#------------------------------------------------------------------------------
#$Date: 2010-05-06 17:22:57 +0300 (Thu, 06 May 2010) $
#$Revision: 1157 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2225730.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2225730_Fobs
loop_
_publ_author_name
'Fun, Hoong-Kun'
'Goh, Jia Hao'
'Yu, Haitao'
'Zhang, Yan'
_publ_section_title
;
 4-[(2,5-Dimethyl-1,3-thiazol-4-yl)methyl]-4-hydroxy-2-methylisoquinoline-1,3(2<i>H</i>,4<i>H</i>)-dione
;
_journal_coeditor_code           SJ2758
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o964
_journal_page_last               o965
_journal_volume                  66
_journal_year                    2010
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 114.304
_cell_angle_gamma                90.000
_cell_length_a                   8.5793
_cell_length_b                   10.4438
_cell_length_c                   17.5496
_exptl_crystal_F_000             664.00
_reflns_d_resolution_high        0.8508
_[local]_cod_data_source_file    sj2758Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' z6m in P2(1)/c (100K)'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            120.48
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 2377.26 2738.89 38.63 o
3 0 0 1020.95 1030.56 9.42 o
4 0 0 381.51 320.18 3.10 o
5 0 0 17.39 16.64 0.68 o
6 0 0 3.37 6.28 0.56 o
7 0 0 936.83 899.69 11.16 o
8 0 0 11.86 10.75 1.43 o
1 1 0 1525.18 1759.13 24.68 o
2 1 0 1258.75 1275.91 20.38 o
3 1 0 9.15 6.40 0.22 o
4 1 0 951.65 1073.94 6.36 o
5 1 0 532.65 521.30 3.69 o
6 1 0 1004.95 970.93 6.83 o
7 1 0 621.68 615.11 6.64 o
8 1 0 729.15 721.10 10.40 o
0 2 0 1309.49 1410.49 33.39 o
1 2 0 2922.90 3606.35 45.37 o
2 2 0 14515.00 -0.12 0.40 o
3 2 0 73.98 75.04 0.71 o
4 2 0 315.76 290.95 2.20 o
5 2 0 1110.24 1129.63 8.03 o
6 2 0 12.26 10.91 0.53 o
7 2 0 619.15 650.72 5.97 o
8 2 0 232.45 216.74 4.13 o
2 3 0 2562.65 2955.02 20.08 o
3 3 0 314.10 284.04 2.53 o
4 3 0 383.92 371.29 2.61 o
5 3 0 192.36 178.37 1.81 o
6 3 0 290.57 296.01 3.64 o
7 3 0 23.12 22.63 0.78 o
8 3 0 11.38 9.67 1.32 o
0 4 0 5105.36 6395.82 86.50 o
1 4 0 787.24 768.06 5.25 o
2 4 0 176.88 182.61 1.30 o
3 4 0 1502.49 1698.23 9.64 o
4 4 0 1919.04 2026.24 12.18 o
5 4 0 72.12 86.53 1.10 o
6 4 0 239.00 228.65 2.30 o
