#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/58/2225822.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225822_Fobs loop_ _publ_author_name 'Seredyuk, Maksym' 'Znovjyak, Kateryna O.' 'Moroz, Yurii S.' 'Pavlenko, Vadim A.' 'Fritsky, Igor O.' _publ_section_title ; catena-Poly[[[aquacopper(II)]bis[\m-bis(3,5-dimethyl-1H-pyrazol-4-yl) selenide]] bis(tetrafluoridoborate) bis(triphenylphosphine oxide) monohydrate] ; _journal_coeditor_code DS2023 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m527 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.744 _cell_angle_gamma 90.000 _cell_length_a 21.4560 _cell_length_b 15.3590 _cell_length_c 18.4910 _exptl_crystal_F_000 2820.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file ds2023Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 11 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 579.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 131474.22 143991.52 2937.14 o 6 0 0 41715.66 38606.15 1245.99 o 8 0 0 63859.07 62829.79 2462.16 o 10 0 0 152766.69 173978.23 7038.84 o 12 0 0 22198.52 20375.75 720.25 o 14 0 0 59114.86 59891.55 2748.61 o 16 0 0 2039.33 1962.79 155.07 o 18 0 0 35430.24 33526.43 2833.11 o 20 0 0 12847.91 12811.55 988.99 o 22 0 0 16083.21 15275.29 1078.48 o 24 0 0 2829.73 2499.63 521.65 o 26 0 0 11244.44 12471.13 905.62 o 3 1 0 48895.32 48917.68 2479.74 o 5 1 0 67543.86 72236.91 959.55 o 7 1 0 36575.94 34582.26 898.95 o 9 1 0 4343.78 4391.70 127.83 o 11 1 0 2148.64 1988.06 115.49 o 13 1 0 96442.42 97179.48 3580.04 o 15 1 0 1676.68 1632.92 89.06 o 17 1 0 7090.00 6929.61 219.81 o 19 1 0 13225.27 12652.34 723.79 o 21 1 0 6566.94 5808.65 270.22 o 23 1 0 1406.13 1385.69 221.57 o 25 1 0 18741.50 18097.15 777.77 o 27 1 0 1585.51 1439.42 292.97 o 2 2 0 35044.11 36778.84 1052.01 o 4 2 0 1096.08 1011.71 55.76 o 6 2 0 2459.74 2165.22 59.83 o 8 2 0 13745.15 13330.51 108.30 o 10 2 0 6868.62 6115.19 108.44 o 12 2 0 2422.49 1875.28 59.36 o 14 2 0 9400.68 9519.60 309.14 o 16 2 0 19304.52 19242.79 360.19 o 18 2 0 3556.98 3384.50 136.01 o 20 2 0 3579.73 2809.21 164.13 o 22 2 0 11.86 222.54 176.58 o 24 2 0 1750.86 1729.98 252.53 o 26 2 0 1976.96 1658.34 288.67 o 1 3 0 154877.33 167123.67 1628.92 o 3 3 0 22459.13 24205.96 153.03 o 5 3 0 63225.80 65569.90 2146.42 o 7 3 0 36738.40 38120.82 967.95 o 9 3 0 2803.45 2139.52 56.29 o 11 3 0 230.29 526.65 60.06 o 13 3 0 5193.39 4276.03 119.15 o 15 3 0 19769.01 20253.99 555.92 o 17 3 0 36597.01 