#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/58/2225818.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225818_Fobs loop_ _publ_author_name 'Chernyshev, V. M.' 'Chernysheva, A. V.' 'Tarasova, E. V.' 'Ivanov, V. V.' 'Starikova, Z. A.' _publ_section_title ; 2-(4-Chlorobenzoyl)-1-(diaminomethylene)hydrazinium chloride monohydrate ; _journal_coeditor_code CV2710 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1152 _journal_page_last o1153 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.360 _cell_angle_gamma 90.000 _cell_length_a 19.3493 _cell_length_b 4.3563 _cell_length_c 14.5158 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8111 _[local]_cod_data_source_file cv2710Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21c in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 166.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 635.37 553.63 9.79 o 3 0 0 2430.56 2143.75 33.20 o 4 0 0 2510.68 2388.41 37.03 o 5 0 0 1260.20 1226.51 19.91 o 6 0 0 692.73 679.08 14.43 o 7 0 0 8482.81 8588.53 130.19 o 8 0 0 778.42 740.22 13.68 o 9 0 0 2617.71 2317.25 37.37 o 10 0 0 328.40 336.17 9.93 o 11 0 0 3901.35 3633.78 68.52 o 12 0 0 772.98 768.04 19.32 o 13 0 0 94.38 86.44 5.84 o 14 0 0 1197.67 1148.14 41.97 o 15 0 0 669.25 719.45 27.10 o 16 0 0 460.94 473.40 18.20 o 17 0 0 5.23 14.06 8.34 o 18 0 0 75.46 82.51 20.01 o 19 0 0 18.60 30.14 10.09 o 20 0 0 187.65 212.74 15.62 o 21 0 0 182.08 223.72 15.51 o 22 0 0 144.36 201.69 16.54 o 23 0 0 252.03 311.15 18.46 o 1 1 0 10758.16 11157.00 119.92 o 2 1 0 6178.13 6684.40 125.81 o 3 1 0 1112.55 990.92 14.01 o 4 1 0 2053.92 2039.44 25.18 o 5 1 0 1556.60 1403.81 17.94 o 6 1 0 1220.50 1210.32 21.03 o 7 1 0 2177.68 1930.29 24.91 o 8 1 0 4.81 34.54 9.39 o 9 1 0 66.94 98.15 8.34 o 10 1 0 771.70 624.67 10.04 o 11 1 0 699.23 577.35 9.65 o 12 1 0 1203.29 1169.09 16.79 o 13 1 0 1043.46 1004.91 19.13 o 14 1 0 480.65 475.55 9.39 o 15 1 0 7.87 18.68 3.81 o 16 1 0 2416.51 2433.54 45.95 o 17 1 0 0.12 22.25 6.07 o 18 1 0 34.55 51.46 7.35 o 19 1 0 1990.99 2021.41 33.90 o 20 1 0 789.21 894.46 23.01 o 21 1 0 200.41 281.56 17.21 o 22 1 0 0.01 1.44 7.25 o 0 2 0 10839.82 12465.55 189.04 o 1 2 0 540.22 989.81 12.60 o 2 2 0 1983.29 2163.86 24.96 o 3 2 0 1596.02 1482.45 19.82 o 4 