#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:36:14 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181179 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/58/2225894.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225894_Fobs loop_ _publ_author_name 'Li, Jinghong' 'Guo, Zhenghua' 'Li, Lianzhi' 'Wang, Daqi' _publ_section_title ; {N-[(2-Oxido-1-naphthyl)methylidene]serinato-\k^3^O,N,O'}(1,10-phenanthroline-\k^2^N,N')copper(II) ; _journal_coeditor_code HY2297 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m516 _journal_volume 66 _journal_year 2010 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.924 _cell_angle_gamma 90.000 _cell_length_a 10.7302 _cell_length_b 6.4687 _cell_length_c 15.7930 _exptl_crystal_F_000 514.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file hy2297Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 090906a in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 128.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 -7 0 25.40 42.19 15.07 o 3 -7 0 40.97 48.28 16.13 o 4 -7 0 0.48 1.16 8.40 o 5 -7 0 174.91 197.31 18.94 o 2 -6 0 90.55 88.58 17.67 o 3 -6 0 41.42 50.29 15.25 o 4 -6 0 22.04 25.94 14.89 o 5 -6 0 13.60 13.24 15.60 o 6 -6 0 162.95 135.35 31.35 o 7 -6 0 195.36 222.03 26.38 o 2 -5 0 670.83 689.17 30.14 o 3 -5 0 111.16 113.04 13.71 o 4 -5 0 126.23 127.71 11.70 o 5 -5 0 289.74 335.63 30.31 o 6 -5 0 63.05 64.29 11.78 o 7 -5 0 2.24 -3.99 7.48 o 8 -5 0 80.98 74.20 12.41 o 9 -5 0 51.18 43.26 10.85 o 2 -4 0 631.85 641.66 25.88 o 3 -4 0 800.56 838.43 28.90 o 4 -4 0 757.17 777.75 28.19 o 5 -4 0 297.48 298.95 15.21 o 6 -4 0 286.43 261.58 12.34 o 7 -4 0 233.99 239.91 16.84 o 8 -4 0 19.76 17.13 8.54 o 9 -4 0 62.27 68.38 11.13 o 10 -4 0 113.33 112.60 13.02 o 2 -3 0 1054.02 1015.35 28.01 o 3 -3 0 480.28 486.91 19.74 o 4 -3 0 643.18 653.07 22.51 o 5 -3 0 481.36 489.35 22.07 o 6 -3 0 351.17 336.71 12.81 o 7 -3 0 225.25 201.51 10.75 o 8 -3 0 417.03 416.87 15.57 o 9 -3 0 175.36 193.35 11.59 o 10 -3 0 29.07 35.43 7.55 o 11 -3 0 79.74 77.88 11.19 o 2 -2 0 242.53 236.66 11.76 o 3 -2 0 2311.86 2408.76 37.64 o 4 -2 0 2009.40 2107.87 36.99 o 5 -2 0 658.64 718.65 20.86 o 6 -2 0 204.72 191.85 9.24 o 7 -2 0 568.35 544.47 15.74 o 8 -2 0 74.22 76.13 7.52 o 9 -2 0 109.26 124.78 9.35 o 10 -2 0 191.17 216.75 12.00 o 11 -2 0 24.24 33.53 10.07 o 12 -2 0 0.42 -5.26 10.93 o 1 -1 0 1273.85 1292.25 20.03 o 2 -1 0 1813.02 1936.93 27.36 o 3 -1 0 1183.06 1177.67 23.46 