34879.45 1126.05 o 19 3 0 22.11 355.76 113.55 o 21 3 0 5555.55 4898.06 494.66 o 23 3 0 6719.33 6806.50 505.64 o 25 3 0 126.60 434.63 222.97 o 27 3 0 53.94 1200.86 538.48 o 0 4 0 51550.88 51437.95 393.15 o 2 4 0 1174.07 1288.31 52.00 o 4 4 0 17398.61 16960.86 158.82 o 6 4 0 38010.34 36111.82 735.78 o 8 4 0 14427.96 13354.46 187.97 o 10 4 0 44650.38 41836.73 805.09 o 12 4 0 667.57 725.71 71.32 o 14 4 0 9780.33 9569.62 334.92 o 16 4 0 61499.36 58314.66 1695.25 o 18 4 0 489.60 580.44 112.39 o 20 4 0 10095.94 10196.75 465.32 o 22 4 0 3413.95 3741.43 192.10 o 24 4 0 122.04 605.64 240.32 o 26 4 0 154.34 24.72 218.23 o 1 5 0 9188.28 9211.35 127.37 o 3 5 0 5149.39 4404.66 97.28 o 5 5 0 713.18 749.36 51.60 o 7 5 0 581.32 787.19 68.40 o 9 5 0 19244.00 17602.78 223.82 o 11 5 0 253.15 354.59 77.18 o 13 5 0 2900.70 2932.66 125.92 o 15 5 0 15070.88 14631.54 367.61 o 17 5 0 3884.94 3739.45 181.05 o 19 5 0 66.48 279.22 119.45 o 21 5 0 5997.10 5845.54 305.77 o 23 5 0 6802.62 7355.93 314.94 o 25 5 0 1011.73 1075.53 649.38 o 0 6 0 64497.47 67972.74 969.44 o 2 6 0 65268.76 66963.54 940.00 o 4 6 0 3010.19 2842.13 95.65 o 6 6 0 18018.99 18836.57 246.75 o 8 6 0 355.15 473.30 66.39 o 10 6 0 2625.50 3006.72 95.57 o 12 6 0 2945.10 2768.78 99.58 o 14 6 0 3422.82 3626.11 181.83 o 16 6 0 1075.62 1112.56 110.93 o 18 6 0 2182.07 1914.44 180.60 o 20 6 0 4935.23 5398.43 312.27 o 22 6 0 2687.62 2708.34 205.58 o 24 6 0 659.61 858.59 263.49 o 1 7 0 1458.70 1846.05 68.12 o 3 7 0 163.60 439.88 66.22 o 5 7 0 10410.12 10919.20 264.19 o 7 7 0 35992.28 34948.39 493.78 o 9 7 0 2008.63 1962.96 90.73 o 11 7 0 17765.14 16980.68 351.19 o 13 7 0 30127.48 30388.31 718.68 o 15 7 0 31.08 379.27 122.65 o 17 7 0 6.64 367.44 125.57 o 19 7 0 2826.88 2580.56 330.67 o 21 7 0 48.62 425.72 247.82 o 23 7 0 3723.98 3953.86 252.71 o 25 7 0 1578.23 1427.73 382.25 o 0 8 0 62669.41 59268.50 1326.80 o 2 8 0 7996.64 8558.50 159.25 o 4 8 0 72.65 159.38 64.67 o 6 8 0 26171.51 25227.22 448.79 o 8 8 0 194.71 356.53 88.72 o 10 8 0 7087.42 7034.81 186.69 o 12 8 0 10661.64 9474.46 271.27 o 14 8 0 50.98 426.50 109.55 o 16 8 0 4179.03 4591.92 171.05 o 18 8 0 9229.26 9577.86 214.47 o 20 8 0 4756.26 4721.13 335.04 o 22 8 0 1095.94 1102.46 246.43 o 24 8 0 659.16 837.79 238.74 o 1 9 0 14878.99 13955.60 338.69 o 3 9 0 5596.87 4552.08 107.34 o 5 9 0 14336.46 14480.11 270.43 o 7 9 0 6418.57 6581.68 146.60 o 9 9 0 17132.95 17649.71 192.83 o 11 9 0 216.58 231.98 94.33 o 13 9 0 26507.96 