2 0 1174.69 1289.94 17.74 o 5 2 0 1702.07 1741.58 23.06 o 6 2 0 158.05 165.63 6.33 o 7 2 0 1003.34 1035.44 13.50 o 8 2 0 30.58 48.90 6.98 o 9 2 0 3227.32 2946.62 37.18 o 10 2 0 219.89 254.61 7.53 o 11 2 0 106.58 94.75 5.89 o 12 2 0 1234.88 1146.29 17.91 o 13 2 0 268.63 266.46 8.40 o 14 2 0 182.60 165.94 7.36 o 15 2 0 81.33 91.76 5.87 o 16 2 0 0.13 -5.93 5.54 o 17 2 0 2.08 9.20 6.16 o 18 2 0 126.25 170.02 11.39 o 19 2 0 237.10 248.89 10.76 o 20 2 0 523.97 540.74 24.15 o 21 2 0 56.23 67.73 10.79 o 1 3 0 297.44 321.45 6.49 o 2 3 0 3.94 10.14 2.78 o 3 3 0 0.01 3.04 3.34 o 4 3 0 623.51 611.81 11.31 o 5 3 0 457.83 466.97 9.76 o 6 3 0 194.50 197.57 6.75 o 7 3 0 636.62 632.75 11.78 o 8 3 0 15.36 23.21 4.25 o 9 3 0 1.12 -1.46 3.71 o 10 3 0 746.62 664.74 12.35 o 11 3 0 54.21 60.69 6.91 o 12 3 0 2.33 1.90 5.77 o 13 3 0 14.50 18.85 6.52 o 14 3 0 204.54 211.71 10.09 o 15 3 0 11.58 16.09 6.85 o 16 3 0 834.28 756.39 17.81 o 17 3 0 69.56 87.61 8.91 o 18 3 0 86.83 129.98 10.01 o 19 3 0 193.00 234.58 11.62 o 0 4 0 20.45 29.53 9.21 o 1 4 0 40.16 59.14 5.54 o 2 4 0 281.61 301.68 9.97 o 3 4 0 239.12 232.15 8.20 o 4 4 0 168.10 191.36 9.13 o 5 4 0 92.15 90.42 6.65 o 6 4 0 102.11 104.72 7.62 o 7 4 0 9.41 10.86 5.32 o 8 4 0 38.71 37.17 7.12 o 9 4 0 31.84 39.40 8.85 o 10 4 0 4.02 5.36 6.90 o 11 4 0 44.79 49.38 8.05 o 12 4 0 187.88 203.65 16.17 o 13 4 0 135.41 161.46 10.83 o 14 4 0 31.59 40.77 8.38 o 15 4 0 2.74 -4.98 7.60 o 1 5 0 67.82 70.80 9.19 o 2 5 0 0.17 34.32 8.22 o 3 5 0 800.21 801.81 19.00 o 4 5 0 0.01 26.26 8.79 o 5 5 0 0.01 -14.17 11.99 o 6 5 0 3.79 3.26 9.44 o 7 5 0 13.22 14.03 9.69 o 8 5 0 92.28 71.94 11.47 o -23 1 1 5.76 6.70 7.81 o -22 1 1 2.34 6.24 9.91 o -21 1 1 16.73 44.92 11.16 o -20 1 1 345.83 375.47 14.40 o -19 1 1 34.64 68.19 10.14 o -18 1 1 65.62 89.85 7.85 o -17 1 1 572.71 571.50 14.08 o -16 1 1 25.48 59.17 6.00 o -15 1 1 159.79 175.59 6.35 o -14 1 1 20.90 35.93 3.99 o -13 1 1 4.95 4.25 3.05 o -12 1 1 30.08 27.74 4.39 o -11 1 1 3.39 11.56 3.18 o -10 1 1 315.85 268.24 5.76 o -9 1 1 429.96 414.81 8.66 o -8 1 1 46.67 54.56 2.68 o -7 1 1 3051.86 2934.61 36.11 o -6 1 1 123.69 184.87 6.28 o -5 1 1 1480.38 1485.16 17.22 o -4 1 1 1144.16 1101.31 12.99 o -3 1 1 1064.06 1077.90 14.00 o -2 1 1 178.58 233.62 13.55 o -1 1 1 3580.13 