7 4 0 181.21 179.06 2.77 o
8 4 0 64.05 66.05 2.53 o
1 5 0 625.12 583.10 3.56 o
2 5 0 1324.52 1333.44 7.44 o
3 5 0 5.21 10.20 0.36 o
4 5 0 434.86 456.18 3.31 o
5 5 0 594.41 583.16 4.24 o
6 5 0 259.89 238.62 2.46 o
7 5 0 182.76 183.60 3.36 o
8 5 0 150.38 171.48 4.89 o
0 6 0 2576.40 2733.38 20.47 o
1 6 0 183.90 176.67 1.38 o
2 6 0 36.78 39.60 0.60 o
3 6 0 0.93 0.98 0.18 o
4 6 0 1019.62 1022.65 6.09 o
5 6 0 1095.13 1073.10 7.39 o
6 6 0 889.43 934.48 9.62 o
7 6 0 68.49 71.33 1.49 o
1 7 0 1411.10 1436.26 8.13 o
2 7 0 12.34 12.36 0.29 o
3 7 0 8.49 6.97 0.43 o
4 7 0 1019.16 1041.01 6.59 o
5 7 0 273.37 265.70 2.49 o
6 7 0 17.45 16.95 0.66 o
7 7 0 337.23 348.00 4.61 o
0 8 0 705.39 703.92 5.16 o
1 8 0 39.51 38.16 0.60 o
2 8 0 540.58 531.34 2.99 o
3 8 0 74.23 73.04 0.91 o
4 8 0 491.14 511.12 3.68 o
5 8 0 8.42 8.46 0.45 o
6 8 0 13.73 16.11 0.86 o
1 9 0 86.49 84.96 0.84 o
2 9 0 18.29 17.77 0.41 o
3 9 0 2.25 2.18 0.23 o
4 9 0 1.77 3.56 0.33 o
5 9 0 171.48 166.14 2.25 o
6 9 0 135.31 134.12 2.83 o
0 10 0 558.23 563.51 5.29 o
1 10 0 53.58 50.79 0.72 o
2 10 0 247.71 245.26 2.62 o
3 10 0 256.90 249.04 2.87 o
4 10 0 391.43 404.18 6.18 o
5 10 0 303.68 319.22 4.65 o
1 11 0 37.24 36.90 0.86 o
2 11 0 1039.51 1107.95 16.21 o
3 11 0 12.13 14.12 1.03 o
4 11 0 91.36 96.91 2.09 o
-8 1 1 5.97 6.77 1.04 o
-7 1 1 1339.29 1341.06 12.08 o
-6 1 1 9.31 8.84 0.45 o
-5 1 1 134.72 107.63 1.27 o
-4 1 1 216.10 218.04 2.17 o
-3 1 1 521.53 540.64 6.61 o
-1 1 1 732.38 682.81 6.76 o
0 1 1 109.66 101.61 1.70 o
2 1 1 285.83 240.04 2.11 o
3 1 1 874.59 882.32 6.44 o
4 1 1 277.11 235.80 1.73 o
5 1 1 332.15 366.76 2.78 o
6 1 1 280.32 275.04 2.35 o
7 1 1 128.58 118.37 1.85 o
8 1 1 21.61 20.89 1.25 o
-8 2 1 98.57 98.38 3.10 o
-7 2 1 547.75 511.70 6.37 o
-6 2 1 394.10 410.55 4.85 o
-5 2 1 292.05 318.87 4.43 o
-4 2 1 212.97 177.54 2.32 o
-3 2 1 4996.24 6556.51 58.92 o
-1 2 1 2.05 4.27 0.23 o
0 2 1 3475.40 5152.01 155.57 o
1 2 1 8776.81 -0.02 0.29 o
2 2 1 30.47 41.49 0.57 o
3 2 1 142.10 154.23 1.26 o
4 2 1 1085.91 1192.02 6.84 o
5 2 1 637.58 622.64 4.32 o
6 2 1 2390.98 2516.14 18.37 o
7 2 1 283.19 273.98 3.03 o
8 2 1 265.17 237.85 6.31 o
-8 3 1 0.94 2.60 0.85 o
-7 3 1 3113.57 3537.93 44.98 o
-6 3 1 113.71 102.45 1.48 o
-5 3 1 555.86 512.51 6.45 o
-4 3 1 127.66 165.73 1.56 o
-3 3 1 132.48 130.92 1.34 o
