o -9 3 1 4287.61 4264.02 130.53 o -8 3 1 947.99 896.26 75.36 o -7 3 1 10151.34 10268.65 167.10 o -6 3 1 288.65 309.60 20.65 o -5 3 1 12008.50 12046.88 177.58 o -4 3 1 76.78 44.09 49.61 o -3 3 1 6168.34 5728.30 109.19 o -2 3 1 16861.84 17959.67 231.38 o -1 3 1 1684.56 1575.55 38.49 o 0 3 1 30679.78 31486.75 391.89 o 1 3 1 416.32 366.38 13.43 o 2 3 1 61282.80 60875.23 750.99 o 3 3 1 871.13 835.30 22.46 o 4 3 1 415.95 479.00 17.70 o 5 3 1 66156.43 66255.67 716.18 o 6 3 1 3456.57 3742.78 81.21 o 7 3 1 38516.39 39244.72 523.17 o 8 3 1 2339.67 2449.26 94.27 o 9 3 1 911.61 985.90 63.96 o 10 3 1 6044.87 6475.50 186.29 o 11 3 1 620.49 603.07 61.29 o 12 3 1 1571.27 1467.75 134.92 o -12 4 1 2814.19 2793.30 122.21 o -11 4 1 601.59 551.15 55.54 o -10 4 1 26081.89 26203.15 603.36 o -9 4 1 18.35 8.87 18.08 o -8 4 1 1048.56 1096.57 58.25 o -7 4 1 5496.13 5481.92 107.02 o -6 4 1 19.37 34.16 9.14 o -5 4 1 2090.34 1725.50 165.82 o -4 4 1 24.30 6.74 7.48 o -3 4 1 1055.56 865.88 32.39 o -2 4 1 19559.27 20257.18 260.59 o -1 4 1 1717.91 1852.73 29.20 o 0 4 1 78379.79 78219.79 822.13 o 1 4 1 5172.01 4978.29 75.08 o 2 4 1 20630.17 19957.44 226.01 o 3 4 1 7834.79 7583.82 111.63 o 4 4 1 239.83 287.21 13.57 o 5 4 1 19157.91 18509.78 251.76 o 6 4 1 820.73 789.54 33.99 o 7 4 1 5257.70 5458.68 111.22 o 8 4 1 268.65 310.75 38.33 o 9 4 1 3209.76 3073.89 113.42 o 10 4 1 10861.20 10976.79 261.59 o 11 4 1 1133.28 1040.50 87.03 o 12 4 1 4642.86 4392.26 163.05 o -12 5 1 5727.78 5732.12 180.44 o -11 5 1 209.14 174.11 37.09 o -10 5 1 631.31 676.25 73.81 o -9 5 1 825.24 764.09 53.94 o -8 5 1 5473.02 5591.77 146.95 o -7 5 1 332.54 361.42 25.72 o -6 5 1 488.37 473.77 26.12 o -5 5 1 2407.23 2256.07 67.24 o -4 5 1 3471.69 3829.85 89.33 o -3 5 1 2106.37 2225.83 42.61 o -2 5 1 1341.74 1302.42 29.47 o -1 5 1 1269.79 1369.36 25.26 o 0 5 1 19656.90 19912.00 220.42 o 1 5 1 1177.88 1188.41 34.75 o 3 5 1 392.92 356.43 15.63 o 4 5 1 15618.03 15985.52 218.94 o 5 5 1 63310.70 62395.80 1415.96 o 6 5 1 6579.23 6670.20 123.02 o 7 5 1 20001.07 19983.51 295.01 o 8 5 1 210.35 229.31 34.30 o 9 5 1 36.89 51.83 37.59 o 10 5 1 7880.89 7848.63 209.11 o 11 5 1 652.80 726.42 66.78 o -12 6 1 204.53 258.39 48.19 o -11 6 1 564.04 609.44 107.28 o -10 6 1 9973.62 9908.66 235.93 o -9 6 1 567.71 528.10 47.55 o -8 6 1 12289.88 12450.25 206.01 o -7 6 1 2405.53 2459.39 66.67 o -6 6 1 11.12 5.84 10.30 o -5 6 1 7738.90 8106.99 164.58 o -4 6 1 6395.89 6865.34 122.77 