3708.88 44.61 o 0 1 1 247.26 285.03 15.81 o 1 1 1 65.03 145.59 4.12 o 2 1 1 634.38 726.90 23.52 o 3 1 1 8639.31 8270.65 97.42 o 4 1 1 2618.30 2423.81 29.87 o 5 1 1 23.43 13.34 6.39 o 6 1 1 1040.15 881.00 12.50 o 7 1 1 1622.11 1504.10 29.65 o 8 1 1 665.41 756.17 13.04 o 9 1 1 392.60 462.48 27.24 o 10 1 1 148.57 166.86 8.09 o 11 1 1 115.04 121.20 4.35 o 12 1 1 363.17 352.36 7.33 o 13 1 1 193.73 206.21 10.91 o 14 1 1 19.94 19.72 4.86 o 15 1 1 14.37 11.42 5.11 o 16 1 1 137.96 153.25 8.38 o 17 1 1 25.93 43.79 5.64 o 18 1 1 11.15 15.28 5.36 o 19 1 1 61.82 89.43 7.19 o 20 1 1 475.24 496.76 13.18 o 21 1 1 0.33 7.10 6.30 o 22 1 1 1.41 4.04 7.83 o -21 2 1 0.52 -5.79 6.74 o -20 2 1 15.05 31.87 7.46 o -19 2 1 83.67 81.23 7.94 o -18 2 1 435.58 445.47 13.68 o -17 2 1 211.10 237.69 9.62 o -16 2 1 230.90 226.08 9.06 o -15 2 1 1014.02 974.53 18.49 o -14 2 1 120.98 133.60 7.78 o -13 2 1 749.45 688.23 11.76 o -12 2 1 480.76 471.55 9.16 o -11 2 1 241.12 233.82 6.20 o -10 2 1 477.29 469.27 8.71 o -9 2 1 1371.44 1433.23 19.73 o -8 2 1 1106.05 970.91 14.17 o -7 2 1 79.49 83.87 6.59 o -6 2 1 660.08 678.02 10.66 o -5 2 1 76.18 71.05 5.04 o -4 2 1 0.80 2.01 3.50 o -3 2 1 357.96 345.65 6.01 o -2 2 1 46.01 46.84 2.78 o -1 2 1 388.40 493.58 12.20 o 0 2 1 1537.68 1655.12 19.48 o 1 2 1 4550.15 4857.83 58.83 o 2 2 1 44.79 57.53 3.43 o 3 2 1 1.13 -1.70 3.69 o 4 2 1 58.80 79.75 5.08 o 5 2 1 650.92 650.84 12.33 o 6 2 1 29.48 33.78 5.66 o 7 2 1 295.04 267.92 6.46 o 8 2 1 37.17 37.46 6.29 o 9 2 1 201.98 215.21 5.95 o 10 2 1 273.99 243.38 6.54 o 11 2 1 291.73 272.39 8.78 o 12 2 1 14.08 14.15 4.87 o 13 2 1 114.58 125.48 7.46 o 14 2 1 7.13 0.12 5.10 o 15 2 1 10.30 19.78 5.99 o 16 2 1 181.62 167.64 13.06 o 17 2 1 75.14 96.67 8.29 o 18 2 1 614.01 593.66 17.78 o 19 2 1 16.02 36.84 7.64 o 20 2 1 1.33 -2.58 6.73 o 21 2 1 9.50 5.91 7.02 o -19 3 1 124.70 126.36 10.10 o -18 3 1 42.35 49.04 8.22 o -17 3 1 56.64 62.49 8.22 o -16 3 1 182.98 206.18 10.62 o -15 3 1 103.49 122.83 8.87 o -14 3 1 3.24 1.32 6.06 o -13 3 1 0.07 -6.17 5.77 o -12 3 1 57.48 63.57 7.20 o -11 3 1 26.86 33.61 4.69 o -10 3 1 930.80 831.29 14.39 o -9 3 1 120.72 129.73 6.18 o -8 3 1 113.96 144.65 8.05 o -7 3 1 582.62 515.61 10.39 o -6 3 1 867.70 830.90 13.95 o -5 3 1 211.95 175.63 6.37 o -4 3 