-2 3 1 3.05 3.07 0.16 o
1 3 1 2586.54 3065.46 22.02 o
2 3 1 774.49 799.10 5.19 o
3 3 1 141.31 106.13 0.87 o
4 3 1 941.22 918.07 5.76 o
5 3 1 607.48 603.19 4.33 o
6 3 1 50.61 55.09 1.19 o
7 3 1 175.56 182.72 2.40 o
8 3 1 1.21 1.35 0.58 o
-8 4 1 614.87 663.00 30.67 o
-7 4 1 588.01 653.08 9.66 o
-6 4 1 586.93 611.66 5.01 o
-5 4 1 282.00 288.21 2.49 o
-4 4 1 194.37 227.75 2.06 o
-3 4 1 7861.74 10704.73 74.32 o
-2 4 1 1119.42 1293.21 8.10 o
-1 4 1 2104.22 2351.15 14.71 o
0 4 1 310.30 301.70 2.30 o
1 4 1 2590.57 2916.81 18.77 o
2 4 1 491.90 480.84 3.08 o
3 4 1 78.32 80.30 0.83 o
4 4 1 654.07 658.44 4.38 o
5 4 1 1114.61 1134.37 8.03 o
6 4 1 200.61 180.29 2.24 o
7 4 1 684.89 728.17 8.34 o
8 4 1 237.57 252.65 6.72 o
-8 5 1 35.21 38.07 1.82 o
-7 5 1 52.77 51.78 1.31 o
-6 5 1 301.61 292.41 2.77 o
-5 5 1 1503.46 1575.27 10.46 o
-4 5 1 738.56 749.44 5.02 o
-3 5 1 3293.51 3747.02 21.92 o
-2 5 1 2999.76 3470.08 18.87 o
-1 5 1 1.94 5.94 0.26 o
0 5 1 3.27 2.13 0.18 o
1 5 1 99.77 100.97 0.87 o
2 5 1 0.07 0.85 0.13 o
3 5 1 109.79 104.59 1.07 o
4 5 1 92.28 87.91 1.00 o
5 5 1 1104.65 1097.28 7.35 o
6 5 1 153.28 159.51 1.91 o
7 5 1 13.45 10.86 0.65 o
8 5 1 14.18 16.29 1.10 o
-8 6 1 42.13 42.33 1.82 o
-7 6 1 3.18 3.99 0.40 o
-6 6 1 246.61 241.01 2.64 o
-5 6 1 51.82 43.31 0.78 o
-4 6 1 78.69 80.33 0.88 o
-3 6 1 27.53 25.96 0.51 o
-2 6 1 5.10 6.31 0.29 o
-1 6 1 1597.94 1735.19 9.93 o
0 6 1 240.07 217.43 1.54 o
1 6 1 9.99 11.21 0.34 o
2 6 1 24.37 26.44 0.50 o
3 6 1 66.75 56.58 0.74 o
4 6 1 700.13 717.07 4.84 o
5 6 1 0.66 1.07 0.22 o
6 6 1 12.57 12.12 0.51 o
7 6 1 0.45 0.89 0.39 o
-7 7 1 29.46 23.75 1.49 o
-6 7 1 26.09 28.30 0.79 o
-5 7 1 1681.36 1695.25 13.67 o
-4 7 1 341.43 316.45 2.34 o
-3 7 1 473.87 483.45 2.86 o
-2 7 1 87.02 86.27 0.76 o
-1 7 1 1107.77 1100.04 5.94 o
0 7 1 436.11 434.33 2.58 o
1 7 1 402.54 385.96 2.47 o
2 7 1 19.73 17.85 0.33 o
3 7 1 194.48 183.46 1.56 o
4 7 1 31.33 29.19 0.56 o
5 7 1 403.56 403.40 3.40 o
6 7 1 124.38 121.76 1.83 o
7 7 1 113.76 115.48 2.59 o
-7 8 1 25.78 22.94 0.75 o
-6 8 1 562.30 602.59 7.70 o
-5 8 1 337.74 330.41 3.47 o
-4 8 1 173.03 146.69 1.42 o
-3 8 1 1853.17 1866.58 10.43 o
-2 8 1 45.55 51.04 0.58 o
-1 8 1 387.41 373.82 2.19 o
0 8 1 152.82 149.15 1.16 o
1 8 1 824.41 799.03 4.58 o
2 8 1 841.33 842.43 4.84 o
3 8 1 13.50 11.56 0.39 o