26700.45 749.81 o 15 9 0 6305.43 6476.62 161.23 o 17 9 0 40.45 321.79 130.78 o 19 9 0 14236.60 15480.65 411.94 o 21 9 0 419.46 427.12 234.25 o 23 9 0 840.94 974.65 282.52 o 0 10 0 1334.10 1642.02 174.37 o 2 10 0 18101.68 17517.90 257.71 o 4 10 0 4041.92 3745.05 188.15 o 6 10 0 7016.27 7172.22 158.90 o 8 10 0 1415.72 1437.37 216.55 o 10 10 0 36.84 391.34 102.84 o 12 10 0 29542.10 28693.23 606.59 o 14 10 0 671.87 639.76 125.36 o 16 10 0 1534.34 1566.21 172.18 o 18 10 0 629.31 856.61 202.93 o 20 10 0 730.10 810.38 212.61 o 22 10 0 2166.49 1996.80 293.85 o 1 11 0 11214.24 11421.24 154.11 o 3 11 0 3948.18 3747.13 111.37 o 5 11 0 968.09 949.62 112.23 o 7 11 0 5411.62 5357.08 142.98 o 9 11 0 5751.99 5493.19 136.03 o 11 11 0 36.12 307.72 106.77 o 13 11 0 3037.39 2845.32 157.54 o 15 11 0 1313.15 1344.03 177.63 o 17 11 0 2011.21 1848.87 188.02 o 19 11 0 1189.82 1259.29 220.58 o 21 11 0 234.39 434.42 209.62 o 23 11 0 30.61 251.17 369.82 o 0 12 0 4126.80 3853.71 243.71 o 2 12 0 1952.03 1794.69 102.53 o 4 12 0 6786.28 6613.87 205.37 o 6 12 0 6108.02 5962.39 148.17 o 8 12 0 175.18 336.50 118.49 o 10 12 0 10759.17 10969.50 236.81 o 12 12 0 2383.29 3041.18 173.59 o 14 12 0 10.02 237.28 148.74 o 16 12 0 2118.35 2205.70 189.02 o 18 12 0 75.76 333.72 186.73 o 20 12 0 28.52 310.08 193.77 o 22 12 0 5012.01 4500.55 585.90 o 1 13 0 9608.78 9510.34 183.69 o 3 13 0 10370.90 9454.27 304.92 o 5 13 0 44.42 341.96 123.04 o 7 13 0 9928.81 9518.16 178.22 o 9 13 0 15869.21 16824.44 265.33 o 11 13 0 883.79 852.27 146.16 o 13 13 0 1080.70 1229.22 166.63 o 15 13 0 6334.26 6426.20 262.93 o 17 13 0 82.60 454.57 267.75 o 19 13 0 11125.99 11463.09 452.64 o 0 14 0 57.83 176.49 181.86 o 2 14 0 5969.63 5789.57 196.23 o 4 14 0 5909.78 5621.28 188.38 o 6 14 0 14608.07 14532.01 286.01 o 8 14 0 8537.23 7818.68 221.82 o 10 14 0 155.79 278.66 164.24 o 12 14 0 3040.95 2945.76 199.15 o 14 14 0 3.77 390.08 193.35 o 16 14 0 4980.94 4848.61 335.40 o 18 14 0 270.91 790.22 280.78 o 1 15 0 908.04 1125.63 197.32 o 3 15 0 355.22 439.18 153.18 o 5 15 0 2456.88 2698.75 164.58 o 7 15 0 1499.36 1321.02 137.44 o 9 15 0 834.77 958.87 177.27 o 11 15 0 222.47 321.26 159.91 o 13 15 0 557.07 578.24 179.15 o 15 15 0 66.66 344.56 199.31 o 17 15 0 187.91 415.32 281.15 o 0 16 0 61.42 204.36 270.40 o 2 16 0 4892.53 5048.30 215.21 o 4 16 0 12344.33 12414.14 289.84 o 6 16 0 5904.37 5981.06 194.07 o 8 16 0 12.32 300.15 159.20 o 10 16 0 1394.92 1662.32 242.11 o 12 16 0 2608.06 