1 44.41 62.27 3.81 o -3 3 1 12.85 10.89 2.80 o -2 3 1 253.08 244.76 5.81 o -1 3 1 413.21 418.23 7.59 o 0 3 1 19.91 30.27 6.23 o 1 3 1 10.09 26.21 3.78 o 2 3 1 880.38 822.35 13.46 o 3 3 1 1763.83 1783.60 24.69 o 4 3 1 1567.93 1603.93 22.69 o 5 3 1 69.99 99.08 5.47 o 6 3 1 141.25 137.18 6.26 o 7 3 1 554.62 511.99 10.34 o 8 3 1 282.08 267.93 9.53 o 9 3 1 15.36 12.06 3.92 o 10 3 1 317.08 290.02 10.16 o 11 3 1 672.51 619.05 14.78 o 12 3 1 388.83 375.90 12.72 o 13 3 1 896.00 855.49 18.39 o 14 3 1 92.71 97.34 9.15 o 15 3 1 147.18 151.85 13.87 o 16 3 1 432.10 414.06 13.33 o 17 3 1 7.83 14.96 7.22 o 18 3 1 28.77 18.22 7.71 o 19 3 1 1.09 12.99 7.79 o -15 4 1 15.93 8.97 7.76 o -14 4 1 17.20 25.97 7.90 o -13 4 1 369.29 354.71 12.97 o -12 4 1 426.84 369.84 12.81 o -11 4 1 41.10 38.99 7.89 o -10 4 1 205.60 202.80 10.77 o -9 4 1 383.29 365.80 12.08 o -8 4 1 595.12 588.31 19.20 o -7 4 1 530.18 492.20 11.60 o -6 4 1 517.18 532.01 11.98 o -5 4 1 93.53 130.60 7.14 o -4 4 1 1279.31 1321.50 20.76 o -3 4 1 462.88 454.40 12.84 o -2 4 1 116.15 161.29 9.66 o -1 4 1 107.44 154.86 10.51 o 0 4 1 924.63 955.30 19.10 o 1 4 1 751.84 757.13 14.10 o 2 4 1 286.54 290.77 9.17 o 3 4 1 16.82 50.71 5.76 o 4 4 1 104.36 130.01 7.33 o 5 4 1 76.91 127.04 7.28 o 6 4 1 518.67 511.59 11.86 o 7 4 1 390.92 365.21 12.00 o 8 4 1 20.57 30.95 7.26 o 9 4 1 736.82 642.94 16.11 o 10 4 1 519.20 467.36 13.94 o 11 4 1 173.13 155.97 10.47 o 12 4 1 22.69 15.26 7.42 o 13 4 1 336.97 278.26 11.95 o 14 4 1 75.86 90.11 9.55 o 15 4 1 38.31 45.36 8.89 o -8 5 1 13.19 2.41 9.67 o -7 5 1 119.20 112.53 17.42 o -6 5 1 591.65 537.32 18.59 o -5 5 1 346.60 341.36 17.65 o -4 5 1 34.35 54.23 12.44 o -3 5 1 149.71 160.61 12.52 o -2 5 1 181.23 199.82 12.36 o -1 5 1 162.36 193.57 14.80 o 0 5 1 18.23 36.65 8.38 o 1 5 1 23.61 36.41 8.63 o 2 5 1 435.68 367.46 16.21 o 3 5 1 232.65 263.15 12.07 o 4 5 1 390.67 388.06 13.61 o 5 5 1 4.78 15.82 9.57 o 6 5 1 186.79 191.15 14.23 o 7 5 1 94.66 119.00 13.16 o 8 5 1 226.67 241.32 15.44 o -23 0 2 2.33 28.24 10.84 o -22 0 2 555.42 620.74 28.63 o -21 0 2 8.58 28.35 9.83 o -20 0 2 202.00 260.17 11.92 o -19 0 2 115.10 140.45 15.48 o -18 0 2 869.53 979.38 20.97 o -17 0 2 6288.01 6493.33 147.87 o -16 0 2 1218.18 1187.29 23.03 o -15 0 2 776.59 758.52 16.24 o -14 0 