4 8 1 136.97 127.61 1.39 o
5 8 1 1051.67 1101.27 12.46 o
6 8 1 1.41 2.41 0.37 o
-6 9 1 193.16 226.25 3.23 o
-5 9 1 777.26 745.24 7.07 o
-4 9 1 53.75 47.94 1.07 o
-3 9 1 142.92 134.33 1.26 o
-2 9 1 27.44 28.12 0.48 o
-1 9 1 1750.72 1823.21 9.54 o
0 9 1 46.04 44.37 0.67 o
1 9 1 325.22 307.96 2.20 o
2 9 1 682.91 662.81 4.27 o
3 9 1 9.99 10.53 0.47 o
4 9 1 469.16 475.41 4.59 o
5 9 1 1248.64 1295.62 13.44 o
6 9 1 82.58 97.88 1.78 o
-5 10 1 67.17 67.92 1.74 o
-4 10 1 138.01 150.13 2.58 o
-3 10 1 812.96 833.63 8.30 o
-2 10 1 400.87 402.84 3.28 o
-1 10 1 227.05 221.17 1.92 o
0 10 1 628.42 626.14 4.85 o
1 10 1 301.46 294.81 2.45 o
2 10 1 20.43 21.39 0.81 o
3 10 1 10.23 11.09 0.46 o
4 10 1 176.91 189.02 3.35 o
5 10 1 3.67 6.28 0.56 o
-4 11 1 172.54 183.69 3.47 o
-3 11 1 23.92 24.18 1.34 o
-2 11 1 393.68 392.76 8.91 o
-1 11 1 0.46 1.49 0.26 o
0 11 1 1.49 2.81 0.35 o
1 11 1 609.86 614.78 6.70 o
2 11 1 49.40 48.26 1.18 o
3 11 1 8.09 7.04 0.80 o
1 12 1 21.89 20.79 1.08 o
-8 0 2 278.04 272.15 11.27 o
-7 0 2 4576.04 5201.99 78.58 o
-6 0 2 1839.01 1876.01 21.10 o
-5 0 2 1826.01 1960.62 19.55 o
-4 0 2 9.32 9.71 0.43 o
-3 0 2 935.83 1021.41 15.40 o
-2 0 2 61.37 98.61 2.04 o
-1 0 2 150.74 152.70 3.49 o
1 0 2 194.86 166.73 2.07 o
2 0 2 2015.94 2017.19 20.56 o
3 0 2 3304.00 4044.98 41.60 o
4 0 2 1988.35 2112.32 17.50 o
5 0 2 532.93 610.21 5.62 o
6 0 2 726.16 778.49 7.20 o
7 0 2 116.92 103.55 2.32 o
8 0 2 239.69 232.00 8.49 o
-8 1 2 386.47 367.61 9.83 o
-7 1 2 45.73 45.11 1.55 o
-6 1 2 440.24 431.76 3.95 o
-5 1 2 65.43 95.07 1.03 o
-4 1 2 694.66 623.75 4.75 o
-3 1 2 1112.37 1098.41 11.96 o
-2 1 2 1.20 1.42 0.14 o
0 1 2 213.06 202.29 2.00 o
1 1 2 1879.17 2201.74 17.49 o
2 1 2 1161.19 1228.09 9.45 o
3 1 2 73.33 82.00 0.84 o
4 1 2 2713.91 3011.17 16.74 o
5 1 2 4.06 2.87 0.22 o
6 1 2 2400.67 2470.36 15.59 o
7 1 2 289.82 291.17 2.99 o
8 1 2 10.65 8.92 1.12 o
-8 2 2 31.34 29.56 3.09 o
-7 2 2 0.69 0.99 0.39 o
-6 2 2 22.74 21.91 0.70 o
-5 2 2 14.31 14.73 0.47 o
-4 2 2 591.91 669.69 8.28 o
-3 2 2 4162.34 5404.93 58.30 o
-1 2 2 320.63 309.19 2.43 o
0 2 2 2989.43 3730.23 37.19 o
1 2 2 19.75 25.58 0.36 o
2 2 2 33.22 28.62 0.41 o
3 2 2 174.24 176.34 1.37 o
4 2 2 317.93 363.28 2.57 o
5 2 2 28.85 33.74 0.59 o
6 2 2 80.49 70.95 1.09 o
7 2 2 36.91 43.13 1.06 o
-8 3 2 173.60 171.54 7.64 o