o 4 -1 0 1654.82 1761.61 30.53 o 5 -1 0 1280.36 1252.31 19.14 o 6 -1 0 98.84 88.34 6.25 o 7 -1 0 6.89 9.11 4.70 o 8 -1 0 280.74 276.98 11.20 o 9 -1 0 331.36 340.06 12.77 o 10 -1 0 140.31 135.77 14.09 o 11 -1 0 130.96 153.64 19.85 o 12 -1 0 207.06 235.18 24.76 o 1 0 0 2498.52 2678.66 21.07 o 2 0 0 415.06 438.84 10.01 o 3 0 0 928.49 867.26 11.16 o 4 0 0 1518.49 1473.25 32.86 o 5 0 0 37.07 43.94 4.17 o 6 0 0 1611.74 1669.58 31.38 o 7 0 0 1258.89 1275.28 19.63 o 8 0 0 35.33 35.12 4.98 o 9 0 0 41.53 44.47 8.32 o 10 0 0 2.46 3.96 9.99 o 11 0 0 60.27 51.76 14.12 o 12 0 0 0.10 14.71 13.71 o 1 1 0 1368.86 1357.70 22.11 o 2 1 0 2045.91 2143.63 17.86 o 3 1 0 1218.02 1249.06 37.01 o 4 1 0 1542.27 1597.69 52.68 o 5 1 0 1246.28 1199.52 48.88 o 6 1 0 113.58 93.37 4.64 o 7 1 0 10.47 15.37 4.53 o 8 1 0 308.47 290.02 22.28 o 9 1 0 345.72 365.83 26.35 o 10 1 0 142.15 129.76 18.97 o 11 1 0 103.77 119.01 19.80 o 12 1 0 192.57 227.91 26.30 o 0 2 0 159.83 123.68 11.29 o 1 2 0 1268.52 1278.20 21.90 o 2 2 0 269.76 273.19 8.57 o 3 2 0 2271.33 2359.93 24.33 o 4 2 0 2122.78 2285.45 67.12 o 5 2 0 647.36 771.79 58.35 o 6 2 0 151.42 137.92 16.19 o 7 2 0 602.80 523.01 30.02 o 8 2 0 66.26 71.03 15.42 o 9 2 0 111.27 111.27 18.38 o 10 2 0 182.98 195.59 23.28 o 11 2 0 21.74 10.70 12.11 o 12 2 0 0.74 6.03 12.65 o 1 3 0 680.09 722.46 19.81 o 2 3 0 1067.30 1051.12 29.28 o 3 3 0 480.45 490.15 15.70 o 4 3 0 648.93 686.68 29.80 o 5 3 0 464.56 463.11 12.79 o 6 3 0 385.94 380.66 26.65 o 7 3 0 207.02 189.92 21.33 o 8 3 0 426.55 408.02 30.90 o 9 3 0 182.95 200.02 23.87 o 10 3 0 31.73 21.80 13.18 o 11 3 0 63.60 68.96 17.43 o 0 4 0 654.45 704.89 32.85 o 1 4 0 100.24 90.52 9.69 o 2 4 0 665.16 705.33 22.68 o 3 4 0 855.98 889.37 24.89 o 4 4 0 755.18 762.59 45.56 o 5 4 0 302.40 296.22 19.17 o 6 4 0 345.75 368.61 28.78 o 7 4 0 179.99 180.52 22.28 o 8 4 0 19.60 21.86 12.94 o 9 4 0 57.11 63.23 16.90 o 10 4 0 111.43 106.89 21.04 o 1 5 0 333.50 336.18 18.25 o 2 5 0 641.47 638.26 24.85 o 3 5 0 94.27 95.69 11.19 o 4 5 0 150.12 121.61 19.62 o 5 5 0 323.06 290.72 25.82 o 8 5 0 68.12 67.30 18.73 o 9 5 0 52.34 70.61 19.56 o 0 6 0 627.08 606.33 37.76 o 1 6 0 60.80 49.50 10.39 o 2 6 0 79.22 78.48 12.50 o 3 6 0 38.88 41.01 15.01 o 4 6 0 35.79 30.08 13.00 o 1 7 0 90.03 105.12 20.33 o 2 7 0 24.98 22.16 14.77 o 3 7 0 45.05 37.46 13.95 o -5 -7 1 8.30 10.25 8.73 o -4 -7 1 99.25 108.69 28.16 o -3 -7 1 33.08 43.64 10.95 o -2 -7 1 53.84 54.57 11.42 o 2 -7 1 29.49 48.63 