2608.96 354.17 o 14 16 0 1684.13 1810.89 237.96 o 16 16 0 3513.69 4502.08 588.96 o 1 17 0 20896.37 20915.65 360.57 o 3 17 0 7913.95 8518.60 277.00 o 5 17 0 224.71 555.93 174.38 o 7 17 0 1069.52 1266.85 192.26 o 9 17 0 14952.20 14903.40 275.53 o 11 17 0 2873.27 2665.50 227.08 o 13 17 0 2473.26 2492.76 271.11 o 0 18 0 899.79 1182.50 369.44 o 2 18 0 1123.36 1244.62 230.80 o 4 18 0 3331.73 3401.72 278.13 o 6 18 0 684.94 586.85 191.99 o 8 18 0 237.44 496.84 225.75 o 10 18 0 850.92 1041.73 236.66 o 1 19 0 979.08 1115.56 259.49 o 3 19 0 189.72 391.49 231.26 o 5 19 0 376.58 591.29 221.83 o 7 19 0 273.12 420.88 189.89 o -27 1 1 1803.36 1669.35 218.98 o -25 1 1 837.92 1000.97 316.46 o -23 1 1 6305.86 5842.52 286.79 o -21 1 1 3639.21 3484.89 166.38 o -19 1 1 2704.39 3173.37 181.82 o -17 1 1 215.52 214.41 101.79 o -15 1 1 35929.67 35961.63 1093.23 o -13 1 1 1230.66 1163.27 56.59 o -11 1 1 883.52 727.79 61.00 o -9 1 1 76.37 244.66 46.94 o -7 1 1 29499.46 29454.93 417.83 o -5 1 1 29912.55 29813.47 557.44 o -3 1 1 35054.02 35701.18 450.75 o 3 1 1 23345.61 23588.28 232.71 o 5 1 1 485.81 4856.01 2167.94 o 7 1 1 48341.98 50036.70 1638.37 o 9 1 1 25064.73 26604.09 681.05 o 11 1 1 17693.30 17153.15 401.99 o 13 1 1 5287.97 5304.94 173.04 o 15 1 1 811.19 751.28 87.71 o 17 1 1 14331.14 13520.49 579.27 o 19 1 1 420.60 377.86 135.35 o 21 1 1 229.81 167.60 229.31 o 23 1 1 8907.83 8577.64 295.28 o 25 1 1 1420.47 1683.18 348.05 o 27 1 1 3349.03 3655.57 338.00 o -26 2 1 3746.31 3391.47 396.26 o -24 2 1 1717.83 1634.27 228.99 o -22 2 1 3814.57 4087.44 221.50 o -20 2 1 9950.30 9906.18 209.32 o -18 2 1 6403.47 6612.00 176.96 o -16 2 1 3.37 351.67 96.23 o -14 2 1 16945.00 16542.90 449.12 o -12 2 1 15278.33 15331.66 388.48 o -10 2 1 6358.90 6303.22 152.45 o -8 2 1 79518.95 80308.44 1057.56 o -6 2 1 5026.08 5138.48 94.98 o -4 2 1 6915.80 6623.85 95.46 o -2 2 1 138564.89 147469.70 3343.50 o 2 2 1 29804.57 29637.58 1366.75 o 4 2 1 361.28 1311.58 383.68 o 6 2 1 46996.34 48888.89 1366.49 o 8 2 1 7149.83 5517.41 94.37 o 10 2 1 90218.31 92783.61 2343.41 o 12 2 1 10774.09 9475.32 228.31 o 14 2 1 13176.46 12779.44 555.77 o 16 2 1 3400.02 2884.54 117.01 o 18 2 1 6645.65 6291.58 170.39 o 20 2 1 6369.62 7041.37 421.29 o 22 2 1 640.66 554.32 211.40 o 24 2 1 1769.57 1810.31 227.54 o 26 2 1 3286.77 3505.38 390.66 o -27 3 1 3856.52 3813.40 474.99 o -25 3 1 1711.60 1779.82 293.30 o -23 3 1 1255.06 1023.43 179.01 o -21 3 1 5895.34 5847.71 386.47 o -19 3 