-7 3 2 44.68 48.92 1.26 o
-6 3 2 298.12 303.64 3.43 o
-5 3 2 1.39 2.32 0.24 o
-4 3 2 722.68 808.99 9.78 o
-3 3 2 1690.96 1959.18 15.24 o
-2 3 2 0.32 1.11 0.11 o
-1 3 2 9289.91 -0.09 0.21 o
0 3 2 2943.08 3639.50 30.17 o
1 3 2 538.86 523.20 4.09 o
2 3 2 337.98 364.79 2.63 o
3 3 2 82.66 92.60 0.83 o
4 3 2 585.22 612.04 3.99 o
5 3 2 90.92 89.82 1.06 o
6 3 2 21.84 26.69 0.79 o
7 3 2 117.30 116.99 1.83 o
8 3 2 0.20 0.26 0.45 o
-8 4 2 841.87 973.51 28.11 o
-7 4 2 97.31 94.55 2.34 o
-6 4 2 877.60 942.33 15.84 o
-5 4 2 218.58 194.03 2.36 o
-4 4 2 982.80 1024.21 5.92 o
-3 4 2 2291.71 2580.32 13.77 o
-2 4 2 74.69 90.79 0.88 o
-1 4 2 40.40 36.74 0.49 o
0 4 2 16.59 22.77 0.45 o
1 4 2 976.42 974.84 6.31 o
2 4 2 4072.77 5070.43 30.57 o
3 4 2 14.52 10.41 0.33 o
4 4 2 29.54 35.54 0.60 o
5 4 2 68.35 59.27 0.94 o
6 4 2 0.74 1.14 0.25 o
7 4 2 39.61 40.56 1.24 o
8 4 2 15.46 15.28 1.07 o
-8 5 2 351.07 413.30 8.11 o
-7 5 2 195.53 209.48 2.61 o
-6 5 2 310.45 315.30 3.04 o
-5 5 2 112.29 102.02 1.20 o
-4 5 2 1338.56 1259.98 7.43 o
-3 5 2 437.19 488.61 3.05 o
-2 5 2 100.65 85.96 0.86 o
-1 5 2 220.70 214.12 1.87 o
0 5 2 211.11 192.39 1.48 o
1 5 2 379.92 349.62 2.32 o
2 5 2 1349.49 1387.22 8.46 o
3 5 2 18.20 24.07 0.54 o
4 5 2 428.47 397.49 2.97 o
5 5 2 496.30 482.63 4.01 o
6 5 2 1093.89 1100.99 9.24 o
7 5 2 84.59 98.11 2.16 o
-8 6 2 122.20 133.87 5.76 o
-7 6 2 66.42 60.44 1.24 o
-6 6 2 2977.25 3243.25 27.52 o
-5 6 2 3883.63 4612.77 28.88 o
-4 6 2 280.56 283.63 1.98 o
-3 6 2 475.78 482.48 3.24 o
-2 6 2 6854.22 8801.48 48.12 o
-1 6 2 2195.46 2364.38 12.90 o
0 6 2 48.84 41.01 0.54 o
1 6 2 416.28 411.39 2.90 o
2 6 2 843.46 760.48 5.42 o
3 6 2 7.31 5.97 0.29 o
4 6 2 610.23 604.31 4.35 o
5 6 2 111.77 114.25 1.34 o
6 6 2 9.08 8.17 0.57 o
7 6 2 334.80 348.80 6.30 o
-7 7 2 1.28 3.07 0.36 o
-6 7 2 493.46 478.12 4.62 o
-5 7 2 1.52 2.76 0.30 o
-4 7 2 1413.54 1436.14 8.00 o
-3 7 2 1.29 2.79 0.27 o
-2 7 2 8.05 10.05 0.28 o
-1 7 2 5.08 7.85 0.30 o
0 7 2 131.55 107.14 0.97 o
1 7 2 763.16 741.06 4.51 o
2 7 2 144.56 152.22 1.41 o
3 7 2 181.96 191.20 1.74 o
4 7 2 1001.14 977.34 8.42 o
5 7 2 262.09 275.60 3.01 o
6 7 2 282.80 269.11 3.06 o
7 7 2 154.23 152.62 5.02 o
-7 8 2 73.23 56.71 1.29 o
-6 8 2 21.55 23.43 0.82 o
-5 8 2 42.92 44.01 0.91 o
-4 8 2 312.67 315.25 2.70 o
-3 8 2 2483.44 2732.92 14.75 o