17.37 o 3 -7 1 39.36 52.47 16.43 o 4 -7 1 102.88 87.39 22.04 o 5 -7 1 8.77 -6.56 12.00 o -7 -6 1 6.61 15.21 9.50 o -6 -6 1 79.30 94.80 13.33 o -5 -6 1 62.98 49.76 11.10 o -4 -6 1 75.16 75.48 11.90 o -3 -6 1 25.45 21.15 13.35 o -2 -6 1 334.96 330.49 28.78 o -1 -6 1 314.47 349.11 28.30 o 2 -6 1 207.80 198.13 19.85 o 5 -6 1 64.91 97.14 20.74 o 6 -6 1 7.48 7.09 13.95 o 7 -6 1 14.62 15.61 9.12 o -9 -5 1 21.64 18.26 9.48 o -8 -5 1 18.45 27.85 9.56 o -7 -5 1 170.24 182.91 16.40 o -6 -5 1 142.21 136.14 17.79 o -5 -5 1 29.54 17.16 12.73 o -4 -5 1 149.66 160.31 22.10 o -3 -5 1 109.67 102.49 10.11 o -2 -5 1 134.09 135.86 11.40 o -1 -5 1 228.84 201.79 19.85 o 0 -5 1 466.39 472.43 27.60 o 1 -5 1 131.62 153.40 15.66 o 2 -5 1 181.13 177.09 17.96 o 3 -5 1 278.18 309.99 21.92 o 4 -5 1 12.49 12.35 9.51 o 5 -5 1 82.83 67.89 12.11 o 6 -5 1 48.88 78.53 20.09 o 7 -5 1 86.83 89.83 13.18 o 8 -5 1 35.79 34.85 9.97 o 9 -5 1 9.54 15.32 8.50 o -10 -4 1 3.73 6.12 8.39 o -9 -4 1 97.39 105.28 12.89 o -8 -4 1 73.51 78.20 11.19 o -7 -4 1 17.97 10.99 8.17 o -6 -4 1 103.18 108.71 8.33 o -5 -4 1 401.98 408.68 14.95 o -4 -4 1 288.69 312.62 14.50 o -3 -4 1 64.79 64.51 7.81 o -2 -4 1 1082.64 1093.90 25.88 o 2 -4 1 391.88 410.68 22.34 o 3 -4 1 418.81 423.21 22.40 o 4 -4 1 387.46 399.92 22.16 o 5 -4 1 728.21 695.26 27.71 o 6 -4 1 65.12 73.33 11.70 o 7 -4 1 24.56 16.59 7.99 o 8 -4 1 215.20 227.01 13.46 o 9 -4 1 138.23 134.47 17.14 o 10 -4 1 5.25 6.44 8.39 o -11 -3 1 6.75 7.07 8.11 o -10 -3 1 307.94 365.99 20.32 o -9 -3 1 208.43 224.34 16.16 o -8 -3 1 6.56 8.90 5.29 o -7 -3 1 461.35 441.59 28.70 o -6 -3 1 275.30 270.55 12.12 o -5 -3 1 9.38 8.04 4.04 o -4 -3 1 563.19 556.64 14.36 o -3 -3 1 1002.58 1004.42 21.30 o -2 -3 1 372.37 411.98 16.84 o 2 -3 1 180.59 189.98 14.18 o 3 -3 1 1616.98 1724.67 39.18 o 4 -3 1 1014.49 1008.26 29.43 o 5 -3 1 38.22 46.62 8.92 o 6 -3 1 198.46 192.58 14.65 o 7 -3 1 136.38 141.15 9.68 o 8 -3 1 140.53 132.02 9.92 o 9 -3 1 260.63 268.09 13.23 o 10 -3 1 235.12 256.27 13.60 o 11 -3 1 36.54 23.44 8.95 o -12 -2 1 70.10 79.77 17.61 o -11 -2 1 84.64 94.44 12.53 o -10 -2 1 9.90 10.82 5.64 o -9 -2 1 223.35 238.47 11.88 o -8 -2 1 465.23 505.01 15.70 o -7 -2 1 151.94 157.98 9.00 o -6 -2 1 283.22 257.04 10.22 o -5 -2 1 685.72 679.35 15.10 o -4 -2 1 1392.67 1348.13 43.07 o -3 -2 1 278.66 311.16 14.27 o -2 -2 1 1408.11 1309.64 69.82 o 2 -2 1 1743.13 1760.01 33.62 o 3 -2 1 527.08 558.17 19.44 o 4 -2 1 176.15 171.18 11.64 o 5 -2 