2 7.71 6.75 4.09 o -13 0 2 958.94 918.01 17.80 o -12 0 2 199.50 231.94 7.59 o -11 0 2 3724.35 3607.75 57.21 o -10 0 2 594.10 586.35 11.94 o -9 0 2 593.50 556.15 11.14 o -8 0 2 13727.99 12721.17 408.15 o -7 0 2 287.09 308.09 10.14 o -6 0 2 3860.21 3652.20 173.85 o -5 0 2 9.78 109.23 6.67 o -4 0 2 100.20 334.94 8.55 o -3 0 2 906.71 1070.81 23.49 o -2 0 2 431.07 397.99 10.28 o -1 0 2 94.92 111.27 6.11 o 0 0 2 1890.36 1999.06 40.58 o 1 0 2 233.29 189.86 9.17 o 2 0 2 12147.66 11942.39 259.77 o 3 0 2 27883.03 27176.46 412.57 o 4 0 2 18.88 -5.00 3.34 o 5 0 2 898.89 804.58 16.76 o 6 0 2 4319.80 4120.77 63.67 o 7 0 2 590.26 621.82 18.19 o 8 0 2 30.03 43.26 7.44 o 9 0 2 1098.86 1231.92 21.68 o 10 0 2 4935.88 5049.60 86.95 o 11 0 2 7.86 20.80 4.40 o 12 0 2 5.80 14.64 3.91 o 13 0 2 753.18 656.93 16.36 o 14 0 2 206.95 221.35 8.19 o 15 0 2 1674.48 1600.28 29.05 o 16 0 2 83.03 151.08 7.93 o 17 0 2 1003.57 1015.56 21.24 o 18 0 2 156.97 216.88 14.62 o 19 0 2 1471.80 1563.37 39.82 o 20 0 2 83.44 177.57 33.91 o 21 0 2 82.26 109.02 17.51 o 22 0 2 424.26 512.44 22.34 o -23 1 2 12.95 21.87 7.81 o -22 1 2 449.59 498.26 14.38 o -21 1 2 33.83 49.40 7.88 o -20 1 2 7.66 17.47 8.12 o -19 1 2 384.46 392.96 12.30 o -18 1 2 60.03 79.04 6.09 o -17 1 2 129.84 167.14 7.16 o -16 1 2 1215.43 1207.10 18.52 o -15 1 2 861.60 821.05 12.47 o -14 1 2 305.62 321.72 6.96 o -13 1 2 1749.29 1653.73 25.54 o -12 1 2 3.75 6.55 3.21 o -11 1 2 1071.51 1063.82 14.98 o -10 1 2 985.27 859.73 12.97 o -9 1 2 1202.30 1198.00 16.49 o -8 1 2 151.92 161.99 3.96 o -7 1 2 865.64 857.56 11.02 o -6 1 2 4241.71 3875.64 42.55 o -5 1 2 842.80 867.83 10.77 o -4 1 2 7125.76 7196.33 100.58 o -2 1 2 75.79 138.15 6.67 o -1 1 2 5444.33 5823.54 62.70 o 0 1 2 49.33 177.00 24.23 o 1 1 2 15147.22 15541.78 224.41 o 2 1 2 7554.39 8167.09 125.68 o 3 1 2 26711.53 27087.40 361.46 o 4 1 2 8900.54 8763.17 104.14 o 5 1 2 5645.82 5367.87 64.61 o 6 1 2 1534.55 1363.58 18.90 o 7 1 2 41.13 47.50 4.25 o 8 1 2 8002.68 7728.29 137.44 o 9 1 2 184.73 228.78 17.71 o 10 1 2 1.83 1.89 3.05 o 11 1 2 1124.23 955.22 23.87 o 12 1 2 658.79 632.41 11.35 o 13 1 2 1207.79 1133.23 25.59 o 14 1 2 298.62 295.35 8.10 o 15 1 2 11.28 14.01 7.18 o 16 1 2 2.78 6.73 4.63 o 17 1 2 922.20 899.26 30.31 o 18 1 2 520.61 514.84 