1 5862.31 5581.22 149.78 o -17 3 1 198.76 337.98 97.17 o -15 3 1 26145.19 24881.99 765.31 o -13 3 1 1729.03 1863.57 105.52 o -11 3 1 22281.80 23180.79 240.93 o -9 3 1 37900.79 39314.03 539.18 o -7 3 1 11480.72 11275.90 238.65 o -5 3 1 10320.07 8934.52 253.78 o -3 3 1 54758.32 55476.45 465.55 o -1 3 1 41600.83 42061.20 525.52 o 1 3 1 49363.79 51537.17 331.20 o 3 3 1 23107.27 24317.46 677.04 o 5 3 1 52807.69 51325.56 1643.28 o 7 3 1 21515.16 21096.23 598.51 o 9 3 1 3821.67 4117.74 122.16 o 11 3 1 42104.77 40085.09 1538.26 o 13 3 1 6348.01 5312.38 175.52 o 15 3 1 46.63 316.77 107.57 o 17 3 1 3450.62 3302.24 271.56 o 19 3 1 631.41 734.34 141.53 o 21 3 1 4980.20 4969.18 211.31 o 23 3 1 13990.22 14276.28 600.48 o 25 3 1 615.53 424.15 237.93 o 27 3 1 2002.71 2008.57 576.72 o -26 4 1 236.69 536.93 359.72 o -24 4 1 348.29 566.38 214.72 o -22 4 1 507.81 462.23 162.19 o -20 4 1 6324.61 6342.22 160.70 o -18 4 1 4480.41 4086.96 129.90 o -16 4 1 978.85 1024.24 116.43 o -14 4 1 699.48 652.20 88.80 o -12 4 1 2665.07 3035.19 116.28 o -10 4 1 3887.36 4162.05 108.51 o -8 4 1 1092.23 1008.95 61.22 o -6 4 1 11583.56 10550.61 314.99 o -4 4 1 15550.50 15111.24 168.82 o -2 4 1 37042.72 38977.02 629.20 o 0 4 1 69427.75 71338.80 755.04 o 2 4 1 5387.42 5137.89 108.68 o 4 4 1 838.63 704.83 45.67 o 6 4 1 12345.62 13335.44 293.97 o 8 4 1 1568.32 1778.46 82.30 o 10 4 1 174.04 389.39 86.30 o 12 4 1 226.39 256.05 81.03 o 14 4 1 1818.26 1901.33 163.09 o 16 4 1 67.21 338.01 111.27 o 18 4 1 1268.59 1070.42 118.72 o 20 4 1 491.40 604.70 134.14 o 22 4 1 1022.80 1217.41 187.72 o 24 4 1 1464.56 1329.08 260.92 o 26 4 1 326.24 432.16 364.53 o -25 5 1 7605.09 7863.67 358.06 o -23 5 1 1574.74 1885.70 248.32 o -21 5 1 8800.94 8493.19 253.33 o -19 5 1 1653.30 1752.55 137.02 o -17 5 1 5655.98 4866.35 367.01 o -15 5 1 2295.56 2059.63 133.31 o -13 5 1 710.83 868.99 102.25 o -11 5 1 14910.15 14111.16 223.39 o -9 5 1 8355.84 9262.47 180.67 o -7 5 1 1660.88 1714.28 66.44 o -5 5 1 18060.40 16068.99 169.60 o -3 5 1 5421.74 5011.06 84.42 o -1 5 1 32690.05 34258.22 207.98 o 1 5 1 61752.39 59143.39 1360.23 o 3 5 1 335.74 557.33 55.73 o 5 5 1 33603.44 33668.96 644.64 o 7 5 1 16206.88 15315.97 423.13 o 9 5 1 19482.79 19842.22 460.12 o 11 5 1 1193.98 1527.26 74.31 o 13 5 1 8993.89 8507.40 360.54 o 15 5 1 12206.47 11119.34 278.52 o 17 5 1 2628.40 3032.02 137.04 o 19 5 1 2141.60 2227.15 178.36 o 21 5 1 976.96 801.14 145.31 o 23 5 1 7547.23 7108.82 435.22 o 25 5 1 