1 2167.99 2090.26 41.13 o 6 -2 1 598.51 566.48 15.35 o 7 -2 1 34.00 28.18 5.34 o 8 -2 1 405.24 406.16 14.55 o 9 -2 1 173.07 180.81 10.71 o 10 -2 1 19.49 31.31 10.62 o 11 -2 1 27.36 27.21 8.91 o 12 -2 1 84.75 107.19 18.50 o -12 -1 1 4.83 5.26 12.88 o -11 -1 1 49.61 51.11 13.77 o -10 -1 1 31.76 42.97 8.75 o -9 -1 1 136.22 125.32 8.65 o -8 -1 1 146.21 138.07 8.64 o -7 -1 1 971.27 1010.55 19.34 o -6 -1 1 801.87 777.51 16.00 o -5 -1 1 138.08 144.18 7.31 o -4 -1 1 2007.19 1973.98 45.39 o -3 -1 1 1705.28 1714.70 38.07 o -2 -1 1 1295.44 1303.86 33.18 o -1 -1 1 1606.07 1697.53 20.55 o 0 -1 1 5080.81 5123.02 49.52 o 1 -1 1 706.73 790.10 17.67 o 2 -1 1 2738.49 2834.04 36.52 o 3 -1 1 637.17 610.88 17.79 o 4 -1 1 2381.28 2491.43 40.89 o 5 -1 1 1282.32 1357.58 38.08 o 6 -1 1 227.00 228.76 9.31 o 7 -1 1 571.39 575.66 14.91 o 8 -1 1 26.59 20.84 5.37 o 9 -1 1 127.86 118.99 8.50 o 10 -1 1 82.18 106.50 11.16 o 11 -1 1 10.90 20.68 12.59 o 12 -1 1 10.99 21.39 13.41 o -12 0 1 104.49 107.25 19.80 o -11 0 1 38.64 41.30 14.06 o -10 0 1 0.84 -1.89 9.22 o -9 0 1 791.96 877.67 25.16 o -8 0 1 442.56 436.11 12.27 o -7 0 1 511.74 510.91 15.17 o -6 0 1 290.68 286.45 9.01 o -5 0 1 3462.59 3641.20 48.08 o -4 0 1 1543.58 1494.82 17.94 o -3 0 1 447.74 440.81 8.09 o -2 0 1 2270.60 2250.22 19.65 o -1 0 1 4966.82 5394.64 57.81 o 1 0 1 7095.66 7282.13 60.80 o 2 0 1 173.36 192.34 5.88 o 3 0 1 3047.55 3085.17 41.95 o 4 0 1 142.05 118.45 5.41 o 5 0 1 470.98 424.74 10.93 o 6 0 1 820.97 804.88 14.61 o 7 0 1 5.95 4.93 3.89 o 8 0 1 420.31 434.39 24.69 o 9 0 1 133.84 151.74 14.57 o 10 0 1 96.31 67.30 14.54 o 11 0 1 107.68 150.27 19.68 o 12 0 1 122.28 153.93 21.98 o -12 1 1 5.85 2.60 13.00 o -11 1 1 40.29 46.45 14.71 o -10 1 1 44.42 57.08 14.42 o -9 1 1 164.62 144.48 19.03 o -8 1 1 147.67 143.33 9.96 o -7 1 1 1038.63 1030.45 16.58 o -6 1 1 805.94 751.18 12.22 o -5 1 1 136.99 139.25 5.31 o -4 1 1 2056.28 2049.66 41.20 o -3 1 1 1744.76 1783.97 61.40 o -2 1 1 1401.96 1415.17 85.86 o -1 1 1 1576.09 1655.71 24.29 o 0 1 1 4979.90 5013.34 88.58 o 1 1 1 782.00 843.31 24.24 o 2 1 1 2618.92 2562.99 27.53 o 3 1 1 605.98 567.45 26.87 o 4 1 1 2582.03 2724.78 53.47 o 5 1 1 1312.21 1389.63 32.78 o 6 1 1 295.83 295.72 22.07 o 7 1 1 551.26 500.01 33.59 o 8 1 1 25.41 20.74 9.75 o 9 1 1 145.26 135.85 18.38 o 10 1 1 106.39 97.32 17.25 o 11 1 1 15.34 15.25 12.23 o 12 1 1 11.71 20.15 13.77 o -12 2 1 73.34 92.77 20.98 o -11 2 1 78.62 81.25 18.73 o -10 2 1 11.08 14.77 