15.38 o 19 1 2 82.66 105.70 7.42 o 20 1 2 77.62 114.63 7.96 o 21 1 2 13.87 10.22 9.04 o 22 1 2 182.29 240.50 12.66 o -22 2 2 55.86 69.54 10.67 o -21 2 2 5.28 4.60 6.48 o -20 2 2 413.08 441.88 13.17 o -19 2 2 20.77 21.76 6.59 o -18 2 2 20.43 31.69 7.25 o -17 2 2 2211.06 2158.85 34.71 o -16 2 2 230.60 234.74 9.09 o -15 2 2 1134.24 1050.43 16.64 o -14 2 2 11.32 14.19 3.84 o -13 2 2 655.09 631.85 11.37 o -12 2 2 538.52 526.17 9.91 o -11 2 2 1168.49 1088.32 16.12 o -10 2 2 1724.88 1629.27 25.15 o -9 2 2 400.04 370.03 7.61 o -8 2 2 931.59 765.49 12.00 o -7 2 2 1190.60 1279.16 17.81 o -6 2 2 3457.62 3367.23 42.00 o -5 2 2 684.69 693.20 10.88 o -4 2 2 41.94 75.93 3.61 o -3 2 2 739.17 717.20 14.63 o -2 2 2 412.68 477.74 8.19 o -1 2 2 54.62 103.02 9.13 o 0 2 2 0.02 93.66 6.20 o 1 2 2 3657.67 3843.85 47.13 o 2 2 2 4301.69 4599.43 55.87 o 3 2 2 1119.21 1020.52 14.71 o 4 2 2 29.31 20.89 3.03 o 5 2 2 688.77 702.76 11.38 o 6 2 2 138.22 117.84 9.23 o 7 2 2 109.05 105.49 9.79 o 8 2 2 60.80 69.13 6.10 o 9 2 2 31.62 42.62 7.58 o 10 2 2 223.95 234.62 6.64 o 11 2 2 0.15 3.28 3.39 o 12 2 2 562.75 539.29 11.79 o 13 2 2 318.44 294.67 8.68 o 14 2 2 46.85 50.36 5.39 o 15 2 2 974.75 1016.92 31.40 o 16 2 2 40.77 40.81 6.80 o 17 2 2 177.77 190.85 12.90 o 18 2 2 96.79 128.35 12.20 o 19 2 2 218.92 219.48 10.85 o 20 2 2 207.30 250.78 11.67 o -19 3 2 94.41 113.41 9.72 o -18 3 2 10.69 5.59 7.17 o -17 3 2 7.45 2.22 6.72 o -16 3 2 1.35 0.60 6.41 o -15 3 2 80.88 115.98 10.22 o -14 3 2 133.11 156.70 10.94 o -13 3 2 274.49 278.70 13.28 o -12 3 2 888.07 875.62 17.14 o -11 3 2 128.77 129.80 10.14 o -10 3 2 0.21 3.40 5.19 o -9 3 2 0.32 0.95 3.40 o -8 3 2 0.04 -3.73 3.38 o -7 3 2 52.44 53.43 3.92 o -6 3 2 50.11 45.69 3.73 o -5 3 2 65.15 85.43 4.76 o -4 3 2 738.39 754.79 11.31 o -3 3 2 524.60 577.84 9.49 o -2 3 2 429.04 553.25 9.90 o -1 3 2 3215.80 3358.96 42.72 o 0 3 2 348.28 422.39 8.94 o 1 3 2 81.65 164.09 6.07 o 2 3 2 675.16 733.37 12.68 o 3 3 2 883.60 961.84 15.29 o 4 3 2 16.81 19.11 4.00 o 5 3 2 1104.68 1070.60 16.76 o 6 3 2 92.46 102.42 5.62 o 7 3 2 118.19 144.19 6.30 o 8 3 2 731.80 663.92 12.15 o 9 3 2 15.77 22.29 8.02 o 10 3 2 456.41 409.88 11.84 o 11 3 2 26.64 33.91 6.60 o 12 3 2 153.06 172.70 14.36 o 13 3 2 788.25 721.08 21.94 o 14 3 2 11.97 3.80 