-2 8 2 206.43 189.62 1.33 o
-1 8 2 28.13 28.10 0.41 o
0 8 2 0.25 0.84 0.14 o
1 8 2 151.83 161.37 1.28 o
2 8 2 285.25 261.84 2.05 o
3 8 2 89.87 82.44 0.96 o
4 8 2 133.15 138.97 1.51 o
5 8 2 66.71 70.16 1.73 o
6 8 2 79.91 77.50 1.58 o
-6 9 2 138.86 123.22 2.41 o
-5 9 2 57.71 56.15 1.10 o
-4 9 2 414.08 417.13 3.59 o
-3 9 2 264.79 254.86 1.92 o
-2 9 2 9.47 8.70 0.30 o
-1 9 2 133.09 129.07 1.12 o
0 9 2 542.02 537.33 3.58 o
1 9 2 86.60 76.70 0.92 o
2 9 2 80.19 79.76 0.93 o
3 9 2 17.15 16.15 0.49 o
4 9 2 58.31 50.44 1.02 o
5 9 2 2.62 3.22 0.34 o
-5 10 2 40.08 38.26 1.14 o
-4 10 2 10.78 11.20 0.58 o
-3 10 2 7.29 5.93 0.45 o
-2 10 2 2269.50 2449.77 18.47 o
-1 10 2 1.32 2.52 0.22 o
0 10 2 25.69 26.84 0.59 o
1 10 2 276.57 261.82 2.42 o
2 10 2 190.26 176.84 2.13 o
3 10 2 101.87 102.32 1.34 o
4 10 2 12.14 11.82 0.72 o
-4 11 2 21.55 27.90 0.95 o
-3 11 2 0.75 1.26 0.47 o
-2 11 2 3.69 4.69 0.45 o
-1 11 2 16.36 16.88 0.57 o
0 11 2 244.22 247.72 2.78 o
1 11 2 124.26 124.95 2.11 o
2 11 2 305.59 326.30 5.20 o
3 11 2 75.09 74.18 2.52 o
0 12 2 19.71 17.52 0.57 o
1 12 2 24.21 24.23 1.17 o
-8 1 3 64.46 68.27 4.95 o
-7 1 3 1050.49 993.69 18.93 o
-6 1 3 153.50 151.64 2.01 o
-5 1 3 8.45 7.38 0.37 o
-4 1 3 84.92 80.36 1.03 o
-3 1 3 2203.44 2532.53 17.74 o
-2 1 3 381.70 356.65 2.45 o
-1 1 3 335.99 311.87 2.94 o
0 1 3 472.99 484.48 4.01 o
1 1 3 2643.37 3062.61 21.38 o
2 1 3 6.50 6.37 0.37 o
3 1 3 3224.02 4037.19 23.77 o
4 1 3 166.07 181.75 1.55 o
5 1 3 526.02 482.52 3.25 o
6 1 3 8.34 13.64 0.49 o
7 1 3 262.48 250.05 3.31 o
-8 2 3 1814.72 1948.23 54.46 o
-7 2 3 84.30 93.81 4.70 o
-6 2 3 470.25 424.17 5.12 o
-5 2 3 987.07 1015.81 17.11 o
-4 2 3 90.40 78.82 1.04 o
-3 2 3 304.95 296.90 3.55 o
-2 2 3 305.24 274.04 2.08 o
0 2 3 1171.48 1082.66 7.99 o
1 2 3 802.30 784.61 4.79 o
2 2 3 1060.03 1251.97 8.33 o
3 2 3 2375.55 2604.69 15.31 o
4 2 3 265.23 181.25 1.52 o
5 2 3 715.12 721.42 4.60 o
6 2 3 364.68 350.39 3.22 o
7 2 3 89.83 99.20 1.79 o
-8 3 3 55.17 63.75 4.49 o
-7 3 3 3539.25 4418.19 121.01 o
-6 3 3 13.31 15.18 0.53 o
-5 3 3 1688.70 1931.39 27.30 o
-4 3 3 1272.18 1325.59 9.53 o
-3 3 3 561.89 460.81 3.07 o
-2 3 3 2440.31 2671.37 16.54 o
-1 3 3 6.17 7.28 0.30 o
0 3 3 63.12 72.31 1.06 o
1 3 3 1710.57 1802.04 10.90 o
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