13.53 o -9 2 1 213.88 204.45 22.93 o -8 2 1 494.21 557.34 33.45 o -7 2 1 137.50 116.64 16.90 o -6 2 1 316.72 315.14 11.43 o -5 2 1 799.46 754.29 17.85 o -4 2 1 1283.80 1345.00 148.70 o -3 2 1 325.66 350.83 12.47 o -2 2 1 1304.97 1275.82 51.05 o -1 2 1 318.26 318.48 12.47 o 0 2 1 586.82 607.18 42.22 o 1 2 1 533.01 516.38 11.12 o 2 2 1 1660.18 1705.78 59.43 o 3 2 1 583.02 618.37 22.16 o 4 2 1 162.00 159.72 8.01 o 5 2 1 2104.40 2166.69 95.77 o 6 2 1 653.75 612.47 29.78 o 7 2 1 30.42 29.66 11.11 o 8 2 1 433.14 417.77 28.66 o 9 2 1 149.49 127.81 19.09 o 10 2 1 22.83 23.64 13.30 o 11 2 1 16.07 20.50 13.59 o 12 2 1 78.70 96.20 20.15 o -11 3 1 11.65 5.20 13.47 o -10 3 1 292.83 294.15 29.55 o -9 3 1 218.29 257.52 26.65 o -8 3 1 7.52 13.24 11.58 o -7 3 1 477.96 486.55 31.50 o -6 3 1 260.27 263.25 22.93 o -5 3 1 10.04 11.10 5.54 o -4 3 1 607.69 589.73 67.04 o -3 3 1 999.99 973.96 55.57 o -2 3 1 422.38 476.78 16.32 o -1 3 1 260.68 301.87 13.73 o 0 3 1 879.24 827.77 22.28 o 1 3 1 231.24 195.75 11.49 o 2 3 1 154.95 165.98 10.08 o 3 3 1 1621.40 1663.85 24.02 o 4 3 1 935.12 921.73 28.42 o 5 3 1 36.32 31.73 7.49 o 6 3 1 150.41 139.91 12.16 o 7 3 1 129.49 151.69 18.91 o 8 3 1 134.55 142.53 20.50 o 9 3 1 269.90 290.67 28.42 o 10 3 1 214.89 204.57 25.76 o 11 3 1 34.81 38.41 15.72 o -10 4 1 3.76 16.19 14.24 o -9 4 1 107.28 105.06 19.68 o -8 4 1 54.69 75.58 17.67 o -7 4 1 19.90 15.01 12.65 o -6 4 1 76.00 62.40 15.48 o -4 4 1 302.07 318.02 26.77 o -3 4 1 63.49 75.52 9.47 o -2 4 1 1047.86 1048.73 27.49 o -1 4 1 528.08 501.00 19.78 o 0 4 1 83.57 69.00 9.00 o 1 4 1 81.68 69.66 8.56 o 2 4 1 361.07 352.00 16.23 o 3 4 1 392.60 415.72 17.02 o 4 4 1 366.17 374.69 22.54 o 5 4 1 773.88 753.95 60.86 o 6 4 1 68.02 76.89 11.43 o 7 4 1 28.49 24.70 12.82 o 8 4 1 201.08 221.83 25.47 o 9 4 1 150.94 138.39 21.98 o 10 4 1 5.12 10.05 13.12 o -3 5 1 95.10 90.12 10.72 o -2 5 1 116.60 109.80 16.55 o -1 5 1 233.59 234.55 15.71 o 0 5 1 441.68 398.92 19.85 o 1 5 1 129.46 124.25 21.51 o 2 5 1 176.78 169.46 13.91 o 3 5 1 242.25 225.96 25.11 o 4 5 1 12.13 5.55 12.41 o 5 5 1 79.72 77.82 16.78 o 6 5 1 49.97 80.07 17.43 o 7 5 1 88.09 99.74 19.85 o 8 5 1 38.41 64.05 17.43 o 9 5 1 7.52 4.14 13.18 o -3 6 1 22.40 6.74 10.22 o -2 6 1 284.39 294.47 20.15 o -1 6 1 308.93 308.54 21.15 o 0 6 1 2.53 -3.50 7.75 o 1 6 1 168.89 163.63 14.84 o 2 6 1 202.94 168.82 23.70 o 3 6 1 61.25 38.88 15.72 o 4 6 1 84.86 46.80 16.13 o 5 6 1 49.19 58.62 17.37 o 6 6 1 13.51 11.46 