6.53 o 15 3 2 115.92 114.15 12.16 o 16 3 2 17.20 7.73 6.94 o 17 3 2 41.52 39.36 8.32 o 18 3 2 12.91 -3.63 7.21 o -15 4 2 150.38 153.88 10.82 o -14 4 2 3.30 7.33 7.32 o -13 4 2 33.85 37.86 8.10 o -12 4 2 100.41 119.26 9.47 o -11 4 2 411.13 395.71 12.84 o -10 4 2 9.04 13.48 6.78 o -9 4 2 179.14 185.38 9.92 o -8 4 2 89.55 97.25 8.28 o -7 4 2 10.77 7.83 5.31 o -6 4 2 153.98 185.45 8.35 o -5 4 2 155.82 175.63 9.26 o -4 4 2 2.40 -1.12 5.25 o -3 4 2 84.42 107.56 8.26 o -2 4 2 16.59 11.23 4.65 o -1 4 2 11.34 11.40 5.98 o 0 4 2 182.24 195.70 9.36 o 1 4 2 87.97 129.05 8.15 o 2 4 2 136.20 150.66 7.47 o 3 4 2 17.06 36.88 5.55 o 4 4 2 430.91 449.13 11.04 o 5 4 2 154.68 187.37 8.39 o 6 4 2 136.66 164.30 9.73 o 7 4 2 0.60 -3.86 6.39 o 8 4 2 13.05 6.14 6.91 o 9 4 2 2.18 1.37 6.68 o 10 4 2 3.66 -9.95 6.64 o 11 4 2 79.22 79.64 8.94 o 12 4 2 0.12 -4.37 7.07 o 13 4 2 0.45 9.61 7.55 o 14 4 2 50.38 31.08 8.52 o -8 5 2 100.10 97.55 11.95 o -7 5 2 1.24 -2.65 9.06 o -6 5 2 110.52 125.01 10.91 o -5 5 2 276.80 273.00 12.30 o -4 5 2 14.09 14.15 7.76 o -3 5 2 65.58 55.16 8.93 o -2 5 2 2.53 8.24 7.54 o -1 5 2 13.53 20.26 7.93 o 0 5 2 105.55 116.51 10.08 o 1 5 2 57.74 74.26 11.99 o 2 5 2 145.25 147.28 10.76 o 3 5 2 220.19 232.60 12.12 o 4 5 2 9.25 14.46 9.69 o 5 5 2 138.92 151.55 13.49 o 6 5 2 218.65 263.17 14.90 o 7 5 2 1.47 19.81 9.98 o -23 1 3 82.62 120.13 13.69 o -22 1 3 9.98 39.44 8.87 o -21 1 3 122.11 178.97 22.53 o -20 1 3 19.35 23.44 9.41 o -19 1 3 0.01 13.77 6.19 o -18 1 3 45.23 59.09 5.61 o -17 1 3 189.66 187.98 7.14 o -16 1 3 190.65 205.39 7.05 o -15 1 3 45.83 75.08 5.22 o -14 1 3 29.83 36.28 3.90 o -13 1 3 158.99 192.81 5.96 o -12 1 3 711.49 718.96 10.61 o -11 1 3 401.67 401.13 7.19 o -10 1 3 1200.06 1199.29 15.33 o -9 1 3 405.43 449.64 7.39 o -8 1 3 507.39 502.63 7.53 o -7 1 3 5.26 6.63 1.72 o -6 1 3 374.05 374.89 6.53 o -5 1 3 2004.63 1948.80 24.44 o -4 1 3 2408.43 2415.93 32.09 o -3 1 3 53.20 164.83 16.73 o -2 1 3 148.08 207.66 15.85 o -1 1 3 328.80 363.34 10.03 o 0 1 3 2824.39 2831.25 31.97 o 1 1 3 301.76 452.90 13.56 o 2 1 3 3829.10 3829.04 64.10 o 3 1 3 3370.80 3581.11 52.41 o 4 1 3 436.19 458.46 11.63 o 5 1 3 112.74 94.46 8.51 o 6 1 3 307.53 315.20 6.30 o 7 1 3 739.06 740.21 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