1647.52 1526.93 328.23 o -26 6 1 102.99 446.69 465.05 o -24 6 1 2104.73 2377.35 287.14 o -22 6 1 1929.75 1963.23 213.74 o -20 6 1 174.05 413.39 165.78 o -18 6 1 26045.13 25600.48 506.30 o -16 6 1 42.36 185.91 100.03 o -14 6 1 13387.83 12150.89 248.11 o -12 6 1 9615.42 8833.65 120.99 o -10 6 1 767.61 1386.99 78.27 o -8 6 1 25727.74 22724.07 438.49 o -6 6 1 68260.88 69093.66 1513.32 o -4 6 1 23439.82 24267.70 199.14 o -2 6 1 483.68 685.65 55.32 o 0 6 1 8170.63 7632.91 173.12 o 2 6 1 25766.74 21656.17 329.50 o 4 6 1 32956.36 32267.55 637.83 o 6 6 1 26709.93 27575.73 518.03 o 8 6 1 38939.10 37927.13 843.67 o 10 6 1 2492.56 2411.36 79.18 o 12 6 1 386.18 434.69 81.82 o 14 6 1 29381.10 29483.15 582.39 o 16 6 1 5598.79 5906.55 182.67 o 18 6 1 4567.98 4115.46 236.63 o 20 6 1 18304.77 19297.28 1110.33 o 22 6 1 2218.27 2375.64 258.12 o 24 6 1 806.38 570.29 308.62 o -25 7 1 3077.62 3674.61 354.10 o -23 7 1 2800.04 2840.16 221.05 o -21 7 1 1158.01 1239.74 233.09 o -19 7 1 3686.74 3954.53 202.10 o -17 7 1 34139.17 34983.51 401.62 o -15 7 1 7922.97 7890.52 186.65 o -13 7 1 41.37 320.59 94.80 o -11 7 1 33796.07 33208.91 764.18 o -9 7 1 1390.34 1163.80 81.43 o -7 7 1 8152.96 8509.17 114.16 o -5 7 1 22323.97 20081.64 156.97 o -3 7 1 5996.94 6081.70 158.56 o -1 7 1 360.54 687.14 67.03 o 1 7 1 74795.54 71164.55 1804.46 o 3 7 1 16.16 184.65 46.28 o 5 7 1 3845.37 3881.85 64.61 o 7 7 1 19249.10 18476.43 330.94 o 9 7 1 5180.45 5024.64 143.10 o 11 7 1 18852.24 18370.04 453.58 o 13 7 1 22073.43 23327.53 589.03 o 15 7 1 12833.46 12799.67 252.64 o 17 7 1 2698.17 2453.31 218.10 o 19 7 1 2369.70 2275.55 209.10 o 21 7 1 14078.53 13706.14 481.11 o 23 7 1 458.33 758.95 226.56 o 25 7 1 1563.82 1494.24 388.24 o -24 8 1 4350.17 4004.06 251.68 o -22 8 1 152.16 283.76 405.82 o -20 8 1 606.51 853.90 242.53 o -18 8 1 2002.90 1864.59 161.48 o -16 8 1 3367.54 3548.54 213.33 o -14 8 1 2424.37 2592.20 167.48 o -12 8 1 26229.58 27253.37 488.84 o -10 8 1 4158.61 3832.37 119.30 o -8 8 1 2002.85 1752.54 122.49 o -6 8 1 4725.02 5086.23 220.97 o -4 8 1 66657.67 68926.34 1113.29 o -2 8 1 22481.71 24391.72 223.83 o 0 8 1 1418.94 1162.04 55.66 o 2 8 1 7662.28 7401.27 219.40 o 4 8 1 5232.65 4553.58 150.10 o 6 8 1 2230.66 1987.17 68.31 o 8 8 1 26891.08 26626.30 724.61 o 10 8 1 6766.73 7114.21 305.35 o 12 8 1 15787.01 15814.00 272.04 o 14 8 1 18133.73 17405.80 316.07 o 16 8 1 1857.96 1749.87 144.90 o 18 8 1 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