11.29 o -1 7 1 20.33 28.47 9.51 o 0 7 1 162.16 126.36 14.42 o 1 7 1 38.87 30.96 15.66 o 2 7 1 25.36 11.46 13.77 o 3 7 1 51.37 49.52 18.08 o 4 7 1 104.92 115.88 23.05 o 5 7 1 7.99 12.53 12.05 o -5 -7 2 80.44 80.24 12.98 o -4 -7 2 2.58 8.60 8.84 o -3 -7 2 1.21 7.82 9.28 o -2 -7 2 90.62 97.32 17.02 o -1 -7 2 104.61 106.30 17.67 o 0 -7 2 74.15 62.04 16.43 o 1 -7 2 77.27 85.09 17.61 o 5 -7 2 30.41 55.19 19.20 o -7 -6 2 209.53 235.06 35.40 o -6 -6 2 203.27 200.40 33.30 o -5 -6 2 21.40 24.60 11.29 o -4 -6 2 36.68 37.61 9.66 o -3 -6 2 45.73 53.87 10.63 o -2 -6 2 25.88 23.90 9.03 o -1 -6 2 244.82 258.40 34.63 o 2 -6 2 20.06 20.62 12.82 o 3 -6 2 169.78 185.37 20.50 o 4 -6 2 168.63 220.29 21.39 o 6 -6 2 45.77 30.79 18.26 o 7 -6 2 39.99 61.87 19.03 o -9 -5 2 28.85 35.04 10.41 o -8 -5 2 105.49 107.97 13.65 o -7 -5 2 2.89 0.24 6.87 o -6 -5 2 123.71 132.13 14.18 o -5 -5 2 208.33 216.40 22.63 o -4 -5 2 148.21 149.82 26.71 o -3 -5 2 51.38 57.64 10.02 o -2 -5 2 507.24 530.04 22.50 o -1 -5 2 223.77 219.76 20.56 o 0 -5 2 82.55 97.68 14.00 o 1 -5 2 257.32 278.14 19.09 o 2 -5 2 554.08 623.11 31.44 o 3 -5 2 198.44 203.51 19.85 o 4 -5 2 453.53 458.66 27.36 o 5 -5 2 148.50 159.96 17.31 o 6 -5 2 66.96 78.71 13.77 o 7 -5 2 7.94 9.65 7.92 o 8 -5 2 69.08 74.38 12.32 o 9 -5 2 80.54 82.03 14.39 o -10 -4 2 177.92 185.97 26.77 o -9 -4 2 53.53 45.15 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559.65 23.81 o 5 -3 2 2269.63 2285.68 48.45 o 6 -3 2 252.55 219.23 16.55 o 7 -3 2 131.45 122.85 13.71 o 8 -3 2 419.60 438.42 22.03 o 9 -3 2 102.38 115.41 9.54 o 10 -3 2 1.31 7.97 6.17 o 11 -3 2 56.74 47.92 10.68 o -12 -2 2 16.03 15.13 13.65 o -11 -2 2 64.84 62.16 15.84 o -10 -2 2 245.88 268.14 13.06 o -9 -2 2 164.95 174.03 10.66 o -8 -2 2 171.18 169.37 10.27 o -7 -2 2 612.78 620.36 16.41 o -6 -2 2 74.71 67.74 6.19 o -5 -2 2 458.35 462.13 14.34 o -4 -2 2 3316.62 3348.49 97.71 o -3 -2 2 2794.73 2883.02 31.21 o -2 -2 2 49.59 50.79 4.70 o -1 -2 2 156.58 145.84 7.88 o 0 -2 2 1227.66 1266.66 19.42 o 1 -2 2 870.18 855.92 19.80 o 2 -2 2 909.92 1000.36 27.18 o 3 -2 2 1635.65 1701.51 56.34 o 4 -2 2 983.43 1055.41 29.66 o 5 -2 2 85.99 77.94 10.10 o 6 -2 2 394.10 386.87 20.27 o 7 -2 2 466.19 470.12 23.58 o 8 -2 2 338.91 321.36 13.15 o 9 -2 2 116.68 123.24 9.36 o 10 -2 2 53.20 64.11 10.36 o 11 -2 2 147.06 148.36 14.43 o 12 -2 2 4.35 6.09 11.52 o -12 -1 2 106.46 120.54 18.97 o -11 -1 2 89.06 102.75 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