o -3 6 1 5407.14 5267.01 84.60 o -2 6 1 9606.18 9286.29 133.19 o -1 6 1 2212.30 2123.10 35.94 o 0 6 1 35671.90 35332.50 382.86 o 1 6 1 1930.63 1912.53 34.59 o 2 6 1 1773.75 1786.71 40.13 o 3 6 1 10435.43 10191.97 148.25 o 4 6 1 406.15 396.31 32.16 o 5 6 1 24984.73 23824.53 402.30 o 6 6 1 604.78 604.34 38.28 o 7 6 1 1734.92 1676.27 57.01 o 8 6 1 1446.03 1419.82 71.94 o 9 6 1 5813.44 5987.73 169.52 o 10 6 1 4178.07 4062.64 141.10 o 11 6 1 2153.91 2161.56 106.30 o -11 7 1 2.63 20.05 21.70 o -10 7 1 2503.26 2467.50 103.10 o -9 7 1 52.14 56.42 24.63 o -8 7 1 7013.72 7222.21 141.28 o -7 7 1 9073.75 8907.69 190.20 o -6 7 1 1165.04 1049.12 48.55 o -5 7 1 122.09 161.01 21.94 o -4 7 1 23.08 15.06 10.61 o -3 7 1 14861.42 13633.38 190.40 o -2 7 1 7073.48 6706.02 104.40 o -1 7 1 166.62 184.05 10.66 o 0 7 1 50681.93 51789.43 555.72 o 1 7 1 3544.74 3510.68 54.69 o 2 7 1 0.84 13.85 6.87 o 3 7 1 16423.33 16163.83 224.13 o 4 7 1 4819.74 4843.27 84.94 o 5 7 1 29774.00 28541.59 558.73 o 6 7 1 3778.06 3835.88 106.06 o 7 7 1 2794.28 2614.22 88.03 o 8 7 1 441.99 430.40 34.26 o 9 7 1 1695.73 1595.08 82.47 o 10 7 1 659.96 616.58 57.76 o 11 7 1 224.64 205.29 43.79 o -11 8 1 35.67 24.85 25.23 o -10 8 1 1889.54 1932.70 92.94 o -9 8 1 75.41 149.53 40.34 o -8 8 1 13380.15 13737.58 226.71 o -7 8 1 121.01 94.79 23.14 o -6 8 1 51.62 23.93 12.53 o -5 8 1 21127.70 20927.34 362.46 o -4 8 1 975.62 1001.38 30.32 o -3 8 1 9438.28 9185.52 139.47 o -2 8 1 34496.37 33775.93 334.83 o -1 8 1 2902.98 2830.21 48.20 o 0 8 1 29033.24 29447.29 327.85 o 1 8 1 7.00 12.67 5.07 o 2 8 1 6403.43 6256.92 103.04 o 3 8 1 17846.29 17029.67 237.11 o 4 8 1 4.10 13.96 7.12 o 5 8 1 8876.72 8663.05 181.15 o 6 8 1 194.73 217.76 37.08 o 7 8 1 780.77 804.10 49.14 o 8 8 1 297.81 270.42 29.41 o 9 8 1 818.99 830.07 63.35 o 10 8 1 110.45 152.04 36.89 o 11 8 1 118.00 96.40 35.81 o -11 9 1 199.28 167.33 40.13 o -10 9 1 381.45 332.76 45.44 o -9 9 1 18.55 25.06 20.24 o -8 9 1 4263.49 4122.46 122.92 o -7 9 1 23882.58 23030.31 556.50 o -6 9 1 4648.73 4645.98 244.95 o -5 9 1 1848.14 1901.42 67.87 o -4 9 1 79.07 78.02 16.11 o -3 9 1 43103.67 42686.88 473.13 o -2 9 1 19690.84 20309.81 211.33 o -1 9 1 3723.58 3723.55 60.53 o 0 9 1 18555.51 19097.15 223.43 o 1 9 1 3272.72 3220.77 55.51 o 2 9 1 6380.80 6481.47 144.17 o 3 9 1 15985.08 15420.74 220.66 o 4 9 1 1381.17 1523.90 58.65 o 5 9 1 6909.70 6473.61 149.63 o 6 9 1 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